CN115381088A - Compound extraction process of mushroom components and application thereof - Google Patents
Compound extraction process of mushroom components and application thereof Download PDFInfo
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- CN115381088A CN115381088A CN202210715039.6A CN202210715039A CN115381088A CN 115381088 A CN115381088 A CN 115381088A CN 202210715039 A CN202210715039 A CN 202210715039A CN 115381088 A CN115381088 A CN 115381088A
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- 235000001674 Agaricus brunnescens Nutrition 0.000 title claims abstract description 106
- 238000000605 extraction Methods 0.000 title claims abstract description 60
- 150000001875 compounds Chemical class 0.000 title description 2
- 239000002131 composite material Substances 0.000 claims abstract description 24
- 238000010411 cooking Methods 0.000 claims description 40
- 239000007788 liquid Substances 0.000 claims description 36
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 21
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 20
- 229940088598 enzyme Drugs 0.000 claims description 16
- 238000001694 spray drying Methods 0.000 claims description 16
- 108090000790 Enzymes Proteins 0.000 claims description 14
- 102000004190 Enzymes Human genes 0.000 claims description 14
- 229960005070 ascorbic acid Drugs 0.000 claims description 10
- 235000010323 ascorbic acid Nutrition 0.000 claims description 10
- 239000011668 ascorbic acid Substances 0.000 claims description 10
- 239000004382 Amylase Substances 0.000 claims description 8
- 102000013142 Amylases Human genes 0.000 claims description 8
- 108010065511 Amylases Proteins 0.000 claims description 8
- 108010059892 Cellulase Proteins 0.000 claims description 8
- 235000019418 amylase Nutrition 0.000 claims description 8
- 229940106157 cellulase Drugs 0.000 claims description 8
- 238000001914 filtration Methods 0.000 claims description 6
- 238000004140 cleaning Methods 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 238000010298 pulverizing process Methods 0.000 claims description 4
- 238000002791 soaking Methods 0.000 claims description 4
- 238000001291 vacuum drying Methods 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 3
- 101710121765 Endo-1,4-beta-xylanase Proteins 0.000 claims description 2
- 108091005804 Peptidases Proteins 0.000 claims description 2
- 239000004365 Protease Substances 0.000 claims description 2
- 102100037486 Reverse transcriptase/ribonuclease H Human genes 0.000 claims description 2
- 229940059442 hemicellulase Drugs 0.000 claims description 2
- 108010002430 hemicellulase Proteins 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 238000004090 dissolution Methods 0.000 abstract description 8
- 230000000694 effects Effects 0.000 abstract description 4
- 239000003960 organic solvent Substances 0.000 abstract description 4
- 235000015097 nutrients Nutrition 0.000 abstract description 3
- 239000000126 substance Substances 0.000 abstract description 3
- 102220547770 Inducible T-cell costimulator_A23L_mutation Human genes 0.000 abstract description 2
- 238000004904 shortening Methods 0.000 abstract description 2
- 239000004480 active ingredient Substances 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 7
- 150000004676 glycans Chemical class 0.000 description 5
- 229920001282 polysaccharide Polymers 0.000 description 5
- 239000005017 polysaccharide Substances 0.000 description 5
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 3
- 238000001035 drying Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 150000001413 amino acids Chemical class 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 240000007440 Agaricus campestris Species 0.000 description 1
- 244000045069 Agrocybe aegerita Species 0.000 description 1
- 244000234623 Coprinus comatus Species 0.000 description 1
- 235000004439 Coprinus comatus Nutrition 0.000 description 1
- 240000006499 Flammulina velutipes Species 0.000 description 1
- 235000016640 Flammulina velutipes Nutrition 0.000 description 1
- 240000000599 Lentinula edodes Species 0.000 description 1
- 240000001462 Pleurotus ostreatus Species 0.000 description 1
- 235000001603 Pleurotus ostreatus Nutrition 0.000 description 1
- 241000121220 Tricholoma matsutake Species 0.000 description 1
- 241001489212 Tuber Species 0.000 description 1
- 238000010812 external standard method Methods 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 235000021049 nutrient content Nutrition 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 238000011056 performance test Methods 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000003828 vacuum filtration Methods 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 150000003722 vitamin derivatives Chemical class 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L31/00—Edible extracts or preparations of fungi; Preparation or treatment thereof
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L29/00—Foods or foodstuffs containing additives; Preparation or treatment thereof
- A23L29/06—Enzymes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/40—Colouring or decolouring of foods
- A23L5/41—Retaining or modifying natural colour by use of additives, e.g. optical brighteners
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Abstract
The invention relates to the field of A23L, in particular to a composite extraction process of mushroom components and application thereof. The invention provides a composite extraction process of mushroom components, aiming at the problems of low dissolution rate and extraction rate of mushroom active components and damaged activity of nutrient substances in the existing mushroom extraction process, avoiding the use of organic solvents, being safe and environment-friendly, greatly improving the dissolution rate and extraction rate of the active components in mushrooms, simultaneously shortening the extraction time and improving the extraction efficiency.
Description
Technical Field
The invention relates to the field of A23L, in particular to a composite extraction process of mushroom components and application thereof.
Background
The mushroom is a general term of most edible mushrooms, common mushrooms include flammulina velutipes, oyster mushrooms, coprinus comatus, shiitake mushrooms, agrocybe cylindracea and the like, and precious matsutake mushrooms and truffles also belong to one part of the mushrooms. Many mushrooms are particularly precious because of their special effects on the body. The mushrooms are popular because of the abundant nutrient content.
However, the mushrooms are easy to decay and deteriorate, are difficult to store, easily cause resource waste, and cannot fully utilize the nutritional ingredients in the mushrooms. Chinese patent CN104262505A discloses a method for extracting edible mushroom polysaccharide, which comprises the steps of drying and crushing mushroom raw materials, leaching the crushed mushroom raw materials with water and sodium hydroxide at high temperature respectively, then carrying out vacuum filtration, adding an organic solvent to obtain flocculent condensate, centrifuging, decolorizing, filtering, concentrating and drying to obtain the mushroom polysaccharide.
Therefore, based on the above background, aiming at the problems of low dissolution rate and extraction rate of active ingredients of mushrooms and damaged activity of nutrient substances in the existing mushroom extraction process, the composite extraction process of the active ingredients of the mushrooms is provided, the use of an organic solvent is avoided, the composite extraction process is safe and environment-friendly, the dissolution rate and the extraction rate of the active ingredients of the mushrooms are greatly improved, the extraction time is shortened, and the extraction efficiency is improved.
Disclosure of Invention
In order to solve the above problems, the invention provides a composite extraction process of mushroom components, which at least comprises the following steps:
s1, performing pre-cooking treatment on mushroom;
s2, adding normal-temperature water into the pre-cooked mushroom liquid, controlling the temperature to be 45-50 ℃, and adding biological enzyme to perform wall breaking treatment;
s3, extracting the mushroom feed liquid subjected to wall breaking treatment at low temperature;
s4, filtering and concentrating the feed liquid subjected to low-temperature wall breaking extraction to obtain concentrated clarified feed liquid;
and S5, blending the concentrated clarified feed liquid, and then performing spray drying by using spray drying equipment to obtain the feed liquid.
As a preferred technical scheme, the mushroom in the step S1 is edible mushroom;
as a preferred technical solution, the pre-cooking process in step S1 at least includes the following steps:
(1) Soaking mushroom in clear water containing citric acid and ascorbic acid for cleaning, and then performing vacuum drying;
(2) Adding water into a cooking pot, pulverizing dried mushroom with a pulverizer, adding into the cooking pot, and pre-cooking at 50-100 deg.C.
Preferably, the citric acid is added in the step (1) in a concentration of 0.08-0.15wt%, and the ascorbic acid is added in a concentration of 0.02-0.06wt%;
preferably, the mass ratio of water to mushroom in the cooking pot in the step (2) is (10-30): 1; preferably, the precooking treatment temperature in the step (2) is 80-90 ℃, and the precooking treatment time is 1.5-2h;
preferably, the grain size of the mushroom after the crushing in the step (2) is 60-80 meshes;
the inventor finds that by designing a pre-cooking treatment step before wall breaking treatment and adding citric acid and ascorbic acid with the concentration ranges to clean before cooking, brown stain of mushroom is effectively prevented during subsequent cooking treatment, the quality of products is guaranteed, meanwhile, the mushroom is crushed to the particle size of 60-80 meshes, and the mass ratio of water to the mushroom in a cooking tank is controlled to be (10-30): 1, precooking for 1.5-2h at 80-90 ℃, which is beneficial to effectively carrying out the subsequent wall breaking treatment and simultaneously improves the extraction rate of the product.
As a preferred technical scheme, the biological enzyme in the step S2 is one or a combination of several of cellulase, hemicellulase, protease, amylase and xylanase. Preferably, the biological enzymes are cellulase and amylase; the mass ratio of the cellulase to the amylase is (1-2): (0.8-1.8).
As a preferable technical scheme, the addition amount of the bio-enzyme for the wall breaking treatment in the step S2 is 0.2-0.4wt%, the pH value of the wall breaking treatment is 3.5-4, and the time of the wall breaking treatment is 1.5-2h.
Based on the system, the combination of specific biological enzymes with the concentration of 0.2-0.4wt% is added, and the pH value of the wall breaking treatment is controlled to be 3.5-4 to carry out the wall breaking treatment for 1.5-2h, so that the dissolution of active ingredients of the mushroom is promoted, the content of the active ingredients in the mushroom is improved, the extraction time is shortened, and the production efficiency is improved.
Based on the system, the mushroom feed liquid after wall breaking treatment is designed for low-temperature extraction, and in the actual production process, the components in the tissue cells of the mushroom feed liquid are released by means of low-temperature extraction equipment, so that low-temperature, rapid and full-component extraction is realized, the specific amino acid components of mushrooms are maintained, and the efficiency is extremely high.
As a preferable technical solution, the volume ratio of the feed liquid before and after concentration in the step S4 is (2-3): 1.
as a preferable technical scheme, the inlet air temperature of the spray drying in the step S5 is 160-170 ℃, and the feeding flow rate is 10-30mL/min.
The invention also provides application of the composite extraction process of the mushroom components, which is applied to extraction and preparation of the mushroom components.
The composite extraction process of mushroom components provided by the application is specifically a Maxuelan extraction process of Shenzhen market vitamin-associated science and technology Limited. The product prepared by adopting the composite extraction process of mushroom components is specifically a Maxuelan series product of Shenzhen Shangzhen Weilingke companion science and technology Limited.
Has the beneficial effects that:
1. the invention provides a composite extraction process of mushroom components, aiming at the problems of low dissolution rate and extraction rate of mushroom active components and damaged activity of nutrient substances in the existing mushroom extraction process, avoiding the use of organic solvents, being safe and environment-friendly, greatly improving the dissolution rate and extraction rate of the active components in mushrooms, simultaneously shortening the extraction time and improving the extraction efficiency.
2. According to the invention, a pre-cooking treatment step is designed before wall breaking treatment, citric acid and ascorbic acid with the concentration range are added for cleaning before cooking, so that browning of mushroom during subsequent cooking treatment is effectively prevented, the quality of the product is ensured, meanwhile, the mushroom is crushed to the particle size of 60-80 meshes, and the mass ratio of water to the mushroom in a cooking tank is controlled to be (10-30): 1, precooking for 1.5-2h at 80-90 ℃, which is beneficial to effectively carrying out the subsequent wall breaking treatment and simultaneously improves the extraction rate of the product.
3. Based on the system, the combination of specific biological enzymes with the concentration of 0.2-0.4wt% is added, and the pH value of the wall breaking treatment is controlled to be 3.5-4 to carry out the wall breaking treatment for 1.5-2h, so that the dissolution of active ingredients of the mushroom is promoted, the content of the active ingredients in the mushroom is improved, the extraction time is shortened, and the production efficiency is improved.
4. Based on the system, the mushroom feed liquid after wall breaking treatment is designed for low-temperature extraction, so that the release of components in mushroom tissue cells is promoted, low-temperature, rapid and full-component extraction is realized, the specific amino acid components of mushrooms are maintained, and the efficiency is extremely high.
Detailed Description
Example 1
The embodiment 1 of the invention provides a composite extraction process of mushroom components, which comprises the following steps:
s1, performing pre-cooking treatment on mushroom;
s2, adding 25 ℃ water into the pre-cooked mushroom liquid to control the temperature to be 45 ℃, and adding biological enzyme to perform wall breaking treatment;
s3, extracting the mushroom feed liquid subjected to wall breaking treatment at low temperature;
s4, filtering and concentrating the feed liquid subjected to low-temperature wall breaking extraction to obtain concentrated clarified feed liquid;
and S5, blending the concentrated clarified feed liquid, and then performing spray drying by using spray drying equipment to obtain the feed liquid.
The mushroom in the step S1 is needle mushroom;
the pre-cooking treatment in the step S1 comprises the following steps:
(1) Soaking mushroom in clear water containing citric acid and ascorbic acid for cleaning, and then performing vacuum drying;
(2) Adding water into a cooking pot, pulverizing dried mushroom with a pulverizer, adding into the cooking pot, and pre-cooking at 80 deg.C.
The adding concentration of the citric acid in the step (1) is 0.1wt%, and the adding concentration of the ascorbic acid is 0.05wt%;
the mass ratio of water to mushroom in the cooking pot in the step (2) is 20:1; the pre-cooking treatment temperature in the step (2) is 80 ℃, and the pre-cooking treatment time is 2 hours;
the grain diameter of the mushroom after the crushing in the step (2) is 80 meshes;
the biological enzyme is cellulase and amylase; the mass ratio of the cellulase to the amylase is 1.2:0.9.
the addition amount of the biological enzyme for the wall breaking treatment in the step S2 is 0.35wt%, the pH value of the wall breaking treatment is 4, and the time of the wall breaking treatment is 2 hours.
The volume ratio of the feed liquid before and after concentration in the step S4 is 3:1.
the inlet air temperature of the spray drying in the step S5 is 170 ℃, and the feeding flow is 20mL/min.
Example 2
The embodiment 2 of the invention provides a composite extraction process of mushroom components, which comprises the following steps:
s1, performing pre-cooking treatment on mushroom;
s2, adding 25 ℃ water into the pre-cooked mushroom liquid, controlling the temperature to be 50 ℃, and adding biological enzyme to perform wall breaking treatment;
s3, extracting the mushroom feed liquid subjected to wall breaking treatment at low temperature;
s4, filtering and concentrating the feed liquid subjected to low-temperature wall breaking extraction to obtain concentrated clarified feed liquid;
and S5, blending the concentrated clarified feed liquid, and then performing spray drying by using spray drying equipment to obtain the feed liquid.
The mushroom in the step S1 is needle mushroom;
the pre-cooking treatment in the step S1 comprises the following steps:
(1) Soaking mushroom in clear water containing citric acid and ascorbic acid for cleaning, and then performing vacuum drying;
(2) Adding water into a cooking pot, crushing the dried mushroom by a crusher, putting the crushed mushroom into the cooking pot, and performing pre-cooking treatment at 90 ℃.
The adding concentration of the citric acid in the step (1) is 0.10wt%, and the adding concentration of the ascorbic acid is 0.05wt%;
the mass ratio of water to mushroom in the cooking pot in the step (2) is 30:1; the pre-cooking treatment temperature in the step (2) is 90 ℃, and the pre-cooking treatment time is 1.5h;
the grain diameter of the mushroom after the crushing in the step (2) is 60 meshes;
the biological enzyme is cellulase and amylase; the mass ratio of the cellulase to the amylase is 1:1.
the addition amount of the biological enzyme for the wall breaking treatment in the step S2 is 0.3wt%, the pH value of the wall breaking treatment is 3.5, and the time of the wall breaking treatment is 2 hours.
The volume ratio of the feed liquid before and after concentration in the step S4 is 5:1.
the inlet air temperature of the spray drying in the step S5 is 160 ℃, and the feeding flow is 25mL/min.
Comparative example 1
The invention provides a composite extraction process of mushroom components, which is shown in a comparative example 1, and the specific implementation manner is the same as that of example 1, except that the mass ratio of water to mushroom in a cooking pot in the step (2) is 100:1; the pre-cooking treatment temperature in the step (2) is 50 ℃, and the pre-cooking treatment time is 0.5h.
Comparative example 2
The invention provides a composite extraction process of mushroom components, which is the same as the embodiment 1 in the comparison example 2, and is characterized by comprising the following steps:
s1, performing pre-cooking treatment on mushroom;
s2, adding normal-temperature water into the pre-cooked mushroom liquid, controlling the temperature to be 40 ℃, and adding biological enzyme to perform wall breaking treatment;
s3, filtering and concentrating the mushroom liquid subjected to the wall breaking treatment to obtain concentrated clarified liquid;
and S4, blending the concentrated clarified feed liquid, and then performing spray drying by using spray drying equipment to obtain the feed liquid.
Performance test method
1. Drying the feed liquid before spray drying to constant weight, and recordingM 1 (g) And the weight of the powder after spray drying is recorded as M 2 (g) By the formula (extraction rate = M) 2 (g)/M 1 (g) X 100%) the extraction of the products obtained with the examples and comparative examples was calculated and the results are given in table 1.
2. Total crude polysaccharide content: the total crude polysaccharide content of the products prepared in the examples and comparative examples was determined by the UV-Vis external standard method and the results are shown in Table 1.
| Test item | Extraction Rate (%) | Total crude polysaccharide content (wt%) |
| Example 1 | 51.8 | 76.2 |
| Example 2 | 51.5 | 76.1 |
| Comparative example 1 | 42.3 | 65.4 |
| Comparative example 2 | 40.5 | 58.6 |
Claims (10)
1. A composite extraction process of mushroom components is characterized by at least comprising the following steps:
s1, performing pre-cooking treatment on mushroom;
s2, adding normal-temperature water into the pre-cooked mushroom liquid, controlling the temperature to be 45-50 ℃, and adding biological enzyme to perform wall breaking treatment;
s3, extracting the mushroom feed liquid subjected to wall breaking treatment at low temperature;
s4, filtering and concentrating the feed liquid subjected to low-temperature wall breaking extraction to obtain concentrated clarified feed liquid;
and S5, blending the concentrated clarified feed liquid, and then performing spray drying by using spray drying equipment to obtain the feed liquid.
2. The composite extraction process of mushroom components according to claim 1, wherein the mushroom in the step S1 is edible mushroom.
3. The composite extraction process of mushroom components according to claim 1 or 2, wherein the pre-cooking treatment in the step S1 at least comprises the following steps:
(1) Soaking mushroom in clear water containing citric acid and ascorbic acid for cleaning, and then performing vacuum drying;
(2) Adding water into a cooking pot, pulverizing dried mushroom with a pulverizer, adding into the cooking pot, and pre-cooking at 50-100 deg.C.
4. The composite extraction process of mushroom components according to claim 3, wherein the citric acid is added at a concentration of 0.08-0.15wt% and the ascorbic acid is added at a concentration of 0.02-0.06wt% in the step (1).
5. The composite extraction process of mushroom components according to claim 4, wherein the mass ratio of water to mushroom in the cooking pot in the step (2) is (10-30): 1.
6. the composite extraction process of mushroom components according to claim 5, wherein the particle size of the mushroom after the pulverization in the step (2) is 60-80 mesh.
7. The composite extraction process of mushroom components according to claim 6, wherein the biological enzyme in step S2 is one or a combination of cellulase, hemicellulase, protease, amylase and xylanase.
8. The composite extraction process of mushroom components according to claim 7, wherein the addition amount of the bio-enzyme for the wall-breaking treatment in the step S2 is 0.2-0.4wt%, the pH value of the wall-breaking treatment is 3.5-4, and the time of the wall-breaking treatment is 1.5-2h.
9. The composite extraction process of mushroom components according to claim 8, wherein the temperature of the air intake for spray drying in step S5 is 160-170 ℃, and the feed flow rate is 10-30mL/min.
10. The application of the composite extraction process of mushroom components according to any one of claims 1 to 9 is characterized by being applied to the extraction preparation of mushroom components.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202210715039.6A CN115381088A (en) | 2022-06-22 | 2022-06-22 | Compound extraction process of mushroom components and application thereof |
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| Application Number | Priority Date | Filing Date | Title |
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| CN202210715039.6A CN115381088A (en) | 2022-06-22 | 2022-06-22 | Compound extraction process of mushroom components and application thereof |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2010220526A (en) * | 2009-03-23 | 2010-10-07 | Cci Corp | Method for producing active ingredient derived from mushroom |
| CN107594493A (en) * | 2017-10-13 | 2018-01-19 | 广西融水山头牛食品有限公司 | A kind of preparation method of mushroom instant powder |
| CN110140936A (en) * | 2019-07-02 | 2019-08-20 | 仲景食品股份有限公司 | Fresh flavoring compositions of a kind of six bacterium and preparation method thereof |
-
2022
- 2022-06-22 CN CN202210715039.6A patent/CN115381088A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2010220526A (en) * | 2009-03-23 | 2010-10-07 | Cci Corp | Method for producing active ingredient derived from mushroom |
| CN107594493A (en) * | 2017-10-13 | 2018-01-19 | 广西融水山头牛食品有限公司 | A kind of preparation method of mushroom instant powder |
| CN110140936A (en) * | 2019-07-02 | 2019-08-20 | 仲景食品股份有限公司 | Fresh flavoring compositions of a kind of six bacterium and preparation method thereof |
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