CN115353932B - Essence composition for controlling saponification speed, application thereof and cold-made soap - Google Patents
Essence composition for controlling saponification speed, application thereof and cold-made soap Download PDFInfo
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- CN115353932B CN115353932B CN202211091670.XA CN202211091670A CN115353932B CN 115353932 B CN115353932 B CN 115353932B CN 202211091670 A CN202211091670 A CN 202211091670A CN 115353932 B CN115353932 B CN 115353932B
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/005—Synthetic soaps
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/02—Compositions of detergents based essentially on soap on alkali or ammonium soaps
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D9/00—Compositions of detergents based essentially on soap
- C11D9/04—Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
- C11D9/44—Perfumes; Colouring materials; Brightening agents ; Bleaching agents
- C11D9/442—Perfumes
Abstract
The invention relates to the field of daily chemical industry, and discloses an essence composition for controlling saponification speed, application thereof and cold soap. The composition contains perfume, inert agent and saponification accelerating agent; the perfume is at least one selected from synthetic perfume and natural plant essential oil; the inert agent is at least one selected from benzyl benzoate, isopropyl myristate and isoparaffin; the accelerated saponification agent is at least one selected from straight-chain alcohol with total carbon atoms of 1-8, branched-chain alcohol with total carbon atoms of 3-8, dipropylene glycol ethyl ether and benzyl alcohol. The essence composition provided by the invention can control the saponification time (namely the saponification speed) of soap liquid, and provides more possibility for creating artistic cold-making soap.
Description
Technical Field
The invention relates to the field of daily chemical industry, in particular to an essence composition for controlling saponification speed, application thereof and cold soap.
Background
Soap is a long-history detergent. In ancient times, people used animal fat to mix with plant ash to make soaps. Along with the development of science, technology and industry, the soap making technology is gradually improved.
At present, most of soaps in the market react with sodium hydroxide at high temperature through grease, sodium chloride is added, and glycerin and higher fatty acid sodium are separated. The higher fatty acid sodium, namely the soap base, is formed into commercial soap, namely the soap base soap through the processes of later drying, adding additives such as perfume, antioxidant and the like, stirring, grinding, layering and forming and the like.
However, the cold soap is produced by mixing vegetable fat and oil with sodium hydroxide at normal temperature, stirring to form a semi-fluid state, introducing the semi-fluid state into a mold, curing for 1-2 days, demolding, slicing, and curing for more than 1 month.
Compared with soap base soap, the cold soap has long saponification time, changeable processing process and large-scale production difficulty. With the development of society, people have improved the quality of life requirement, cold soap is touted because of its pattern and style are various, rich in natural glycerin, plant purification, and various additives such as honey, radix Arnebiae extract, green tea, seven-seed powdery mildew, etc. can be added in the preparation process.
However, unlike soap-based soaps, the addition of fragrance in chilled soaps requires a number of considerations. Wherein, the addition of essence has a great influence on the saponification time of the cold soap. Specifically, in the mixed solution of vegetable oil and sodium hydroxide which react for a certain time, when a slight stirring trace appears after the mixed solution is scratched on the surface (light T), essence is added, and the mixed solution can be immediately solidified (heavy T) by the aid of the essence, so that the mixed solution is not uniformly mixed and molded for a sufficient operation time; the essence can cause precipitation of the mixed solution, so that saponification is uneven.
For a long time, the production of cold soap cannot be scaled up, largely because the saponification time is not controlled, and the time from soap liquid saponification to mold filling and the time to mold release are too long. For producing cold-made soap with beautiful patterns, soap liquid needs to be adjusted into different colors, and the soap liquid is molded layer by layer, scraped into required shapes and molded; after the soap has certain hardness, the next layer of soap solution is added.
Therefore, it is urgent to study the control of saponification speed by controlling saponification time of cold soap with essence and adjusting the components of essence according to the technological requirements of different cold soaps.
Disclosure of Invention
The invention aims to overcome the defect that the saponification time of the cold soap cannot be controlled in the existing process for preparing the cold soap, so that large-scale production cannot be realized.
In order to achieve the above object, a first aspect of the present invention provides a perfume composition for controlling saponification speed, which comprises perfume, inert agent, and saponification accelerating agent;
the perfume is at least one selected from synthetic perfume and natural plant essential oil;
the inert agent is at least one selected from benzyl benzoate, isopropyl myristate and isoparaffin;
the accelerated saponification agent is at least one selected from linear alcohol with total carbon atoms of 1-8, branched alcohol with total carbon atoms of 3-8, dipropylene glycol ethyl ether and benzyl alcohol;
the content of the perfume is 10-99.9wt%, the content of the inert agent is 0.1-90wt% and the content of the accelerated saponification agent is 0-89.9wt% based on the total weight of the perfume composition.
In a second aspect the present invention provides the use of a flavour composition for controlling the rate of saponification as described in the first aspect hereinbefore in the preparation of a chilled soap.
The third aspect of the invention provides a cold-made soap, which comprises a soap base and essence, wherein the soap base comprises vegetable oil, sodium hydroxide and water; the perfume is the perfume composition for controlling saponification speed in the first aspect;
the content of the essence is 0.01-10wt% based on the total weight of the soap base.
Compared with the prior art, the invention has at least the following advantages:
the essence composition with specific proportion provided by the invention can realize accurate control of saponification speed in the preparation process of the cold soap, control of operation time and curing time, solve the problem that the existing essence has uncontrollable influence on cold soap liquid, greatly improve the preparation efficiency of the cold soap, shorten the operation time for creating artistic cold soap, provide more possibility for creating artistic cold soap, and the prepared cold soap has fine texture and changeable fragrance.
Detailed Description
The endpoints and any values of the ranges disclosed herein are not limited to the precise range or value, and are understood to encompass values approaching those ranges or values. For numerical ranges, one or more new numerical ranges may be found between the endpoints of each range, between the endpoint of each range and the individual point value, and between the individual point value, in combination with each other, and are to be considered as specifically disclosed herein.
As previously mentioned, a first aspect of the present invention provides a flavour composition for controlling the rate of saponification, the composition comprising a perfume, an inert agent, an accelerated saponification agent;
the perfume is at least one selected from synthetic perfume and natural plant essential oil;
the inert agent is at least one selected from benzyl benzoate, isopropyl myristate and isoparaffin;
the accelerated saponification agent is at least one selected from linear alcohol with total carbon atoms of 1-8, branched alcohol with total carbon atoms of 3-8, dipropylene glycol ethyl ether and benzyl alcohol;
the content of the perfume is 10-99.9wt%, the content of the inert agent is 0.1-90wt% and the content of the accelerated saponification agent is 0-89.9wt% based on the total weight of the perfume composition.
Preferably, the perfume is present in an amount of 20 to 95wt%, the inert agent is present in an amount of 5 to 60wt%, and the accelerated saponification agent is present in an amount of 0 to 40wt%, based on the total weight of the perfume composition.
It should be noted that, in combination with technical means known in the art, a person skilled in the art may adjust the type of perfume in the perfume composition and the content of each type of perfume according to the desired type of perfume, the desired pleasure of perfume, and the like.
Preferably, the accelerated saponification agent is selected from at least one of dipropylene glycol ethyl ether and benzyl alcohol.
Preferably, the inert agent is selected from at least one of isopropyl myristate, isomeric dodecane and isomeric hexadecane.
According to a preferred embodimentIn the composition, the perfume contains a ringAt least one of muguet aldehyde, heliotropin, breeze aldehyde, methylhexyl cinnamaldehyde, ligustrum lucidum aldehyde, peach aldehyde, laginella, ethyl 2-methylbutyrate, leaf alcohol acetate, dimethylbenzyl alcohol butyrate, methyl dihydrojasmonate, o-tert-butylcyclohexyl acetate, phenoxyethyl isobutyrate, eugenol, matrieth, damascone, ambergris ketone, propiolactone, musk, brazil orange oil, sandalwood 208 and sandalwood 210; and
the inert agent is isopropyl myristate.
According to another preferred embodimentIn the composition, the perfume contains at least one of leaf alcohol acetate, citronellyl acetate, sclareolide, octanal, decanal, dodecanal, lagomorphanol, calyxl, methylhexyl cinnamaldehyde, neo-heliotropin, hydroxyvanillin, melon aldehyde, phenylacetaldehyde dimethyl acetal, ethylcitral, white convaldehyde, methoxyshandalal, ligustral, cyanine aldehyde, benzyl acetate, tricyclodecenyl propionate, malate, geranyl acetate, methyl dihydrojasmonate, isopentyl acetate, o-tert-butylcyclohexyl acetate, phenethyl acetate, suggeratel, methyl salicylate, green phenol, ethyl tricyclodecanecarboxylate, neryl acetate, rose ether, sea ketone, isomethyl ionone, butyl damascone, open-rice ketone, damascenone, ambenone, amberg lactone, musk T, sandalwood oil, D-limonene, indole aralkyl, acetyl eugenol and zein the perfume; and
the inert agent is a combination of isopropyl myristate and isohexadecane.
Preferably, the perfume is at least one selected from the group consisting of ester perfumes having a total number of carbon atoms of more than 10, alcohol perfumes having a total number of carbon atoms of more than 10, aldehyde perfumes, ketone perfumes, nitrile perfumes, ether perfumes, and hydrocarbon perfumes.
Preferably, the natural plant essential oil is at least one selected from grapefruit essential oil, cypress essential oil, ginger essential oil, chamomile essential oil, myrrh essential oil, white pine essential oil, frankincense essential oil, jade sandalwood essential oil, alnica essential oil, turmeric essential oil, brazil sweet orange oil, miscellaneous lavender oil, and lemon grass oil.
Preferably, the ester synthetic perfume with the total number of carbon atoms being more than 10 is selected from at least one of citronellyl acetate, linalyl acetate, neryl acetate, sclareolide, ethyl tricyclodecanecarboxylate, methyl dihydrojasmonate, musk T, dimethylbenzyl orthoalcohol acetate, dimethylbenzyl orthoalcohol butyrate, p-tert-butylcyclohexyl 4-acetate, o-tert-butylcyclohexyl acetate, phenoxyethyl isobutyrate, myricyl aldehyde, peach aldehyde, tricyclodecenyl propionate, sugrel ester, sunflower seed lactone, cyclopentadecanolide and methyl high cis-dihydrojasmonate.
Preferably, the alcohol synthetic perfume with total carbon number more than 10 is at least one selected from sandalwood 803, sandalwood 208, sandalwood 210 and Saussurea alcohol.
Preferably, the aldehyde synthetic perfume is at least one selected from undecnal, dodecanal, melon aldehyde, white mugwort aldehyde, heliotropin, cyclic mugwort aldehyde, breeze aldehyde, methylhexyl cinnamaldehyde, glossy privet aldehyde, lagerstroemia aldehyde, ambergris ketone, octanal, decanal, vanillin, meldonium aldehyde, phenylacetaldehyde dimethyl acetal, methoxyshandalal and cyanine aldehyde.
Preferably, the ketone synthetic perfume is selected from at least one of damascone, cyclohexadecenone, acetophenone, sea ketone, isomethyl ionone, methyl ionone, dihydro jasmone, cis-jasmone, alpha damascone, delta damascone, kemamone, spirocyclic peganum ketone.
Preferably, the nitrile synthetic perfume is at least one selected from ethyl citrate, citronellyl nitrile, tangerine nitrile, rose nitrile and grapefruit nitrile.
Preferably, the ether synthetic perfume is selected from at least one of rose ether, jiale musk, methyl cedar ether, orange flower ether, piper ether and cress ether.
Preferably, the hydrocarbon synthetic perfume is at least one selected from limonene, D-limonene, hyacinth, ethoxycyclododecyl methane.
In the invention, the saponification speed of the cold soap liquid is controlled by adjusting the type and the dosage of the accelerating saponification agent in the essence composition. Illustratively, the saponification time of the cold soap stock solution can be achieved without promoting saponification, heavy T in 5-10 minutes, heavy T in 10-15 minutes, heavy T in 15-30 minutes, etc.
As previously mentioned, a second aspect of the present invention provides the use of a flavour composition for controlling the rate of saponification as described in the first aspect hereinbefore in the preparation of a chilled soap.
As described above, the third aspect of the present invention provides a chilled soap comprising a soap base and a perfume, wherein the soap base comprises vegetable oil, sodium hydroxide and water; the perfume is the perfume composition for controlling saponification speed in the first aspect;
the content of the essence is 0.01-10wt% based on the total weight of the soap base.
The type and amount of the vegetable fat and the amount of the sodium hydroxide and the water are not particularly limited in the present invention, and those skilled in the art can select them according to the technical means known in the art, and the following description of the present invention exemplarily provides a preferred embodiment, and those skilled in the art should not understand the limitation of the present invention.
The invention will be described in detail below by way of examples.
In the following examples, unless otherwise specified, all raw materials used are commercially available, and animal fragrances such as musk, ambergris, etc. are synthetic raw materials of non-animal origin; the perfume and the usage amount are required to meet the international relevant regulations.
In the present invention, the room temperature means 25±2℃.
Example 1: essence composition X1
TABLE 1
Example 2: essence composition X2
TABLE 2
Examples 3 to 6: essence composition X3-X6
Examples 3-6 employed a similar formulation to example 2, except that:
in example 3, 20g of benzyl alcohol (accelerated saponification agent) was used instead of 20g of isohexadecane, and the rest was the same as in example 2, to obtain a perfume composition X3; that is, in this example, the benzyl alcohol was used in an amount of 20g and the isohexadecane was used in an amount of 20g;
in example 4, 40g of benzyl alcohol was used instead of 40g of isohexadecane, the remainder being the same as in example 2, to give a perfume composition X4; that is, the benzyl alcohol in this example was used in an amount of 40g, and no isohexadecane was contained;
in example 5, 12g of dipropylene glycol ethyl ether (accelerated saponification agent) was used instead of 12g of isohexadecane, and the rest was the same as in example 2, to obtain a fragrance composition X5; that is, in this example, the amount of benzyl alcohol was 12g and the amount of isohexadecane was 28g;
in example 6, 6g of dipropylene glycol ethyl ether was used instead of 6g of isohexadecane, and the rest was the same as in example 2, to obtain a perfume composition X6; that is, the benzyl alcohol was used in an amount of 6g and 34g of isohexadecane in this example.
Example 7: essence composition X7
TABLE 3 Table 3
Comparative example 1: fragrance composition DX1
TABLE 4 Table 4
Comparative example 2: fragrance composition DX2
TABLE 5
Preparation example
37.47g of sodium hydroxide is added into 75g of water to obtain alkali liquor;
heating 54.00g coconut oil, 67.50g palm oil, 81.00 olive oil, 27.00 grape seed oil, 27.00 sweet almond oil and 13.50g shea butter at 50deg.C for 3min, and cooling to 35deg.C to obtain oil phase;
and stirring the oil phase and the alkali liquor cooled to room temperature by using a handheld electric stirrer at 3000rpm every 1min for 20s until the viscosity of the soap solution increases, and removing trace after the soap solution passes through the liquid level for 3s to obtain light T soap solution.
Test case
The 3wt% fragrance composition of examples and comparative examples was added to the light T soap solution prepared in the preparation example, stirred at 60rpm for 1min, and left to stand for observing the time for which the soap solution appeared to be heavy T, the operability of the soap solution for 5min after stirring, and the fluidity of the soap solution for 15min after stirring, see in particular table 6.
TABLE 6
As can be seen from the results of Table 6, the use of the fragrance composition provided by the present invention allows control of the saponification time (i.e., saponification rate) of the soap solution, providing more possibilities for creating artistic chilled soaps.
The preferred embodiments of the present invention have been described in detail above, but the present invention is not limited thereto. Within the scope of the technical idea of the invention, a number of simple variants of the technical solution of the invention are possible, including combinations of the individual technical features in any other suitable way, which simple variants and combinations should likewise be regarded as being disclosed by the invention, all falling within the scope of protection of the invention.
Claims (9)
1. An essence composition for controlling saponification speed, which is characterized in that the composition contains perfume, inert agent and saponification accelerating agent;
the perfume is at least one selected from synthetic perfume and natural plant essential oil;
the inert agent is at least one selected from isopropyl myristate, isododecane and isohexadecane;
the accelerated saponification agent is at least one selected from dipropylene glycol ethyl ether and benzyl alcohol;
the content of the perfume is 10-99.9wt%, the content of the inert agent is 0.1-90wt% and the content of the accelerated saponification agent is 0-89.9wt% based on the total weight of the perfume composition.
2. The composition of claim 1, wherein the perfume is present in an amount of 20-95wt%, the inert agent is present in an amount of 5-60wt%, and the accelerated saponification agent is present in an amount of 0-40wt%, based on the total weight of the perfume composition.
3. The composition according to claim 1 or 2, wherein in the composition, the perfume contains at least one of ring lily aldehyde, neo-heliotropin, breeze aldehyde, methyl hexyl cinnamaldehyde, glossy privet aldehyde, peach aldehyde, laginella aldehyde, ethyl 2-methylbutyrate, leaf alcohol acetate, dimethylbenzyl alcohol butyrate, methyl dihydrojasmonate, o-tert-butylcyclohexyl acetate, phenoxyethyl isobutyrate, eugenol, chamomile, damascone, amberg ketone, propiolactone, jiale musk, brazil orange oil, sandalwood 208 and sandalwood 210; and
the inert agent is isopropyl myristate.
4. The composition of claim 1 or 2, wherein in the composition, the perfume comprises at least one of leaf alcohol acetate, citronellyl acetate, sclareolide, octanal, decanal, dodecanal, lagomorphan, sal aldehyde, methylhexyl cinnamaldehyde, heliotropin, hydroxycampoulin, melon aldehyde, phenylacetaldehyde dimethyl acetal, ethylcitrate, white convaldehyde, methoxyshandalal, privet aldehyde, cyanine aldehyde, benzyl acetate, tricyclodecenyl propionate, malate, geranyl acetate, methyl dihydrojasmonate, isopentyl acetate, o-tert-butylcyclohexyl acetate, phenethyl acetate, cyclobalanoate, methyl salicylate, green flower phenol, ethyl tricyclodecanecarboxylate, orange flower acetate, rose ether, sea ketone, isopropyl ionone, butanone, open-mesityl ketone, ambroxy ketone, xanthone, cyclopentadecanolide, musk T, sandalwood, heterolavender oil, D-limonene, indole, acetyl eugenol 803, and isoeugenol; and
the inert agent is a combination of isopropyl myristate and isohexadecane.
5. The composition according to claim 1 or 2, wherein the perfume is at least one selected from the group consisting of ester perfumes having a total number of carbon atoms of more than 10, alcohol perfumes having a total number of carbon atoms of more than 10, aldehyde perfumes, ketone perfumes, nitrile perfumes, ether perfumes, hydrocarbon perfumes;
the natural plant essential oil is at least one selected from grapefruit essential oil, cypress essential oil, ginger essential oil, chamomile essential oil, myrrh essential oil, white pine essential oil, olibanum essential oil, jade sandalwood essential oil, albergamot essential oil, turmeric essential oil, brazil sweet orange oil, miscellaneous lavender oil and lemon grass oil.
6. The composition of claim 5, wherein the ester synthetic perfume having a total number of carbon atoms greater than 10 is selected from at least one of citronellyl acetate, linalyl acetate, neryl acetate, sclareolide, ethyl tricyclodecanecarboxylate, methyl dihydrojasmonate, musk T, dimethylbenzyl orthoacetate, dimethylbenzyl orthobutyrate, p-tert-butylcyclohexyl 4-acetate, o-tert-butylcyclohexyl acetate, phenoxyethyl isobutyrate, myricyl aldehyde, peach aldehyde, tricyclodecenyl propionate, sugrel ester, sunflower seed lactone, cyclopentadecanolide, methyl high cis-dihydrojasmonate; and/or the number of the groups of groups,
the alcohol synthetic perfume with total carbon atoms more than 10 is selected from at least one of sandalwood 803, sandalwood 208, sandalwood 210 and Saururi herba; and/or the number of the groups of groups,
the aldehyde synthetic perfume is at least one selected from undecnal, dodecanal, muskmelon aldehyde, white mugwort aldehyde, heliotropin, ring mugwort aldehyde, breeze aldehyde, methyl hexyl cinnamaldehyde, glossy privet aldehyde, rabbit ear aldehyde, ambergris ketone, octanal, decanal, vanillin, melittin, phenylacetaldehyde dimethyl acetal, methoxyshandalal and anthocyanin.
7. The composition of claim 5, wherein the ketone synthetic perfume is selected from at least one of damascenone, cyclohexadecenone, acetophenone, sea ketone, isomethyl ionone, methyl ionone, dihydro jasmone, cis jasmone, alpha damascenone, delta damascenone, kemesityl, spirocyclic galbanum; and/or the number of the groups of groups,
the nitrile synthetic perfume is at least one selected from ethyl citrate, citronellonitrile, tangerine nitrile, rose nitrile and grapefruit nitrile; and/or the number of the groups of groups,
the ether synthetic perfume is at least one selected from rose ether, jiale musk, methyl cypress ether, orange flower ether, piper nigrum ether and cress ether; and/or the number of the groups of groups,
the hydrocarbon synthetic perfume is at least one selected from limonene, D-limonene, hyacinth, and ethoxycyclododecyl methane.
8. Use of a flavour composition for controlling the rate of saponification according to any one of claims 1 to 7 in the preparation of a chilled soap.
9. The cold soap is characterized by comprising a soap base and essence, wherein the soap base comprises vegetable oil, sodium hydroxide and water; the perfume is the perfume composition for controlling saponification speed according to any one of claims 1 to 8;
the content of the essence is 0.01-10wt% based on the total weight of the soap base.
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