CN115353279A - Method for preparing patterned glass by coating and tempering sequentially - Google Patents
Method for preparing patterned glass by coating and tempering sequentially Download PDFInfo
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- CN115353279A CN115353279A CN202211109030.7A CN202211109030A CN115353279A CN 115353279 A CN115353279 A CN 115353279A CN 202211109030 A CN202211109030 A CN 202211109030A CN 115353279 A CN115353279 A CN 115353279A
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- 239000011521 glass Substances 0.000 title claims abstract description 80
- 238000000576 coating method Methods 0.000 title claims abstract description 44
- 239000011248 coating agent Substances 0.000 title claims abstract description 42
- 238000000034 method Methods 0.000 title claims abstract description 27
- 238000005496 tempering Methods 0.000 title claims abstract description 16
- 238000004140 cleaning Methods 0.000 claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 claims abstract description 22
- 239000003292 glue Substances 0.000 claims abstract description 8
- 238000007688 edging Methods 0.000 claims abstract description 7
- 238000005406 washing Methods 0.000 claims abstract description 6
- 238000005520 cutting process Methods 0.000 claims abstract description 4
- 238000000227 grinding Methods 0.000 claims abstract description 4
- 238000007789 sealing Methods 0.000 claims abstract description 4
- 238000007650 screen-printing Methods 0.000 claims description 26
- 238000001755 magnetron sputter deposition Methods 0.000 claims description 15
- 239000010410 layer Substances 0.000 claims description 11
- 238000001035 drying Methods 0.000 claims description 9
- 239000003973 paint Substances 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 239000013077 target material Substances 0.000 claims description 6
- 239000011247 coating layer Substances 0.000 claims description 5
- POAOYUHQDCAZBD-UHFFFAOYSA-N 2-butoxyethanol Chemical compound CCCCOCCO POAOYUHQDCAZBD-UHFFFAOYSA-N 0.000 claims description 3
- 244000137852 Petrea volubilis Species 0.000 claims description 3
- 150000001412 amines Chemical class 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 3
- 238000007865 diluting Methods 0.000 claims description 3
- 238000010981 drying operation Methods 0.000 claims description 3
- 239000003822 epoxy resin Substances 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 239000000049 pigment Substances 0.000 claims description 3
- 238000005498 polishing Methods 0.000 claims description 3
- 229920000647 polyepoxide Polymers 0.000 claims description 3
- 230000001681 protective effect Effects 0.000 claims description 3
- 230000002277 temperature effect Effects 0.000 claims 1
- 238000003892 spreading Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 2
- 230000003287 optical effect Effects 0.000 description 2
- 238000007792 addition Methods 0.000 description 1
- 239000000956 alloy Substances 0.000 description 1
- 229910045601 alloy Inorganic materials 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000007888 film coating Substances 0.000 description 1
- 238000009501 film coating Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002736 metal compounds Chemical class 0.000 description 1
- 239000002923 metal particle Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000007639 printing Methods 0.000 description 1
- 230000005855 radiation Effects 0.000 description 1
- 230000035945 sensitivity Effects 0.000 description 1
Images
Classifications
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B27/00—Tempering or quenching glass products
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M1/00—Inking and printing with a printer's forme
- B41M1/12—Stencil printing; Silk-screen printing
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M1/00—Inking and printing with a printer's forme
- B41M1/26—Printing on other surfaces than ordinary paper
- B41M1/34—Printing on other surfaces than ordinary paper on glass or ceramic surfaces
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M7/00—After-treatment of prints, e.g. heating, irradiating, setting of the ink, protection of the printed stock
- B41M7/009—After-treatment of prints, e.g. heating, irradiating, setting of the ink, protection of the printed stock using thermal means, e.g. infrared radiation, heat
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/102—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions other than those only involving unsaturated carbon-to-carbon bonds
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/15—Deposition methods from the vapour phase
- C03C2218/154—Deposition methods from the vapour phase by sputtering
- C03C2218/156—Deposition methods from the vapour phase by sputtering by magnetron sputtering
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/30—Aspects of methods for coating glass not covered above
- C03C2218/31—Pre-treatment
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/30—Aspects of methods for coating glass not covered above
- C03C2218/32—After-treatment
- C03C2218/328—Partly or completely removing a coating
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Thermal Sciences (AREA)
- Wood Science & Technology (AREA)
- Ceramic Engineering (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Printing Methods (AREA)
- Surface Treatment Of Glass (AREA)
Abstract
The invention provides a method for preparing patterned glass by coating and tempering, belonging to the technical field of glass deep processing; a method for preparing patterned glass by coating and tempering sequentially comprises the following steps: slicing: selecting a glass original sheet, and cutting the glass original sheet according to production requirements; B. grinding and washing: edging the glass sheet and cleaning the glass sheet; C. c, manufacturing a screen plate: manufacturing a screen plate by using 150-250 meshes of gauze, coating photosensitive glue on the gauze under the screen stretching pressure of 15-20N, spreading a film with a hollow pattern on the gauze after the photosensitive glue is dried, enabling the film to be in close contact with the gauze, sealing the four sides of the film, vacuumizing to enable the contact surface of the film and the gauze to be attached without a cavity as much as possible, and finally exposing and developing the film to enable the film pattern to be supported on the gauze. The glass has the advantages of simplicity, effectiveness, high production efficiency, high yield and the like.
Description
Technical Field
The invention belongs to the technical field of glass fine and deep processing, and particularly relates to a method for preparing patterned glass by coating and tempering.
Background
Coated glass is also known as reflective glass. The coated glass is prepared by coating one or more layers of metal, alloy or metal compound films on the surface of glass to change the optical performance of the glass and meet certain specific requirements. The coated glass adopts a magnetron sputtering process to carry out physical coating on a glass interface so as to reduce heat transfer loss of the glass caused by radiation, effectively inhibit infrared light transmission, and reduce heat exchange at two sides of the glass so as to achieve good energy-saving performance, optical performance and environmental protection performance, so that the coated glass is popular with architectural designers and widely applied to buildings around the world. However, with the increasing demand of the market today for aesthetic diversification of glass, it is required that the glass not only has energy saving performance, but also presents delicate patterns.
In the prior art, the method for preparing the Low-e coated glass with patterns is represented by the following three methods:
1. high-temperature glaze silk-screen method: glaze with gloss is needed in the silk-screen printing process, so that the preparation cost is low; secondly, because the metal particles are added into the lustrous glaze, the gauze with the printing mesh number of 90-120 meshes is needed, and the pattern contour is not smooth and has burrs.
2. The paster coating method comprises the following steps: sticking a sticker with a hollow pattern, which is carved in advance, on the surface of the glass, and then coating a film; the method has the defects that the integrity of the sticker is poor, and after the film coating is finished, the efficiency of tearing the sticker is low and the film layer is easy to damage.
3. A patch coating method: covering the surface of the glass by adopting a patch manufactured according to the shape of the pattern, and then coating the film on the glass; the process has the limitation that the patterns which can be processed by the process are concise and not complicated.
Disclosure of Invention
The invention aims to provide a method for preparing patterned glass by coating and tempering in the prior art, and the technical problem to be solved by the invention is how to optimize the production process of the patterned glass, so that the patterned glass is simpler and has high yield.
The purpose of the invention can be realized by the following technical scheme: the method for preparing the pattern glass by coating and toughening is characterized by comprising the following steps:
A. slicing: selecting a glass original sheet, and cutting the glass original sheet according to production requirements;
B. grinding and washing: edging the glass sheet and cleaning the glass sheet;
C. manufacturing a screen plate: manufacturing a screen plate by using 150-250 meshes of gauze, wherein the screen stretching pressure is between 15-20N, then coating photosensitive glue on the gauze, after the photosensitive glue is dried, laying a film with a hollow pattern in advance on the gauze, enabling the film to be in close contact with the gauze, sealing the four sides of the film, vacuumizing to enable the contact surface of the film and the gauze to be attached without a cavity as much as possible, and finally exposing and developing the film to enable the film pattern to be supported on the gauze;
D. preparing the coating: the paint consists of epoxy resin mixture 50-55 wt%, ethylene glycol monobutyl ether 12-14 wt%, fatty amine curing agent 4-6 wt% and pigment and stuffing 19-22 wt%; fully mixing the components, and diluting to ensure that the components can meet the requirements of silk screen printing;
E. and (3) silk-screen printing: mounting the manufactured screen plate on a screen printing machine, polishing a scraper and an oil knife by using fine sand paper of 800-1000 meshes, mounting the screen plate on a clamp of the screen printing machine, setting parameters such as pressure, tool stopping position and screen distance of the screen printing machine, and pouring a proper amount of prepared coating into the screen plate to perform screen printing operation;
F. drying: putting the glass after the silk-screen printing of the pattern into drying equipment, drying and curing the silk-screen pattern, controlling the temperature of the drying operation at 200-230 ℃ and the operation time at 10-12 minutes;
G. secondary cleaning: feeding the glass with the paint dried into a cleaning machine to complete secondary cleaning, so that the surface of the glass is clean and dustless;
H. magnetron sputtering coating: according to the structure of the film layers on the glass and the thickness of each film layer, setting technological parameters of target materials, the number of the target materials, air pressure, protective gas components and the like at each section of a magnetron sputtering coating production line, and then conveying the glass into a coating cavity of the magnetron sputtering coating production line to finish magnetron sputtering coating operation;
I. tempering: sending the glass subjected to edging and cleaning into a tempering furnace for glass tempering operation; in the toughening process, the coating layer can be sintered and fluffy due to the high-temperature effect.
J. And (3) washing for three times: sending the toughened and cooled coated glass into a cleaning machine, and cleaning the toughened and cooled coated glass with clear water for three times; at the moment, the paint layer with fluffy surface can be easily cleaned, and further, the hollow-out Low-E film pattern is presented on the glass surface.
The method adopts the coating which can be solidified at Low temperature, is insoluble in water and can be sintered and loosened at high temperature to carry out pattern silk-screen printing, so that the pattern can be washed by water after the silk-screen printing is finished, and does not fall off, after the magnetron sputtering coating is finished, the pattern is automatically loosened in the toughening process, and then the coating layer is washed and removed, and the Low-E film with the hollowed pattern is obtained.
The invention has the advantages that:
1. the low-e film pattern glass processed by the process solves the problems that the colored glaze glass pattern does not have reflected light and glossiness, metallic color on glaze color, instability of bright color, sensitivity of color allocation and the like.
2. By using the production process, the building glass not only has pattern and color diversity, but also has energy-saving property.
3. The process has the advantages of simple production process flow, high efficiency and good product stability, and is suitable for continuous large-scale production.
Drawings
FIG. 1 is a flow chart of a method for preparing patterned glass according to an embodiment of the present invention.
Detailed Description
The following are specific embodiments of the present invention and are further described with reference to the drawings, but the present invention is not limited to these embodiments.
As shown in fig. 1, a method for preparing patterned glass by coating and tempering sequentially comprises the following steps:
A. slicing: selecting a glass original sheet, and cutting the glass original sheet according to production requirements;
B. grinding and washing: edging the glass sheet and cleaning the glass sheet;
C. manufacturing a screen plate: manufacturing a screen plate by using 150-250 meshes of gauze, wherein the screen stretching pressure is between 15-20N, then coating photosensitive glue on the gauze, after the photosensitive glue is dried, laying a film with a hollow pattern in advance on the gauze, enabling the film to be in close contact with the gauze, sealing the four sides of the film, vacuumizing to enable the contact surface of the film and the gauze to be attached without a cavity as much as possible, and finally exposing and developing the film to enable the film pattern to be supported on the gauze;
D. preparing the coating: the paint consists of epoxy resin mixture 50-55 wt%, ethylene glycol monobutyl ether 12-14 wt%, fatty amine curing agent 4-6 wt% and pigment and stuffing 19-22 wt%; fully mixing the components, and diluting to ensure that the components can meet the requirements of silk screen printing;
E. and (3) silk-screen printing: mounting the manufactured screen plate on a screen printing machine, polishing a scraper and an oil knife by using fine sand paper of 800-1000 meshes, mounting the screen plate on a clamp of the screen printing machine, setting parameters such as pressure, tool stopping position and screen distance of the screen printing machine, and pouring a proper amount of prepared coating into the screen plate to perform screen printing operation;
F. drying: putting the glass after the silk-screen printing of the pattern into drying equipment, drying and curing the silk-screen pattern, controlling the temperature of the drying operation at 200-230 ℃ and the operation time at 10-12 minutes;
G. secondary cleaning: feeding the glass with the paint dried into a cleaning machine to complete secondary cleaning, so that the surface of the glass is clean and dustless;
H. magnetron sputtering coating: according to the structure of the film layers on the glass and the thickness of each film layer, setting technological parameters of target materials, the number of the target materials, air pressure, protective gas components and the like at each section of a magnetron sputtering coating production line, and then conveying the glass into a coating cavity of the magnetron sputtering coating production line to finish magnetron sputtering coating operation;
I. tempering: sending the glass subjected to edging and cleaning into a tempering furnace for glass tempering operation; in the toughening process, the coating layer can be sintered and fluffy due to the high-temperature effect.
J. And (3) cleaning for three times: sending the toughened and cooled coated glass into a cleaning machine, and cleaning the toughened and cooled coated glass with clear water for three times; at the moment, the paint layer with the fluffy surface can be easily cleaned, and then the hollow Low-E film pattern is presented on the glass surface.
The method adopts the coating which can be solidified at Low temperature, is insoluble in water and can be sintered and loosened at high temperature to carry out pattern silk-screen printing, so that the pattern can be washed by water after the silk-screen printing is finished, and does not fall off, after the magnetron sputtering coating is finished, the pattern is automatically loosened in the toughening process, and then the coating layer is washed and removed, and the Low-E film with the hollowed pattern is obtained.
The specific embodiments described herein are merely illustrative of the spirit of the invention. Various modifications or additions may be made to the described embodiments or alternatives may be employed by those skilled in the art without departing from the spirit or ambit of the invention as defined in the appended claims.
Claims (1)
1. The method for preparing the pattern glass by coating and toughening is characterized by comprising the following steps:
A. slicing: selecting a glass original sheet, and cutting the glass original sheet according to production requirements;
B. grinding and washing: edging the glass sheet and cleaning the glass sheet;
C. manufacturing a screen plate: manufacturing a screen plate by using 150-250 meshes of gauze, wherein the screen stretching pressure is between 15-20N, then coating photosensitive glue on the gauze, after the photosensitive glue is dried, laying a film with a hollow pattern in advance on the gauze, enabling the film to be in close contact with the gauze, sealing the four sides of the film, vacuumizing to enable the contact surface of the film and the gauze to be attached without a cavity as much as possible, and finally exposing and developing the film to enable the film pattern to be supported on the gauze;
D. preparing the coating: the paint consists of epoxy resin mixture 50-55 wt%, ethylene glycol monobutyl ether 12-14 wt%, fatty amine curing agent 4-6 wt% and pigment and stuffing 19-22 wt%; fully mixing the components, and diluting to ensure that the components can meet the requirements of silk screen printing;
E. silk-screen printing: mounting the manufactured screen plate on a screen printing machine, polishing a scraper and an oil knife by using fine sand paper of 800-1000 meshes, mounting the screen plate on a clamp of the screen printing machine, setting parameters such as pressure, tool stopping position and screen distance of the screen printing machine, and pouring a proper amount of prepared coating into the screen plate to perform screen printing operation;
F. drying: putting the glass after the silk-screen printing of the pattern into drying equipment, drying and curing the silk-screen pattern, controlling the temperature of the drying operation at 200-230 ℃ and the operation time at 10-12 minutes;
G. secondary cleaning: feeding the glass with the paint dried into a cleaning machine to complete secondary cleaning, so that the surface of the glass is clean and dustless;
H. magnetron sputtering coating: according to the structure of the film layers on the glass and the thickness of each film layer, setting technological parameters of target materials, the number of the target materials, air pressure, protective gas components and the like at each section of a magnetron sputtering coating production line, and then conveying the glass into a coating cavity of the magnetron sputtering coating production line to finish magnetron sputtering coating operation;
I. tempering: sending the glass subjected to edging and cleaning into a tempering furnace for glass tempering operation; in the toughening process, the coating layer can be sintered and loosened due to the high temperature effect.
J. And (3) washing for three times: sending the toughened and cooled coated glass into a cleaning machine, and cleaning the toughened and cooled coated glass with clear water for three times; at the moment, the paint layer with the fluffy surface can be easily cleaned, and then the hollow Low-E film pattern is presented on the glass surface.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211109030.7A CN115353279A (en) | 2022-09-13 | 2022-09-13 | Method for preparing patterned glass by coating and tempering sequentially |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202211109030.7A CN115353279A (en) | 2022-09-13 | 2022-09-13 | Method for preparing patterned glass by coating and tempering sequentially |
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| Publication Number | Publication Date |
|---|---|
| CN115353279A true CN115353279A (en) | 2022-11-18 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202211109030.7A Pending CN115353279A (en) | 2022-09-13 | 2022-09-13 | Method for preparing patterned glass by coating and tempering sequentially |
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| Country | Link |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116285542A (en) * | 2023-03-16 | 2023-06-23 | 咸宁南玻节能玻璃有限公司 | Tearable masking film coating, preparation method thereof and method for preparing coated pattern glass by using tearable masking film coating |
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| CN102501451A (en) * | 2011-11-25 | 2012-06-20 | 林嘉宏 | Temperable di-silver low-emissivity coated glass and manufacturing process thereof |
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| CN108017291A (en) * | 2017-12-15 | 2018-05-11 | 安徽恒春玻璃股份有限公司 | A kind of colored glazed glass and preparation method thereof |
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2022
- 2022-09-13 CN CN202211109030.7A patent/CN115353279A/en active Pending
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| KR20070105440A (en) * | 2006-04-26 | 2007-10-31 | 김태석 | Method for glass plate with ornamental intaglio pattern and thereof |
| CN1951985A (en) * | 2006-10-20 | 2007-04-25 | 南京工业大学 | Transparent heat insulation film and preparation method thereof |
| CN102730981A (en) * | 2011-04-15 | 2012-10-17 | 中航三鑫股份有限公司 | Method for processing colored glazing glass with double colors pattern |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN116285542A (en) * | 2023-03-16 | 2023-06-23 | 咸宁南玻节能玻璃有限公司 | Tearable masking film coating, preparation method thereof and method for preparing coated pattern glass by using tearable masking film coating |
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Application publication date: 20221118 |
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