CN115283113B - Feed additive and preparation process thereof - Google Patents

Feed additive and preparation process thereof Download PDF

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Publication number
CN115283113B
CN115283113B CN202210330179.1A CN202210330179A CN115283113B CN 115283113 B CN115283113 B CN 115283113B CN 202210330179 A CN202210330179 A CN 202210330179A CN 115283113 B CN115283113 B CN 115283113B
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grinding
feed additive
diameter
chromium
feed
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CN115283113A (en
Inventor
魏正显
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Baiyin Xinyinxin Industry And Trade Co ltd
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Baiyin Xinyinxin Industry And Trade Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C21/00Disintegrating plant with or without drying of the material
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K20/00Accessory food factors for animal feeding-stuffs
    • A23K20/20Inorganic substances, e.g. oligoelements
    • A23K20/24Compounds of alkaline earth metals, e.g. magnesium
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K40/00Shaping or working-up of animal feeding-stuffs
    • A23K40/10Shaping or working-up of animal feeding-stuffs by agglomeration; by granulation, e.g. making powders
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23KFODDER
    • A23K50/00Feeding-stuffs specially adapted for particular animals
    • A23K50/70Feeding-stuffs specially adapted for particular animals for birds
    • A23K50/75Feeding-stuffs specially adapted for particular animals for birds for poultry
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/10Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls with one or a few disintegrating members arranged in the container
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C17/00Disintegrating by tumbling mills, i.e. mills having a container charged with the material to be disintegrated with or without special disintegrating members such as pebbles or balls
    • B02C17/18Details
    • B02C17/20Disintegrating members
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C23/00Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
    • B02C23/18Adding fluid, other than for crushing or disintegrating by fluid energy
    • B02C23/20Adding fluid, other than for crushing or disintegrating by fluid energy after crushing or disintegrating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C4/00Crushing or disintegrating by roller mills
    • B02C4/28Details
    • B02C4/42Driving mechanisms; Roller speed control
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B24GRINDING; POLISHING
    • B24BMACHINES, DEVICES, OR PROCESSES FOR GRINDING OR POLISHING; DRESSING OR CONDITIONING OF ABRADING SURFACES; FEEDING OF GRINDING, POLISHING, OR LAPPING AGENTS
    • B24B27/00Other grinding machines or devices
    • B24B27/033Other grinding machines or devices for grinding a surface for cleaning purposes, e.g. for descaling or for grinding off flaws in the surface

Abstract

The application provides a feed additive and a preparation process thereof, and relates to the technical field of feeds. The manufacturing process combines rotary grinding, roller grinding and chrome ball milling to grind and polish the ore raw materials, so that the complex grinding process can be simplified, and meanwhile, the harmful substances introduced into the feed by a grinding mode can be avoided. In the manufacturing process, the particle size of the additive is smaller through a roller milling mode, then the raw materials are made into rice grains through chrome ball milling with various mixing diameters, so that the surfaces of the raw materials are smooth and have no edges and corners, and therefore, when the feed additive is used by poultry animals, the feed additive can not scratch organs such as oral cavities, throats, esophagus, crop and intestinal tracts of the poultry animals, and the infectious diseases of the poultry caused by damage of digestive systems can be effectively reduced.

Description

Feed additive and preparation process thereof
Technical Field
The application relates to the technical field of feeds, in particular to a feed additive and a preparation process thereof.
Background
Poultry refers to artificially fed birds, primarily for the purpose of obtaining their meat, eggs and feathers, as well as other uses. Typically, the animals are of the Phasianidae and Duck families, such as chickens, ducks, geese, quails, and the like, as well as birds of other families, such as turkeys, pigeons, and various singers. The meat and egg of poultry are rich in nutrition. The meat of poultry is rich in proteins, and also in phosphorus and other minerals, as well as in a large amount of complex vitamin B. Compared to most beef and pork, poultry has lower meat fat, while poultry liver is rich in vitamin a. For small farms and domestic diets, poultry are relatively more convenient living things because of their smaller individual size.
When raising poultry, a reasonably proportioned feed is required, and feed additives are particularly important for feeds. Because the existing calcium-containing feed additive mostly uses ores as additives, the ores are added through crushing when in use, and at the moment, the ores are easy to damage the esophagus and the digestive organs of the poultry, so that the digestive organ is infected with diseases, and the diseases are not easy to absorb, so that the use value is low.
Therefore, in order to solve the problems, a preparation method of the ore additive which has no damage to the digestive organs of the poultry is provided.
Disclosure of Invention
The application aims to provide a manufacturing process of poultry feed additive, which can manufacture ore additives in a combined grinding and polishing mode, is simple to manufacture, and the formed product is in the shape of rice grains, so that the effect of avoiding damage to esophagus and digestive organs of poultry animals is achieved, and the eating value is higher.
The application also aims to provide a feed additive which is prepared by the preparation process, has a rice grain shape, does not damage the esophagus and digestive organs of the poultry, can promote the absorption capacity of the poultry to inorganic elements in the mineral additive, and has good use effect.
The application solves the technical problems by adopting the following technical scheme.
On one hand, the application provides a preparation process of a feed additive, which mainly comprises the following steps:
pretreating ore raw materials, performing rotary rust removal, and then sorting to obtain rust removal powder; grinding the rust-removing powder by a pair of rollers to obtain fine powder; mixing chromium balls with various diameters, and grinding the fine powder by the mixed chromium balls to obtain a prefabricated product; and (3) carrying out multistage separation on the prefabricated products to obtain feed additives and residual products, wherein the particle size of the feed additives is 6-120 meshes.
In another aspect, the application provides a feed additive prepared by the preparation process of the feed additive.
The preparation process of the feed additive and the obtained feed additive have at least the following beneficial effects:
1. the application provides a manufacturing process of a feed additive, which combines a rotary mill, a pair-roller mill and a chrome ball mill to grind and polish ore raw materials, has the advantages of the grinding mode, can simplify the complicated grinding process, can avoid the harmful substances from being introduced into the feed by the grinding mode, and achieves the expected effect.
2. In the manufacturing process, the particle size of the additive is smaller in a double-roll grinding mode, and then the raw materials are made into rice grains through chromium ball milling of various mixed diameters, so that the method has the advantages of being simple in process and easy to operate, the yield of the feed additive can be improved, the utilization rate of the raw materials in the manufacturing process is maximized, and the economic benefit is high.
3. The rice-shaped feed additive prepared by the preparation process has smooth surface and no edges and corners, so that when the feed additive is used by poultry animals, the feed additive can not scratch organs such as oral cavity, throat, esophagus, crop, intestinal tract and the like of the poultry animals, thereby effectively reducing infectious diseases of the poultry caused by damage of digestive systems; in addition, the feed additive is in the shape of rice grains, so that the contact area of the feed additive is large, and at the moment, the absorption rate of the poultry to inorganic elements can be effectively improved after the feed additive is eaten, and the eating effect is good.
4. The feed additive prepared by the preparation process is similar to rice or millet, so that the dosage of organic feed can be reduced, and the raising cost can be lowered.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present application, the drawings that are needed in the embodiments will be briefly described below, it being understood that the following drawings only illustrate some embodiments of the present application and therefore should not be considered as limiting the scope, and other related drawings may be obtained according to these drawings without inventive effort for a person skilled in the art.
FIG. 1 is a photograph of a feed additive provided by the present application;
FIG. 2 is a photograph of an ore material provided by the present application (not prepared by the process of the present application);
fig. 3 is a photograph of crushed ore raw materials (not prepared by the preparation process according to the present application).
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present application more clear, the technical solutions of the embodiments of the present application will be clearly and completely described below. The specific conditions are not noted in the examples and are carried out according to conventional conditions or conditions recommended by the manufacturer. The reagents or apparatus used were conventional products commercially available without the manufacturer's attention.
It should be noted that, without conflict, the embodiments of the present application and features of the embodiments may be combined with each other. The present application will be described in detail with reference to specific examples.
On one hand, the application provides a preparation process of a feed additive, which mainly comprises the following steps:
pretreating ore raw materials, performing rotary rust removal, and then sorting to obtain rust removal powder; grinding the rust-removing powder by a pair of rollers to obtain fine powder; mixing chromium balls with various diameters, and grinding the fine powder by the mixed chromium balls to obtain a prefabricated product; and (3) carrying out multistage separation on the prefabricated products to obtain feed additives and residual products, wherein the particle size of the feed additives is 6-120 meshes.
Specifically, after the ore raw materials are pretreated, raw materials which are clean, low in water content and meeting requirements are obtained, at the moment, the raw materials are fed into a rotary mill to carry out rotary rust removal, and substances formed on the surfaces of the raw materials (influencing the quality of feed additives) can be removed through physical actions such as mutual collision, impact and friction among the raw materials, so that the expected rust removal effect is achieved. After rust removal, rust layer substances can be effectively prevented from being mixed into the feed additive, so that the use of poultry animals is influenced, and the meat quality of the poultry animals is further prevented from being influenced.
And after rotary rust removal, sorting is performed. In the application, the sorting mode is stepped jump type air separation, and the rust layer removed substances can be removed by the mode, so that the raw material for completely removing rust can be obtained. Because the mass of the rust layer material is lighter and the mass of the raw material is far greater than that of the rust layer material, the rust layer material can be completely removed by sorting in the way, and the requirements of finished products of feed additives are met.
It should be noted that in the process of rotary rust removal, the ore raw material with larger particle size can be crushed into the raw material with smaller particle size due to high-speed impact and collision, and the special crushing process can be omitted at this time, so that the process flow can be effectively simplified, the production time can be shortened, and the economic effect can be improved.
And (5) after the rust removing powder is prepared, performing double-roll grinding. The obtained rust-removing powder is uniformly pressed and ground in a roll grinding manner, and at this time, the rust-removing powder can be ground into fine powder with smaller particle size. Because the uniform pressure grinding is carried out in the roller grinding process, the controllability of the particle size of the fine powder is stronger in the grinding process, and meanwhile, the particle size of the rust removing powder can be quickly reduced, so that the expected effect is achieved.
It should be noted that the particle size of the fine powder is below 0.6cm after the uniform pressure grinding of the roller mill, and the particle size of the pretreated raw material is below 3cm, so that the particle size reduction effect is obvious, and the technological process of crushing and reducing the particle size can be saved.
And (3) after the fine powder is prepared, performing chromium ball milling. According to the application, the metal chromium balls with different diameters are mixed, and then the fine powder is added for grinding and polishing, so that the blocky or irregular fine powder can be gradually ground into rice-grain-shaped balls in the grinding process, and the expected manufacturing effect is achieved.
It should be noted here that the reason for selecting the metallic chrome balls for grinding and polishing is as follows: compared with steel balls, iron balls and the like, the metal chromium balls can not generate residual iron in the grinding and polishing processes, so that the metal iron is prevented from being contained in the feed additive, and the feed additive manufactured in the process is prevented from threatening poultry animals. The steel balls and the iron balls can generate scrap iron and/or rust by friction and collision in the polishing process, and the generated scrap iron and/or rust can be attached to the feed additive, so that the damage to poultry is generated. The metal chromium ball does not generate the phenomenon, so the safety is higher. Meanwhile, the wear resistance of the metal chromium balls is better, so that the metal chromium balls have higher use value and practical value when used for preparing feed additives.
After the prefabricated product is prepared, raw materials with various particle sizes can be separated, and the prefabricated product with 6 meshes to 120 meshes can be separated, so that the qualified feed additive can be obtained.
In the application, the multi-stage separation is performed by multi-stage cyclone air separation, and the wind speed is 18-23 m/s.
And then, continuously sorting the obtained residual products to obtain the high-grade feed additive meeting different requirements. Meanwhile, the sieved products can be respectively used as feed additives for young birds, middle birds and old birds according to the sieving particle size. Therefore, the feed additive and the product manufactured by the method can be used as feed, and the utilization rate is high.
In conclusion, the manufacturing process combines the rotary mill, the pair roller mill and the chrome ball mill to grind and polish the ore raw materials, so that the advantages of the grinding mode are achieved, the complicated grinding process can be simplified, meanwhile, the harmful substances can be prevented from being introduced into the feed by the grinding mode, and the expected effect is achieved.
In addition, in the manufacturing process, the particle size of the additive is smaller through a double-roller grinding mode, and then the raw materials are manufactured into smooth rice-shaped spheres through chrome ball milling of various mixed diameters, so that the method has the advantages of being simple in process and easy to operate, the yield of the feed additive can be improved, the utilization rate of the raw materials in the manufacturing process is maximized, and the economic benefit is higher.
In the application, the fine powder is ground by chromium balls as follows: mixing chromium balls with the diameter of 100mm, chromium balls with the diameter of 80mm, chromium balls with the diameter of 60mm and chromium balls with the diameter of 40mm, and carrying out primary grinding on the fine powder to obtain a coarse grinding product; mixing 30mm diameter chromium balls, 20mm diameter chromium balls and 10mm diameter chromium balls, and polishing the rough polished product for the second time to obtain the preform.
In detail, after mixing chromium balls with diameters of 40mm, 60mm, 80mm and 100mm, adding fine powder, polishing the surface of the fine powder with edges and corners to be smooth, and meanwhile, due to different diameters of the metal chromium balls, polishing the fine powder into a rice grain-shaped spherical structure in the polishing process, so that the expected effect is achieved.
And (3) grinding and polishing to obtain a coarse grinding product. And then the coarse grinding product is polished by metal chromium balls with the diameters of 10mm, 20mm and 30mm, and the coarse grinding product is further polished, so that the surface of the coarse grinding product is smoother, and the prepared feed additive is smooth in surface and does not damage organs such as oral cavity, throat, crop, intestinal tract and the like of poultry animals.
In the application, when the rotary rust removal is carried out, the rotary grinding rotating speed is 1400rpm-1500rpm, and the rotary rust removal time is 20s-30s. In addition, in the application, when the rotary mill is operated, the power is 500kw, and under the conditions, after the rotary mill stays for 20-35 s in the rotary mill equipment, the rust layer on the surface of the calcium ore can be completely removed, so that the expected effect is achieved.
In the application, when the double-roller grinding is carried out, the grinding pressure is 65bar-70bar, and the grinding time is 1s-3s.
In addition, in the present application, the maximum value of the pressure may be 2000pa to 3000pa, and thus, the pressure may be appropriately increased according to the actual operation situation or based on consideration of environmental factors.
In the present application, the particle size of the fine powder is 0.6cm or less. The raw materials below 3cm are pressed and ground to below 0.6cm, the pressing and grinding efficiency is high, meanwhile, the process can be simplified, and meanwhile, the expected effect can be achieved, so that the feed additive meets the qualified standard.
In the present application, the pretreatment of the ore raw material includes the following steps: ore raw materials are crushed again under the condition of drying, and the ore raw materials are separated to be less than 3cm for rotary rust removal. The water content of the raw materials can be effectively reduced after the drying, the efficiency of the separation and grinding processes is high, and the loss rate of the raw materials can be effectively reduced.
In the application, the residual products are screened and classified by a closed screen to obtain the product.
In the application, the ore raw material is calcium carbonate ore. The calcium carbonate ore is used as raw material to prepare the feed additive containing calcium. Of course, the ore with similar hardness or structure to the calcium carbonate ore can be polished and manufactured by the process to manufacture a product in the shape of rice grains.
In another aspect, the application provides a feed additive prepared by the preparation process. Specifically, the rice-shaped feed additive prepared by the preparation process has smooth surface and no edges and corners, so that when the feed additive is used by poultry animals, the feed additive can not scratch organs such as oral cavity, throat, esophagus, crop, intestinal tract and the like of the poultry animals, thereby effectively reducing infectious diseases of the poultry caused by damage of digestive systems; in addition, the feed additive is in the shape of rice grains, so that the contact area of the feed additive is large, and at the moment, the absorption rate of the poultry to inorganic elements can be effectively improved after the feed additive is eaten, and the eating effect is good.
The features and capabilities of the present application are described in further detail below in connection with the examples.
Example 1
The aim of the embodiment is to provide a manufacturing process of a feed additive, which comprises the following steps:
pretreating a calcium carbonate ore raw material, performing rotary rust removal, wherein the rotary grinding rotating speed is 1450rpm, the residence time in rotary grinding equipment is 30s, the power of the rotary grinding equipment is 500kw when the rotary grinding equipment operates, and then performing separation by stepped jump type air separation to obtain rust removal powder; carrying out double-roll grinding on the rust removing powder under the condition of grinding pressure of 65bar, wherein the grinding time is 1s-3s, and the fine powder is prepared, and the particle size of the fine powder is below 0.6 cm; mixing the chromium balls with various diameters, and grinding the fine powder by the mixed chromium balls to obtain a prefabricated product; the preform was subjected to multi-stage classification by multi-stage cyclone classification at a wind speed of 20m/s, whereby a feed additive having a particle size of 120 mesh and a residual product were obtained.
The specific steps of grinding the fine powder by chromium balls are as follows: mixing a chromium ball with the diameter of 100mm, a chromium ball with the diameter of 80mm, a chromium ball with the diameter of 60mm and a chromium ball with the diameter of 40mm, and carrying out primary grinding on the fine powder to obtain a coarse grinding product; mixing the chromium balls with the diameter of 30mm, the chromium balls with the diameter of 20mm and the chromium balls with the diameter of 10mm, and polishing the coarse polished product for the second time to obtain the prefabricated product.
Example 2
The aim of the embodiment is to provide a manufacturing process of a feed additive, which comprises the following steps:
pretreating a calcium carbonate ore raw material, performing rotary rust removal, wherein the rotary grinding rotating speed is 1400rpm, the residence time in rotary grinding equipment is 20s, the power of the rotary grinding equipment is 500kw when the rotary grinding equipment operates, and then separating by gradient jump type air separation to obtain rust removal powder; carrying out double-roll grinding on the rust removing powder under the condition of grinding pressure of 65bar, wherein the grinding time is 1s-3s, and the fine powder is prepared, and the particle size of the fine powder is below 0.6 cm; mixing the chromium balls with various diameters, and grinding the fine powder by the mixed chromium balls to obtain a prefabricated product; the preform was subjected to multi-stage classification by multi-stage cyclone classification at a wind speed of 18m/s, whereby a feed additive having a particle size of 120 mesh and a residual product were obtained. Screening and grading the rest products by a closed screen to obtain feed products suitable for young birds, medium birds and old birds respectively.
The specific steps of grinding the fine powder by chromium balls are as follows: mixing a chromium ball with the diameter of 100mm, a chromium ball with the diameter of 80mm, a chromium ball with the diameter of 60mm and a chromium ball with the diameter of 40mm, and carrying out primary grinding on the fine powder to obtain a coarse grinding product; mixing the chromium balls with the diameter of 30mm, the chromium balls with the diameter of 20mm and the chromium balls with the diameter of 10mm, and polishing the coarse polished product for the second time to obtain the prefabricated product.
Example 3
The aim of the embodiment is to provide a manufacturing process of a feed additive, which comprises the following steps:
crushing a calcium carbonate ore raw material under a drying condition, screening out raw materials with the size of less than 3cm, carrying out rotary rust removal, wherein the rotary grinding rotating speed is 1450rpm, the residence time in rotary grinding equipment is 30s, the power of the rotary grinding equipment is 500kw when the rotary grinding equipment operates, and then carrying out separation by ladder-shaped jump type winnowing to obtain rust removal powder; carrying out double-roll grinding on the rust removing powder under the condition of grinding pressure of 65bar, wherein the grinding time is 1s-3s, and the fine powder is prepared, and the particle size of the fine powder is below 0.6 cm; mixing the chromium balls with various diameters, and grinding the fine powder by the mixed chromium balls to obtain a prefabricated product; the preform was subjected to multi-stage classification by multi-stage cyclone classification at a wind speed of 20m/s, whereby a feed additive having a particle size of 120 mesh and a residual product were obtained. Screening and grading the rest products by a closed screen to obtain feed products suitable for young birds, medium birds and old birds respectively.
The specific steps of grinding the fine powder by chromium balls are as follows: mixing a chromium ball with the diameter of 100mm, a chromium ball with the diameter of 80mm, a chromium ball with the diameter of 60mm and a chromium ball with the diameter of 40mm, and carrying out primary grinding on the fine powder to obtain a coarse grinding product; mixing the chromium balls with the diameter of 30mm, the chromium balls with the diameter of 20mm and the chromium balls with the diameter of 10mm, and polishing the coarse polished product for the second time to obtain the prefabricated product.
Example 4
The aim of the embodiment is to provide a manufacturing process of a feed additive, which comprises the following steps:
crushing a calcium carbonate ore raw material under a drying condition, screening out raw materials with the size of less than 3cm, carrying out rotary rust removal, wherein the rotary grinding rotating speed is 1500rpm, the residence time in rotary grinding equipment is 35s, the power of the rotary grinding equipment is 500kw when the rotary grinding equipment operates, and then carrying out separation by ladder-shaped jump type winnowing to obtain rust removal powder; carrying out double-roll grinding on the rust removing powder under the condition of grinding pressure of 70bar, wherein the grinding time is 1s-3s, and the fine powder is prepared, and the particle size of the fine powder is below 0.6 cm; mixing the chromium balls with various diameters, and grinding the fine powder by the mixed chromium balls to obtain a prefabricated product; and carrying out multistage separation on the prefabricated products in a multistage cyclone separation mode, wherein the wind speed is 23m/s, so that the feed additive and the residual products are obtained, and the particle size of the feed additive is 6-14 meshes. Screening and grading the rest products by a closed screen to obtain feed products suitable for young birds, medium birds and old birds respectively.
The specific steps of grinding the fine powder by chromium balls are as follows: mixing a chromium ball with the diameter of 100mm, a chromium ball with the diameter of 80mm, a chromium ball with the diameter of 60mm and a chromium ball with the diameter of 40mm, and carrying out primary grinding on the fine powder to obtain a coarse grinding product; mixing the chromium balls with the diameter of 30mm, the chromium balls with the diameter of 20mm and the chromium balls with the diameter of 10mm, and polishing the coarse polished product for the second time to obtain the prefabricated product.
Example 5
The aim of the embodiment is to provide a manufacturing process of a feed additive, which comprises the following steps:
crushing a calcium carbonate ore raw material under a drying condition, screening out raw materials with the size of less than 3cm, carrying out rotary rust removal, wherein the rotary grinding rotating speed is 1500rpm, the residence time in rotary grinding equipment is 35s, the power of the rotary grinding equipment is 500kw when the rotary grinding equipment operates, and then carrying out separation by ladder-shaped jump type winnowing to obtain rust removal powder; carrying out double-roll grinding on the rust removing powder under the condition of grinding pressure of 70bar, wherein the grinding time is 1s-3s, and the fine powder is prepared, and the particle size of the fine powder is below 0.6 cm; mixing the chromium balls with various diameters, and grinding the fine powder by the mixed chromium balls to obtain a prefabricated product; and carrying out multistage separation on the prefabricated products in a multistage cyclone separation mode, wherein the wind speed is 23m/s, so that the feed additive and the residual products are obtained, and the particle size of the feed additive is 40-60 meshes. Screening and grading the rest products by a closed screen to obtain feed products suitable for young birds, medium birds and old birds respectively.
The specific steps of grinding the fine powder by chromium balls are as follows: mixing a chromium ball with the diameter of 100mm, a chromium ball with the diameter of 80mm, a chromium ball with the diameter of 60mm and a chromium ball with the diameter of 40mm, and carrying out primary grinding on the fine powder to obtain a coarse grinding product; mixing the chromium balls with the diameter of 30mm, the chromium balls with the diameter of 20mm and the chromium balls with the diameter of 10mm, and polishing the coarse polished product for the second time to obtain the prefabricated product.
Example 6
The purpose of this example was to add the feed additives prepared by the preparation process provided in examples 1 to 3 to the basal feeds for chickens to prepare a chicken feed 1, a chicken feed 2 and a chicken feed 3, respectively.
Comparative example 1
The comparative example differs from example 3 in that the grinding was performed using chromium balls of the same diameter, the diameter of each of the chromium balls was 80mm, and the number of the chromium balls was identical.
The feed additive prepared by the preparation process is added into basic feed of chickens to prepare the chicken feed.
Comparative example 2
The comparative example differs from example 3 in that the rotational speed of the rotary mill is 800rpm.
The feed additive prepared by the preparation process is added into basic feed of chickens to prepare the chicken feed.
Comparative example 3
The difference between this comparative example and example 3 is that the pressure of the counter roller mill is 40bar.
The feed additive prepared by the preparation process is added into basic feed of chickens to prepare the chicken feed.
Effect example 1
The feed additive prepared in example 1 was compared with the ore raw material not subjected to the above-mentioned manufacturing process, and the comparison results are shown in fig. 1 and 2.
As can be seen from the figures, the calcium-containing feed additive prepared in examples 1-3 had smooth surfaces and had a spherical shape in the form of rice grains, and the expected effect could be achieved. The surface of the ore raw material which is not subjected to the preparation process has edges and corners, and when the ore raw material is crushed and directly added into feed, the ore raw material is easily damaged in the oral cavity, throat, crop, intestinal tract and the like of the poultry animal as shown in fig. 3.
It should be noted here that comparative example 1 was not polished with chromium balls of different diameters, and thus had a spherical shape instead of rice grains.
Effect example 2
The chicken feeds prepared in example 6 and the chicken feeds prepared in comparative examples 1 to 3 were fed to chickens, and the feeding results were observed. The number of chickens in each group was 20, the initial average weight was (1.8.+ -. 1.67) kg, and the weight range was 1.5kg-2.4kg. The feeding method is that the feed is fed twice a day, the feeding amount is the same, and the feeding quality of each group is the same.
Setting of control group: ore raw materials which were not polished by the manufacturing process of the present application were screened to obtain 120 mesh additives, which were then mixed with basal feeds and fed under the same conditions as in the examples and comparative examples.
TABLE 1 feeding results
As can be seen from the table, the preparation process provided by the application can effectively reduce the intestinal tract disease infection rate of chickens after polishing the calcium-containing ore raw materials, and can improve the absorption effect of the calcium and other nutritional ingredients in the feed, and at the moment, the average weight gain of the chickens is higher, the feeding effect is better, and the use value is higher.
In summary, the application provides a manufacturing process of a feed additive, which combines rotary grinding, roller grinding and chrome ball grinding to grind and polish ore raw materials, has the advantages of the grinding mode, can simplify complicated grinding process, and can avoid the grinding mode to introduce harmful substances into feed so as to achieve the expected effect. In the manufacturing process, the particle size of the additive is smaller in a double-roll grinding mode, and then the raw materials are made into rice grains through chromium ball milling of various mixed diameters, so that the method has the advantages of being simple in process and easy to operate, the yield of the feed additive can be improved, the utilization rate of the raw materials in the manufacturing process is maximized, and the economic benefit is high. The rice-shaped feed additive prepared by the preparation process has smooth surface and no edges and corners, so that when the feed additive is used by poultry animals, the feed additive can not scratch organs such as oral cavity, throat, esophagus, crop, intestinal tract and the like of the poultry animals, thereby effectively reducing infectious diseases of the poultry caused by damage of digestive systems; in addition, the feed additive is in the shape of rice grains, so that the contact area of the feed additive is large, and at the moment, the absorption rate of the poultry to inorganic elements can be effectively improved after the feed additive is eaten, and the eating effect is good. The feed additive prepared by the preparation process is similar to rice or millet, so that the dosage of organic feed can be reduced, and the raising cost can be lowered.
The embodiments described above are some, but not all embodiments of the application. The detailed description of the embodiments of the application is not intended to limit the scope of the application, as claimed, but is merely representative of selected embodiments of the application. All other embodiments, which can be made by those skilled in the art based on the embodiments of the application without making any inventive effort, are intended to be within the scope of the application.

Claims (8)

1. The preparation process of the feed additive is characterized by comprising the following steps of:
crushing ore raw materials under the condition of drying, separating ore raw materials below 3cm, performing rotary rust removal in rotary grinding, and removing substances formed on the surfaces of the ore raw materials through the physical actions of mutual collision, impact and friction among the raw materials; sorting to obtain rust-removing powder; grinding the rust-removing powder by a pair of rollers to obtain fine powder; mixing chromium balls with various diameters, mixing chromium balls with the diameter of 100mm, chromium balls with the diameter of 80mm, chromium balls with the diameter of 60mm and chromium balls with the diameter of 40mm, and carrying out primary grinding on the fine powder to obtain a coarse ground product; mixing the chromium balls with the diameter of 30mm, the chromium balls with the diameter of 20mm and the chromium balls with the diameter of 10mm, and polishing the coarse polished product for the second time to obtain a rice-shaped spherical prefabricated product; and (3) carrying out multistage separation on the prefabricated products to obtain feed additives and residual products, wherein the particle size of the feed additives is 6-120 meshes.
2. The process for preparing a feed additive according to claim 1, wherein the rotary grinding speed is 1400rpm-1500rpm and the rotary rust removing time is 20s-35 s.
3. The process for preparing a feed additive according to any one of claims 1 to 2, wherein the grinding is carried out at a pressure of 65bar to 70bar for a period of 1s to 3s.
4. The process for producing a feed additive according to claim 3, wherein the fine powder has a particle size of 0.6 to cm.
5. The process for preparing a feed additive according to claim 1, wherein the remaining product is classified by a closed sieve to obtain a product.
6. The process for preparing a feed additive according to claim 1, wherein the ore raw material is calcium carbonate ore.
7. The process for preparing the feed additive according to claim 1, wherein the multi-stage separation is performed by multi-stage cyclone separation, and the wind speed is 18m/s-23m/s.
8. A feed additive, characterized in that it is produced by the production process of the feed additive according to any one of claims 1 to 7.
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