CN115282631B - Chitosan oligosaccharide component extraction element - Google Patents
Chitosan oligosaccharide component extraction element Download PDFInfo
- Publication number
- CN115282631B CN115282631B CN202111639359.XA CN202111639359A CN115282631B CN 115282631 B CN115282631 B CN 115282631B CN 202111639359 A CN202111639359 A CN 202111639359A CN 115282631 B CN115282631 B CN 115282631B
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- CN
- China
- Prior art keywords
- stirring plate
- chitosan oligosaccharide
- upper cover
- extraction tank
- stirring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- RQFQJYYMBWVMQG-IXDPLRRUSA-N chitotriose Chemical compound O[C@@H]1[C@@H](N)[C@H](O)O[C@H](CO)[C@H]1O[C@H]1[C@H](N)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)N)[C@@H](CO)O1 RQFQJYYMBWVMQG-IXDPLRRUSA-N 0.000 title claims abstract description 64
- 238000000605 extraction Methods 0.000 title claims abstract description 53
- 230000000144 pharmacologic effect Effects 0.000 claims abstract description 13
- 210000005069 ears Anatomy 0.000 claims abstract 3
- 238000003756 stirring Methods 0.000 claims description 97
- 239000000284 extract Substances 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 239000004615 ingredient Substances 0.000 claims description 3
- 238000013019 agitation Methods 0.000 abstract description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 229920001661 Chitosan Polymers 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 239000003814 drug Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 229920001542 oligosaccharide Polymers 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 230000006978 adaptation Effects 0.000 description 2
- -1 amino oligosaccharide Chemical class 0.000 description 2
- 230000002146 bilateral effect Effects 0.000 description 2
- 238000003958 fumigation Methods 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 241000238557 Decapoda Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 238000002144 chemical decomposition reaction Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000000593 degrading effect Effects 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 150000002482 oligosaccharides Chemical class 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0223—Moving bed of solid material
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0006—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid
- C08B37/0024—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid beta-D-Glucans; (beta-1,3)-D-Glucans, e.g. paramylon, coriolan, sclerotan, pachyman, callose, scleroglucan, schizophyllan, laminaran, lentinan or curdlan; (beta-1,6)-D-Glucans, e.g. pustulan; (beta-1,4)-D-Glucans; (beta-1,3)(beta-1,4)-D-Glucans, e.g. lichenan; Derivatives thereof
- C08B37/0027—2-Acetamido-2-deoxy-beta-glucans; Derivatives thereof
- C08B37/003—Chitin, i.e. 2-acetamido-2-deoxy-(beta-1,4)-D-glucan or N-acetyl-beta-1,4-D-glucosamine; Chitosan, i.e. deacetylated product of chitin or (beta-1,4)-D-glucosamine; Derivatives thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The invention discloses a chitosan oligosaccharide component extraction device, which comprises an extractor integral structure, wherein the extractor integral structure comprises a pharmacological extraction tank, an extraction tank upper cover, an agitation plate hanging frame and a chitosan oligosaccharide agitation plate, the extraction tank upper cover is nested at the outer side of the agitation plate hanging frame, the chitosan oligosaccharide agitation plate is arranged at the bottom end of the agitation plate hanging frame, two sides of the top end of the pharmacological extraction tank are symmetrically provided with tank ears, and the bottom end of the pharmacological extraction tank is provided with an extraction tank base.
Description
Technical Field
The invention belongs to the technical field of traditional Chinese medicine component extraction equipment, and particularly relates to a chitosan oligosaccharide component extraction device.
Background
The chitosan oligosaccharide, also called as chitosan oligosaccharide and chitosan oligosaccharide, is an oligosaccharide product with polymerization degree of 2-20, which is obtained by degrading chitosan by a special biological enzyme technology (reports of chemical degradation and microwave degradation technology are also used), has molecular weight of less than or equal to 3200Da, and is a low molecular weight product with good water solubility, large function and high bioactivity. The chitosan has the unique functions of high solubility, complete dissolution in water, easy absorption and utilization by organism, etc., and the effect is 14 times of that of chitosan.
The chitosan oligosaccharide is the only positive charge cation alkaline amino oligosaccharide in nature and is animal cellulose. The chitosan oligosaccharide is a small molecule oligosaccharide with amino groups, which is degraded by chitosan derived from shrimp and crab shells, and is a sugar chain with polymerization degree of 2-20.
There are many extraction modes of chitosan oligosaccharide components, generally, the raw materials are firstly crushed into particles, then the particles are extracted into water by fumigation, decoction and other modes, and then the effective components of the chitosan oligosaccharide are concentrated and extracted by filtration, distillation, purification and other modes, but the fumigation and the decoction modes all require higher temperature, and the mode is not suitable for extracting the chitosan oligosaccharide which is easy to denature at high temperature, so that the method is not scientific and practical.
Disclosure of Invention
The invention aims to provide a chitosan oligosaccharide component extraction device so as to solve the problems in the background technology.
In order to achieve the above purpose, the present invention provides the following technical solutions: the utility model provides a chitosan oligosaccharide ingredient extraction element, includes extractor overall structure, extractor overall structure includes pharmacology extraction tank, extracts tank upper cover, stirring board gallows and chitosan oligosaccharide stirring board, it is nested in the outside of stirring board gallows to extract tank upper cover, chitosan oligosaccharide stirring board installs the bottom at stirring board gallows, pharmacology extraction tank's top bilateral symmetry is provided with the cage shoe, and pharmacology extraction tank's bottom is provided with extracts tank base, the upper surface of cage shoe is provided with the spacing double-screw bolt of upper cover, the outside nestification of the spacing double-screw bolt of upper cover has the spacing cap of upper cover, it is spacing fixed through the spacing cap of upper cover to extract tank upper cover and pharmacology extraction tank, pharmacology extraction tank's bottom one side is provided with the solution delivery tube, the one end of solution delivery tube is provided with the pipe cap.
Preferably, the stirring plate hanging frame comprises stirring plate hanging rods, two stirring plate hanging rods are arranged, a hanging rod handle is arranged between the top ends of the stirring plate hanging rods, lifting ring limiting pieces are arranged on one side of the bottom ends of the stirring plate hanging rods, and lifting ring limiting grooves are formed in one sides of the lifting ring limiting pieces and the stirring plate hanging rods.
Preferably, one side of the chitosan oligosaccharide stirring plate is provided with a stirring plate hanging ring, liquid draining holes are uniformly formed in the inner edge of the chitosan oligosaccharide stirring plate, the other side of the chitosan oligosaccharide stirring plate is uniformly provided with a stirring rod, and a hanging ring seat is arranged between the stirring plate hanging ring and the chitosan oligosaccharide stirring plate.
Preferably, the size phase adaptation of rings spacing groove and stirring board rings, rings spacing piece and stirring board jib pass through bolt fixed connection.
Preferably, the inside symmetry of extracting jar upper cover has seted up the spacing hole of jib, the spacing hole of jib and the size looks adaptation of stirring board jib, the bottom side center of extracting jar upper cover is provided with drive screw.
Preferably, the upper cover limiting cap and the upper cover limiting stud are connected through threaded screwing.
Preferably, the pipe cap is connected with the solution delivery pipe through screw threads in a screwing mode, and a filter screen is arranged inside one end, far away from the pipe cap, of the solution delivery pipe.
Preferably, the center of the chitosan oligosaccharide stirring plate is provided with a threaded hole matched with the driving screw, and the chitosan oligosaccharide stirring plate is connected with the driving screw through threaded screwing.
Compared with the prior art, the invention has the beneficial effects that: according to the novel extraction method, after chitosan oligosaccharide particles and normal-temperature water are placed into the medicine extraction tank, the stirring plate hanging frame is directly and repeatedly lifted and pressed, when the stirring plate hanging frame drives the chitosan oligosaccharide stirring plate to lift, the chitosan oligosaccharide stirring plate can automatically rotate under the drive of the external threads of the driving screw, the rotating chitosan oligosaccharide stirring plate can repeatedly stir and squeeze the middle chitosan oligosaccharide, pharmacological components of the chitosan oligosaccharide are extracted at normal temperature, the extraction method is simple and convenient, the high-temperature extraction modes such as decoction and the like are avoided, and the practicability is higher.
Drawings
FIG. 1 is a schematic perspective view of the present invention;
FIG. 2 is a schematic perspective view showing the connection mode among the upper cover of the extracting pot, the hanger of the stirring plate and the stirring plate of the chitosan oligosaccharide;
FIG. 3 is a schematic perspective view of a chitosan oligosaccharide stirring plate according to the invention;
FIG. 4 is a schematic perspective view showing the connection between the upper lid of the extraction tank and the hanger of the agitation plate in accordance with the present invention;
FIG. 5 is a schematic view of a partial perspective view of the connection between the hanger ring and hanger bar of the stirring plate of the present invention;
FIG. 6 is a schematic view of a partial three-dimensional explosion structure of the mounting mode of the lifting ring limiting piece of the invention;
in the figure: 1. the overall structure of the extractor; 101. a pharmacological extraction pot; 111. a cage ear; 112. an upper cover limit stud; 113. an upper cover limit cap; 114. a solution delivery tube; 115. a tube cap; 116. an extraction tank base; 102. an extraction tank upper cover; 121. a boom limit hole; 122. driving a screw; 103. an agitating plate hanger; 131. stirring plate suspenders; 132. a boom handle; 133. a hanging ring limiting piece; 134. a hanging ring limit groove; 104. a chitosan oligosaccharide stirring plate; 141. a liquid discharge hole; 142. an agitating rod; 143. stirring plate hanging rings; 144. and a hanging ring seat.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention.
Referring to fig. 1-6, the present invention provides the following technical solutions: the utility model provides a chitosan oligosaccharide ingredient extraction device, including extractor overall structure 1, extractor overall structure 1 includes pharmacology extraction tank 101, extract tank upper cover 102, stirring board gallows 103 and chitosan oligosaccharide stirring board 104, it is nested in the outside of stirring board gallows 103 to extract tank upper cover 102, chitosan oligosaccharide stirring board 104 installs in the bottom of stirring board gallows 103, pharmacology extraction tank 101's top bilateral symmetry is provided with cage shoe 111, and pharmacology extraction tank 101's bottom is provided with extraction tank base 116, cage shoe 111's upper surface is provided with upper cover spacing double-screw bolt 112, upper cover spacing cap 113 is nested in the outside of upper cover spacing double-screw bolt 112, extraction tank upper cover 102 and pharmacology extraction tank 101 are spacing fixed through upper cover spacing cap 113, pharmacology extraction tank 101's bottom one side is provided with solution delivery tube 114, one end of solution delivery tube 114 is provided with tube cap 115.
In order to enable the stirring plate hanging frame 103 to drive the chitosan oligosaccharide stirring plate 104 to lift, in this embodiment, preferably, the stirring plate hanging frame 103 comprises two stirring plate hanging rods 131, a hanging rod handle 132 is arranged between the top ends of the two stirring plate hanging rods 131, a hanging ring limiting piece 133 is arranged on one side of the bottom end of the stirring plate hanging rod 131, and hanging ring limiting grooves 134 are formed in one sides of the hanging ring limiting piece 133 and the stirring plate hanging rod 131.
In order to make the chitosan oligosaccharide stirring plate 104 smoothly rotate in a lifting state, in this embodiment, preferably, one side of the chitosan oligosaccharide stirring plate 104 is provided with a stirring plate lifting ring 143, the inner edge of the chitosan oligosaccharide stirring plate 104 is uniformly provided with a liquid discharge hole 141, the other side of the chitosan oligosaccharide stirring plate 104 is uniformly provided with a stirring rod 142, and a lifting ring seat 144 is arranged between the stirring plate lifting ring 143 and the chitosan oligosaccharide stirring plate 104.
In order to make the rotation resistance of the stirring plate hanging ring 143 smaller, in this embodiment, it is preferable that the hanging ring limiting groove 134 and the stirring plate hanging ring 143 are matched in size, and the hanging ring limiting piece 133 and the stirring plate hanging rod 131 are fixedly connected through bolts.
In order to facilitate drawing and pressing down of the stirring plate hanging rod 131, in this embodiment, preferably, hanging rod limiting holes 121 are symmetrically formed in the upper cover 102 of the extraction tank, the size of the hanging rod limiting holes 121 is matched with that of the stirring plate hanging rod 131, and a driving screw 122 is arranged in the center of the bottom side of the upper cover 102 of the extraction tank.
In order to enable the upper cap limit cap 113 to press and fix the upper cap 102 of the extraction tank, in this embodiment, it is preferable that the upper cap limit cap 113 and the upper cap limit stud 112 are connected by screwing.
In order to better filter the solution, in this embodiment, it is preferable that the cap 115 and the solution delivery tube 114 are screwed together, and a filter screen is provided inside one end of the solution delivery tube 114 away from the cap 115.
In order to enable the chitosan oligosaccharide stirring plate 104 to automatically rotate in the lifting process, in this embodiment, preferably, a threaded hole matched with the driving screw 122 is formed in the center of the chitosan oligosaccharide stirring plate 104, and the chitosan oligosaccharide stirring plate 104 and the driving screw 122 are connected through threaded screwing.
In order to avoid the chitosan oligosaccharide from blocking the drain hole 141, in this embodiment, it is preferable that a filter screen is provided at the bottom side of the drain hole 141.
The working principle and the using flow of the invention are as follows: after the invention is installed, the invention is firstly checked for installation and safety protection, then the invention can be used, when in use, the upper cover limit cap 113 is firstly screwed and disassembled, then the upper cover 102 of the extraction tank, the stirring plate hanging frame 103 and the chitosan oligosaccharide stirring plate 104 are taken out, then a proper amount of the crushed chitosan oligosaccharide raw material and normal temperature water are respectively poured into the medicine extraction tank 101, then the upper cover 102 of the extraction tank, the stirring plate hanging frame 103 and the chitosan oligosaccharide stirring plate 104 are replaced, the upper cover limit cap 113 is screwed and screwed, at the moment, the boom handle 132 is repeatedly pulled and pressed down, the stirring plate hanging rod 131 drives the chitosan oligosaccharide stirring plate 104 to lift and descend in the pulling and pressing processes, the chitosan oligosaccharide stirring plate 104 is matched with the threads on the outer side of the driving screw 122 in the lifting and descending processes, the rotating chitosan oligosaccharide stirring plate 104 drives the stirring rod 142 to stir and squeeze the chitosan oligosaccharide, the pharmacological components of the chitosan oligosaccharide are lifted, after the corresponding container is fully stirred, the pharmacological components of the chitosan oligosaccharide are placed at the tail end of the delivery container, and the pharmacological components are contained in the tube 114, and the pharmacological components are poured out.
Although embodiments of the present invention have been shown and described, it will be understood by those skilled in the art that various changes, modifications, substitutions and alterations can be made therein without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (1)
1. The utility model provides a chitosan oligosaccharide ingredient extraction element, includes extractor overall structure (1), extractor overall structure (1) are including pharmacology extraction tank (101), extract tank upper cover (102), stirring board gallows (103) and chitosan oligosaccharide stirring board (104), its characterized in that: the extraction tank upper cover (102) is nested outside the stirring plate hanging frame (103), the chitosan oligosaccharide stirring plate (104) is installed at the bottom end of the stirring plate hanging frame (103), tank ears (111) are symmetrically arranged on two sides of the top end of the pharmacological extraction tank (101), an extraction tank base (116) is arranged at the bottom end of the pharmacological extraction tank (101), an upper cover limit stud (112) is arranged on the upper surface of the tank ears (111), an upper cover limit cap (113) is nested outside the upper cover limit stud (112), the extraction tank upper cover (102) and the pharmacological extraction tank (101) are limited and fixed through the upper cover limit cap (113), a solution delivery pipe (114) is arranged on one side of the bottom end of the pharmacological extraction tank (101), and a pipe cap (115) is arranged at one end of the solution delivery pipe (114);
the stirring plate hanging frame (103) comprises stirring plate hanging rods (131), two stirring plate hanging rods (131) are arranged, a hanging rod handle (132) is arranged between the top ends of the two stirring plate hanging rods (131), a hanging ring limiting piece (133) is arranged on one side of the bottom end of each stirring plate hanging rod (131), and hanging ring limiting grooves (134) are formed in one side of each hanging ring limiting piece (133) and one side of each stirring plate hanging rod (131);
one side of the chitosan oligosaccharide stirring plate (104) is provided with stirring plate hanging rings (143), liquid discharge holes (141) are uniformly formed in the inner edge of the chitosan oligosaccharide stirring plate (104), stirring rods (142) are uniformly arranged on the other side of the chitosan oligosaccharide stirring plate (104), and hanging ring seats (144) are arranged between the stirring plate hanging rings (143) and the chitosan oligosaccharide stirring plate (104);
the sizes of the lifting ring limiting grooves (134) and the stirring plate lifting rings (143) are matched, and the lifting ring limiting pieces (133) and the stirring plate lifting rods (131) are fixedly connected through bolts;
the extraction tank is characterized in that a boom limiting hole (121) is symmetrically formed in the extraction tank upper cover (102), the boom limiting hole (121) is matched with the stirring plate boom (131) in size, and a driving screw (122) is arranged in the center of the bottom side of the extraction tank upper cover (102);
the upper cover limit cap (113) and the upper cover limit stud (112) are connected through screw threads in a screwing mode;
the pipe cap (115) is connected with the solution delivery pipe (114) through screw threads in a screwing mode, and a filter screen is arranged inside one end, far away from the pipe cap (115), of the solution delivery pipe (114);
screw holes matched with the driving screw rods (122) are formed in the centers of the chitosan oligosaccharide stirring plates (104), and the chitosan oligosaccharide stirring plates (104) and the driving screw rods (122) are connected through screw threads in a screwing mode.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111639359.XA CN115282631B (en) | 2021-12-29 | 2021-12-29 | Chitosan oligosaccharide component extraction element |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111639359.XA CN115282631B (en) | 2021-12-29 | 2021-12-29 | Chitosan oligosaccharide component extraction element |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN115282631A CN115282631A (en) | 2022-11-04 |
| CN115282631B true CN115282631B (en) | 2024-02-02 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202111639359.XA Active CN115282631B (en) | 2021-12-29 | 2021-12-29 | Chitosan oligosaccharide component extraction element |
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| Country | Link |
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| CN (1) | CN115282631B (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008284474A (en) * | 2007-05-18 | 2008-11-27 | Apt Machinery:Kk | Revolving/rotating mixer |
| JP2009106847A (en) * | 2007-10-30 | 2009-05-21 | Fukoku Kogyo Kk | Coagulation reactor |
| CN108852840A (en) * | 2018-07-12 | 2018-11-23 | 合肥七小俊生物科技有限公司 | A kind of Chinese medicine ceramic medicine decoction device |
| CN213159488U (en) * | 2020-09-07 | 2021-05-11 | 浙江博美生物技术有限公司 | Extraction equipment with self-filtering function |
| CN213466850U (en) * | 2020-10-22 | 2021-06-18 | 河南应用技术职业学院 | Extraction and separation device for chemical engineering practical training |
-
2021
- 2021-12-29 CN CN202111639359.XA patent/CN115282631B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008284474A (en) * | 2007-05-18 | 2008-11-27 | Apt Machinery:Kk | Revolving/rotating mixer |
| JP2009106847A (en) * | 2007-10-30 | 2009-05-21 | Fukoku Kogyo Kk | Coagulation reactor |
| CN108852840A (en) * | 2018-07-12 | 2018-11-23 | 合肥七小俊生物科技有限公司 | A kind of Chinese medicine ceramic medicine decoction device |
| CN213159488U (en) * | 2020-09-07 | 2021-05-11 | 浙江博美生物技术有限公司 | Extraction equipment with self-filtering function |
| CN213466850U (en) * | 2020-10-22 | 2021-06-18 | 河南应用技术职业学院 | Extraction and separation device for chemical engineering practical training |
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| Publication number | Publication date |
|---|---|
| CN115282631A (en) | 2022-11-04 |
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