CN115282631A - Chitosan oligosaccharide component extraction device - Google Patents
Chitosan oligosaccharide component extraction device Download PDFInfo
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- CN115282631A CN115282631A CN202111639359.XA CN202111639359A CN115282631A CN 115282631 A CN115282631 A CN 115282631A CN 202111639359 A CN202111639359 A CN 202111639359A CN 115282631 A CN115282631 A CN 115282631A
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- China
- Prior art keywords
- chitosan oligosaccharide
- stirring plate
- upper cover
- board
- stirring
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Links
- RQFQJYYMBWVMQG-IXDPLRRUSA-N chitotriose Chemical compound O[C@@H]1[C@@H](N)[C@H](O)O[C@H](CO)[C@H]1O[C@H]1[C@H](N)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O2)N)[C@@H](CO)O1 RQFQJYYMBWVMQG-IXDPLRRUSA-N 0.000 title claims abstract description 65
- 238000000605 extraction Methods 0.000 title claims abstract description 44
- 238000003756 stirring Methods 0.000 claims abstract description 102
- 239000004615 ingredient Substances 0.000 claims description 8
- 239000007788 liquid Substances 0.000 claims description 4
- 239000000203 mixture Substances 0.000 claims description 4
- 230000002146 bilateral effect Effects 0.000 claims description 3
- 230000000144 pharmacologic effect Effects 0.000 abstract description 8
- 229920001661 Chitosan Polymers 0.000 description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 239000002245 particle Substances 0.000 description 4
- 229920001542 oligosaccharide Polymers 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 239000000284 extract Substances 0.000 description 2
- 238000003958 fumigation Methods 0.000 description 2
- 150000002482 oligosaccharides Chemical class 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 241000238557 Decapoda Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- 125000003277 amino group Chemical group 0.000 description 1
- -1 amino oligosaccharide Chemical class 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 230000000903 blocking effect Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 229920002678 cellulose Polymers 0.000 description 1
- 239000001913 cellulose Substances 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- 238000002144 chemical decomposition reaction Methods 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 238000006731 degradation reaction Methods 0.000 description 1
- 230000000593 degrading effect Effects 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0223—Moving bed of solid material
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08B—POLYSACCHARIDES; DERIVATIVES THEREOF
- C08B37/00—Preparation of polysaccharides not provided for in groups C08B1/00 - C08B35/00; Derivatives thereof
- C08B37/0006—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid
- C08B37/0024—Homoglycans, i.e. polysaccharides having a main chain consisting of one single sugar, e.g. colominic acid beta-D-Glucans; (beta-1,3)-D-Glucans, e.g. paramylon, coriolan, sclerotan, pachyman, callose, scleroglucan, schizophyllan, laminaran, lentinan or curdlan; (beta-1,6)-D-Glucans, e.g. pustulan; (beta-1,4)-D-Glucans; (beta-1,3)(beta-1,4)-D-Glucans, e.g. lichenan; Derivatives thereof
- C08B37/0027—2-Acetamido-2-deoxy-beta-glucans; Derivatives thereof
- C08B37/003—Chitin, i.e. 2-acetamido-2-deoxy-(beta-1,4)-D-glucan or N-acetyl-beta-1,4-D-glucosamine; Chitosan, i.e. deacetylated product of chitin or (beta-1,4)-D-glucosamine; Derivatives thereof
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Materials Engineering (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
Abstract
The invention discloses a chitosan oligosaccharide component extraction device, which comprises an extractor overall structure, wherein the extractor overall structure comprises a pharmacological extraction tank, an extraction tank upper cover, a stirring plate hanger and a chitosan oligosaccharide stirring plate, the extraction tank upper cover is nested at the outer side of the stirring plate hanger, the chitosan oligosaccharide stirring plate is installed at the bottom end of the stirring plate hanger, two sides of the top end of the pharmacological extraction tank are symmetrically provided with tank lugs, and the bottom end of the pharmacological extraction tank is provided with an extraction tank base.
Description
Technical Field
The invention belongs to the technical field of traditional Chinese medicine component extraction equipment, and particularly relates to a chitosan oligosaccharide component extraction device.
Background
Chitosan oligosaccharide, also called chitosan oligosaccharide and oligochitosan, is an oligosaccharide product with polymerization degree of 2-20, which is obtained by degrading chitosan by special biological enzyme technology (also reported by using chemical degradation and microwave degradation technology), has molecular weight of less than or equal to 3200Da, and is a low-molecular-weight product with good water solubility, large functional effect and high biological activity. It has several unique functions of high solubility, complete water solubility, easy absorption and utilization by organism, etc. and its action is 14 times that of chitosan.
The chitosan oligosaccharide is the only cationic basic amino oligosaccharide with positive charges in the nature, and is animal cellulose. Chitosan oligosaccharide is small molecular oligosaccharide with amino group degraded by chitosan derived from shrimp and crab shell, and is sugar chain with polymerization degree of 2-20.
The extraction methods of the components of the chitosan oligosaccharide are various, the raw materials are generally firstly required to be crushed into particles, then the particles are extracted into water in modes such as fumigation and decoction, and then the effective components of the chitosan oligosaccharide are concentrated and extracted in modes such as filtration, distillation and purification, but the fumigation and the cooking modes both require higher temperature, and the methods are not suitable for extracting the chitosan oligosaccharide which is easy to change at high temperature and are not scientific and practical enough.
Disclosure of Invention
The present invention is directed to provide a chitosan oligosaccharide ingredient extraction device to solve the above problems of the background art.
In order to achieve the purpose, the invention provides the following technical scheme: the utility model provides a chitosan oligosaccharide composition extraction element, includes extractor overall structure, extractor overall structure includes that pharmacology draws the jar, draws jar upper cover, stirs board gallows and chitosan oligosaccharide and stirs the movable plate, it nests in the outside of stirring the movable plate gallows to draw jar upper cover, chitosan oligosaccharide stirs the movable plate and installs the bottom of stirring the board gallows, the top bilateral symmetry that pharmacology drawed jar is provided with the jar ear, and pharmacology draw the bottom of jar and be provided with and draw a jar base, the upper surface of jar ear is provided with the spacing double-screw bolt of upper cover, the outside of the spacing double-screw bolt of upper cover is nested has the spacing cap of upper cover, draw jar upper cover and pharmacology and draw jar through the spacing fixed of the spacing cap of upper cover, bottom one side that pharmacology drawed the jar is provided with the solution contact tube, the one end of solution contact tube is provided with the pipe cap.
Preferably, stir the board gallows including stirring the board jib, it is provided with two to stir the board jib, and two it is provided with the jib handle to stir between the top of board jib, and stirs bottom one side of board jib and be provided with the spacing piece of rings, the rings spacing groove has all been seted up to the spacing piece of rings and one side of stirring the board jib.
Preferably, one side of the chitosan oligosaccharide stirring plate is provided with a stirring plate hanging ring, the inner edge of the chitosan oligosaccharide stirring plate is uniformly provided with a liquid discharge hole, the other side of the chitosan oligosaccharide stirring plate is uniformly provided with a stirring rod, and a hanging ring seat is arranged between the stirring plate hanging ring and the chitosan oligosaccharide stirring plate.
Preferably, the hanging ring limiting groove is matched with the hanging ring of the stirring plate in size, and the hanging ring limiting piece is fixedly connected with the stirring plate suspender through a bolt.
Preferably, the inside of the extraction tank upper cover is symmetrically provided with suspender limiting holes, the suspender limiting holes are matched with the size of the stirring plate suspender, and the center of the bottom side of the extraction tank upper cover is provided with a driving screw rod.
Preferably, the upper cover limiting cap and the upper cover limiting stud are connected in a screwing mode through threads.
Preferably, the pipe cap and the solution delivery pipe are connected in a screwing mode through threads, and a filter screen is arranged inside one end, far away from the pipe cap, of the solution delivery pipe.
Preferably, the center of the chitosan oligosaccharide stirring plate is provided with a threaded hole matched with the driving screw, and the chitosan oligosaccharide stirring plate is connected with the driving screw in a screwing manner through threads.
Compared with the prior art, the invention has the beneficial effects that: according to the invention, a novel extraction mode is adopted, after chitosan oligosaccharide particles and normal-temperature water are placed in the pharmacological extraction tank, the stirring plate hanger is directly and repeatedly lifted and pressed, when the stirring plate hanger drives the chitosan oligosaccharide stirring plate to lift, the chitosan oligosaccharide stirring plate can automatically rotate under the driving of the external thread of the driving screw, the rotating chitosan oligosaccharide stirring plate can repeatedly stir and extrude the chitosan oligosaccharide, the pharmacological components of the chitosan oligosaccharide are extracted at normal temperature, the extraction mode is simple and convenient, high-temperature extraction modes such as decoction and the like are avoided, and the practicability is stronger.
Drawings
FIG. 1 is a schematic perspective view of the present invention;
FIG. 2 is a schematic perspective view of the connection between the upper cover of the extraction tank, the hanging bracket of the stirring plate, and the stirring plate of chitosan oligosaccharide;
FIG. 3 is a schematic perspective view of a chitosan oligosaccharide agitating plate according to the present invention;
FIG. 4 is a schematic perspective view of the connection between the upper cover of the extraction tank and the hanger for the agitating plate according to the present invention;
FIG. 5 is a schematic view of a partial perspective structure of a connection mode between a stirring plate hanging ring and a stirring plate hanging rod of the present invention;
FIG. 6 is a schematic view of a local three-dimensional explosion structure of a mounting manner of a lifting ring limiting piece according to the present invention;
in the figure: 1. the whole structure of the extractor; 101. a pharmacological extraction tank; 111. a can ear; 112. an upper cover limit stud; 113. a limiting cap is covered on the upper cover; 114. a solution delivery pipe; 115. a pipe cap; 116. an extraction tank base; 102. the extraction tank is covered; 121. a boom limit hole; 122. a drive screw; 103. a stir plate hanger; 131. a stir plate boom; 132. a boom handle; 133. a hoisting ring limiting sheet; 134. a hoisting ring limiting groove; 104. stirring the plate; 141. a liquid discharge hole; 142. a stirring rod; 143. stirring the plate hoisting ring; 144. a suspension ring seat.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention.
Referring to fig. 1-6, the present invention provides the following technical solutions: the utility model provides a chitosan oligosaccharide composition extraction element, including extractor overall structure 1, extractor overall structure 1 includes pharmacology extraction tank 101, extract a jar upper cover 102, stir board gallows 103 and chitosan oligosaccharide and stir board 104, it nests in the outside of stirring board gallows 103 to extract jar upper cover 102, chitosan oligosaccharide stirs the bottom that board 104 was installed and is stirring board gallows 103, the top bilateral symmetry of pharmacology extraction tank 101 is provided with jar ear 111, and the bottom of pharmacology extraction tank 101 is provided with extracts jar base 116, the upper surface of jar ear 111 is provided with upper cover limit stud 112, the outside of upper cover limit stud 112 is nested has upper cover limit cap 113, it is spacing fixed that extraction tank upper cover 102 and pharmacology extraction tank 101 pass through upper cover limit cap 113, bottom one side of pharmacology extraction tank 101 is provided with solution delivery tube 114, the one end of solution delivery tube 114 is provided with pipe cap 115.
In order to enable the stirring plate hanger 103 to drive the chitosan oligosaccharide stirring plate 104 to lift, in this embodiment, preferably, the stirring plate hanger 103 includes two stirring plate hangers 131, two stirring plate hangers 131 are provided, a hanger handle 132 is provided between the top ends of the two stirring plate hangers 131, a hanging ring limiting piece 133 is provided at one side of the bottom end of the stirring plate hanger 131, and hanging ring limiting grooves 134 are provided at both sides of the hanging ring limiting piece 133 and the stirring plate hanger 131.
In order to enable the chitosan oligosaccharide stirring plate 104 to smoothly rotate in the hanging state, in this embodiment, it is preferable that one side of the chitosan oligosaccharide stirring plate 104 is provided with a stirring plate hanging ring 143, the inner edge of the chitosan oligosaccharide stirring plate 104 is uniformly provided with liquid drainage holes 141, the other side of the chitosan oligosaccharide stirring plate 104 is uniformly provided with a stirring rod 142, and a hanging ring seat 144 is provided between the stirring plate hanging ring 143 and the chitosan oligosaccharide stirring plate 104.
In order to make the rotation resistance of the agitating plate hanging ring 143 small, in this embodiment, it is preferable that the hanging ring limiting groove 134 and the agitating plate hanging ring 143 are matched in size, and the hanging ring limiting piece 133 and the agitating plate hanging bar 131 are fixedly connected by a bolt.
In order to facilitate the pulling and pushing of the stirring plate hanger 131, in this embodiment, preferably, hanger limiting holes 121 are symmetrically formed in the extracting tank upper cover 102, the hanger limiting holes 121 and the stirring plate hanger 131 are matched in size, and a driving screw 122 is disposed at the center of the bottom side of the extracting tank upper cover 102.
In order to enable the upper cover limiting cap 113 to press and fix the upper cover 102 of the extraction tank, in the present embodiment, it is preferable that the upper cover limiting cap 113 and the upper cover limiting stud 112 are screwed together.
In order to better filter the solution, in this embodiment, it is preferable that the pipe cap 115 and the solution delivery pipe 114 are screwed together, and a filter screen is disposed inside one end of the solution delivery pipe 114 away from the pipe cap 115.
In order to enable the chitooligosaccharide stirring plate 104 to automatically rotate during the lifting process, in this embodiment, it is preferable that a threaded hole matched with the driving screw 122 is formed in the center of the chitooligosaccharide stirring plate 104, and the chitooligosaccharide stirring plate 104 and the driving screw 122 are connected by screwing.
In order to prevent the chitosan oligosaccharide from blocking the drainage hole 141, in the present embodiment, it is preferable that a filter is disposed at the bottom side of the drainage hole 141.
The working principle and the using process of the invention are as follows: after the extraction tank is installed, firstly, the installation and the safety protection of the extraction tank are checked, then, the extraction tank can be used, when the extraction tank is used, the upper cover limiting cap 113 is screwed and disassembled, then, the upper cover 102 of the extraction tank, the stirring plate hanger 103 and the chitosan oligosaccharide stirring plate 104 are taken out, then, a proper amount of chitosan oligosaccharide raw materials crushed into particles and normal temperature water are respectively poured into the pharmacological extraction tank 101, then, the upper cover 102 of the extraction tank, the stirring plate hanger 103 and the chitosan oligosaccharide stirring plate 104 are put back, the upper cover limiting cap 113 is screwed and screwed tightly, at the moment, the suspender handle 132 is repeatedly pulled and pressed, the stirring plate suspender 131 drives the chitosan oligosaccharide stirring plate 104 to lift and descend, the chitosan oligosaccharide stirring plate 104 is matched with the thread on the outer side of the driving screw rod 122 in the lifting and descending processes, the stirring plate is driven by the thread to automatically rotate, the rotating chitosan oligosaccharide stirring plate 104 drives the stirring plate 142 to stir and extrude the chitosan oligosaccharide, the extraction work of chitosan oligosaccharide components is realized, after the corresponding container is fully stirred, the tail end 114 of the solution guide pipe is opened, and the pharmacological solution containing the pipe 115 can be poured out.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that various changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.
Claims (8)
1. The utility model provides a chitosan oligosaccharide composition extraction element, includes extractor overall structure (1), extractor overall structure (1) including pharmacology draw jar (101), draw jar upper cover (102), stir board gallows (103) and chitosan oligosaccharide stir board (104), its characterized in that: draw jar upper cover (102) nestification and stir the outside of board gallows (103), the bottom at stirring board gallows (103) is installed in chitosan oligosaccharide stirring board (104), the top bilateral symmetry that pharmacology drawed jar (101) is provided with pot ear (111), and the bottom that pharmacology drawed jar (101) is provided with draws jar base (116), the upper surface of pot ear (111) is provided with upper cover limit stud (112), the outside of upper cover limit stud (112) is nested has upper cover limit cap (113), draw jar upper cover (102) and pharmacology drawed jar (101) through upper cover limit cap (113) spacing fixed, the bottom one side that pharmacology drawed jar (101) is provided with solution delivery tube (114), the one end of solution delivery tube (114) is provided with pipe cap (115).
2. The chitosan oligosaccharide ingredient extracting apparatus as claimed in claim 1, wherein: mix board gallows (103) including stirring board jib (131), it is provided with two to stir board jib (131), and two it is provided with jib handle (132) to stir between the top of board jib (131), and stirs bottom one side of board jib (131) and be provided with rings spacing piece (133), rings spacing groove (134) have all been seted up to one side of rings spacing piece (133) and stirring board jib (131).
3. The chitosan oligosaccharide ingredient extracting apparatus as claimed in claim 2, wherein: one side of the chitosan oligosaccharide stirring plate (104) is provided with a stirring plate hanging ring (143), the inner edge of the chitosan oligosaccharide stirring plate (104) is uniformly provided with a liquid discharge hole (141), the other side of the chitosan oligosaccharide stirring plate (104) is uniformly provided with a stirring rod (142), and a hanging ring seat (144) is arranged between the stirring plate hanging ring (143) and the chitosan oligosaccharide stirring plate (104).
4. The chitosan oligosaccharide ingredient extracting apparatus as claimed in claim 3, wherein: the lifting ring limiting groove (134) is matched with the stirring plate lifting ring (143) in size, and the lifting ring limiting piece (133) is fixedly connected with the stirring plate hanging rod (131) through a bolt.
5. The chitosan oligosaccharide ingredient extracting apparatus as claimed in claim 2, wherein: the inside of the extraction tank upper cover (102) is symmetrically provided with suspender limiting holes (121), the suspender limiting holes (121) are matched with the size of the stirring plate suspender (131), and the center of the bottom side of the extraction tank upper cover (102) is provided with a driving screw (122).
6. The chitosan oligosaccharide ingredient extracting apparatus as claimed in claim 1, wherein: the upper cover limiting cap (113) and the upper cover limiting stud (112) are connected in a screwing mode through threads.
7. The chitosan oligosaccharide ingredient extracting apparatus as claimed in claim 1, wherein: the pipe cap (115) is connected with the solution delivery pipe (114) in a screwing mode through threads, and a filter screen is arranged inside one end, far away from the pipe cap (115), of the solution delivery pipe (114).
8. The chitosan oligosaccharide ingredient extracting apparatus as claimed in claim 5, wherein: the center of the chitosan oligosaccharide stirring plate (104) is provided with a threaded hole matched with the driving screw rod (122), and the chitosan oligosaccharide stirring plate (104) is connected with the driving screw rod (122) in a screwing manner through threads.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111639359.XA CN115282631B (en) | 2021-12-29 | 2021-12-29 | Chitosan oligosaccharide component extraction element |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111639359.XA CN115282631B (en) | 2021-12-29 | 2021-12-29 | Chitosan oligosaccharide component extraction element |
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| Publication Number | Publication Date |
|---|---|
| CN115282631A true CN115282631A (en) | 2022-11-04 |
| CN115282631B CN115282631B (en) | 2024-02-02 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN202111639359.XA Active CN115282631B (en) | 2021-12-29 | 2021-12-29 | Chitosan oligosaccharide component extraction element |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008284474A (en) * | 2007-05-18 | 2008-11-27 | Apt Machinery:Kk | Revolving/rotating mixer |
| JP2009106847A (en) * | 2007-10-30 | 2009-05-21 | Fukoku Kogyo Kk | Coagulation reactor |
| CN108852840A (en) * | 2018-07-12 | 2018-11-23 | 合肥七小俊生物科技有限公司 | A kind of Chinese medicine ceramic medicine decoction device |
| CN213159488U (en) * | 2020-09-07 | 2021-05-11 | 浙江博美生物技术有限公司 | Extraction equipment with self-filtering function |
| CN213466850U (en) * | 2020-10-22 | 2021-06-18 | 河南应用技术职业学院 | Extraction and separation device for chemical engineering practical training |
-
2021
- 2021-12-29 CN CN202111639359.XA patent/CN115282631B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2008284474A (en) * | 2007-05-18 | 2008-11-27 | Apt Machinery:Kk | Revolving/rotating mixer |
| JP2009106847A (en) * | 2007-10-30 | 2009-05-21 | Fukoku Kogyo Kk | Coagulation reactor |
| CN108852840A (en) * | 2018-07-12 | 2018-11-23 | 合肥七小俊生物科技有限公司 | A kind of Chinese medicine ceramic medicine decoction device |
| CN213159488U (en) * | 2020-09-07 | 2021-05-11 | 浙江博美生物技术有限公司 | Extraction equipment with self-filtering function |
| CN213466850U (en) * | 2020-10-22 | 2021-06-18 | 河南应用技术职业学院 | Extraction and separation device for chemical engineering practical training |
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| Publication number | Publication date |
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| CN115282631B (en) | 2024-02-02 |
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