CN115282628B - Tantalum ethoxide purification equipment - Google Patents
Tantalum ethoxide purification equipment Download PDFInfo
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- CN115282628B CN115282628B CN202211233571.0A CN202211233571A CN115282628B CN 115282628 B CN115282628 B CN 115282628B CN 202211233571 A CN202211233571 A CN 202211233571A CN 115282628 B CN115282628 B CN 115282628B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
- B01D3/146—Multiple effect distillation
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0003—Condensation of vapours; Recovering volatile solvents by condensation by using heat-exchange surfaces for indirect contact between gases or vapours and the cooling medium
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
- B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
- B01D5/006—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Abstract
The invention discloses tantalum ethoxide purification equipment, and relates to the technical field of tantalum ethoxide production. This tantalum ethanol purification equipment, including the bottom plate, the edge fixedly connected with supporting leg of bottom plate lower surface, circular hole has been seted up to the upper surface of bottom plate, the circular hole department cover that the bottom plate upper surface was seted up is equipped with heating device, heating device's upper surface is provided with the erlenmeyer flask, the opening part cover of erlenmeyer flask is equipped with the sealing plug, the sealing plug is that the upper surface is provided with the blast pipe, through setting up the erlenmeyer flask, can be used for placing the tantalum ethanol solution that needs the purification, during the operation, place tantalum ethanol solution among the erlenmeyer flask to the hole department of blast pipe insertion sealing plug later presses the sealing plug to the bottleneck department of erlenmeyer flask, makes the erlenmeyer flask reach sealed effect, prevents to pollute the laboratory among the air among the gas leakage that produces among the erlenmeyer flask after the heating, reaches the effect of going on simultaneously of many purifications.
Description
Technical Field
The invention relates to the technical field of tantalum ethoxide production, in particular to tantalum ethoxide purification equipment.
Background
Tantalum ethoxide is an organic raw material and has a molecular formula of C 10 H 25 O 5 Ta, molecular weight 406.2901, purification refers to separating impurities from the mixture to increase its purity. Purification as an important chemical method has important roles not only in chemical research but also in chemical production. Of great importanceThe chemical research and the chemical production of (1) are mainly based on purification. The term "physical" or "chemical" refers to a process of removing impurities from a mixture to obtain a pure substance. If the impurities are chemically changed during purification, the impurities do not need to be recovered to the original substances, and the purification method is mainly divided into a physical method and a chemical method;
the boiling point of tantalum ethoxide is 155 ℃, which is higher than that of water, so that a distillation purification method can be adopted, and the tantalum ethoxide solution needs to be purified for multiple times to reach the required purity; however, the purification instrument on the market can only carry out one-time purification once, but can not carry out purification for multiple times at the same time, the purification efficiency is low, and the tantalum ethoxide can volatilize after multiple operations, so that the purity of the tantalum ethoxide solution can be reduced.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides tantalum ethoxide purification equipment, which solves the problems of low purification efficiency caused by the fact that the tantalum ethoxide solution cannot be purified for multiple times and is low in purity caused by the fact that tantalum ethoxide volatilizes when the tantalum ethoxide solution is transferred to a conical flask.
In order to achieve the purpose, the invention is realized by the following technical scheme: a tantalum ethoxide purification device comprises a bottom plate, wherein supporting legs are fixedly connected at corners of the lower surface of the bottom plate, a circular hole is formed in the upper surface of the bottom plate, a heating device is sleeved at the circular hole formed in the upper surface of the bottom plate, a conical bottle is arranged on the upper surface of the heating device, a sealing plug is sleeved at an opening of the conical bottle, an exhaust pipe is arranged on the upper surface of the sealing plug, the conical bottle can be used for placing tantalum ethoxide solution to be purified, during operation, the tantalum ethoxide solution is placed in the conical bottle, the exhaust pipe is inserted into the hole of the sealing plug, then the sealing plug is pressed to the bottle neck of the conical bottle, the conical bottle achieves a sealing effect, gas generated in the heated conical bottle is prevented from leaking into air to pollute a laboratory, and the exhaust pipe penetrates through the upper surface of the sealing plug and extends to the lower surface of the sealing plug, the end of the exhaust pipe, which is far away from the conical flask, is provided with a condensing device, the effect of condensing the heated gas in the conical flask can be achieved through the arrangement of the condensing device, so that the required ethanol-tantalum solution is collected, the upper surface of the bottom plate is provided with a square hole, a partition plate is arranged at the square hole arranged on the upper surface of the bottom plate, a collecting box is arranged on the upper surface of the partition plate, an air guide pipe is arranged at the inner cavity of the collecting box, the air guide pipe penetrates through the top surface of the inner cavity of the collecting box and extends to the upper surface of the collecting box, one end of the air guide pipe, which is far away from the collecting box, is connected with the condensing device, a water vapor discharge pipe is arranged at the inner cavity of the collecting box, the water vapor discharge pipe penetrates through the top surface of the inner cavity of the collecting box and extends to the upper surface of the collecting box, and the heated liquid in the conical flask can be collected through the collecting box, and then the water in the tantalum ethoxide solution is further evaporated through secondary heating, so that the effect of high purification is achieved, the boiling point of the tantalum ethoxide solution is at the temperature of centigrade, so that the content of the tantalum ethoxide solution in the gas generated by the liquid subjected to secondary heating is very low, and the generated gas is discharged into the air through a water vapor discharge pipe.
Preferably, the upper surface of bottom plate is provided with the support base, the last fixed surface of support base is connected with spacing post, the surface cover of spacing post is equipped with the connecting rod, the one end that spacing post was kept away from to the connecting rod is provided with the centre gripping post, the surface at the air duct is established to the centre gripping post cover, through setting up support base, spacing post, connecting rod and centre gripping post, can carry out the centre gripping to the air duct, during the operation, establishes the surface at spacing post to the connecting rod cover, fixes the centre gripping post among the solid fixed ring of connecting rod again, makes the air duct fix the grip ring department at the centre gripping post at last.
Preferably, the condensing device comprises a condensing device shell, a water outlet pipe is arranged on the left side surface of the condensing device shell, the water outlet pipe penetrates through the outer surface of the condensing device shell and extends to the inner wall of the condensing device shell, a water inlet pipe is arranged on the right side outer surface of the condensing device shell, the water inlet pipe penetrates through the outer surface of the condensing device shell and extends to the inner wall of the condensing device shell, mixed gas of ethanol-tantalum solution and water in the conical flask can be cooled and re-liquefied through the arrangement of the condensing device, an operator enables the water inlet pipe to be connected with a water tap during operation, the water outlet pipe is connected to a water drainage tank, the water tap is opened after connection is completed, so that the gas in the condensing device shell is filled with water, the gas in the purifying liquid collecting pipe can be gradually cooled and cut to be liquefied under the action of water flow, a purifying liquid collecting pipe is arranged on the bottom surface of an inner cavity of the condensing device shell, a circle is arranged on the bottom surface of the purifying liquid collecting pipe, one end, far away from the conical flask, is arranged at the circle hole, a circle hole arranged at the circle hole arranged on the bottom surface of the purifying liquid collecting pipe, a square hole arranged on the right side surface of the purifying liquid collecting pipe, and a square hole is arranged at the square position of the gas guide pipe.
Preferably, heating device includes the heating device shell, the inner chamber department of heating device shell is provided with the heating motor, the one end of heating motor is provided with heating coil, heating coil is connected with the output of heating motor, heating coil's lower surface is provided with the coil support column, coil support column fixed connection is in the inner chamber bottom surface of heating device shell, through setting up heating device, can heat the ethanol tantalum solution in the erlenmeyer flask to make the water boiling evaporation in the ethanol tantalum solution, reach the effect to the ethanol tantalum solution purification in the erlenmeyer flask, in operation, after having placed the erlenmeyer flask and having installed the experimental apparatus, operating personnel makes the heating motor insert the switch of power and opening the heating motor, the heating motor begins to work, can make the heating coil produce high temperature, and the high-temperature gas that produces gives off to the bottom surface of erlenmeyer flask from placing between the baffle, reaches the effect of heating ethanol tantalum solution in the erlenmeyer flask and carrying out the heating, circular hole has been seted up to the inner chamber bottom surface of heating device shell, the circular hole department cover that the heating device shell inner chamber bottom surface was seted up is equipped with the fan, the bottom surface of heating device shell is equipped with the fan and places the circular hole, and the bottom surface of placing baffle and the circular base is connected with the heating coil and places the heating device and places the heat and the setting up the gap and the baffle.
Preferably, a hole is formed in one side, away from the heating motor, of the outer surface of the heating device shell, a heat conduction pipe is arranged at the hole formed in the outer surface of the heating device shell, a reheating device is fixedly connected to one end, away from the heating device shell, of the heat conduction pipe, heat in the heating device shell can be transferred into the reheating device through the heat conduction pipe, solution in the collecting box can be reheated through the reheating device, water occupying a large proportion is changed into steam to be evaporated, and therefore purity in the collecting box is improved.
Preferably, the reheating device is included in the heating box, a square hole is formed in the upper surface of the heating box, a heat collecting device shell is sleeved at the square hole formed in the upper surface of the heating box, a heat collecting device is arranged in an inner cavity of the heat collecting device shell, the heat collecting device comprises a heat collecting device support column, the heat collecting device support column is fixedly connected to the inner wall of the heat collecting device shell, a fixing ring is fixedly connected to the upper surface of the heat collecting device support column, a fan-shaped support column is fixedly connected to the inner ring surface of the fixing ring, one end, far away from the fixing ring, of the fan-shaped support column is fixedly connected to the inner ring surface of the fixing ring, a rotating column is sleeved on the inner ring surface of the limiting ring, a fan blade is fixedly connected to the outer bottom end surface of the rotating column, a rotating disc is fixedly connected to one end, far away from the fan blade, of the rotating disc, through the heat collecting device, hot air transmitted to the heating box through the heat collecting pipe can be collected to several points of the collecting box, steam is accelerated to be generated in the collecting box, and during operation, after the hot air is blown from the heating box through the heat collecting box, the inclined plate, the fan blade can drive the rotating disc to rotate under the rotating disc under the rotating effect of the rotating disc, so that the hot air is uniformly blown to the hot air discharged from the upper surface of the collecting box, and the collecting box, the hot air discharged through the collecting box, and the collecting box, the hot air is uniformly discharged through the collecting box, and the collecting box.
The invention provides tantalum ethoxide purification equipment. The method has the following beneficial effects:
1. this tantalum ethoxide purification equipment, through setting up the erlenmeyer flask, can be used for placing the tantalum ethoxide solution that needs the purification, in operation, place tantalum ethoxide solution among the erlenmeyer flask, and insert the hole department of sealing plug to the blast pipe, later press the sealing plug to the bottleneck department of erlenmeyer flask, make the erlenmeyer flask reach sealed effect, prevent to pollute the laboratory in the air is revealed to the gas that produces among the heating erlenmeyer flask, through the setting of condensing equipment, can reach the effect to the gas condensation after heating among the erlenmeyer flask, thereby collect required tantalum ethoxide solution, can collect the liquid that heats in the erlenmeyer flask through setting up the collecting box, further make the water evaporation in the tantalum ethoxide solution through the secondary heating, thereby reach high purification's effect, because the boiling point of tantalum ethoxide solution is in the degree centigrade, so the content of tantalum ethoxide solution is few in the gas that the liquid that passes through the secondary heating produced, the gas discharges to the air in through the vapor discharge pipe.
2. This ethanol tantalum purification equipment through setting up support base, spacing post, connecting rod and centre gripping post, can carry out the centre gripping to the air duct, during the operation, overlaps the connecting rod cover and establishes the surface at spacing post, fixes the centre gripping post among the solid fixed ring of connecting rod again, makes the air duct fix the retainer ring department at the centre gripping post at last.
3. This tantalum ethoxide purification equipment can make the tantalum ethoxide solution in the erlenmeyer flask and the mist cooling of water form liquid again through condensing equipment's setting, and the during operation, operating personnel make advance water piping connection tap, make outlet pipe connection to water drainage tank again, open tap after having connected for fill water among the condensing equipment shell, under the effect of rivers, gas among the purification liquid collecting pipe can cool off the liquefaction gradually.
4. This tantalum ethoxide purification equipment, through setting up heating device, can heat the tantalum ethoxide solution in the erlenmeyer flask, thereby make the water boiling evaporation in the tantalum ethoxide solution, reach the effect to the tantalum ethoxide solution purification in the erlenmeyer flask, in operation, after having placed the erlenmeyer flask and having installed the experimental device, operating personnel makes the switch that adds the electrical machine access power and open the heating motor, add the electrical machine and begin work, can make heating coil produce the high temperature, the high-temperature gas who produces gives off to the bottom surface of erlenmeyer flask from placing between the baffle, reach the effect that heats the tantalum ethoxide solution in the erlenmeyer flask, through setting up the fan, can blow the bottom surface to the erlenmeyer flask through placing the gap between the baffle to the heat that heating coil produced.
5. This tantalum ethanol purification equipment, through setting up the heat pipe, can be among the heat transfer to reheating device among the heating device shell, reheating device's setting can make the solution in the collection box heat again, make the water that accounts for a large proportion become the steam evaporation, thereby improve the purity among the collecting box, setting through heat gathering device, can gather the steam that the heat pipe transmitted among the heating box, on gathering several points of collecting the box, thereby the production of vapor among the acceleration collecting box, in operation, after wind-force that the fan produced makes steam blow to among the heating box among the heat pipe, the fan piece can drive the rotation post and produce the rotation under the influence of wind-force, thereby make the rolling disc produce the rotation, in the pivoted process, steam is discharged by hot-blast discharge pipe, the setting of swash plate makes steam blow to the appointed region of collecting box evenly, reach the effect of rapid heating.
Drawings
FIG. 1 is a schematic view of the tantalum ethoxide purification apparatus of the present invention;
FIG. 2 is a schematic sectional view of a tantalum ethoxide purification apparatus according to the present invention;
FIG. 3 is a schematic view of the exploded structure of the tantalum ethoxide purification apparatus of the present invention;
FIG. 4 is a schematic view of a heating apparatus according to the present invention;
FIG. 5 is a schematic cross-sectional view of a condensing unit according to the present invention;
FIG. 6 is a schematic view of the structure of the collecting box of the present invention;
FIG. 7 is a schematic view of a reheating apparatus according to the present invention;
FIG. 8 is a schematic view of the heat collector of the present invention;
FIG. 9 is a detailed structure diagram of the heat collecting device of the present invention.
In the figure: 1. a base plate; 2. supporting legs; 3. a heating device; 4. a conical flask; 5. an exhaust pipe; 6. a sealing plug; 7. a condensing unit; 8. a reheating device; 9. a heat conducting pipe; 10. a collection box; 11. a partition plate; 12. a reheating device fixing plate; 13. a bracket base; 14. a limiting column; 15. a connecting rod; 16. a clamping post; 17. an air duct; 18. a water vapor discharge pipe; 31. a heating device housing; 32. a heating motor; 33. a heating coil; 34. a coil support post; 35. placing a base; 36. placing a partition plate; 37. a fan; 38. a heating device support leg; 71. a condensing unit housing; 72. a water outlet pipe; 73. a water inlet pipe; 74. a purified liquid collecting pipe; 81. a heating box; 82. a heat collection device housing; 83. a heat collecting device; 831. a heat collection device support column; 832. a sloping plate; 833. a fixing ring; 834. a fan-shaped support column; 835. a limiting ring; 836. rotating the column; 837. a fan blade; 838. rotating the disc; 839. and a hot air discharge pipe.
Detailed Description
The present invention will be described in further detail with reference to the accompanying drawings and specific embodiments. The embodiments of the present invention have been presented for purposes of illustration and description, and are not intended to be exhaustive or limited to the invention in the form disclosed. Many modifications and variations will be apparent to those of ordinary skill in the art. The embodiment was chosen and described in order to best explain the principles of the invention and the practical application, and to enable others of ordinary skill in the art to understand the invention for various embodiments with various modifications as are suited to the particular use contemplated.
As shown in fig. 1 to 9, the present invention provides a technical solution: a tantalum ethoxide purification device comprises a base plate 1, wherein supporting legs 2 are fixedly connected at corners of the lower surface of the base plate 1, a circular hole is formed in the upper surface of the base plate 1, a heating device 3 is sleeved at the circular hole formed in the upper surface of the base plate 1, a conical bottle 4 is arranged on the upper surface of the heating device 3, a sealing plug 6 is sleeved at an opening of the conical bottle 4, an exhaust pipe 5 is arranged on the upper surface of the sealing plug 6, the conical bottle 4 can be used for containing tantalum ethoxide solution to be purified, during operation, the tantalum ethoxide solution is placed in the conical bottle 4, the exhaust pipe 5 is inserted into the hole of the sealing plug 6, then the sealing plug 6 is pressed to the bottleneck of the conical bottle 4, the conical bottle 4 achieves a sealing effect, and gas generated in the conical bottle 4 after heating is prevented from leaking into air to pollute a laboratory, the exhaust pipe 5 penetrates through the upper surface of the sealing plug 6 and extends to the lower surface of the sealing plug 6, a condensing device 7 is arranged at one end of the exhaust pipe 5, which is far away from the conical flask 4, through the arrangement of the condensing device 7, the effect of condensing the heated gas in the conical flask 4 can be achieved, so that the required ethanol tantalum solution is collected, a square hole is formed in the upper surface of the bottom plate 1, a partition plate 11 is arranged at the square hole formed in the upper surface of the bottom plate 1, a collecting box 10 is arranged on the upper surface of the partition plate 11, an air guide pipe 17 is arranged at the inner cavity of the collecting box 10, the air guide pipe 17 penetrates through the top surface of the inner cavity of the collecting box 10 and extends to the upper surface of the collecting box 10, one end, which is far away from the collecting box 10, of the air guide pipe 17 is connected with the condensing device 7, a water vapor discharge pipe 18 is arranged at the inner cavity of the collecting box 10, and the water vapor discharge pipe 18 penetrates through the top surface of the inner cavity of the collecting box 10 and extends to the upper surface of the collecting box 10, the collecting box 10 is arranged to collect the heated liquid in the conical flask 4, and then the secondary heating is carried out to further evaporate the water in the tantalum ethoxide solution, so as to achieve the effect of high purification, because the boiling point of the tantalum ethoxide solution is 155 ℃, the content of the tantalum ethoxide solution in the gas generated by the liquid subjected to the secondary heating is very low, the generated gas is discharged into the air through the water vapor discharge pipe 18, the upper surface of the bottom plate 1 is provided with the bracket base 13, the upper surface of the bracket base 13 is fixedly connected with the limit column 14, the outer surface of the limit column 14 is sleeved with the connecting rod 15, one end of the connecting rod 15 far away from the limit column 14 is provided with the clamping column 16, the clamping column 16 is sleeved on the outer surface of the gas guide pipe 17, and the gas guide pipe 17 can be clamped by arranging the bracket base 13, the limit column 14, the connecting rod 15 and the clamping column 16, during operation, the connecting rod 15 is sleeved on the outer surface of the limiting column 14, the clamping column 16 is fixed in the fixing ring of the connecting rod 15, finally the gas guide pipe 17 is fixed at the clamping ring of the clamping column 16, the condensing device 7 comprises a condensing device shell 71, a water outlet pipe 72 is arranged on the left side surface of the condensing device shell 71, the water outlet pipe 72 penetrates through the outer surface of the condensing device shell 71 and extends to the inner wall of the condensing device shell 71, a water inlet pipe 73 is arranged on the right side outer surface of the condensing device shell 71, the water inlet pipe 73 penetrates through the outer surface of the condensing device shell 71 and extends to the inner wall of the condensing device shell 71, the mixed gas of the ethanol tantalum solution and the water in the conical flask 4 can be cooled to be in a liquid state again through the arrangement of the condensing device 7, and an operator enables the water inlet pipe 73 to be connected with a faucet during operation, then the water outlet pipe 72 is connected to a water drainage tank, after the connection, a water tap is opened, so that the condensing device shell 71 is filled with water, gas in the purified liquid collecting pipe 74 is gradually cooled and liquefied under the action of water flow, the purified liquid collecting pipe 74 is arranged on the bottom surface of the inner cavity of the condensing device shell 71, a round hole is formed in the bottom surface of the purified liquid collecting pipe 74, one end, away from the conical flask 4, of the exhaust pipe 5 is sleeved at the round hole formed in the bottom surface of the purified liquid collecting pipe 74, a square hole is formed in the right side surface of the purified liquid collecting pipe 74, the air guide pipe 17 is sleeved at the square hole formed in the right side surface of the purified liquid collecting pipe 74, the heating device 3 comprises a heating device shell 31, a heating motor 32 is arranged in the inner cavity of the heating device shell 31, a heating coil 33 is arranged at one end of the heating motor 32, and the heating coil 33 is connected with the output end of the heating motor 32, the lower surface of the heating coil 33 is provided with a coil supporting column 34, the coil supporting column 34 is fixedly connected to the bottom surface of the inner cavity of the heating device shell 31, the heating device 3 is arranged to heat the tantalum ethoxide solution in the conical flask 4, so that water in the tantalum ethoxide solution is boiled and evaporated, the effect of purifying the tantalum ethoxide solution in the conical flask 4 is achieved, in the working process, after the conical flask 4 is placed and experimental equipment is installed, an operator enables the heating motor 32 to be connected to a power supply and turns on a switch of the heating motor 32, the heating motor 32 starts to work, the heating coil 33 can generate high temperature, the generated high-temperature gas is diffused to the bottom surface of the conical flask 4 from the space between the placing partition plates 36, the effect of heating the tantalum ethoxide solution in the conical flask 4 is achieved, the bottom surface of the inner cavity of the heating device shell 31 is provided with a circular hole, a fan 37 is sleeved at a circular hole formed in the bottom surface of the inner cavity of the heating device shell 31, a heating device supporting leg 38 is fixedly connected to the bottom surface of the heating device shell 31, a circular hole is formed in the upper surface of the heating device shell 31, a placing base 35 is arranged at the circular hole formed in the upper surface of the heating device shell 31, a placing partition plate 36 is fixedly connected to the bottom surface of the placing base 35, heat generated by the heating coil 33 can be blown to the bottom surface of the conical flask 4 through a gap between the placing partition plates 36 by arranging the fan 37, a hole is formed in the outer surface of the heating device shell 31 at one side far away from the heating motor 32, a heat conduction pipe 9 is arranged at the hole formed in the outer surface of the heating device shell 31, a reheating device 8 is fixedly connected to one end of the heat conduction pipe 9 far away from the heating device shell 31, and by arranging the heat conduction pipe 9, the solution in the collecting box 10 can be reheated by the reheating device 8, a large proportion of water is changed into steam to be evaporated, so that the purity in the collecting box 10 is improved, the reheating device 8 is fixedly connected to the lower surface of the reheating device 8 by a reheating device fixing plate 12, the other end of the reheating device fixing plate 12 is fixedly connected to the bottom surface of the bottom plate 1, the reheating device 8 is arranged in a heating box 81, a square hole is formed in the upper surface of the heating box 81, a heat collecting device shell 82 is sleeved at the square hole formed in the upper surface of the heating box 81, a heat collecting device 83 is arranged in the inner cavity of the heat collecting device shell 82, the heat collecting device 83 comprises a heat collecting device supporting column 831, the heat collecting device supporting column 831 is fixedly connected to the inner wall of the heat collecting device shell 82, the upper surface of the heat collecting device supporting column 831 is fixedly connected with a fixing ring 833, the inner ring surface of the fixing ring 833 is fixedly connected with a fan-shaped supporting column 834, one end of the fan-shaped supporting column 834, which is far away from the fixing ring 833, is fixedly connected with a limiting ring 835, the inner ring surface of the limiting ring 835 is sleeved with a rotating column 836, the outer surface of the bottom end of the rotating column 836 is fixedly connected with a fan blade 837, one end of the rotating column 836, which is far away from the fan blade 837, is fixedly connected with a rotating disc 838, through the arrangement of the heat collecting device 83, hot air transmitted into the heating box 81 by the heat conducting pipe 9 can be collected and collected onto several points of the collecting box 10, so that the generation of water vapor in the collecting box 10 is accelerated, during operation, after the hot air is blown into the heating box 81 from the heat conducting pipe 9 by the wind force generated by the fan 37, the fan blade 837 can drive the rotating column 836 to rotate under the influence of the wind force, so that the rotating disc 838 rotates, the upper surface of the rotating disc 838 is provided with a square hole, the square hole is fixedly connected with a sloping plate 839, an inner cavity of the exhaust pipe 832, the hot air is uniformly blown out of the collecting box, and the hot air is uniformly heated by the hot air exhaust pipe 832, and the hot air is uniformly heated by the hot air exhaust pipe 8310.
When in use, the conical bottle 4 is arranged and can be used for placing tantalum ethoxide solution to be purified, during operation, the tantalum ethoxide solution is placed in the conical bottle 4, the exhaust pipe 5 is inserted into the hole of the sealing plug 6, then the sealing plug 6 is pressed to the bottle mouth of the conical bottle 4, so that the conical bottle 4 achieves the sealing effect, gas generated in the heated conical bottle 4 is prevented from leaking into the air to pollute a laboratory, the effect of condensing the heated gas in the conical bottle 4 can be achieved through the arrangement of the condensing device 7, the required tantalum ethoxide solution is collected, liquid generated by heating in the conical bottle 4 can be collected through the collection box 10, water in the tantalum ethoxide solution is further evaporated through secondary heating, the high purification effect is achieved, and the boiling point of the tantalum ethoxide solution is 155 ℃, therefore, the content of the tantalum ethoxide solution in the gas generated by the liquid heated for the second time is very low, the generated gas is discharged into the air through the water vapor discharge pipe 18, the gas guide pipe 17 can be clamped by arranging the bracket base 13, the limiting column 14, the connecting rod 15 and the clamping column 16, during operation, the connecting rod 15 is sleeved on the outer surface of the limiting column 14, the clamping column 16 is fixed in the fixing ring of the connecting rod 15, finally the gas guide pipe 17 is fixed at the clamping ring of the clamping column 16, the mixed gas of the tantalum ethoxide solution and the water in the conical flask 4 can be cooled to be in a liquid state again through the arrangement of the condensing device 7, during operation, an operator enables the water inlet pipe 73 to be connected with a faucet, then the water outlet pipe 72 is connected with a water discharge tank, after the connection, the faucet is opened, so that the shell 71 of the condensing device is filled with the water, and the gas in the purifying liquid collecting pipe 74 can be gradually cooled and liquefied under the action of the water flow, by arranging the heating device 3, the tantalum ethoxide solution in the conical flask 4 can be heated, so that water in the tantalum ethoxide solution is boiled and evaporated, and the effect of purifying the tantalum ethoxide solution in the conical flask 4 is achieved, in operation, after the conical flask 4 is placed and experimental equipment is installed, an operator enables the heating motor 32 to be connected with a power supply and turns on a switch of the heating motor 32, the heating motor 32 starts to work, so that the heating coil 33 generates high temperature, the generated high-temperature gas is diffused to the bottom surface of the conical flask 4 from the space between the partition plates 36, the effect of heating the tantalum ethoxide solution in the conical flask 4 is achieved, by arranging the fan 37, the heat generated by the heating coil 33 can be blown to the bottom surface of the conical flask 4 through the gap between the partition plates 36, by arranging the heat conduction pipe 9, the heat in the shell 31 of the heating device can be transferred to the reheating device 8, the reheating device 8 is arranged to reheat the solution in the collecting tank 10 to evaporate a large proportion of water into steam, thereby improving the purity in the collecting tank 10, the heat collecting device 83 is arranged to collect the hot air transferred from the heat conduction pipe 9 to the heating tank 81 and collect the hot air on several points of the collecting tank 10, thereby accelerating the generation of water vapor in the collecting tank 10, when the fan 37 is operated, the fan 837 drives the rotating column 836 to rotate under the influence of wind power after the hot air is blown from the heat conduction pipe 9 to the heating tank 81 by the wind power generated by the fan 37, so that the rotating disc 838 rotates, during the rotation, the hot air is discharged from the hot air discharge pipe 839, and the inclined plate 832 enables the hot air to be uniformly blown to a designated area of the collecting tank 10, thereby achieving the effect of rapid heating.
It is to be understood that the described embodiments are merely a few embodiments of the invention, and not all embodiments. All other embodiments, which can be derived by one of ordinary skill in the art and related arts based on the embodiments of the present invention without any creative effort, shall fall within the protection scope of the present invention. Structures, devices, and methods of operation not specifically described or illustrated herein are generally practiced in the art without specific recitation or limitation.
Claims (4)
1. The utility model provides a tantalum ethoxide purification equipment, includes bottom plate (1), its characterized in that: the corner of the lower surface of the bottom plate (1) is fixedly connected with a supporting leg (2), a round hole is formed in the upper surface of the bottom plate (1), a heating device (3) is sleeved at the round hole formed in the upper surface of the bottom plate (1), a conical bottle (4) is arranged on the upper surface of the heating device (3), a sealing plug (6) is sleeved at an opening of the conical bottle (4), an exhaust pipe (5) is arranged on the upper surface of the sealing plug (6), the exhaust pipe (5) penetrates through the upper surface of the sealing plug (6) and extends to the lower surface of the sealing plug (6), and a condensing device (7) is arranged at one end, far away from the conical bottle (4), of the exhaust pipe (5);
the upper surface of the bottom plate (1) is provided with a square hole, a partition plate (11) is arranged at the square hole arranged on the upper surface of the bottom plate (1), a collecting box (10) is arranged on the upper surface of the partition plate (11), an air duct (17) is arranged at the inner cavity of the collecting box (10), the air duct (17) penetrates through the top surface of the inner cavity of the collecting box (10) and extends to the upper surface of the collecting box (10), one end, far away from the collecting box (10), of the air duct (17) is connected with a condensing device (7), a water vapor discharge pipe (18) is arranged at the inner cavity of the collecting box (10), and the water vapor discharge pipe (18) penetrates through the top surface of the inner cavity of the collecting box (10) and extends to the upper surface of the collecting box (10);
the heating device (3) comprises a heating device shell (31), a heating motor (32) is arranged in an inner cavity of the heating device shell (31), a heating coil (33) is arranged at one end of the heating motor (32), the heating coil (33) is connected with an output end of the heating motor (32), a coil supporting column (34) is arranged on the lower surface of the heating coil (33), and the coil supporting column (34) is fixedly connected to the bottom surface of the inner cavity of the heating device shell (31);
a circular hole is formed in the bottom surface of an inner cavity of the heating device shell (31), a fan (37) is sleeved at the circular hole formed in the bottom surface of the inner cavity of the heating device shell (31), a heating device supporting leg (38) is fixedly connected to the bottom surface of the heating device shell (31), a circular hole is formed in the upper surface of the heating device shell (31), a placing base (35) is arranged at the circular hole formed in the upper surface of the heating device shell (31), and a placing partition plate (36) is fixedly connected to the bottom surface of the placing base (35);
a hole is formed in one side, away from the heating motor (32), of the outer surface of the heating device shell (31), a heat conduction pipe (9) is arranged at the hole formed in the outer surface of the heating device shell (31), one end, away from the heating device shell (31), of the heat conduction pipe (9) is fixedly connected with a reheating device (8), the lower surface of the reheating device (8) is fixedly connected with a reheating device fixing plate (12), and the other end of the reheating device fixing plate (12) is fixedly connected to the bottom surface of the bottom plate (1);
the reheating device (8) comprises a heating box (81), a square hole is formed in the upper surface of the heating box (81), a heat collecting device shell (82) is sleeved at the square hole formed in the upper surface of the heating box (81), a heat collecting device (83) is arranged at the inner cavity of the heat collecting device shell (82), the heat collecting device (83) comprises a heat collecting device supporting column (831), the heat collecting device supporting column (831) is fixedly connected to the inner wall of the heat collecting device shell (82), a fixing ring (833) is fixedly connected to the upper surface of the heat collecting device supporting column (831), a fan-shaped supporting column (834) is fixedly connected to the inner ring surface of the fixing ring (833), and a limiting ring (835) is fixedly connected to one end, away from the fixing ring (833), of the fan-shaped supporting column (834);
the utility model discloses a fan, including spacing ring (835), rotation post (836), the bottom surface fixedly connected with fan (837) of rotation post (836), the one end fixedly connected with rolling disc (838) of fan (837) is kept away from in rotation post (836), square hole has been seted up to the upper surface of rolling disc (838), square hole department fixedly connected with hot-blast discharge pipe (839) that the upper surface of rolling disc (838) was seted up, fixedly connected with swash plate (832) between the opposite face of hot-blast discharge pipe (839) inner chamber.
2. The apparatus of claim 1, wherein the apparatus comprises: the upper surface of bottom plate (1) is provided with support base (13), the last fixed surface of support base (13) is connected with spacing post (14), the surface cover of spacing post (14) is equipped with connecting rod (15), the one end that spacing post (14) were kept away from in connecting rod (15) is provided with centre gripping post (16), the surface at air duct (17) is established to centre gripping post (16) cover.
3. The tantalum ethoxide purification apparatus according to claim 1, wherein: condensing equipment (7) are including condensing equipment shell (71), the left side surface of condensing equipment shell (71) is provided with outlet pipe (72), outlet pipe (72) run through the surface of condensing equipment shell (71) and extend to the inner wall department of condensing equipment shell (71), the right side surface of condensing equipment shell (71) is provided with inlet tube (73), inlet tube (73) run through the surface of condensing equipment shell (71) and extend to the inner wall department of condensing equipment shell (71).
4. The apparatus of claim 3, wherein: condensing equipment shell (71) inner chamber bottom surface is provided with purification liquid collecting pipe (74), circular hole has been seted up to the bottom surface of purification liquid collecting pipe (74), the circular hole department that purification liquid collecting pipe (74) bottom surface was seted up is established to a pot head that erlenmeyer flask (4) was kept away from in blast pipe (5), square hole has been seted up on the right side surface of purification liquid collecting pipe (74), square hole department that purification liquid collecting pipe (74) right side surface was seted up is established to air duct (17) cover.
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| CN202211233571.0A CN115282628B (en) | 2022-10-10 | 2022-10-10 | Tantalum ethoxide purification equipment |
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| CN202211233571.0A CN115282628B (en) | 2022-10-10 | 2022-10-10 | Tantalum ethoxide purification equipment |
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| CN115282628B true CN115282628B (en) | 2022-12-16 |
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Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06220069A (en) * | 1991-11-25 | 1994-08-09 | Japan Energy Corp | Purification of tantalum alkoxide, high-purity tantalum alkoxide and gas phase growth using the same material |
| CN207856341U (en) * | 2017-12-29 | 2018-09-14 | 宜制觅智能设备（上海）有限公司 | High-efficiency evaporator with atomising device |
| CN211111139U (en) * | 2019-10-31 | 2020-07-28 | 烟台达瑞克生物工程有限公司 | Purification device for solution preparation |
| CN214115394U (en) * | 2020-12-24 | 2021-09-03 | 济宁长兴塑料助剂有限公司 | Novel ethylene glycol purification device |
| CN113351131A (en) * | 2021-07-16 | 2021-09-07 | 宁夏东方钽业股份有限公司 | Preparation equipment and method of tantalum alkoxide |
| CN113577808A (en) * | 2021-08-16 | 2021-11-02 | 伯乐氛(北京)环境技术有限公司 | Organic waste gas solvent separation and purification device and purification process |
| CN113827993A (en) * | 2021-09-30 | 2021-12-24 | 稀美资源(广东)有限公司 | Metal alkoxide purification equipment and purification method |
| CN215480793U (en) * | 2021-07-05 | 2022-01-11 | 河南中烟工业有限责任公司 | Distillation equipment for extracting tobacco geranium spice |
| CN215741848U (en) * | 2021-08-18 | 2022-02-08 | 江苏三鹏生物化工有限公司 | Purification device is used in production of 2-chlorine nicotinonitrile |
| CN216170019U (en) * | 2021-11-12 | 2022-04-05 | 浙江金诺和药业有限公司 | A purification device for producing polyethylene glycol |
| CN114392635A (en) * | 2022-02-28 | 2022-04-26 | 稀美资源(广东)有限公司 | Tantalum ethoxide automatic constant-temperature collecting and subpackaging device |
| CN114984893A (en) * | 2022-08-08 | 2022-09-02 | 稀美资源(广东)有限公司 | Tantalum ethoxide production is with solid waste treatment device with multi-stage filtration function |
| CN115054931A (en) * | 2022-08-18 | 2022-09-16 | 稀美资源(广东)有限公司 | A splitter for tantalum ethoxide coarse product |
-
2022
- 2022-10-10 CN CN202211233571.0A patent/CN115282628B/en active Active
Patent Citations (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH06220069A (en) * | 1991-11-25 | 1994-08-09 | Japan Energy Corp | Purification of tantalum alkoxide, high-purity tantalum alkoxide and gas phase growth using the same material |
| CN207856341U (en) * | 2017-12-29 | 2018-09-14 | 宜制觅智能设备（上海）有限公司 | High-efficiency evaporator with atomising device |
| CN211111139U (en) * | 2019-10-31 | 2020-07-28 | 烟台达瑞克生物工程有限公司 | Purification device for solution preparation |
| CN214115394U (en) * | 2020-12-24 | 2021-09-03 | 济宁长兴塑料助剂有限公司 | Novel ethylene glycol purification device |
| CN215480793U (en) * | 2021-07-05 | 2022-01-11 | 河南中烟工业有限责任公司 | Distillation equipment for extracting tobacco geranium spice |
| CN113351131A (en) * | 2021-07-16 | 2021-09-07 | 宁夏东方钽业股份有限公司 | Preparation equipment and method of tantalum alkoxide |
| CN113577808A (en) * | 2021-08-16 | 2021-11-02 | 伯乐氛(北京)环境技术有限公司 | Organic waste gas solvent separation and purification device and purification process |
| CN215741848U (en) * | 2021-08-18 | 2022-02-08 | 江苏三鹏生物化工有限公司 | Purification device is used in production of 2-chlorine nicotinonitrile |
| CN113827993A (en) * | 2021-09-30 | 2021-12-24 | 稀美资源(广东)有限公司 | Metal alkoxide purification equipment and purification method |
| CN216170019U (en) * | 2021-11-12 | 2022-04-05 | 浙江金诺和药业有限公司 | A purification device for producing polyethylene glycol |
| CN114392635A (en) * | 2022-02-28 | 2022-04-26 | 稀美资源(广东)有限公司 | Tantalum ethoxide automatic constant-temperature collecting and subpackaging device |
| CN114984893A (en) * | 2022-08-08 | 2022-09-02 | 稀美资源(广东)有限公司 | Tantalum ethoxide production is with solid waste treatment device with multi-stage filtration function |
| CN115054931A (en) * | 2022-08-18 | 2022-09-16 | 稀美资源(广东)有限公司 | A splitter for tantalum ethoxide coarse product |
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| CN115282628A (en) | 2022-11-04 |
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