CN115262250A - Functional garment fabric additive and preparation method thereof - Google Patents
Functional garment fabric additive and preparation method thereof Download PDFInfo
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- CN115262250A CN115262250A CN202211012679.7A CN202211012679A CN115262250A CN 115262250 A CN115262250 A CN 115262250A CN 202211012679 A CN202211012679 A CN 202211012679A CN 115262250 A CN115262250 A CN 115262250A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/46—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing natural macromolecular substances or derivatives thereof
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/64—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders using compositions containing low-molecular-weight organic compounds without sulfate or sulfonate groups
- D06P1/642—Compounds containing nitrogen
- D06P1/6426—Heterocyclic compounds
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67333—Salts or hydroxides
- D06P1/6735—Salts or hydroxides of alkaline or alkaline-earth metals with anions different from those provided for in D06P1/67341
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67383—Inorganic compounds containing silicon
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/673—Inorganic compounds
- D06P1/67391—Salts or oxidising-compounds mixtures
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- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention discloses a functional garment fabric additive and a preparation method thereof, belonging to the technical field of garment fabric additives and comprising the following components: DTA, corn starch, trimethyl chitosan, acrylic acid, citric acid, ionic liquid containing hydroxyl, ethanol, deionized water, metal nano powder, sodium acetate, sodium metaborate, molecular sieve, silica gel and ZrO 2 Nanopowder and TiO 2 The nano-particles comprise the following components in parts by weight: 3-5 parts of DTA,18-40 parts of corn starch, 10-25 parts of trimethyl chitosan, 6-15 parts of acrylic acid, 1-5 parts of citric acid, 1-6 parts of hydroxyl-containing ionic liquid, 40-70 parts of ethanol, 50-80 parts of deionized water, 20-25 parts of sodium acetate, 10-15 parts of sodium metaborate, 3-5 parts of molecular sieve, 5-8 parts of silica gel, zrO 2 2 10-16 parts of nano powder and TiO 2 15-24 parts of nano particles. According to the functional garment fabric additive and the preparation method thereof, the natural plant dyeing treatment liquid is obtained, so that the problems that the dyed fabric is poor in color fixing effect and easy to fade or decolor in the prior art are solved.
Description
Technical Field
The invention belongs to the technical field of garment fabric additives, and particularly relates to a functional garment fabric additive and a preparation method thereof.
Background
The fabric additive is a mixture or auxiliary material for improving the quality, performance and use effect of chemical products, and is added into electroplating solution for improving the performance or coating quality of the electroplating solution, and the dosage of the material is usually small
Garment materials is after processing is accomplished, and the clothing is made through processes such as drawing a design, tailorring in the later stage, and some additives need be added to it mostly to current surface fabric preparation for the surface fabric has its unique characteristic, and current surface fabric additive in the in-service use, the fixation effect is relatively poor often appears, and after the washing many times in the actual dress, the condition that the surface fabric fades appears, thereby influence user's the experience of wearing.
Disclosure of Invention
The invention aims to solve the problems that in the prior art, the color fixing effect is poor frequently, and the wearing experience of a user is influenced due to the fact that the fabric is faded and decolored after being washed for many times in actual wearing, and provides a functional clothing fabric additive and a preparation method thereof.
In order to achieve the purpose, the invention adopts the following technical scheme:
an additive for functional clothing material is disclosed, comprises the following components: DTA, corn starch, trimethyl chitosan, acrylic acid, citric acid, ionic liquid containing hydroxyl, ethanol, deionized water, metal nano powder, sodium acetate, sodium metaborate, molecular sieve, silica gel and ZrO 2 Nanopowder and TiO 2 And (3) nanoparticles.
Preferably, the adhesive comprises, by weight, 3-5 parts of DTA, 18-40 parts of corn starch, 10-25 parts of trimethyl chitosan, 6-15 parts of acrylic acid, 1-5 parts of citric acid, 1-6 parts of hydroxyl-containing ionic liquid, 40-70 parts of ethanol, 50-80 parts of deionized water, and sodium acetate20-25 parts of sodium metaborate, 10-15 parts of sodium metaborate, 3-5 parts of molecular sieve, 5-8 parts of silica gel and ZrO 2 10-16 parts of nano powder and TiO 2 15-24 parts of nano particles.
Preferably, the ionic liquid containing hydroxyl is a compound of 1-hydroxyethyl-3-methylimidazole tetrafluoroborate and 1-butyl-3-methylimidazole tetrafluoroborate.
Preferably, the metal nano powder is at least one of nano copper powder, nano silver powder and nano zinc powder.
Preferably, the weight ratio of the molecular sieve to the silica gel is 3:5.
preferably, the ZrO 2 Nano powder, tiO 2 The nano particles are a mixture consisting of 2:3 by weight ratio.
A preparation method of a functional garment fabric additive comprises the following steps:
s1, weighing raw materials of each component according to requirements;
s2, adding DTA, trimethyl chitosan, acrylic acid, hydroxyl-containing ionic liquid and ethanol into deionized water, and uniformly stirring to obtain a reagent A;
and (S3) the step of (C), adding metal nano powder, sodium acetate, sodium metaborate, molecular sieve and silica gel ZrO 2 Nano powder, tiO 2 Adding the nanoparticles into the reagent A to obtain a reagent B, adjusting the temperature, and uniformly stirring;
and S4, adding corn starch and citric acid into the reagent B, heating, keeping for a certain time, and cooling to room temperature.
Preferably, in S2, the stirring speed is 400-500r/min, and the stirring time is 40-70min.
Preferably, in S3, the temperature is adjusted to 70-80 ℃, and the stirring time is 50-80min.
Preferably, in S4, the heating temperature is 80-100 ℃ and the heating time is 30-40 minutes.
In conclusion, the technical effects and advantages of the invention are as follows: the functional garment fabric additive and the preparation method thereof comprise the following components in parts by weight: 3 parts of DTA, 18 parts of corn starch, 10 parts of trimethyl chitosan, 6 parts of acrylic acid and 2 parts of citric acid, wherein the DTA and the natural plant dye are added into deionized water together in actual use, and then the deionized water and the natural plant dye are uniformly stirred to obtain natural plant dyeing treatment liquid, so that the polyester fabric is dyed, the dyeing process is simplified, and meanwhile, the fabric is energy-saving and environment-friendly, has strong water absorption, and solves the problems that in the prior art, the dyed fabric has poor color fixing effect and is easy to fade or decolor.
Detailed Description
The technical solutions in the present disclosure will be clearly and completely described below with reference to the present disclosure, and it is obvious that the described contents are only a part of the present disclosure, and not all of the present disclosure. All other matters which can be obtained by a person skilled in the art without making creative efforts based on the contents of the present invention belong to the protection scope of the present invention.
Example 1
A functional garment fabric additive comprises the following raw materials in parts by weight: according to the weight portion, the material comprises 3 portions of DTA, 18 portions of corn starch, 10 portions of trimethyl chitosan, 6 portions of acrylic acid, 2 portions of citric acid, 1 portion of ionic liquid containing hydroxyl, 40 portions of ethanol, 50 portions of deionized water, 20 portions of sodium acetate, 10 portions of sodium metaborate, 3 portions of molecular sieve, 5 portions of silica gel, zrO, sodium hydroxide and sodium hydroxide 2 10 portions of nano powder and TiO 2 And 15 parts of nanoparticles.
The ionic liquid containing hydroxyl is 1-hydroxyethyl-3-methylimidazolium tetrafluoroborate compound.
The metal nano powder is nano copper powder.
A preparation method of a functional garment fabric additive comprises the following steps: s1, weighing raw materials of each component according to requirements;
s2, adding DTA, trimethyl chitosan, acrylic acid, hydroxyl-containing ionic liquid and ethanol into deionized water, and uniformly stirring to obtain a reagent A;
s3, adding metal nano powder, sodium acetate, sodium metaborate, molecular sieve and silica gel ZrO 2 Nano powder, tiO 2 Adding the nanoparticles into the reagent A to obtain a reagent B, adjusting the temperature, and uniformly stirring;
and S4, adding corn starch and citric acid into the reagent B, heating, keeping for a certain time, and cooling to room temperature.
In the S2, the stirring speed is 450r/min, and the stirring time is 60min;
in the step S3, the temperature is adjusted to be 75 ℃, and the stirring time is 70min;
in S4, the heating temperature was 90 ℃ and the temperature was maintained for 35 minutes.
Comparative example 1:
a functional garment fabric additive comprises the following raw materials in parts by weight: according to the weight portion, the material comprises 4 portions of DTA, 30 portions of corn starch, 18 portions of trimethyl chitosan, 8 portions of acrylic acid, 1 portion of citric acid, 1 portion of ionic liquid containing hydroxyl, 40 portions of ethanol, 50 portions of deionized water, 20 portions of sodium acetate, 10 portions of sodium metaborate, 3 portions of molecular sieve, 5 portions of silica gel, zrO 2 10 portions of nano powder and TiO 2 And 15 parts of nanoparticles.
The ionic liquid containing hydroxyl is 1-butyl-3-methylimidazolium tetrafluoroborate compound.
The metal nano powder is nano zinc powder.
A preparation method of a functional garment fabric additive comprises the following steps: s1, weighing raw materials of each component according to requirements;
s2, adding DTA, trimethyl chitosan, acrylic acid, hydroxyl-containing ionic liquid and ethanol into deionized water, and uniformly stirring to obtain a reagent A;
s3, adding metal nano powder, sodium acetate, sodium metaborate, molecular sieve and silica gel ZrO 2 Nano powder, tiO 2 Adding the nanoparticles into the reagent A to obtain a reagent B, adjusting the temperature, and uniformly stirring;
and S4, adding corn starch and citric acid into the reagent B, heating, keeping for a certain time, and cooling to room temperature.
In the S2, the stirring speed is 450r/min, and the stirring time is 60min;
in the step S3, the temperature is adjusted to be 75 ℃, and the stirring time is 70min;
in S4, the heating temperature was 90 ℃ and the temperature was maintained for 35 minutes.
Example 2:
a functional garment fabric additive comprises the following raw materials in parts by weight: according to the weight portion, the material comprises 4 portions of DTA, 32 portions of corn starch, 20 portions of trimethyl chitosan, 13 portions of acrylic acid, 3 portions of citric acid, 4 portions of ionic liquid containing hydroxyl, 55 portions of ethanol, 65 portions of deionized water, 23 portions of sodium acetate, 13 portions of sodium metaborate, 4 portions of molecular sieve, 6 portions of silica gel, zrO 4 portions of 2 13 parts of nano powder and TiO 2 20 parts of nano particles.
The ionic liquid containing hydroxyl is 1-hydroxyethyl-3-methylimidazolium tetrafluoroborate compound.
The metal nano powder is nano copper powder.
A preparation method of a functional garment fabric additive comprises the following steps: s1, weighing raw materials of each component according to requirements;
s2, adding DTA, trimethyl chitosan, acrylic acid, hydroxyl-containing ionic liquid and ethanol into deionized water, and uniformly stirring to obtain a reagent A;
s3, adding metal nano powder, sodium acetate, sodium metaborate, molecular sieve and silica gel ZrO 2 Nano powder, tiO 2 Adding the nanoparticles into the reagent A to obtain a reagent B, adjusting the temperature, and uniformly stirring;
and S4, adding corn starch and citric acid into the reagent B, heating, keeping for a certain time, and cooling to room temperature.
In the S2, the stirring speed is 450r/min, and the stirring time is 60min;
in S3, adjusting the temperature to 75 ℃ and stirring for 70min;
in S4, the heating temperature was 90 ℃ and the temperature was maintained for 35 minutes.
Comparative example 2:
a functional garment fabric additive comprises the following raw materials in parts by weight: according to the weight portion, the material comprises 4 portions of DTA, 32 portions of corn starch, 20 portions of trimethyl chitosan, 13 portions of acrylic acid, 3 portions of citric acid, 2 portions of ionic liquid containing hydroxyl, 65 portions of ethanol, 75 portions of deionized water, 23 portions of sodium acetate, 13 portions of sodium metaborate and 4 portions of molecular sieve6 parts of silica gel and ZrO 2 13 parts of nano powder and TiO 2 20 parts of nano particles.
The ionic liquid containing hydroxyl is 1-hydroxyethyl-3-methylimidazolium tetrafluoroborate compound.
The metal nano powder is nano silver powder.
A preparation method of a functional garment fabric additive comprises the following steps: s1, weighing raw materials of each component according to requirements;
s2, adding DTA, trimethyl chitosan, acrylic acid, hydroxyl-containing ionic liquid and ethanol into deionized water, and uniformly stirring to obtain a reagent A;
s3, adding metal nano powder, sodium acetate, sodium metaborate, molecular sieve and silica gel ZrO 2 Nano powder, tiO 2 Adding the nanoparticles into the reagent A to obtain a reagent B, adjusting the temperature, and uniformly stirring;
s4, adding corn starch and citric acid into the reagent B, heating, keeping for a certain time, and cooling to room temperature.
In S2, the stirring speed is 450r/min, and the stirring time is 60min;
in the step S3, the temperature is adjusted to be 75 ℃, and the stirring time is 70min;
in S4, the heating temperature was 90 ℃ and the temperature was maintained for 35 minutes.
Example 3: a functional garment fabric additive comprises the following raw materials in parts by weight: according to the weight portion, the material comprises 5 portions of DTA, 40 portions of corn starch, 25 portions of trimethyl chitosan, 15 portions of acrylic acid, 5 portions of citric acid, 6 portions of ionic liquid containing hydroxyl, 70 portions of ethanol, 80 portions of deionized water, 25 portions of sodium acetate, 15 portions of sodium metaborate, 5 portions of molecular sieve, 8 portions of silica gel, zrO 2 16 parts of nano powder and TiO 2 And 24 parts of nanoparticles.
The ionic liquid containing hydroxyl is 1-hydroxyethyl-3-methylimidazolium tetrafluoroborate compound.
The metal nano powder is nano copper powder.
A preparation method of a functional garment fabric additive comprises the following steps: s1, weighing raw materials of each component according to requirements;
s2, adding DTA, trimethyl chitosan, acrylic acid, hydroxyl-containing ionic liquid and ethanol into deionized water, and uniformly stirring to obtain a reagent A;
s3, adding metal nano powder, sodium acetate, sodium metaborate, molecular sieve and silica gel ZrO 2 Nano powder, tiO 2 Adding the nanoparticles into the reagent A to obtain a reagent B, adjusting the temperature, and uniformly stirring;
and S4, adding corn starch and citric acid into the reagent B, heating, keeping for a certain time, and cooling to room temperature.
In the S2, the stirring speed is 450r/min, and the stirring time is 60min;
in S3, the temperature is adjusted to be 75 ℃, stirring for 70min;
in S4, the heating temperature was 90 ℃ and the temperature was maintained for 35 minutes.
Comparative example 3:
a functional garment fabric additive comprises the following raw materials in parts by weight: according to the weight portion, the material comprises 5 portions of DTA, 40 portions of corn starch, 25 portions of trimethyl chitosan, 15 portions of acrylic acid, 5 portions of citric acid, 6 portions of ionic liquid containing hydroxyl, 70 portions of ethanol, 80 portions of deionized water, 25 portions of sodium acetate, 15 portions of sodium metaborate, 5 portions of molecular sieve, 8 portions of silica gel, zrO, 5 portions of sodium metaborate 2 16 parts of nano powder and TiO 2 And 24 parts of nanoparticles.
The ionic liquid containing hydroxyl is 1-butyl-3-methylimidazolium tetrafluoroborate compound.
The metal nano powder is nano silver powder.
A preparation method of a functional garment fabric additive comprises the following steps: s1, weighing raw materials of each component according to requirements;
s2, adding DTA, trimethyl chitosan, acrylic acid, hydroxyl-containing ionic liquid and ethanol into deionized water, and uniformly stirring to obtain a reagent A;
s3, adding metal nano powder, sodium acetate, sodium metaborate, molecular sieve and silica gel ZrO 2 Nano powder, tiO 2 Adding nanoparticles into reagent A to obtain reagent B, adjusting temperature, anduniformly stirring;
and S4, adding corn starch and citric acid into the reagent B, heating, keeping for a certain time, and cooling to room temperature.
In the S2, the stirring speed is 450r/min, and the stirring time is 60min;
in the step S3, the temperature is adjusted to be 75 ℃, and the stirring time is 70min;
in S4, the heating temperature was 90 ℃ and the temperature was maintained for 35 minutes.
In summary, 3 parts of DTA, 18 parts of corn starch, 10 parts of trimethyl chitosan, 6 parts of acrylic acid, 2 parts of citric acid, 1 part of ionic liquid containing hydroxyl, 40 parts of ethanol, 50 parts of deionized water, 20 parts of sodium acetate, 10 parts of sodium metaborate, 3 parts of molecular sieve, 5 parts of silica gel, zrO 3 2 10 portions of nano powder and TiO 2 When 15 parts of nano particles are mixed, the prepared fabric has the best effect and better color fixing effect, has better stability to heat and acid and alkali and good compatibility with salts, and greatly reduces the possibility of fading or decoloring, thereby improving the stability of the additive and further solving the problems of poor color fixing effect and easy fading or decoloring of the dyed fabric in the prior art.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (10)
1. The functional garment fabric additive is characterized by comprising the following components: DTA, corn starch, trimethyl chitosan, acrylic acid, citric acid, ionic liquid containing hydroxyl, ethanol, deionized water, metal nano powder, sodium acetate, sodium metaborate, molecular sieve, silica gel and ZrO 2 Nanopowder and TiO 2 And (3) nanoparticles.
2. The functional garment material additive as claimed in claim 1, which isIs characterized by comprising 3-5 parts of DTA, 18-40 parts of corn starch, 10-25 parts of trimethyl chitosan, 6-15 parts of acrylic acid, 1-5 parts of citric acid, 1-6 parts of ionic liquid containing hydroxyl, 40-70 parts of ethanol, 50-80 parts of deionized water, 20-25 parts of sodium acetate, 10-15 parts of sodium metaborate, 3-5 parts of molecular sieve, 5-8 parts of silica gel, zrO, and the like 2 10-16 parts of nano powder and TiO 2 15-24 parts of nano particles.
3. The additive for functional garment materials according to any one of claims 1 to 2, wherein the hydroxyl group-containing ionic liquid is a combination of 1-hydroxyethyl-3-methylimidazolium tetrafluoroborate and 1-butyl-3-methylimidazolium tetrafluoroborate.
4. The functional garment material additive as claimed in any one of claims 1 to 2, wherein the metal nanopowder is at least one of a copper nanopowder, a silver nanopowder and a zinc nanopowder.
5. The functional garment material additive according to any one of claims 1-2, wherein the molecular sieve and the silica gel are present in a weight ratio of 3:5.
6. functional garment material additive according to any of claims 1-2, wherein the ZrO-Si-O-R-O-is present 2 Nano powder, tiO 2 The nano particles are a mixture consisting of 2:3 by weight ratio.
7. A preparation method of a functional garment fabric additive is characterized by comprising the following steps:
s1, weighing raw materials of each component according to requirements;
s2, adding DTA, trimethyl chitosan, acrylic acid, hydroxyl-containing ionic liquid and ethanol into deionized water, and uniformly stirring to obtain a reagent A;
s3, adding metal nano powder, sodium acetate, sodium metaborate, molecular sieve and silica gel ZrO 2 Nano powderBulk, tiO 2 Adding the nanoparticles into the reagent A to obtain a reagent B, adjusting the temperature, and uniformly stirring;
and S4, adding corn starch and citric acid into the reagent B, heating, keeping for a certain time, and cooling to room temperature.
8. The preparation method of the functional garment material additive as claimed in claim 7, wherein in S2, the stirring speed is 400-500r/min, and the stirring time is 40-70min.
9. The method for preparing the functional clothing fabric additive according to claim 7, wherein in S3, the temperature is adjusted to 70-80 ℃, and the stirring time is 50-80min.
10. The method for preparing the functional garment material additive according to claim 7, wherein in S4, the heating temperature is 80-100 ℃, and the heating time is kept for 30-40 minutes.
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| US4891047A (en) * | 1985-11-19 | 1990-01-02 | Director-General of the Sericultural Experiment station, Ministry of Agriculture, Forestry and Fisheries of Japan | Process for dyeing fibers with a dye liquor containing granules of silica gel |
| WO2011118908A2 (en) * | 2010-03-23 | 2011-09-29 | (주)엔지텍 | Functional coating agent using nanometal and polyphenol |
| CN106544910A (en) * | 2015-09-18 | 2017-03-29 | 江苏阳光毛纺服装技术开发有限公司 | A kind of fixing finish method of cashmere fabric |
| CN110438824A (en) * | 2018-05-04 | 2019-11-12 | 句容市华冠服帽厂 | A kind of coating dyeing and finishing technology of silk fiber fabric |
| CN109593396A (en) * | 2018-12-17 | 2019-04-09 | 广西师范大学 | A kind of ageing resistance dye and its preparation method and application |
| CN109797574A (en) * | 2019-01-22 | 2019-05-24 | 乐清市雅格狮丹服饰有限公司 | A kind of suiting high color fastness dyeing |
| CN110952346A (en) * | 2019-12-23 | 2020-04-03 | 湖州睿阁琪服饰有限公司 | Polyester dyeing additive suitable for children clothing fabric |
| CN112981989A (en) * | 2021-02-26 | 2021-06-18 | 杭州华丝夏莎纺织科技有限公司 | Printing and dyeing additive and method for dyeing real silk/viscose composite fabric |
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