CN115253918A - Rare earth oxide production extractant adds device - Google Patents
Rare earth oxide production extractant adds device Download PDFInfo
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- CN115253918A CN115253918A CN202210893715.9A CN202210893715A CN115253918A CN 115253918 A CN115253918 A CN 115253918A CN 202210893715 A CN202210893715 A CN 202210893715A CN 115253918 A CN115253918 A CN 115253918A
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- 229910001404 rare earth metal oxide Inorganic materials 0.000 title claims abstract description 23
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 10
- 238000002156 mixing Methods 0.000 claims abstract description 94
- 230000003014 reinforcing effect Effects 0.000 claims abstract description 10
- 238000000605 extraction Methods 0.000 claims description 65
- 239000007788 liquid Substances 0.000 claims description 31
- 238000007789 sealing Methods 0.000 claims description 21
- 238000007667 floating Methods 0.000 claims description 17
- 238000003756 stirring Methods 0.000 claims description 15
- 230000002787 reinforcement Effects 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 description 43
- 239000003814 drug Substances 0.000 description 25
- 229910052761 rare earth metal Inorganic materials 0.000 description 6
- 150000002910 rare earth metals Chemical class 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 230000009471 action Effects 0.000 description 3
- 229910052747 lanthanoid Inorganic materials 0.000 description 3
- 150000002602 lanthanoids Chemical class 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 2
- 238000010030 laminating Methods 0.000 description 2
- 230000000737 periodic effect Effects 0.000 description 2
- 229910052706 scandium Inorganic materials 0.000 description 2
- SIXSYDAISGFNSX-UHFFFAOYSA-N scandium atom Chemical compound [Sc] SIXSYDAISGFNSX-UHFFFAOYSA-N 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 229910052727 yttrium Inorganic materials 0.000 description 2
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 238000005272 metallurgy Methods 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 125000003003 spiro group Chemical group 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/02—Feed or outlet devices; Feed or outlet control devices for feeding measured, i.e. prescribed quantities of reagents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/02—Apparatus therefor
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B59/00—Obtaining rare earth metals
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Manufacturing & Machinery (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Environmental & Geological Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Geochemistry & Mineralogy (AREA)
- Extraction Or Liquid Replacement (AREA)
Abstract
The invention relates to the technical field of rare earth oxide production, in particular to an extracting agent adding device for rare earth oxide production, which comprises a base plate, a bearing frame, an extracting agent tank, an adding and mixing component, a transfer component, an extracting component and two reinforcing components, wherein the bearing frame is arranged at the top of the base plate, the extracting agent tank is vertically arranged at the top of the bearing frame, the two reinforcing components are symmetrically arranged at the top of the bearing frame, the two reinforcing components are respectively abutted against the outer wall of the extracting agent tank, the adding and mixing component is arranged below the top of the bearing frame and is communicated with the extracting agent tank, the transfer component is arranged on the outer wall of the bottom end of the adding and mixing component, the extracting component is arranged at the top of the base plate, and the extracting component is positioned below the transfer component.
Description
Technical Field
The invention relates to the technical field of rare earth oxide production, in particular to an extracting agent adding device for rare earth oxide production.
Background
Rare earth (Rareaearth) is a general name of seventeen metal elements including lanthanide elements, scandium and yttrium in the chemical periodic table. There are 250 kinds of rare-earth ores in nature. Since rare earth minerals found in the 18 th century were few, only a small amount of water-insoluble oxide could be produced by chemical methods, and historically, this oxide was conventionally called "soil" and hence named rare earth. The rare earth element oxide refers to 15 kinds of lanthanide element oxides having atomic numbers of 57 to 71 in the periodic table, and 17 kinds of element oxides of scandium (Sc) and yttrium (Y) having similar chemical properties to the lanthanide elements. The rare earth elements are widely applied in the fields of petroleum, chemical industry, metallurgy, textile, ceramics, glass, permanent magnet materials and the like, the value of rare earth oxides is increasing along with the technological progress and the continuous breakthrough of application technology, the rare earth oxides need to be decomposed, filtered, extracted, precipitated, finally washed, filtered and burned in the production process of the rare earth oxides, and the extract liquid needs to be dripped in the extraction process.
The existing device for adding the extractant in the rare earth oxide production generally needs manual quantitative manual addition of the extractant to the adding device, so that the accuracy is low, and the manual addition cost is high.
Disclosure of Invention
The invention aims to provide an extracting agent adding device for producing rare earth oxides, which aims to solve the problems that the extracting agent needs to be manually and quantitatively added into an adding device generally in the background technology, the accuracy is low, and the manual adding cost is high.
The technical scheme of the invention is as follows:
the utility model provides a rare earth oxide production extractant adds device, includes the base plate, bears frame, extractant jar, adds hybrid module, transfer subassembly, extraction subassembly and two reinforcement subassemblies, bear the top of installing at the base plate, the vertical top that sets up bearing frame of extractant jar, two it sets up at the top that bears the frame to consolidate the subassembly symmetry to two reinforcement subassemblies contradict with the outer wall of extractant jar respectively, it installs in the top below that bears the frame to add hybrid module to it is linked together with the extractant jar to add hybrid module, the transfer unit mount is on the bottom outer wall that adds hybrid module, the extraction unit mount is at the top of base plate to the extraction subassembly is located the below of transfer subassembly.
Further, it includes standpipe, first solenoid valve, blending tank, first inlet pipe, second inlet pipe, hybrid component, unloading pipe and second solenoid valve to add hybrid component, the standpipe is vertical to be set up in the top below that bears the frame to the top of standpipe is linked together with the inside of extractant jar, first solenoid valve is installed on the standpipe, the bottom at the standpipe is installed to the blending tank to the inside of blending tank is linked together with the bottom of standpipe, first inlet pipe and second inlet pipe symmetry set up on the top outer wall of blending tank to first inlet pipe and second inlet pipe all are linked together with the inside of blending tank, hybrid component installs in the blending tank to the bottom of hybrid component extends to the bottom of blending tank, the vertical setting of unloading pipe is in the bottom of blending tank to the top of unloading pipe is linked together with the inside of blending tank, the second solenoid valve is installed on the unloading pipe.
Further, mixing unit includes mixing shaft, hybrid motor and four stirring boards, the mixing shaft rotates and installs in the hybrid tank, four the stirring board is around the axle center equidistant setting of mixing shaft on the outer wall of mixing shaft, every all be equipped with a plurality of logical groove on the stirring board, the vertical setting of hybrid motor is in the bottom of hybrid tank to hybrid motor's output shaft and mixing hub connection.
Further, the transfer subassembly includes fixed plate, rotation axis, rotary disk, driving motor, action wheel, follows driving wheel, belt and four quantitative transfer parts, the fixed plate level sets up on the bottom outer wall of blending tank, the rotation axis rotates and installs on the fixed plate, the bottom at the rotation axis is installed to the rotary disk, the vertical top that sets up at the fixed plate of driving motor, the action wheel is installed on driving motor's output shaft, install the top at the rotation axis from the driving wheel, the belt cover is established in the outside of action wheel and follow driving wheel, four quantitative transfer parts set up on the rotary disk equidistantly around the centre of a circle of rotary disk.
Further, every quantitative transfer part all includes graduated flask, position circle, kickboard, first recess, second recess, infrared emitter, infrared receiver and closure, the graduated flask is vertical to be set up at the top of rotary disk, the bottom of graduated flask is equipped with the connecting pipe rather than inside being linked together, be equipped with the third solenoid valve on the connecting pipe, the position circle sets up the top at the graduated flask, the kickboard slidable mounting is in the graduated flask to the center department of kickboard is equipped with the through-hole, first recess is seted up on the outer wall of kickboard, the second recess is seted up on the top inner wall of graduated flask to the second recess corresponds with first recess, infrared emitter installs in first recess, infrared receiver installs in the second recess, the closure is installed at the top of rotary disk to the top of closure and the top laminating of position circle.
Further, the closure piece includes the guide rail, removes frame, closing plate, first lead screw slip table and connecting plate, the guide rail level sets up the top at the rotary disk, remove frame slidable mounting on the guide rail, the closing plate is installed on the top of removing the frame to the bottom of closing plate and the top laminating of position circle, first lead screw slip table level sets up the top at the rotary disk, the connecting plate is installed on the removal of first lead screw slip table is served to the connecting plate is connected with removing the frame.
Further, the extraction subassembly includes support frame, mobile station, second lead screw slip table, loading board, two slide rails and two extraction ponds, the support frame erects at the top of base plate to the support frame is located the below of rotary disk, two the slide rail symmetry sets up the top at the support frame, mobile station slidable mounting is on two slide rails, two the extraction pond symmetry sets up the top at the mobile station, second lead screw slip table level sets up the top at the support frame, the loading board is installed on the removal of second lead screw slip table is served to the loading board is connected with the mobile station.
Further, every the reinforcement component all includes L template, hydraulic rod and arc, the L template is installed at the top of bearing the frame, the hydraulic rod level sets up on the outer wall of L template, the arc is installed on hydraulic rod's output to the arc is contradicted with the outer wall of extractant jar.
Furthermore, the top spiro union of extractant jar has sealed lid, be equipped with a plurality of antiskid groove on the outer wall of sealed lid, sealed covering is equipped with the feed liquor pipe, be equipped with the valve on the feed liquor pipe.
Compared with the prior art, the invention provides an extracting agent adding device for producing rare earth oxide by improving the extracting agent adding device, which has the following improvements and advantages that:
one is as follows: according to the automatic quantitative extraction agent adding device, the extraction agent is poured into the extraction agent tank, the adding and mixing assembly works to convey the extraction agent in the extraction agent tank to the extraction agent tank, meanwhile, the extraction agent needs to be mixed with other agents for use, the other agents are conveyed into the adding and mixing assembly, the adding and mixing assembly works to stir and mix the extraction agent and the other agents, the adding and mixing assembly conveys the mixed extraction agent liquid medicine into the transfer assembly, the transfer assembly works to quantitatively transfer and store the extraction agent liquid medicine, and finally the transfer assembly quantitatively conveys the extraction agent liquid medicine into the extraction assembly, so that the purpose of automatically and quantitatively adding the extraction agent liquid medicine is achieved, manual adding is not needed, the accuracy is improved, and the labor cost is reduced.
And the second step is as follows: the second electromagnetic valve is opened, the extraction agent liquid medicine in the mixing tank enters the measuring cylinder through the blanking pipe, the floating plate gradually floats upwards along with the liquid level in the measuring cylinder, when the floating plate drives the infrared transmitter to float upwards to correspond to the infrared receiver, the infrared receiver receives an infrared signal sent by the infrared transmitter, the second electromagnetic valve is closed at the moment, the extraction agent liquid medicine in the measuring cylinder achieves the purpose of quantitative transfer and storage, then the sealing part is used for sealing the top end of the measuring cylinder, the floating plate is prevented from floating upwards to the outside of the measuring cylinder by the positioning ring, finally the third electromagnetic valve is opened, and the extraction agent liquid medicine in the measuring cylinder is quantitatively conveyed into the extraction assembly through the connecting pipe.
And the third step: according to the invention, the two extraction tanks are circularly added with the extraction agent liquid medicine, so that the two extraction tanks are prevented from being incapable of working, the second screw rod sliding table works to drive the bearing plate to move, the bearing plate drives the moving table to move on the two sliding rails, the moving table drives the two extraction tanks to move, the positions of the two extraction tanks are conveniently switched, and further, the four quantitative transfer components can quantitatively convey the extraction agent liquid medicine to the two extraction tanks.
Drawings
The invention is further explained below with reference to the figures and examples:
FIG. 1 is a first perspective view of the present invention;
FIG. 2 is a schematic perspective view of the present invention;
FIG. 3 is a third schematic perspective view of the present invention;
FIG. 4 is a partial perspective view of the first embodiment of the present invention;
FIG. 5 is a partial cross-sectional view of the first embodiment of the present invention;
FIG. 6 is a partial perspective view of the second embodiment of the present invention;
FIG. 7 is a schematic view of a third embodiment of the present invention;
FIG. 8 is a fourth schematic partial perspective view of the present invention;
FIG. 9 is a partial top view of the present invention;
FIG. 10 isbase:Sub>A cross-sectional view taken along line A-A of FIG. 9;
fig. 11 is a schematic diagram of a partial three-dimensional structure of the present invention.
Description of reference numerals:
the device comprises a base plate 1, a bearing frame 2, an extracting agent tank 3, a sealing cover 31, an anti-skid groove 32, a liquid inlet pipe 33, a valve 34, an adding and mixing assembly 4, a vertical pipe 41, a first electromagnetic valve 42, a mixing tank 43, a first feed pipe 44, a second feed pipe 45, a mixing part 46, a mixing shaft 461, a mixing motor 462, a stirring plate 463, a through groove 464, a blanking pipe 47, a second electromagnetic valve 48, a transfer assembly 5, a fixed plate 51, a rotating shaft 52, a rotating disc 53, a driving motor 54, a driving wheel 55, a driven wheel 56, a belt 57, a quantitative transfer part 58, a measuring cylinder 581, a connecting pipe 5811, a third electromagnetic valve 5812, a positioning ring 582, a floating plate 583, a through hole 5831, a first groove 584, a second groove 585, an infrared emitter 586, an infrared receiver 587, a sealing part 588, a guide rail 5881, a moving frame 5882, a sealing plate 5883, a first screw sliding table 5884, a connecting plate 5885, an extracting assembly 6, a supporting frame 61, a moving table 62, a second sliding table 63, a bearing plate 64, a reinforcing assembly 66, a reinforcing assembly 7, a sliding rail 71, a sliding rail 73 and an arc-shaped plate 73.
Detailed Description
The present invention is described in detail below, and technical solutions in the embodiments of the present invention are clearly and completely described, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The invention provides an extraction agent adding device for producing rare earth oxide, which comprises a base plate 1, a bearing frame 2, an extraction agent tank 3, an adding and mixing component 4, a transfer component 5, an extraction component 6 and two reinforcing components 7, as shown in figures 1-11, wherein the bearing frame 2 is arranged at the top of the base plate 1, the extraction agent tank 3 is vertically arranged at the top of the bearing frame 2, the two reinforcing components 7 are symmetrically arranged at the top of the bearing frame 2, the two reinforcing components 7 are respectively abutted against the outer walls of the extraction agent tank 3, the adding and mixing component 4 is arranged below the top of the bearing frame 2, the adding and mixing component 4 is communicated with the extraction agent tank 3, the transfer component 5 is arranged on the outer wall of the bottom end of the adding and mixing component 4, the extraction component 6 is arranged at the top of the base plate 1, and the extraction component 6 is positioned below the transfer component 5; pour into the extractant into extractant through realizing to extractant jar 3, then add 4 work of mixed subassembly and carry the extractant in extractant jar 3 to wherein, other medicaments cooperation use need be mixed to the extractant simultaneously, other medicaments are carried to in adding mixed subassembly 4, add 4 work of mixed subassembly and stir the mixture with extractant and other medicaments wherein after that, add the extractant liquid medicine after mixed of mixed subassembly 4 afterwards and carry to transfer subassembly 5 in, transfer subassembly 5 work carries out quantitative transfer to extractant liquid medicine and stores, transfer subassembly 5 carries extractant liquid medicine ration to extraction subassembly 6 in finally, and then realize the purpose of automatic ration interpolation extractant liquid medicine, need not artifical manual interpolation, the accuracy is improved, and reduce the human cost.
Specifically, the adding and mixing assembly 4 comprises a vertical pipe 41, a first solenoid valve 42, a mixing tank 43, a first feeding pipe 44, a second feeding pipe 45, a mixing part 46, a blanking pipe 47 and a second solenoid valve 48, wherein the vertical pipe 41 is vertically arranged below the top of the carrier 2, the top end of the vertical pipe 41 is communicated with the inside of the extractant tank 3, the first solenoid valve 42 is arranged on the vertical pipe 41, the mixing tank 43 is arranged at the bottom end of the vertical pipe 41, the inside of the mixing tank 43 is communicated with the bottom end of the vertical pipe 41, the first feeding pipe 44 and the second feeding pipe 45 are symmetrically arranged on the outer wall of the top end of the mixing tank 43, the first feeding pipe 44 and the second feeding pipe 45 are communicated with the inside of the mixing tank 43, the mixing part 46 is arranged in the mixing tank 43, the bottom end of the mixing part 46 extends to the bottom of the mixing tank 43, the blanking pipe 47 is vertically arranged at the bottom of the mixing tank 43, and the top end of the blanking pipe 47 is communicated with the inside of the mixing tank 43, and the second solenoid valve 48 is arranged on the blanking pipe 47; the extractant in the extractant jar 3 is opened through first solenoid valve 42 and the extractant enters into blending tank 43 through standpipe 41, then first inlet pipe 44 and second inlet pipe 45 carry other medicaments to blending tank 43 in, mixing element 46 work is stirred the extractant and other medicaments wherein and is mixed, second solenoid valve 48 after mixing opens, the extractant liquid medicine in the blending tank 43 enters into to transfer subassembly 5 in through unloading pipe 47, make things convenient for transfer subassembly 5 work to carry the extractant liquid medicine ration to in the extraction subassembly 6.
Specifically, the mixing component 46 includes a mixing shaft 461, a mixing motor 462 and four stirring plates 463, the mixing shaft 461 is rotatably installed in the mixing tank 43, the four stirring plates 463 are arranged on the outer wall of the mixing shaft 461 at equal intervals around the axial center of the mixing shaft 461, each stirring plate 463 is provided with a plurality of through grooves 464, the mixing motor 462 is vertically arranged at the bottom of the mixing tank 43, and the output shaft of the mixing motor 462 is connected with the mixing shaft 461; drive mixing shaft 461 through mixing motor 462 work and rotate, and mixing shaft 461 drives four stirring boards 463 and rotates, and four stirring boards 463 rotate and stir the extraction agent and other medicaments in to blending tank 43 and mix, and extraction agent and other medicaments fuse with higher speed, improve the quality of extraction.
Specifically, the transfer assembly 5 comprises a fixed plate 51, a rotating shaft 52, a rotating disc 53, a driving motor 54, a driving wheel 55, a driven wheel 56, a belt 57 and four quantitative transfer components 58, wherein the fixed plate 51 is horizontally arranged on the outer wall of the bottom end of the mixing tank 43, the rotating shaft 52 is rotatably mounted on the fixed plate 51, the rotating disc 53 is mounted at the bottom of the rotating shaft 52, the driving motor 54 is vertically arranged at the top of the fixed plate 51, the driving wheel 55 is mounted on the output shaft of the driving motor 54, the driven wheel 56 is mounted at the top end of the rotating shaft 52, the belt 57 is sleeved outside the driving wheel 55 and the driven wheel 56, and the four quantitative transfer components 58 are arranged on the rotating disc 53 at equal intervals around the center of the rotating disc 53; the driving wheel 55 is driven to rotate by the work of the driving motor 54, the driving wheel 55 drives the driven wheel 56 to rotate by utilizing the belt 57, the driven wheel 56 drives the rotating shaft 52 and the rotating disc 53 to synchronously rotate, the rotating disc 53 drives the four quantitative transferring parts 58 to sequentially pass through the lower part of the discharging pipe 47, and the four quantitative transferring parts 58 are convenient for quantitatively transferring and storing the extracting agent and the liquid medicine.
Specifically, each of the quantitative transferring members 58 comprises a measuring cylinder 581, a positioning ring 582, a floating plate 583, a first groove 584, a second groove 585, an infrared emitter 586, an infrared receiver 587 and a closure member 588, wherein the measuring cylinder 581 is vertically arranged at the top of the rotating disc 53, the bottom of the measuring cylinder 581 is provided with a connecting pipe 5811 communicated with the inside of the measuring cylinder 581, the connecting pipe 5811 is provided with a third solenoid valve 5812, the positioning ring 582 is arranged at the top of the measuring cylinder 581, the floating plate 583 is slidably arranged in the measuring cylinder 581, a through hole 5831 is arranged at the center of the floating plate 583, the first groove 584 is arranged on the outer wall of the floating plate 583, the second groove 585 is arranged on the inner wall of the top end of the measuring cylinder 581, the second groove 585 corresponds to the first groove 584, the infrared emitter 586 is arranged in the first groove 584, the infrared receiver 587 is arranged in the second groove 585, the closure member 585 is arranged at the top of the rotating disc 53, and the top end of the closure member 588 is attached to the top of the positioning ring 582; the second electromagnetic valve 48 is opened, the extracting agent liquid in the mixing tank 43 enters the measuring cylinder 581 through the feeding pipe 47, the floating plate 583 gradually floats upwards along with the liquid level in the measuring cylinder 581, when the floating plate 583 drives the infrared emitter 586 to float upwards to correspond to the infrared receiver 587, the infrared receiver 587 receives an infrared signal sent by the infrared emitter 586, at this time, the second electromagnetic valve 48 is closed, the extracting agent liquid in the measuring cylinder 581 achieves the purpose of quantitative transfer and storage, then the sealing part 588 works to seal the top end of the measuring cylinder 581, the positioning ring 582 prevents the floating plate 583 from floating upwards to the outside of the measuring cylinder 581, finally, the third electromagnetic valve 5812 is opened, the extracting agent liquid in the measuring cylinder 581 is quantitatively conveyed into the extracting component 6 through the connecting pipe 5811, the purpose of automatically and quantitatively adding the extracting agent liquid is achieved, manual adding is not needed, accuracy is improved, and labor cost is reduced.
Specifically, the enclosure 588 comprises a guide rail 5881, a moving rack 5882, a sealing plate 5883, a first screw rod sliding table 5884 and a connecting plate 5885, wherein the guide rail 5881 is horizontally arranged at the top of the rotating disk 53, the moving rack 5882 is slidably arranged on the guide rail 5881, the sealing plate 5883 is arranged at the top end of the moving rack 5882, the bottom of the sealing plate 5883 is attached to the top of the positioning ring 582, the first screw rod sliding table 5884 is horizontally arranged at the top of the rotating disk 53, the connecting plate 5885 is arranged at the moving end of the first screw rod sliding table 5884, and the connecting plate 5885 is connected with the moving rack 5882; work through first lead screw slip table 5884 drives the connecting plate 5885 and removes, and connecting plate 5885 drives and removes frame 5882 and moves on guide rail 5881, removes frame 5882 and drives sealing plate 5883 and remove to the top of position circle 582, and the bottom of sealing plate 5883 is laminated with the top of position circle 582 this moment, and then has reached and has sealed the purpose to the top of graduated flask 581.
Specifically, the extraction assembly 6 includes a support frame 61, a moving table 62, a second screw rod sliding table 63, a bearing plate 64, two sliding rails 65 and two extraction cells 66, the support frame 61 is erected on the top of the substrate 1, the support frame 61 is located below the rotating disc 53, the two sliding rails 65 are symmetrically arranged on the top of the support frame 61, the moving table 62 is slidably mounted on the two sliding rails 65, the two extraction cells 66 are symmetrically arranged on the top of the moving table 62, the second screw rod sliding table 63 is horizontally arranged on the top of the support frame 61, the bearing plate 64 is mounted on the moving end of the second screw rod sliding table 63, and the bearing plate 64 is connected with the moving table 62; two extraction ponds 66 circulate and add extractant liquid medicine, avoid two unable work of extraction pond 66, and second lead screw slip table 63 work drives loading board 64 and removes, and loading board 64 drives mobile station 62 and removes on two slide rails 65, and mobile station 62 drives two extraction ponds 66 and removes, conveniently switches the position of two extraction ponds 66, and then four ration transfer parts 58 homoenergetic carry out extractant liquid medicine ration to two extraction ponds 66 and carry.
Specifically, each reinforcing assembly 7 comprises an L-shaped plate 71, a hydraulic push rod 72 and an arc-shaped plate 73, wherein the L-shaped plate 71 is installed at the top of the bearing frame 2, the hydraulic push rod 72 is horizontally arranged on the outer wall of the L-shaped plate 71, the arc-shaped plate 73 is installed at the output end of the hydraulic push rod 72, and the arc-shaped plate 73 is abutted against the outer wall of the extracting agent tank 3; work through hydraulic push rod 72 drives arc 73 and removes, and arc 73 removes to contradict with the outer wall of extractant jar 3, and it is spacing that arc 73 contradicts extractant jar 3, avoids extractant jar 3 to drop from the top that bears frame 2.
Specifically, the top end of the extractant tank 3 is screwed with a sealing cover 31, the outer wall of the sealing cover 31 is provided with a plurality of anti-skid grooves 32, the sealing cover 31 is provided with a liquid inlet pipe 33, and the liquid inlet pipe 33 is provided with a valve 34; the sealing cover 31 is screwed out from the top end of the extracting agent tank 3, so that the extracting agent tank 3 is conveniently overhauled, the valve 34 is opened, and the extracting agent is conveniently poured into the extracting agent tank 3 through the liquid inlet pipe 33.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.
Claims (9)
1. A rare earth oxide production extractant adds device which characterized in that: including base plate (1), bear frame (2), extractant jar (3), add mixing element (4), transfer subassembly (5), extraction subassembly (6) and two reinforcement subassembly (7), bear the top of frame (2) and install at base plate (1), the vertical top that bears frame (2) that sets up of extractant jar (3), two reinforce the top that subassembly (7) symmetry set up and bear frame (2) to two reinforcement subassemblies (7) are contradicted with the outer wall of extractant jar (3) respectively, add mixing element (4) and install the top below that bears frame (2) to it is linked together with extractant jar (3) to add mixing element (4), transfer subassembly (5) are installed on the bottom outer wall that adds mixing element (4), the top at base plate (1) is installed to extraction subassembly (6) are located the below of transfer subassembly (5).
2. The extraction agent adding device for producing rare earth oxide according to claim 1, characterized in that: the adding and mixing component (4) comprises a vertical pipe (41), a first electromagnetic valve (42), a mixing tank (43), a first feeding pipe (44), a second feeding pipe (45), a mixing part (46), a blanking pipe (47) and a second electromagnetic valve (48), the vertical tube (41) is vertically arranged below the top of the bearing frame (2), and the top end of the vertical pipe (41) is communicated with the inside of the extracting agent tank (3), the first electromagnetic valve (42) is arranged on a vertical pipe (41), the mixing tank (43) is arranged at the bottom end of the vertical pipe (41), and the interior of the mixing tank (43) is communicated with the bottom end of the vertical pipe (41), the first feeding pipe (44) and the second feeding pipe (45) are symmetrically arranged on the outer wall of the top end of the mixing tank (43), and the first feeding pipe (44) and the second feeding pipe (45) are both communicated with the interior of the mixing tank (43), the mixing element (46) is mounted in a mixing tank (43), and the bottom end of the mixing part (46) extends to the bottom of the mixing tank (43), the blanking pipe (47) is vertically arranged at the bottom of the mixing tank (43), and the top end of the blanking pipe (47) is communicated with the interior of the mixing tank (43), the second electromagnetic valve (48) is arranged on the blanking pipe (47).
3. The extraction agent adding device for producing rare earth oxide according to claim 2, characterized in that: mixing element (46) include mixing shaft (461), hybrid motor (462) and four stirring boards (463), mixing shaft (461) rotates to be installed in blending tank (43), four stirring boards (463) set up on the outer wall of mixing shaft (461) around the axle center of mixing shaft (461) is equidistant, every all be equipped with a plurality of logical groove (464) on stirring board (463), the vertical bottom that sets up at blending tank (43) of hybrid motor (462) to the output shaft and mixing shaft (461) of hybrid motor (462) are connected.
4. The extraction agent adding device for producing rare earth oxide according to claim 2, characterized in that: the transfer assembly (5) comprises a fixing plate (51), a rotating shaft (52), a rotating disc (53), a driving motor (54), a driving wheel (55), a driven wheel (56), a belt (57) and four quantitative transfer components (58), wherein the fixing plate (51) is horizontally arranged on the outer wall of the bottom end of the mixing tank (43), the rotating shaft (52) is rotatably arranged on the fixing plate (51), the rotating disc (53) is arranged at the bottom of the rotating shaft (52), the driving motor (54) is vertically arranged at the top of the fixing plate (51), the driving wheel (55) is arranged on an output shaft of the driving motor (54), the driven wheel (56) is arranged at the top end of the rotating shaft (52), the belt (57) is sleeved outside the driving wheel (55) and the driven wheel (56), and the four quantitative transfer components (58) are equidistantly arranged on the rotating disc (53) around the circle center of the rotating disc (53).
5. The extraction agent adding device for producing rare earth oxide according to claim 4, characterized in that: each quantitative transfer component (58) comprises a measuring cylinder (581), a positioning ring (582), a floating plate (583), a first groove (584), a second groove (585), an infrared emitter (586), an infrared receiver (587) and a closure (588), wherein the measuring cylinder (581) is vertically arranged at the top of the rotating disc (53), a connecting pipe (5811) communicated with the interior of the measuring cylinder (581) is arranged at the bottom of the measuring cylinder (581), a third electromagnetic valve (5812) is arranged on the connecting pipe (5811), the positioning ring (582) is arranged at the top of the measuring cylinder (581), the floating plate (583) is slidably arranged in the measuring cylinder (581), a through hole (5831) is arranged at the center of the floating plate (583), the first groove (584) is arranged on the outer wall of the floating plate (583), the second groove (585) is arranged on the inner wall of the top end of the measuring cylinder (581), the second groove (585) corresponds to the first groove (584), the infrared emitter (584) is arranged in the first groove (584), the second groove (588) is arranged on the top of the infrared receiver (584), and the top of the infrared receiver (587) is attached to the closure (582).
6. The extraction agent adding device for producing rare earth oxide according to claim 5, characterized in that: the closing member (588) comprises a guide rail (5881), a moving frame (5882), a sealing plate (5883), a first screw rod sliding table (5884) and a connecting plate (5885), wherein the guide rail (5881) is horizontally arranged at the top of the rotating disc (53), the moving frame (5882) is slidably arranged on the guide rail (5881), the sealing plate (5883) is arranged at the top end of the moving frame (5882), the bottom of the sealing plate (5883) is attached to the top of a positioning ring (582), the first screw rod sliding table (5884) is horizontally arranged at the top of the rotating disc (53), the connecting plate (5885) is arranged at the moving end of the first screw rod sliding table (5884), and the connecting plate (5885) is connected with the moving frame (5882).
7. The extraction agent adding device for producing rare earth oxide according to claim 4, characterized in that: extraction subassembly (6) are including support frame (61), mobile station (62), second lead screw slip table (63), loading board (64), two slide rails (65) and two extraction ponds (66), the top at base plate (1) is erect in support frame (61) to support frame (61) are located the below of rotary disk (53), two slide rail (65) symmetry sets up the top at support frame (61), mobile station (62) slidable mounting is on two slide rails (65), two extraction ponds (66) symmetry sets up the top at mobile station (62), second lead screw slip table (63) level sets up the top at support frame (61), loading board (64) are installed on the removal end of second lead screw slip table (63) to loading board (64) are connected with mobile station (62).
8. The extraction agent adding device for producing rare earth oxide according to claim 1, characterized in that: each the reinforcing component (7) comprises an L-shaped plate (71), a hydraulic push rod (72) and an arc-shaped plate (73), the L-shaped plate (71) is installed at the top of the bearing frame (2), the hydraulic push rod (72) is horizontally arranged on the outer wall of the L-shaped plate (71), the arc-shaped plate (73) is installed at the output end of the hydraulic push rod (72), and the arc-shaped plate (73) is abutted to the outer wall of the extracting agent tank (3).
9. The extraction agent adding device for producing rare earth oxide according to claim 1, characterized in that: the top end of the extractant tank (3) is in threaded connection with a sealing cover (31), the outer wall of the sealing cover (31) is provided with a plurality of anti-skidding grooves (32), the sealing cover (31) is provided with a liquid inlet pipe (33), and the liquid inlet pipe (33) is provided with a valve (34).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210893715.9A CN115253918A (en) | 2022-07-27 | 2022-07-27 | Rare earth oxide production extractant adds device |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210893715.9A CN115253918A (en) | 2022-07-27 | 2022-07-27 | Rare earth oxide production extractant adds device |
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| CN115253918A true CN115253918A (en) | 2022-11-01 |
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| CN104120258A (en) * | 2014-07-25 | 2014-10-29 | 广西师范大学 | Method for non-saponification extraction and separation of light rare earth elements |
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| CN214131585U (en) * | 2021-07-14 | 2021-09-07 | 潍坊三昌化工科技有限公司 | PX heterogeneous grade mixed xylene mixing and adding device |
| CN113895665A (en) * | 2021-09-10 | 2022-01-07 | 上海素莲食品科技有限公司 | Canned plant protein ham packaging equipment and working method thereof |
| CN114452861A (en) * | 2022-03-09 | 2022-05-10 | 叶旭鹏 | Building construction compounding device |
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2022
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Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104120258A (en) * | 2014-07-25 | 2014-10-29 | 广西师范大学 | Method for non-saponification extraction and separation of light rare earth elements |
| CN210057452U (en) * | 2019-05-14 | 2020-02-14 | 云南太瑞生物科技有限公司 | Extraction device for cannabidiol preparation process |
| CN112572854A (en) * | 2020-12-07 | 2021-03-30 | 湖南四方糖业有限公司 | Anti-sticking guide type extrusion-free brown sugar quantitative subpackaging mechanism |
| CN214131585U (en) * | 2021-07-14 | 2021-09-07 | 潍坊三昌化工科技有限公司 | PX heterogeneous grade mixed xylene mixing and adding device |
| CN113895665A (en) * | 2021-09-10 | 2022-01-07 | 上海素莲食品科技有限公司 | Canned plant protein ham packaging equipment and working method thereof |
| CN114452861A (en) * | 2022-03-09 | 2022-05-10 | 叶旭鹏 | Building construction compounding device |
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