CN115216794A - Tetramethyl ammonium hydroxide electrolytic device convenient to clearance has and prevents splashing - Google Patents

Tetramethyl ammonium hydroxide electrolytic device convenient to clearance has and prevents splashing Download PDF

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Publication number
CN115216794A
CN115216794A CN202210940326.7A CN202210940326A CN115216794A CN 115216794 A CN115216794 A CN 115216794A CN 202210940326 A CN202210940326 A CN 202210940326A CN 115216794 A CN115216794 A CN 115216794A
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China
Prior art keywords
electrolysis
clearance
device main
groove
water
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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CN202210940326.7A
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Chinese (zh)
Inventor
季中伟
马立军
张建元
乔正收
马海文
崔文亮
刘庆五
王金城
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Zhenjiang Runjing High Purity Chemical Technology Co ltd
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Zhenjiang Runjing High Purity Chemical Technology Co ltd
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Priority to CN202210940326.7A priority Critical patent/CN115216794A/en
Publication of CN115216794A publication Critical patent/CN115216794A/en
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    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B9/00Cells or assemblies of cells; Constructional parts of cells; Assemblies of constructional parts, e.g. electrode-diaphragm assemblies; Process-related cell features
    • C25B9/60Constructional parts of cells
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B15/00Operating or servicing cells
    • C25B15/08Supplying or removing reactants or electrolytes; Regeneration of electrolytes
    • CCHEMISTRY; METALLURGY
    • C25ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
    • C25BELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
    • C25B3/00Electrolytic production of organic compounds
    • C25B3/01Products
    • C25B3/09Nitrogen containing compounds

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Electrolytic Production Of Non-Metals, Compounds, Apparatuses Therefor (AREA)

Abstract

The invention discloses a conveniently cleaned anti-splashing tetramethylammonium hydroxide electrolysis device, which comprises a device main body, supporting legs, a feeding hole, a liquid outlet and a motor, wherein the bottom of the device main body is provided with the supporting legs. This tetramethyl ammonium hydroxide electrolytic device who prevents splashing convenient to clearance has, be provided with the clearance post, the clearance post is located the top of the device electrolysis trough, can remove the clearance post with the sprinkler bead through the inside telescopic link of clearance post, make the sprinkler bead remove to the top position of electrolysis trough, pressurization through the water pump, make rivers spray through the sprinkler bead, wash the inner wall of electrolysis trough, reach the mesh of clearing up the electrolysis trough, for the dismantlement of replacement to electrolysis device is washd, the clearance degree of difficulty to the device has been reduced, cleaning efficiency has been improved, the use degree of difficulty of the device has been reduced, and the design through the feed inlet, raw materials when having reduced the device reinforced splashes, the convenience that the device used has been improved.

Description

Tetramethyl ammonium hydroxide electrolytic device convenient to clearance has and prevents splashing
Technical Field
The invention relates to the technical field of electrolysis devices, in particular to a tetramethylammonium hydroxide electrolysis device which is convenient to clean and has the function of preventing splashing.
Background
Electrolysis is the process of passing an electric current through an electrolyte solution or a molten electrolyte (also called electrolyte) to cause redox reactions at the cathode and anode, and electrochemical cells can undergo electrolysis upon application of a direct current voltage. A process of synthesizing a high-purity substance from a chemical and treating the surface of the material by an electrochemical reaction occurring at the interface between an electrode as an electron conductor and an electrolyte as an ion conductor. When the power is on, cations in the electrolyte move to the cathode to absorb electrons, and reduction is carried out to generate new substances; the anions in the electrolyte move to the anode, releasing electrons, and oxidation occurs, and new species are also generated. In the extension process of tetramethyl ammonium hydroxide, the electrolysis mode is mostly adopted, tetramethyl ammonium chloride is used as a raw material for production, the existing electrolysis device for tetramethyl ammonium hydroxide production needs to be cleaned on the inner wall of the electrolysis device after being used, and the electrolysis device needs to be disassembled when being cleaned, so that the cleaning of the electrolysis device is inconvenient.
Therefore, we have proposed an apparatus for electrolyzing tetramethylammonium hydroxide with splash prevention, which is easy to clean, so as to solve the problems proposed in the above.
Disclosure of Invention
The invention aims to provide a conveniently cleaned anti-splashing tetramethylammonium hydroxide electrolysis device, which aims to solve the problem that the conventional electrolysis device for producing tetramethylammonium hydroxide in the market in the background art needs to clean the inner wall of the electrolysis device after use and needs to be disassembled during cleaning, so that the electrolysis device is inconvenient to clean.
In order to achieve the purpose, the invention provides the following technical scheme: the utility model provides a tetramethyl ammonium hydroxide electrolytic device with prevent splashing convenient to clearance, includes device main part, supporting leg, feed inlet, liquid outlet and motor, the supporting leg is installed to the bottom of device main part, and the upside of device main part installs the feed inlet, the liquid outlet is installed to the bottom of device main part, and the motor is installed at the top of device main part.
Preferably, a water storage tank is installed on the right side of the top of the device main body, a waste gas tank is installed on the right side of the device main body, a gas treatment device is connected to the waste gas tank, and an air inlet pipe is connected to the gas treatment device.
Preferably, the feed chute has been seted up to the inside of feed inlet, the bottom of feed chute is connected with the splashproof groove, and the width of splashproof groove is greater than the width of feed chute, the internally mounted of splashproof groove has the filter screen, the right-hand member of splashproof groove links to each other with the catheter, the lower extreme and the electrolysis trough of catheter communicate with each other, the electrolysis trough is seted up in the device main part, the internally mounted of electrolysis trough has the electrolysis electrode.
Preferably, the motor is provided with a stirring shaft, the bottom end of the stirring shaft is inserted into the electrolytic bath, stirring plates are arranged on the left side and the right side of the stirring shaft, the height of each stirring plate is smaller than that of each electrolytic electrode, and a supporting top plate is arranged at the top of the electrolytic bath.
Preferably, the supporting top plate is provided with two cleaning columns, the two cleaning columns are distributed on the supporting top plate, the supporting top plate is provided with air holes, the two groups of air holes are circularly distributed on the supporting top plate and penetrate through the upper surface and the lower surface of the supporting top plate, two water guide pipes are arranged between the cleaning columns, and one end of each water guide pipe is connected to the water storage tank.
Preferably, the top of the supporting top plate is provided with an air guide plate, a tapered groove is formed in the air guide plate, and the tapered groove is communicated with the air inlet pipe.
Preferably, a water pipe pressing block is installed at the top of the cleaning column, the water guide pipe is fixed through the water pipe pressing block, a lifting groove is formed in the cleaning column, and the bottom of the lifting groove is communicated with the bottom surface of the cleaning column.
Preferably, the water pump is installed on the top of lifting groove inside, and the end of intaking of water pump links to each other with the aqueduct, be connected with the outlet pipe on the water pump, the internally mounted in lifting groove has the backup pad, the telescopic link is installed to the bottom of backup pad, the bottom of telescopic link links to each other with the connecting plate, the outer sleeve is installed to the bottom of connecting plate.
Preferably, the bottom of the outer sleeve is provided with a water spraying head, the bottom of the water outlet pipe is provided with a pressing plate, the upper side of the pressing plate is provided with a sealing gasket, the sealing gasket is sleeved on the outer side of the water outlet pipe, a sliding groove is formed in the outer sleeve, and the inner diameter of the sliding groove is equal to the outer diameter of the pressing plate.
Compared with the prior art, the invention has the beneficial effects that: this tetramethyl ammonium hydroxide electrolytic device that has and prevents splashing convenient to clearance, be provided with the clearance post, the clearance post is located the top of the device electrolysis trough, can remove the cleaning post with the sprinkler bead through the inside telescopic link of clearance post, make the sprinkler bead remove to the top position of electrolysis trough, pressurization through the water pump, make rivers spray through the sprinkler bead, wash the inner wall of electrolysis trough, reach the purpose of clearing up the electrolysis trough, it washs to electrolysis trough's dismantlement to replace, the clearance degree of difficulty to the device has been reduced, cleaning efficiency has been improved, the use degree of difficulty of the device has been reduced, and the design through the feed inlet, raw materials when having reduced the device reinforced splashes, the convenience that the device used has been improved.
Drawings
FIG. 1 is a schematic view of an elevational structure of an easy-to-clean anti-spatter apparatus for electrolyzing tetramethylammonium hydroxide according to the present invention;
FIG. 2 is a schematic top view of an easy-to-clean tetramethylammonium hydroxide electrolyzer with splash protection;
FIG. 3 is a schematic diagram of a vertical cross-sectional structure of an easy-to-clean anti-spatter tetramethylammonium hydroxide electrolyzer;
FIG. 4 is a schematic cross-sectional view of an apparatus body of an easy-to-clean anti-spatter tetramethylammonium hydroxide electrolyzer;
FIG. 5 is a schematic top view of a top support plate of an easy-to-clean tetramethyl ammonium hydroxide electrolyzer with splash protection;
FIG. 6 is a schematic view of a vertical cross-sectional structure of a cleaning column of an anti-splashing tetramethylammonium hydroxide electrolysis device convenient for cleaning;
FIG. 7 is a schematic vertical sectional view of an outer sleeve of an anti-spatter tetramethylammonium hydroxide electrolyzer easy to clean.
In the figure: 1. a device main body; 2. supporting legs; 3. a feed inlet; 4. a liquid outlet; 5. a motor; 6. a water storage tank; 7. an exhaust gas tank; 8. a gas processing device; 9. an air inlet pipe; 10. a feed chute; 11. a splash-proof slot; 12. a filter screen; 13. a catheter; 14. an electrolytic cell; 15. an electrolysis electrode; 16. a stirring shaft; 17. a stirring plate; 18. supporting a top plate; 19. cleaning the column; 20. air holes are formed; 21. a water conduit; 22. a gas guide plate; 23. pressing the water pipe; 24. a lifting groove; 25. a water pump; 26. a water outlet pipe; 27. a support plate; 28. a telescopic rod; 29. a connecting plate; 30. an outer sleeve; 31. a sprinkler head; 32. pressing a plate; 33. a gasket; 34. a sliding groove.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1-7, the present invention provides a technical solution: the utility model provides a tetramethyl ammonium hydroxide electrolytic device that conveniently clears up has and prevents splashing, including device main part 1, supporting leg 2, feed inlet 3, liquid outlet 4, motor 5, storage water tank 6, exhaust gas tank 7, gaseous processing apparatus 8, intake pipe 9, feed chute 10, splashproof groove 11, filter screen 12, catheter 13, electrolysis trough 14, electrolysis electrode 15, (mixing) shaft 16, stirring board 17, supporting roof 18, clearance post 19, bleeder vent 20, aqueduct 21, air deflector 22, water pipe briquetting 23, lift groove 24, water pump 25, outlet pipe 26, backup pad 27, telescopic link 28, connecting plate 29, outer sleeve 30, sprinkler bead 31, clamp plate 32, sealed pad 33 and sliding tray 34, supporting leg 2 is installed to the bottom of device main part 1, and feed inlet 3 is installed to the upside of device main part 1, liquid outlet 4 is installed to the bottom of device main part 1, and motor 5 is installed to the top of device main part 1.
Storage water tank 6 is installed on the top right side of device main part 1, and the exhaust gas case 7 is installed on the right side of device main part 1, is connected with gas treatment device 8 on the exhaust gas case 7, is connected with intake pipe 9 on the gas treatment device 8, collects waste gas through body treatment device 8, the unified processing of being convenient for.
The feeding groove 10 is formed in the feeding hole 3, the splash-proof groove 11 is connected to the bottom of the feeding groove 10, the width of the splash-proof groove 11 is larger than that of the feeding groove 10, liquid is prevented from colliding with the splash-proof groove 11, the filter screen 12 is arranged inside the splash-proof groove 11, the right end of the splash-proof groove 11 is connected with the liquid guide pipe 13, the lower end of the liquid guide pipe 13 is communicated with the electrolytic cell 14, the electrolytic cell 14 is arranged in the device main body 1, and the electrolytic electrode 15 is arranged inside the electrolytic cell 14.
Install (mixing) shaft 16 on the motor 5, the inside of 14 is inserted to the bottom of electrolysis trough to the (mixing) shaft 16, and stirring board 17 is installed to the left and right sides of (mixing) shaft 16, and stirring board 17 highly is less than electrolysis electrode 15's height, slowly stirs electrolyte through stirring board 17, improves electrolysis efficiency, and roof 18 is installed at the top of electrolysis trough 14.
Install clearance post 19 on the supporting roof 18, clearance post 19 distributes on the supporting roof 18 has two, has seted up bleeder vent 20 on the supporting roof 18, and bleeder vent 20 is circular distribution on the supporting roof 18 and has two sets ofly, and bleeder vent 20 runs through between the top and bottom of supporting roof 18, through 21 lines of aqueduct between the clearance post 19, on the one end of aqueduct 21 was connected to storage water tank 6, is convenient for supply water for clearance post 19.
The top of roof support 18 is provided with air guide plate 22, and the bell jar has been seted up to air guide plate 22's inside, and the bell jar is linked together with intake pipe 9, is convenient for collect waste gas through air guide plate 22.
The top of clearance post 19 is installed water pipe briquetting 23, fixes aqueduct 21 through water pipe briquetting 23, and the lift groove 24 has been seted up to the inside of clearance post 19, and the bottom of lift groove 24 is linked together with the bottom surface of clearance post 19.
The water pump 25 is installed on the top end inside the lifting groove 24, the water inlet end of the water pump 25 is connected with the water guide pipe 21, the water outlet pipe 26 is connected onto the water pump 25, the supporting plate 27 is installed inside the lifting groove 24, the telescopic rod 28 is installed at the bottom of the supporting plate 27, the bottom of the telescopic rod 28 is connected with the connecting plate 29, the outer sleeve 30 is installed at the bottom of the connecting plate 29, and the outer sleeve 30 is pushed to stretch through the telescopic rod 28.
The bottom of the outer sleeve 30 is provided with a sprinkler head 31, the bottom of the water outlet pipe 26 is provided with a pressing plate 32, the upper side of the pressing plate 32 is provided with a sealing gasket 33, the sealing gasket 33 is sleeved outside the water outlet pipe 26, the inner part of the outer sleeve 30 is provided with a sliding groove 34, the inner diameter of the sliding groove 34 is equal to the outer diameter of the pressing plate 32, and the position of the sprinkler head 31 is adjusted through the outer sleeve 30, so that the sprinkler head 31 can be lowered into the electrolytic tank 14.
The working principle of the embodiment is as follows: when using this tetramethyl ammonium hydroxide electrolytic device who has of preventing splashing convenient to clearance, at first remove the device to the place that needs to use, support through supporting leg 2, can add electrolyte tetramethyl ammonium chloride to the feed chute 10 in feed inlet 3 in, make electrolyte pass feed chute 10 and get into in splash proof groove 11, prevent splashing of liquid through the size difference between splash proof groove 11 and feed chute 10, make electrolyte filter through filter screen 12 in splash proof groove 11, rethread catheter 13 with electrolyte water conservancy diversion to in electrolytic bath 14, start motor 5, make motor 5 drive (mixing) shaft 16 slow rotation, (mixing) shaft 16 drives (mixing) board 17 and rotates, stir electrolyte slowly through (mixing) board 17, electrify electrolysis electrode 15, make electrolysis electrode 15 electrolyze, the gas that the electrolysis produced passes support roof 18 through bleeder vent 20, through the gathering of gas deflector 22, make waste gas pass through intake pipe 9 and get into gas processing apparatus 8, through the preliminary treatment of gas processing apparatus 8, make the interior storage of getting into waste gas tank 7 in the chlorine, wait to accomplish the electrolysis, discharge outlet is discharged tetramethyl ammonium hydroxide main part 1 through 4.
Then, the telescopic rod 28 is started, the telescopic rod 28 pushes the connecting plate 29 to descend, the connecting plate 29 pushes the water spraying head 31 to descend through the outer sleeve 30, the water spraying head 31 gradually moves out of the lifting groove 24, meanwhile, the outer sleeve 30 moves downwards on the water outlet pipe 26, the pressing plate 32 at the bottom end of the water outlet pipe 26 gradually moves to the top end of the sliding groove 34, the sliding groove 34 is tightly attached to the top surface of the outer sleeve 30 through the sealing gasket 33, the water pump 25 is started, the water pump 25 pumps water in the water storage tank 6 through the water guide pipe 21, the water pump 25 conveys the water into the sliding groove 34 through the water outlet pipe 26, the water is conveyed into the water spraying head 31 through the sliding groove 34 and is sprayed out through the water spraying head 31 to flush the inner wall of the electrolytic bath 14, and the contents which are not described in detail in this specification belong to the prior art well known by those skilled in the art.
Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that various changes in the embodiments and/or modifications of the invention can be made, and equivalents and modifications of some features of the invention can be made without departing from the spirit and scope of the invention.

Claims (9)

1. The utility model provides a tetramethyl ammonium hydroxide electrolytic device that has and prevent splashing convenient to clearance, includes device main part (1), supporting leg (2), feed inlet (3), liquid outlet (4) and motor (5), its characterized in that: supporting legs (2) are installed to the bottom of device main part (1), and feed inlet (3) are installed to the upside of device main part (1), liquid outlet (4) are installed to the bottom of device main part (1), and motor (5) are installed at the top of device main part (1).
2. The tetramethylammonium hydroxide electrolysis apparatus with splash prevention for easy cleaning according to claim 1, wherein: a water storage tank (6) is installed on the right side of the top of the device main body (1), a waste gas tank (7) is installed on the right side of the device main body (1), a gas treatment device (8) is connected to the waste gas tank (7), and a gas inlet pipe (9) is connected to the gas treatment device (8).
3. The tetramethylammonium hydroxide electrolysis apparatus with splash prevention for easy cleaning according to claim 1, wherein: feed chute (10) have been seted up to the inside of feed inlet (3), the bottom of feed chute (10) is connected with splashproof groove (11), and the width of splashproof groove (11) is greater than the width of feed chute (10), the internally mounted of splashproof groove (11) has filter screen (12), the right-hand member of splashproof groove (11) links to each other with catheter (13), the lower extreme and electrolysis trough (14) of catheter (13) are linked together, establish in device main part (1) electrolysis trough (14), the internally mounted of electrolysis trough (14) has electrolysis electrode (15).
4. The tetramethylammonium hydroxide electrolysis apparatus with splash prevention for easy cleaning according to claim 1, wherein: install (mixing) shaft (16) on motor (5), the inside of electrolysis trough (14) is inserted to the bottom of (mixing) shaft (16), stirring board (17) are installed to the left and right sides of (mixing) shaft (16), the height that highly is less than electrolysis electrode (15) of stirring board (17), supporting roof (18) are installed at the top of electrolysis trough (14).
5. The tetramethylammonium hydroxide electrolysis apparatus with splash prevention for easy cleaning according to claim 4, wherein: install clearance post (19) on supporting roof (18), clearance post (19) have two on supporting roof (18) distribute, bleeder vent (20) have been seted up on supporting roof (18), bleeder vent (20) are circular distribution on supporting roof (18) and have two sets ofly, and bleeder vent (20) run through between the upper and lower face of supporting roof (18), through aqueduct (21) two lines between clearance post (19), the one end of aqueduct (21) is connected to on storage water tank (6).
6. The tetramethylammonium hydroxide electrolysis apparatus with splash prevention for easy cleaning according to claim 4, wherein: the top of the supporting top plate (18) is provided with an air guide plate (22), a tapered groove is formed in the air guide plate (22), and the tapered groove is communicated with the air inlet pipe (9).
7. The tetramethylammonium hydroxide electrolysis apparatus with splash prevention for easy cleaning according to claim 5, wherein: the water pipe pressure block (23) is installed at the top of the cleaning column (19), the water guide pipe (21) is fixed through the water pipe pressure block (23), the lifting groove (24) is formed in the cleaning column (19), and the bottom of the lifting groove (24) is communicated with the bottom surface of the cleaning column (19).
8. The apparatus for electrolyzing tetramethylammonium hydroxide with splash-proof capability as claimed in claim 7, wherein: water pump (25) are installed on the inside top in lift groove (24), and the end of intaking of water pump (25) links to each other with aqueduct (21), be connected with outlet pipe (26) on water pump (25), the internally mounted of lift groove (24) has backup pad (27), telescopic link (28) are installed to the bottom of backup pad (27), the bottom of telescopic link (28) links to each other with connecting plate (29), outer sleeve (30) are installed to the bottom of connecting plate (29).
9. The apparatus for electrolyzing tetramethylammonium hydroxide with splash-proof capability as claimed in claim 8, wherein: the utility model discloses a water spray pump, including outer sleeve (30), outlet pipe (26), clamp plate (32), the upside of clamp plate (32) is provided with sealed pad (33), sealed pad (33) cover is in the outside of outlet pipe (26), sliding tray (34) have been seted up to the inside of outer sleeve (30), the internal diameter of sliding tray (34) equals the external diameter of clamp plate (32).
CN202210940326.7A 2022-08-05 2022-08-05 Tetramethyl ammonium hydroxide electrolytic device convenient to clearance has and prevents splashing Withdrawn CN115216794A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202210940326.7A CN115216794A (en) 2022-08-05 2022-08-05 Tetramethyl ammonium hydroxide electrolytic device convenient to clearance has and prevents splashing

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202210940326.7A CN115216794A (en) 2022-08-05 2022-08-05 Tetramethyl ammonium hydroxide electrolytic device convenient to clearance has and prevents splashing

Publications (1)

Publication Number Publication Date
CN115216794A true CN115216794A (en) 2022-10-21

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CN202210940326.7A Withdrawn CN115216794A (en) 2022-08-05 2022-08-05 Tetramethyl ammonium hydroxide electrolytic device convenient to clearance has and prevents splashing

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Application publication date: 20221021