CN115192493A - 一种迷迭香氨基酸沐浴露及其制备方法 - Google Patents
一种迷迭香氨基酸沐浴露及其制备方法 Download PDFInfo
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- 244000178231 Rosmarinus officinalis Species 0.000 title claims description 4
- 238000002360 preparation method Methods 0.000 title abstract description 10
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- 241001529742 Rosmarinus Species 0.000 claims abstract description 49
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims abstract description 45
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 42
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims abstract description 30
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- SXHLENDCVBIJFO-UHFFFAOYSA-M sodium;2-[2-(2-dodecoxyethoxy)ethoxy]ethyl sulfate Chemical compound [Na+].CCCCCCCCCCCCOCCOCCOCCOS([O-])(=O)=O SXHLENDCVBIJFO-UHFFFAOYSA-M 0.000 claims abstract description 17
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- WNWHHMBRJJOGFJ-UHFFFAOYSA-N isooctadecyl alcohol Natural products CC(C)CCCCCCCCCCCCCCCO WNWHHMBRJJOGFJ-UHFFFAOYSA-N 0.000 claims abstract description 13
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- XUMBMVFBXHLACL-UHFFFAOYSA-N Melanin Chemical compound O=C1C(=O)C(C2=CNC3=C(C(C(=O)C4=C32)=O)C)=C2C4=CNC2=C1C XUMBMVFBXHLACL-UHFFFAOYSA-N 0.000 description 2
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Abstract
本发明属于洗护用品技术领域,具体涉及一种迷迭香氨基酸沐浴露及其制备方法,包括如下质量百分比含量的组分:水70~73%、月桂醇聚醚硫酸酯钠8~10%、椰油酰胺丙基甜菜碱4~6%、甲基椰油酰基牛磺酸钠4~7%、椰油酰胺MEA 0.5~1.5%、氯化钠4~5%、胶原氨基酸类0.3~0.5%、异硬脂醇乙酰谷氨酰胺酯0.3~0.4%、迷迭香提取物0.3~0.6%、迷迭香叶提取物0.3~0.6%、羟丙基甲基纤维素0.6~1.0%、甘油0.05~0.12%、迷迭叶油0.05~0.15%、EDTA二钠0.05~0.15%、1,2‑已二醇0.03~0.06%、辛酰羟肟酸0.05~0.15%、柠檬酸0.05~0.15%。本发明的沐浴露添加了迷迭香植萃精华和氨基酸,亲近肌肤pH值,不含防腐剂,温和无刺激,免疫力较低的儿童、老人和孕妇也可以安全使用,使用该沐浴露洗浴时泡沫感强且易冲洗,浴后肌肤清爽、滋润保湿,且能达到美白和止痒的效果,用户体验感很好。
Description
技术领域
本发明属于洗护用品技术领域,具体涉及一种迷迭香氨基酸沐浴露及其制备方法。
背景技术
沐浴露又称沐浴乳,是洗澡时使用的一种清洁用品,沐浴露通过除去过量污垢和油脂来清洁皮肤。传统沐浴露主要注重清洁力和去污力,为了提高其清洁力和去污力,往往加入碱性极强的表面活性剂、发泡剂以及皂基等成分,而人体皮肤是呈弱酸性的,长期使用这类沐浴露会对皮肤产生刺激。
随着人们生活水平的提高,人们对沐浴露的功能要求越来越多,不单单只是清洁力和去污力,沐浴时和沐浴后的体验感也成为人们关注的重点,例如,沐浴时的泡沫感,泡沫是否容易冲洗,浴后肌肤的清爽感、滋润保湿感、以及能否达到美白和止痒效果。
目前市售的沐浴露功能比较单一,不能兼具以上功能,用户体验感不太好;且市售沐浴露大多属于化学合成洗涤剂,为了实现清洁、防腐、润滑等功能会添加一些伤害皮肤的成分,长久使用会表现出难以复原的伤害,例如,为了防止沐浴露变质会加入防腐剂,如防腐剂DMDM乙内酰脲,其是通过释放甲醛来营造不适合微生物生存的环境,以达到防腐和杀菌抑菌的效果,温度越高释放的量越大,在沐浴露中用来洗澡容易引起局部的刺激性反应,当接触超过正常代谢的甲醛就会进入到血液,对身体造成伤害,尤其是免疫力较低的儿童、老人和孕妇更要拒绝这类成分。
因此,研制出一款温和、安全无刺激、洗浴时泡沫感强,易冲洗,浴后肌肤清爽、滋润保湿,且能达到美白和止痒效果的沐浴露是产品的研发方向。
发明内容
本发明的目的是为了克服现有技术的不足,而提供一种迷迭香氨基酸沐浴露及其制备方法。
本发明的目的是这样实现的:
一种迷迭香氨基酸沐浴露,包括如下质量百分比含量的组分:水70~73%、月桂醇聚醚硫酸酯钠8~10%、椰油酰胺丙基甜菜碱4~6%、甲基椰油酰基牛磺酸钠4~7%、椰油酰胺MEA 0.5~1.5%、氯化钠4~5%、胶原氨基酸类0.3~0.5%、异硬脂醇乙酰谷氨酰胺酯0.3~0.4%、迷迭香提取物0.3~0.6%、迷迭叶提取物0.3~0.6%、羟丙基甲基纤维素0.6~1.0%、甘油0.05~0.12%、迷迭香叶油0.05~0.15%、EDTA二钠0.05~0.15%、1,2-已二醇0.03~0.06%、辛酰羟肟酸0.05~0.15%、柠檬酸0.05~0.15%。
进一步地,所述迷迭香氨基酸沐浴露,包括如下质量百分比含量的组分:水71~72%、月桂醇聚醚硫酸酯钠8~9%、椰油酰胺丙基甜菜碱4~5%、甲基椰油酰基牛磺酸钠5~6%、椰油酰胺MEA 0.8~1.0%、氯化钠4~4.5%、胶原氨基酸类0.3~0.4%、异硬脂醇乙酰谷氨酰胺酯0.3~0.35%、迷迭香提取物0.4~0.5%、迷迭香叶提取物0.5~0.6%、羟丙基甲基纤维素0.7~0.9%、甘油0.08~0.12%、迷迭叶油0.08~0.12%、EDTA二钠0.08~0.12%、1,2-已二醇0.04~0.05%、辛酰羟肟酸0.10~0.12%、柠檬酸0.08~0.10%。
进一步地,所述迷迭香氨基酸沐浴露,包括如下质量百分比含量的组分:水71.5%、月桂醇聚醚硫酸酯钠9%、椰油酰胺丙基甜菜碱5%、甲基椰油酰基牛磺酸钠6%、椰油酰胺MEA 1%、氯化钠4.4%、胶原氨基酸类0.4%、异硬脂醇乙酰谷氨酰胺酯0.35%、迷迭香提取物0.5%、迷迭香叶提取物0.5%、羟丙基甲基纤维素0.8%、甘油0.1%、迷迭叶油0.1%、EDTA二钠0.1%、1,2-已二醇0.05%、辛酰羟肟酸0.1%、柠檬酸0.1%。
进一步地,所述月桂醇聚醚硫酸酯钠的质量浓度为70%。
进一步地,所述椰油酰胺丙基甜菜碱的质量浓度65%。
进一步地,所述迷迭香氨基酸沐浴露的pH值为5.5~6.5。
本发明还公开了所述迷迭香氨基酸沐浴露的制备方法,包括如下步骤:
(1)称取配方量的各组分物料,将生产设备清洁干净并消毒;
(2)将水、月桂醇聚醚硫酸酯钠、椰油酰胺丙基甜菜碱、甲基椰油酰基牛磺酸钠、椰油酰胺MEA、异硬脂醇乙酰谷氨酰胺酯、EDTA二钠加入搅拌锅内,加热至80℃搅拌3~5min使其完全溶解,搅拌20min后继续搅拌使之降温;
(3)降温至40℃以下时,再依次加入氯化钠、胶原氨基酸类、迷迭香提取物、迷迭香叶提取物、羟丙基甲基纤维素、甘油、迷迭香叶油、1,2-已二醇、辛酰羟肟酸、柠檬酸,搅拌至均匀后,继续搅拌20min;
(4)取样送检,待检验合格后出锅静置,得到迷迭香氨基酸沐浴露。
进一步地,所述步骤(2)中,搅拌速度为750~850r/min。
进一步地,所述步骤(3)中,搅拌速度均为450~550r/min。
与现有技术相比,本发明的有益效果是:
1.本发明的迷迭香氨基酸沐浴露,是氨基酸无皂基配方,洁面级清洁,亲近肌肤pH值,温和洁净无刺激,婴儿、孕产妇可以安全使用;起泡快,强效去油,易冲洗不粘腻,清爽而舒适;不添加酒精、防腐剂、激素、荧光剂、重金属和矿物油,安全无刺激。
2.本发明的迷迭香氨基酸沐浴露,成分迷迭香植萃精华具有超强抗氧化活性,能有效抑制黑色素的形成,具有极佳的美白保湿效果,迷迭香植萃精华还具有很强的抗炎活性,可以抗菌抑菌,保护和强化皮肤,促进血液循环,舒缓肌肤;成分辛酰羟肟酸具有较强的抗菌能力,是新型的防腐剂替代物质,且成分1,2-已二醇也具有抗菌的效果,比较安全,可以放心使用;成分甲基椰油酰基牛磺酸钠为氨基酸类表面活性剂,氨基酸精华搭配迷迭香植物精粹,温和洁净不伤肌肤;蕴含甘油、氨基酸、迷迭叶油等滋养保湿成分,补水清润,深层滋润肌肤。
3.本发明的迷迭香氨基酸沐浴露,添加迷迭香植萃精华和氨基酸,亲肤配方,清爽怡人,泡沫细腻,易冲洗,让肌肤体验清爽舒适,细腻呵护每寸肌肤,令肌肤自然滑嫩。
具体实施方式
下面通过具体的实施方式对本发明做更加详细的描述。
实施例1
一种迷迭香氨基酸沐浴露,包括如下质量百分比含量的组分:水70%、月桂醇聚醚硫酸酯钠9%、椰油酰胺丙基甜菜碱5.5%、甲基椰油酰基牛磺酸钠7%、椰油酰胺MEA 1%、氯化钠4.5%、胶原氨基酸类0.3%、异硬脂醇乙酰谷氨酰胺酯0.4%、迷迭香提取物0.6%、迷迭香叶提取物0.5%、羟丙基甲基纤维素0.7%、甘油0.08%、迷迭叶油0.08%、EDTA二钠0.12%、1,2-已二醇0.05%、辛酰羟肟酸0.12%、柠檬酸0.05%。
实施例2
一种迷迭香氨基酸沐浴露,包括如下质量百分比含量的组分:水71%、月桂醇聚醚硫酸酯钠8%、椰油酰胺丙基甜菜碱6%、甲基椰油酰基牛磺酸钠5%、椰油酰胺MEA 1.5%、氯化钠5%、胶原氨基酸类0.5%、异硬脂醇乙酰谷氨酰胺酯0.35%、迷迭香提取物0.5%、迷迭香叶提取物0.6%、羟丙基甲基纤维素1%、甘油0.05%、迷迭叶油0.12%、EDTA二钠0.08%、1,2-已二醇0.06%、辛酰羟肟酸0.15%、柠檬酸0.09%。
实施例3
一种迷迭香氨基酸沐浴露,包括如下质量百分比含量的组分:水71.5%、月桂醇聚醚硫酸酯钠9%、椰油酰胺丙基甜菜碱5%、甲基椰油酰基牛磺酸钠6%、椰油酰胺MEA 1%、氯化钠4.4%、胶原氨基酸类0.4%、异硬脂醇乙酰谷氨酰胺酯0.35%、迷迭香提取物0.5%、迷迭香叶提取物0.5%、羟丙基甲基纤维素0.8%、甘油0.1%、迷迭叶油0.1%、EDTA二钠0.1%、1,2-已二醇0.05%、辛酰羟肟酸0.1%、柠檬酸0.1%。
实施例4
一种迷迭香氨基酸沐浴露,包括如下质量百分比含量的组分:水72%、月桂醇聚醚硫酸酯钠10%、椰油酰胺丙基甜菜碱4%、甲基椰油酰基牛磺酸钠7%、椰油酰胺MEA 0.5%、氯化钠4%、胶原氨基酸类0.32%、异硬脂醇乙酰谷氨酰胺酯0.3%、迷迭香提取物0.3%、迷迭香叶提取物0.6%、羟丙基甲基纤维素0.6%、甘油0.12%、迷迭叶油0.05%、EDTA二钠0.05%、1,2-已二醇0.03%、辛酰羟肟酸0.05%、柠檬酸0.08%。
实施例5
一种迷迭香氨基酸沐浴露,包括如下质量百分比含量的组分:水73%、月桂醇聚醚硫酸酯钠8%、椰油酰胺丙基甜菜碱6%、甲基椰油酰基牛磺酸钠4%、椰油酰胺MEA 0.8%、氯化钠5%、胶原氨基酸类0.5%、异硬脂醇乙酰谷氨酰胺酯0.4%、迷迭香提取物0.4%、迷迭香叶提取物0.3%、羟丙基甲基纤维素0.9%、甘油0.1%、迷迭叶油0.15%、EDTA二钠0.15%、1,2-已二醇0.04%、辛酰羟肟酸0.11%、柠檬酸0.15%。
实施例1~5所述迷迭香氨基酸沐浴露的制备方法,包括如下步骤:
(1)称取配方量的各组分物料,将生产设备清洁干净并消毒;
(2)将水、月桂醇聚醚硫酸酯钠、椰油酰胺丙基甜菜碱、甲基椰油酰基牛磺酸钠、椰油酰胺MEA、异硬脂醇乙酰谷氨酰胺酯、EDTA二钠加入搅拌锅内,加热至80℃搅拌5min使其完全溶解,在800r/min的搅拌速度下搅拌20min后继续搅拌使之降温;
(3)降温至40℃以下时,再依次加入氯化钠、胶原氨基酸类、迷迭香提取物、迷迭香叶提取物、羟丙基甲基纤维素、甘油、迷迭香叶油、1,2-已二醇、辛酰羟肟酸、柠檬酸,搅拌至均匀后,在500r/min的搅拌速度下继续搅拌20min;
(4)取样送检,待检验合格后出锅静置,得到迷迭香氨基酸沐浴露。
对比例1
对比例1的沐浴露所含组分以及制备方法参照实施例1,不同点在于不添加迷迭香提取物、迷迭香叶提取物、迷迭香叶油,水的质量百分比含量为71.18%。
对比例2
对比例2的沐浴露所含组分以及制备方法参照实施例2,不同点在于不添加甲基椰油酰基牛磺酸钠,水的质量百分比含量为76%。
对比例3
对比例3的沐浴露所含组分以及制备方法参照实施例3,不同点在于不添加胶原氨基酸类,水的质量百分比含量为71.9%。
刺激性测试
选出50名受试志愿者,随机分为5组,每组10人,进行产品刺激性测试,在每位测试者的手背中部以及手臂前部分别圈出一块3cm×3cm的测试区域、在小腿下部圈出一块5cm×5cm的测试区域,在第一组受试志愿者的测试区域涂抹实施例1制得的迷迭香氨基酸沐浴露,在第二组受试志愿者的测试区域涂抹实施例2制得的迷迭香氨基酸沐浴露,在第三组受试志愿者的测试区域涂抹实施例3制得的迷迭香氨基酸沐浴露,在第四组受试志愿者的测试区域涂抹实施例4制得的迷迭香氨基酸沐浴露,在第五组受试志愿者的测试区域涂抹实施例5制得的迷迭香氨基酸沐浴露;涂抹后观察1小时,每组受试志愿者均未出现红肿、瘙痒和疼痛等不良反应,表明本发明实施例1~5制备的迷迭香氨基酸沐浴露对皮肤无刺激,可以放心使用。
使用效果测试
为进一步检验本发明所提供的迷迭香氨基酸沐浴露的实际效果,发明人做了进一步的对比试验。
试验样品:本发明实施例1~5制得的迷迭香氨基酸沐浴露,以及本发明对比例1~3制得的沐浴露。
试验测试指标:沐浴露的泡沫感、易冲洗程度,以及浴后肌肤的滋润程度、保湿程度、美白效果和止痒效果。
试验人群:选出160名受试志愿者,其中,男性80人,女性80人;随机分为8组,每组20人。
试验方法:第一至第五组试验人群分别使用实施例1~5制得的迷迭香氨基酸沐浴露;第五至第八组试验人群分别使用对比例1~3制得的沐浴露;每天晚上使用一次,连续使用两周,对使用效果进行打分,评分标准采用5分制,5分表示非常好,1分表示非常差,统计使用效果,取平均值。
测试结果如下表所示:
由上表数据可知,使用本发明含有迷迭香提取物、迷迭香叶提取物、迷迭香叶油、甲基椰油酰基牛磺酸钠和胶原氨基酸类的实施例1~5的迷迭香氨基酸沐浴露,洗浴时泡沫感强且易冲洗,浴后肌肤的滋润程度、保湿程度、美白效果和止痒效果很好。
而使用不含迷迭香提取物、迷迭香叶提取物和迷迭香叶油的对比例1的沐浴露,洗浴时泡沫感强且易冲洗,但浴后肌肤的滋润程度和保湿程度均不如实施例1~5,美白效果和止痒效果较差;使用不含甲基椰油酰基牛磺酸钠的对比例2的沐浴露,洗浴时泡沫感不强且不易冲洗,浴后肌肤的滋润程度、保湿程度、美白效果和止痒效果均不如实施例1~5;使用不含胶原氨基酸类的对比例3的沐浴露,洗浴时泡沫感不强且不易冲洗,浴后肌肤的滋润程度、保湿程度、美白效果和止痒效果均不如实施例1~5。
以上实施例仅仅是对本发明的解释,其并不是对本发明的限制,对于本领域一般技术人员而言,在不背离本发明原理和精神的前提下对其所作出的任何显而易见的改动,都应当被认为包含在本发明的权利要求保护范围之内。
Claims (9)
1.一种迷迭香氨基酸沐浴露,其特征在于,包括如下质量百分比含量的组分:水70~73%、月桂醇聚醚硫酸酯钠8~10%、椰油酰胺丙基甜菜碱4~6%、甲基椰油酰基牛磺酸钠4~7%、椰油酰胺MEA 0.5~1.5%、氯化钠4~5%、胶原氨基酸类0.3~0.5%、异硬脂醇乙酰谷氨酰胺酯0.3~0.4%、迷迭香提取物0.3~0.6%、迷迭叶提取物0.3~0.6%、羟丙基甲基纤维素0.6~1.0%、甘油0.05~0.12%、迷迭香叶油0.05~0.15%、EDTA二钠0.05~0.15%、1,2-已二醇0.03~0.06%、辛酰羟肟酸0.05~0.15%、柠檬酸0.05~0.15%。
2.如权利要求1所述的迷迭香氨基酸沐浴露,其特征在于,包括如下质量百分比含量的组分:水71~72%、月桂醇聚醚硫酸酯钠8~9%、椰油酰胺丙基甜菜碱4~5%、甲基椰油酰基牛磺酸钠5~6%、椰油酰胺MEA 0.8~1.0%、氯化钠4~4.5%、胶原氨基酸类0.3~0.4%、异硬脂醇乙酰谷氨酰胺酯0.3~0.35%、迷迭香提取物0.4~0.5%、迷迭香叶提取物0.5~0.6%、羟丙基甲基纤维素0.7~0.9%、甘油0.08~0.12%、迷迭叶油0.08~0.12%、EDTA二钠0.08~0.12%、1,2-已二醇0.04~0.05%、辛酰羟肟酸0.10~0.12%、柠檬酸0.08~0.10%。
3.如权利要求2所述的迷迭香氨基酸沐浴露,其特征在于,包括如下质量百分比含量的组分:水71.5%、月桂醇聚醚硫酸酯钠9%、椰油酰胺丙基甜菜碱5%、甲基椰油酰基牛磺酸钠6%、椰油酰胺MEA 1%、氯化钠4.4%、胶原氨基酸类0.4%、异硬脂醇乙酰谷氨酰胺酯0.35%、迷迭香提取物0.5%、迷迭香叶提取物0.5%、羟丙基甲基纤维素0.8%、甘油0.1%、迷迭叶油0.1%、EDTA二钠0.1%、1,2-已二醇0.05%、辛酰羟肟酸0.1%、柠檬酸0.1%。
4.如权利要求1~3任一项所述的迷迭香氨基酸沐浴露,其特征在于,所述月桂醇聚醚硫酸酯钠的质量浓度为70%。
5.如权利要求1~3任一项所述的迷迭香氨基酸沐浴露,其特征在于,所述椰油酰胺丙基甜菜碱的质量浓度65%。
6.如权利要求1~3任一项所述的迷迭香氨基酸沐浴露,其特征在于,所述迷迭香氨基酸沐浴露的pH值为5.5~6.5。
7.一种制备权利要求1~3任一项所述迷迭香氨基酸沐浴露的方法,其特征在于,包括如下步骤:
(1)称取配方量的各组分物料,将生产设备清洁干净并消毒;
(2)将水、月桂醇聚醚硫酸酯钠、椰油酰胺丙基甜菜碱、甲基椰油酰基牛磺酸钠、椰油酰胺MEA、异硬脂醇乙酰谷氨酰胺酯、EDTA二钠加入搅拌锅内,加热至80℃搅拌3~5min使其完全溶解,搅拌20min后继续搅拌使之降温;
(3)降温至40℃以下时,再依次加入氯化钠、胶原氨基酸类、迷迭香提取物、迷迭香叶提取物、羟丙基甲基纤维素、甘油、迷迭香叶油、1,2-已二醇、辛酰羟肟酸、柠檬酸,搅拌至均匀后,继续搅拌20min;
(4)取样送检,待检验合格后出锅静置,得到迷迭香氨基酸沐浴露。
8.如权利要求7所述迷迭香氨基酸沐浴露的制备方法,其特征在于,所述步骤(2)中,搅拌速度为750~850r/min。
9.如权利要求7所述迷迭香氨基酸沐浴露的制备方法,其特征在于,所述步骤(3)中,搅拌速度均为450~550r/min。
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CN115836981A (zh) * | 2022-12-09 | 2023-03-24 | 福建省梦娇兰日用化学品有限公司 | 一种升级型儿童沐浴露及其制备方法 |
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