CN115138424B - High-purity lycium ruthenicum anthocyanin purification device and purification method thereof - Google Patents
High-purity lycium ruthenicum anthocyanin purification device and purification method thereof Download PDFInfo
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- CN115138424B CN115138424B CN202210771946.2A CN202210771946A CN115138424B CN 115138424 B CN115138424 B CN 115138424B CN 202210771946 A CN202210771946 A CN 202210771946A CN 115138424 B CN115138424 B CN 115138424B
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- 238000000746 purification Methods 0.000 title claims abstract description 33
- 229930002877 anthocyanin Natural products 0.000 title claims abstract description 29
- 235000010208 anthocyanin Nutrition 0.000 title claims abstract description 29
- 239000004410 anthocyanin Substances 0.000 title claims abstract description 29
- 150000004636 anthocyanins Chemical class 0.000 title claims abstract description 29
- 238000000034 method Methods 0.000 title claims abstract description 16
- 241000169546 Lycium ruthenicum Species 0.000 title claims description 26
- 244000241838 Lycium barbarum Species 0.000 claims abstract description 14
- 235000015459 Lycium barbarum Nutrition 0.000 claims abstract description 14
- 238000005192 partition Methods 0.000 claims abstract description 14
- 230000005540 biological transmission Effects 0.000 claims abstract description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 14
- 238000002156 mixing Methods 0.000 claims description 14
- 238000007789 sealing Methods 0.000 claims description 13
- 238000000926 separation method Methods 0.000 claims description 9
- 238000001914 filtration Methods 0.000 claims description 5
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000002386 leaching Methods 0.000 claims description 4
- 239000002184 metal Substances 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 2
- 230000001681 protective effect Effects 0.000 claims description 2
- 238000005096 rolling process Methods 0.000 claims description 2
- 238000009434 installation Methods 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 4
- 238000000605 extraction Methods 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000011403 purification operation Methods 0.000 description 3
- 206010003210 Arteriosclerosis Diseases 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- 229940123457 Free radical scavenger Drugs 0.000 description 1
- 235000015468 Lycium chinense Nutrition 0.000 description 1
- 230000032683 aging Effects 0.000 description 1
- 208000011775 arteriosclerosis disease Diseases 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 210000004204 blood vessel Anatomy 0.000 description 1
- 208000026106 cerebrovascular disease Diseases 0.000 description 1
- 230000002526 effect on cardiovascular system Effects 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 239000002516 radical scavenger Substances 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C1/00—Crushing or disintegrating by reciprocating members
- B02C1/14—Stamping mills
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D35/00—Filtering devices having features not specifically covered by groups B01D24/00 - B01D33/00, or for applications not specifically covered by groups B01D24/00 - B01D33/00; Auxiliary devices for filtration; Filter housing constructions
- B01D35/16—Cleaning-out devices, e.g. for removing the cake from the filter casing or for evacuating the last remnants of liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
- B01D36/04—Combinations of filters with settling tanks
- B01D36/045—Combination of filters with centrifugal separation devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F33/00—Other mixers; Mixing plants; Combinations of mixers
- B01F33/80—Mixing plants; Combinations of mixers
- B01F33/836—Mixing plants; Combinations of mixers combining mixing with other treatments
- B01F33/8361—Mixing plants; Combinations of mixers combining mixing with other treatments with disintegrating
- B01F33/83612—Mixing plants; Combinations of mixers combining mixing with other treatments with disintegrating by crushing or breaking
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C23/00—Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C23/00—Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
- B02C23/08—Separating or sorting of material, associated with crushing or disintegrating
- B02C23/10—Separating or sorting of material, associated with crushing or disintegrating with separator arranged in discharge path of crushing or disintegrating zone
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C23/00—Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
- B02C23/18—Adding fluid, other than for crushing or disintegrating by fluid energy
- B02C23/36—Adding fluid, other than for crushing or disintegrating by fluid energy the crushing or disintegrating zone being submerged in liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B1/00—Centrifuges with rotary bowls provided with solid jackets for separating predominantly liquid mixtures with or without solid particles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B7/00—Elements of centrifuges
- B04B7/08—Rotary bowls
- B04B7/18—Rotary bowls formed or coated with sieving or filtering elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B04—CENTRIFUGAL APPARATUS OR MACHINES FOR CARRYING-OUT PHYSICAL OR CHEMICAL PROCESSES
- B04B—CENTRIFUGES
- B04B9/00—Drives specially designed for centrifuges; Arrangement or disposition of transmission gearing; Suspending or balancing rotary bowls
- B04B9/02—Electric motor drives
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D311/00—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings
- C07D311/02—Heterocyclic compounds containing six-membered rings having one oxygen atom as the only hetero atom, condensed with other rings ortho- or peri-condensed with carbocyclic rings or ring systems
- C07D311/04—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring
- C07D311/58—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4
- C07D311/60—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with aryl radicals attached in position 2
- C07D311/62—Benzo[b]pyrans, not hydrogenated in the carbocyclic ring other than with oxygen or sulphur atoms in position 2 or 4 with aryl radicals attached in position 2 with oxygen atoms directly attached in position 3, e.g. anthocyanidins
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Mechanical Engineering (AREA)
- Disintegrating Or Milling (AREA)
- Apparatuses For Bulk Treatment Of Fruits And Vegetables And Apparatuses For Preparing Feeds (AREA)
Abstract
A high-purity black matrimony vine anthocyanin purification device and a purification method thereof relate to an anthocyanin purification device and a method. The first support rotates the gear wheel and the pinion of installation meshing, the coaxial fixed axostylus axostyle of gear wheel rotates with the second support to be connected, and two fixed direction crossbars in edge, barrel cartridge is on the axostylus axostyle, two link and direction crossbars cartridge are fixed to the barrel, annular slab upper end is articulated with the second support, the lower extreme has adjusting bolt to contradict, the mouth of pipe of barrel is sealed to have the cock stem and is contradicted on annular slab, the pressure spring supports between gear wheel and barrel, there is the partition plectane in the middle of the axostylus axostyle and sets up a plurality of broken holes, the barrel lateral wall has rectangular filter screen and fixed closure apron, collect the cover and establish the barrel, the base is equipped with the chute, drive motor can carry out the transmission between gear wheel and pinion and switch. The transmission of driving motor switches and cooperates the inclination adjustment of annular plate, realizes that the barrel smashes, mixes, separates three mode, and is simple high-efficient.
Description
Technical Field
The invention relates to an anthocyanin purifying device and method, in particular to a high-purity lycium ruthenicum anthocyanin purifying device and method, and belongs to the technical field of anthocyanin extraction and processing.
Background
The anthocyanin content in the lycium ruthenicum is very high, which is several times that of common food, has the reputation of anthocyanin king, is the strongest free radical scavenger discovered so far, is widely used for preventing and treating cardiovascular and cerebrovascular diseases, can inhibit free radicals in blood vessels, and has the functions of resisting aging, resisting oxidation and preventing arteriosclerosis.
Traditional lycium ruthenicum anthocyanin purification operation needs to be respectively subjected to operations of grinding and crushing, organic solution extraction, separation and filtration, raw materials are transferred among different devices for multiple times, simplification of production is not facilitated, operation is time-consuming and labor-consuming, and extraction efficiency and purity are low. Therefore, there is a need for a simple and efficient purification device and method for lycium ruthenicum anthocyanin to solve the above problems.
Disclosure of Invention
The invention aims to provide a high-purity lycium ruthenicum anthocyanin purification device and a purification method thereof, which can realize three working modes of crushing, uniformly mixing and separating a barrel body through the transmission switching of a driving motor and the inclination adjustment of an annular plate, and simply and efficiently finish anthocyanin purification operation of lycium ruthenicum.
In order to achieve the above purpose, the invention adopts the following technical scheme:
the utility model provides a high purity black matrimony vine anthocyanin purification device, including base, gear wheel, pinion, barrel, annular slab, collection cover and driving motor, the interval is fixed with first support and second support on the base, first support top inboard rotation installs intermeshing's gear wheel and pinion, gear wheel inboard coaxial fixation has the axostylus axostyle, the axostylus axostyle tip with second support rotates to be connected, gear wheel inboard edge symmetry is fixed with two guide rail, the barrel runs through two centre bore along the axial and cartridge on the axostylus axostyle, two centre bore and axostylus axostyle correspond the position and are equipped with the sealing washer respectively, the barrel is equipped with two linking bridge adjacent to the one end edge symmetry of gear wheel, two linking bridge are equipped with the guiding hole and respectively with two guide rail cartridge is assembled and is closed, the annular slab is close to the annular slab contact, the annular slab is close to the filter screen is equipped with in the annular slab, the annular slab is close to the side wall of barrel is equipped with in the annular slab, the annular slab is equipped with the sealing washer, the annular slab is close to the filter screen is equipped with on the side wall along the barrel, the side wall is equipped with the side wall of the axial is close to the filter screen along the axial extension, the filter screen is equipped with the filter screen on the side wall of the base is close to the side wall along the side of the side wall of the barrel, the filter screen is close to the side of the filter screen is fixed to the side of the filter, the driving motor is arranged on the base and can be used for carrying out transmission switching between the large gear and the small gear.
A purification method of a high-purity lycium ruthenicum anthocyanin purification device comprises the following steps of:
step one: mixing the black matrimony vine with water, injecting into the cylinder through the pipe orifice, tightening the plug rod and ensuring good contact with the annular plate;
step two: starting a crushing mode, tightening an adjusting bolt to enable the lower end of the annular plate to lift and incline, driving a pinion to drive a large gear to rotate by a driving motor, enabling a cylinder body to reciprocate along a shaft rod while rotating along with the large gear under the action of a pressure spring, the annular plate and two guide cross bars, enabling lycium ruthenicum to repeatedly pass through a partition circular plate under pressure and finishing crushing under the action of crushing holes;
step three: opening a mixing mode, unscrewing an adjusting bolt to enable the annular plate to be vertical, injecting ethanol solution into the cylinder through the pipe orifice, controlling the pinion to drive the large gear to rotate by the driving motor, enabling the cylinder to rotate along with the large gear only at a low speed, and mixing the internal solution uniformly to finish ethanol leaching;
step four: the separation mode is started, the annular plate is still vertical, the sealing cover plate is detached to expose the long-strip filter screen, the driving motor controls the large gear to rotate, the cylinder body only rotates fast along with the large gear, the filtering separation is carried out through the long-strip filter screen under the centrifugal action, filtered solution is sprayed on the inner wall of the collecting cover and then flows to the bottom along the wall down to flow out through the chute, and the broken residues of the lycium ruthenicum are left in the cylinder body.
Compared with the prior art, the invention has the beneficial effects that: according to the invention, the driving motor is used for carrying out transmission switching between the large gear and the small gear, so that two rotation speeds of the cylinder body can be realized, namely the rotation speed and the same speed can be realized, the inclination adjustment of the annular plate is matched during the speed reduction rotation, the crushing mode that the cylinder body rotates and simultaneously reciprocates along the shaft rod can be realized, and the mixing mode that the cylinder body only rotates can be realized, the cylinder body moves and extrudes the black matrimony vine to repeatedly pass through the crushing Kong Wancheng of the partition circular plate for crushing in the crushing mode, the crushed black matrimony vine and the added ethanol are uniformly mixed in the mixing mode to finish leaching, and the closed cover plate on the cylinder body is removed during the rotation at the same speed to expose the strip filter screen for filtering separation under the centrifugal effect.
Drawings
FIG. 1 is an isometric view of a comminution mode of a high purity lycium ruthenicum anthocyanin purification device of the present invention;
FIG. 2 is an isometric view of a blending pattern of the high purity lycium ruthenicum anthocyanin purification device of the present invention;
FIG. 3 is an isometric view of a separation mode of the high purity lycium ruthenicum anthocyanin purification device of the present invention;
FIG. 4 is an isometric view of a drive motor and base assembly of the present invention;
FIG. 5 is an isometric view of the closure cap and stopper rod of the present invention in a disassembled configuration with the barrel;
fig. 6 is an isometric view of a collection cover of the present invention.
Detailed Description
The technical solutions of the present invention will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present invention, and it is apparent that the described embodiments are only some embodiments of the invention, but not all embodiments, and all other embodiments obtained by those skilled in the art without making creative efforts based on the embodiments of the present invention are all within the protection scope of the present invention.
As shown in fig. 1 to 6, a high purity lycium ruthenicum anthocyanin purification device comprises a base 1, a large gear 2, a small gear 3, a cylinder 5, an annular plate 6, a collection cover 8 and a driving motor 10.
Referring to fig. 1-3, a first bracket 1-1 and a second bracket 1-2 are fixed on a base 1 at intervals, a large gear 2 and a small gear 3 which are meshed with each other are rotatably mounted on the inner side of the top of the first bracket 1-1, a shaft lever 2-1 is coaxially fixed on the inner side of the large gear 2, the end part of the shaft lever 2-1 is rotatably connected with the second bracket 1-2, and two guide cross bars 2-2 are symmetrically fixed on the inner side edge of the large gear 2.
Referring to fig. 1 and 5, the cylinder 5 axially penetrates through two central holes 5-1 and is inserted into the shaft lever 2-1, sealing rings are respectively arranged at positions corresponding to the two central holes 5-1 and the shaft lever 2-1, two connecting frames 5-2 are symmetrically fixed at edges of one end, adjacent to the large gear 2, of the cylinder 5, and the two connecting frames 5-2 are provided with guide holes and are respectively inserted into the two guide cross bars 2-2.
Referring to fig. 1 and 4, the annular plate 6 is attached to the inner side of the second bracket 1-2 and sleeved on the shaft lever 2-1, the upper end of the annular plate 6 is hinged to the second bracket 1-2, and the second bracket 1-2 is screwed with the adjusting bolt 1-6 and abuts against the lower end of the annular plate 6.
As shown in fig. 1 and 5, one end edge of the cylinder 5 adjacent to the second bracket 1-2 is penetrated with a pipe orifice 5-3, the pipe orifice 5-3 is in threaded connection and packaged with a plug rod 5-4 and is abutted against the annular plate 6, further, a rolling ball 5-5 is arranged at the outer end of the plug rod 5-4, friction with the annular plate 6 can be reduced to enable the cylinder 5 to rotate more smoothly, a pressure spring 9 is sleeved on the shaft lever 2-1 and supported between the large gear 2 and the cylinder 5, the pressure spring 9 adopts a high-strength spring and can also be replaced by other supporting members with stronger elasticity, for example, two cylinders are symmetrically fixed at the dislocation position of the inner edge of the large gear 2 and the guide cross rod 2-2 to support the cylinder 5, kinetic energy for moving the cylinder 5 to the annular plate 6 is provided for the cylinder 5 through the cylinders, the middle position of the shaft lever 2-1 is coaxially fixed with a partition circular plate 7, the edge of the partition circular plate 7 is provided with a sealing ring which is closely attached to the inner wall of the barrel 5, the surface of the partition circular plate 7 is provided with a plurality of crushing holes, further, the partition circular plate 7 is positioned in each crushing hole and is radially fixed with a metal wire, crushing Kong Shiyou is effectively promoted when the black matrimony vine passes through crushing Kong Shiyou, the side wall of the barrel 5 is axially provided with a strip filter screen 5-6, the outside of the strip filter screen 5-6 is tightly fixed with a sealing cover plate 5-7 through screws, the diameter of the filtering hole of the strip filter screen 5-6 is smaller than the diameter of the crushing hole of the partition circular plate 7 is smaller than the diameter of the black matrimony vine, and further, the inner side surface of the sealing cover plate 5-7 is adhered with a leakage-proof rubber mat, so that the sealing effect can be effectively ensured and liquid seepage can be avoided.
Referring to fig. 1 and 6, the collecting cover 8 is fixed on the base 1, the cross section of the collecting cover is omega-shaped, and covers the cylinder 5, further, the inner sides of two ends of the collecting cover 8 are respectively fixed with a protective edge 8-1 along the edges of the collecting cover, so that liquid is prevented from splashing out from the space between the two ends of the collecting cover 8 and the cylinder 5 in the rotating separation process, a chute 1-3 extending outwards from the bottom of the collecting cover 8 is arranged on the surface of the base 1 along the direction of the shaft rod 2-1, and the driving motor 10 is arranged on the base 1 and can drive and switch between the large gear 2 and the small gear 3.
Referring to fig. 1 to 4, a specific preferred structure is that a transfer disc 4 is coaxially fixed on the outer sides of a large gear 2 and a pinion 3 respectively, a platform 1-4 is arranged on a base 1 and used for installing a driving motor 10, a U-shaped chute 1-5 is arranged on the surface of the platform 1-4, the driving motor 10 is fixed on a sliding seat 10-1 and is in sliding connection with the U-shaped chute 1-5, a limiting pin 10-2 is radially fixed on the outer end of an output shaft of the driving motor 10, clamping grooves corresponding to the limiting pins 10-2 are respectively arranged on the outer surfaces of the two transfer discs 4, and the limiting pins 10-2 can be respectively in insertion fit with the clamping grooves corresponding to the transfer discs 4 when the driving motor 10 slides to the positions on two sides of the U-shaped chute 1-5, so that transmission switching of the driving motor 10 between the large gear 2 and the pinion 3 is realized.
Further, two support arms are arranged behind two sides of the U-shaped sliding groove 1-5 on the surface of the platform 1-4 and are respectively screwed with the support bolts 1-7, when the driving motor 10 slides to the two sides of the U-shaped sliding groove 1-5, the driving motor 10 can be positioned by tightening the corresponding support bolts 1-7, and transmission failure caused by the fact that the limiting pin 10-2 is separated from the adapter plate 4 due to the sliding of the driving motor 10 is avoided.
A purification method of a high-purity lycium ruthenicum anthocyanin purification device comprises the following steps of:
step one: mixing the black matrimony vine with water and injecting the mixture into the cylinder 5 through the pipe orifice 5-3, tightening the plug rod 5-4 and ensuring good contact with the annular plate 6, wherein the total volume of the mixed black matrimony vine and water is as large as possible, preferably more than 2/3 of the volume of the cylinder 5, so as to avoid the phenomenon that the liquid level at one side rises and loses the effect of penetrating through the partition circular plate 7 in the reciprocating movement process of the cylinder 5;
step two: starting a crushing mode, screwing up the adjusting bolt 1-6 to enable the lower end of the annular plate 6 to be lifted and inclined, wherein the inclination angle is preferably 30-45 degrees, the driving motor 10 controls the pinion 3 to drive the large gear 2 to rotate, the cylinder 5 moves back and forth along the shaft rod 2-1 while rotating along with the large gear 2 under the action of the pressure spring 9, the annular plate 6 and the two guide cross rods 2-2, and the black matrimony vine repeatedly passes through the partition circular plate 7 under pressure and is crushed under the action of crushing holes, and the metal wires fixed in the crushing holes can effectively improve the crushing effect;
step three: opening a mixing mode, unscrewing the adjusting bolts 1-6 to enable the annular plate 6 to restore to be vertical, injecting ethanol solution into the cylinder 5 through the pipe orifice 5-3, controlling the pinion 3 to drive the large gear 2 to rotate by the driving motor 10, enabling the cylinder 5 to only rotate slowly along with the large gear 2 (the pinion 3 drives the reduction ratio of the large gear 2 to rotate), and uniformly mixing the internal solution to finish ethanol leaching;
step four: the separation mode is started, the annular plate 6 is still vertical, the sealing cover plate 5-7 is detached to expose the strip filter screen 5-6, the driving motor 10 controls the large gear 2 to rotate, the cylinder 5 only rotates rapidly along with the large gear 2 (the driving motor 10 directly drives the large gear 2 to rotate at the same speed ratio, the small gear 3 idles), the filtered solution is separated through the strip filter screen 5-6 under the centrifugal action, the filtered solution is sprayed on the inner wall of the collecting cover 8, flows downwards along the wall to flow out of the bottom through the chute 1-3, and the broken black wolfberry leaves in the cylinder 5.
According to the purification device, three working modes of crushing, uniformly mixing and separating of the barrel 5 can be realized through matching of the independent driving motor 10 with the inclination adjustment of the annular plate 6, three functions are integrated, the structure is simple, the anthocyanin purification operation of the lycium ruthenicum is convenient to finish efficiently, the driving motor 10 can be powered by an external power supply, a power supply can be configured below the platform 1-4 of the base 1, the driving motor 10 can be controlled to be turned on or off through the configuration of a switch, and the bottom of the base 1 can be provided with rollers to promote the overall movement flexibility.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential characteristics thereof. The present embodiments are, therefore, to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Furthermore, it should be understood that although the present disclosure describes embodiments, not every embodiment is provided with a separate embodiment, and that this description is provided for clarity only, and that the disclosure is not limited to the embodiments described in detail below, and that the embodiments described in the examples may be combined as appropriate to form other embodiments that will be apparent to those skilled in the art.
Claims (10)
1. A high-purity black matrimony vine anthocyanin purification device, its characterized in that: the device comprises a base (1), a large gear (2), a pinion (3), a cylinder (5), an annular plate (6), a collecting cover (8) and a driving motor (10), wherein a first bracket (1-1) and a second bracket (1-2) are fixed on the base (1) at intervals, the inner side of the top of the first bracket (1-1) is rotatably provided with the large gear (2) and the pinion (3) which are meshed with each other, the inner side of the large gear (2) is coaxially fixed with a shaft lever (2-1), the end part of the shaft lever (2-1) is rotationally connected with the second bracket (1-2), the inner side edge of the large gear (2) is symmetrically fixed with two guide cross bars (2-2), the cylinder (5) axially penetrates through two center holes (5-1) and is inserted on the shaft lever (2-1), sealing rings are respectively arranged at corresponding positions of the two center holes (5-1) and the shaft lever (2-1), two connecting frames (5-2) are symmetrically fixed at one end edge of the cylinder (5) adjacent to the large gear (2), the two connecting frames (5-2) are respectively provided with two guide cross bars, the annular plate (6) is attached to the inner side of the second bracket (1-2) and sleeved on the shaft lever (2-1), the upper end of the annular plate (6) is hinged with the second bracket (1-2), the second bracket (1-2) is rotatably connected with an adjusting bolt (1-6) and is abutted against the lower end of the annular plate (6), a pipe orifice (5-3) is penetrated through the edge of one end of the cylinder (5) adjacent to the second bracket (1-2), the pipe orifice (5-3) is spirally connected with a plug rod (5-4) and is abutted against the annular plate (6), the shaft lever (2-1) is sleeved with a pressure spring (9) and supported between the large gear (2) and the cylinder (5), a partition circular plate (7) is coaxially fixed in the middle position of the shaft lever (2-1), the edge of the partition circular plate (7) is provided with a sealing ring which is tightly attached to the inner wall of the cylinder (5), the partition circular plate (7) is provided with a plurality of crushing holes, the side wall of the cylinder (5) is axially provided with a strip filter screen (5-6), the strip filter screen (5-6) is externally fixed on the cylinder (1) through a screw cover (5-8), the strip filter screen (5-6) is tightly fixed on the base (1), the surface of the base (1) is provided with a chute (1-3) extending outwards from the bottom of the collecting cover (8) along the direction of the shaft lever (2-1), and the driving motor (10) is arranged on the base (1) and can carry out transmission switching between the large gear (2) and the small gear (3).
2. The high purity lycium ruthenicum anthocyanin purification device of claim 1, wherein the device comprises: the novel power transmission device is characterized in that a switching disc (4) is coaxially fixed to the outer side of the large gear (2) and the outer side of the small gear (3) respectively, a platform (1-4) is arranged on the base (1) and used for installing a driving motor (10), a U-shaped sliding groove (1-5) is formed in the surface of the platform (1-4), the driving motor (10) is fixed to the sliding seat (10-1) and is in sliding connection with the U-shaped sliding groove (1-5), a limiting pin (10-2) is radially fixed to the outer end of an output shaft of the driving motor (10), clamping grooves corresponding to the limiting pins (10-2) are formed in the outer surfaces of the two switching discs (4) respectively, and the limiting pins (10-2) can be respectively in plug-in fit with the clamping grooves corresponding to the switching discs (4) when the driving motor (10) slides to the two sides of the U-shaped sliding groove (1-5).
3. The high purity lycium ruthenicum anthocyanin purification device of claim 2, wherein the device comprises: two support arms are arranged behind two sides of the U-shaped sliding groove (1-5) on the surface of the platform (1-4) and are respectively screwed with support bolts (1-7), and when the driving motor (10) slides to the two sides of the U-shaped sliding groove (1-5), the corresponding support bolts (1-7) are screwed to position the driving motor (10).
4. The high purity lycium ruthenicum anthocyanin purification device of claim 1, wherein the device comprises: the inner sides of the two ends of the collecting cover (8) are respectively fixed with a protective edge (8-1) along the edges thereof.
5. The high purity lycium ruthenicum anthocyanin purification device of claim 1, wherein the device comprises: the outer end of the plug rod (5-4) is provided with a rolling ball (5-5) which is abutted against the annular plate (6).
6. The high purity lycium ruthenicum anthocyanin purification device of claim 1, wherein the device comprises: the inner side surface of the sealing cover plate (5-7) is adhered with a leakage-proof rubber cushion.
7. The high purity lycium ruthenicum anthocyanin purification device of claim 1, wherein the device comprises: the isolating circular plate (7) is positioned in each crushing hole and is radially fixed with a metal wire.
8. A purification method of the high purity lycium ruthenicum anthocyanin purification device according to claim 1, wherein the purification method comprises the following steps: the purification method comprises the following steps:
step one: mixing lycium ruthenicum and water, injecting the mixture into the cylinder (5) through a pipe orifice (5-3), screwing up a plug rod (5-4) and ensuring good contact with an annular plate (6);
step two: starting a crushing mode, tightening an adjusting bolt (1-6) to enable the lower end of an annular plate (6) to lift and incline, controlling a pinion (3) to drive a large gear (2) to rotate by a driving motor (10), and enabling a cylinder body (5) to reciprocate along a shaft rod (2-1) while rotating along with the large gear (2) under the action of a pressure spring (9), the annular plate (6) and two guide cross bars (2-2), wherein the black matrimony vine repeatedly passes through a partition circular plate (7) under pressure and is crushed under the action of crushing holes;
step three: opening a mixing mode, unscrewing the adjusting bolts (1-6) to enable the annular plate (6) to be vertical, injecting ethanol solution into the cylinder (5) through the pipe orifice (5-3), driving the pinion (3) to drive the large gear (2) to rotate by the driving motor (10), and uniformly mixing the internal solution by the cylinder (5) along with the large gear (2) to finish ethanol leaching;
step four: the separation mode is started, the annular plate (6) is still vertical, the sealing cover plate (5-7) is detached to expose the long-strip filter screen (5-6), the driving motor (10) controls the large gear (2) to rotate, the barrel (5) only rotates rapidly along with the large gear (2), filtering separation is carried out through the long-strip filter screen (5-6) under the centrifugal action, filtered solution is sprayed on the inner wall of the collecting cover (8) and then flows downwards along the wall to the bottom to flow out through the chute (1-3), and the broken residues of the lycium ruthenicum are left in the barrel (5).
9. The purification method according to claim 8, wherein: in the first step, the total volume of the black matrimony vine and water after being mixed accounts for more than 2/3 of the volume of the cylinder (5).
10. The purification method according to claim 8, wherein: the inclination angle of the middle annular plate (6) in the step II is 30-45 degrees.
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| CN115608237B (en) * | 2022-11-02 | 2023-04-21 | 连云港昌瑞科技有限公司 | High-efficiency cigarette adhesive stirring equipment and stirring method |
| CN117138390B (en) * | 2023-10-30 | 2023-12-29 | 山东省蚕业研究所 | Mulberry polyphenol extraction equipment and use method |
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| WO2014208967A1 (en) * | 2013-06-25 | 2014-12-31 | (주)슈퍼지티코리아 | All-in-one food waste processing apparatus for pulverizing, separating and compressing large quantities, and dehydrating |
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