CN115125093A - Plum wine or plum wine-containing beverage - Google Patents

Plum wine or plum wine-containing beverage Download PDF

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CN115125093A
CN115125093A CN202210276380.6A CN202210276380A CN115125093A CN 115125093 A CN115125093 A CN 115125093A CN 202210276380 A CN202210276380 A CN 202210276380A CN 115125093 A CN115125093 A CN 115125093A
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plum
wine
plum wine
containing beverage
content
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米泽知绘
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Suntory Holdings Ltd
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Suntory Holdings Ltd
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    • CCHEMISTRY; METALLURGY
    • C12BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
    • C12GWINE; PREPARATION THEREOF; ALCOHOLIC BEVERAGES; PREPARATION OF ALCOHOLIC BEVERAGES NOT PROVIDED FOR IN SUBCLASSES C12C OR C12H
    • C12G3/00Preparation of other alcoholic beverages
    • C12G3/04Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs
    • C12G3/06Preparation of other alcoholic beverages by mixing, e.g. for preparation of liqueurs with flavouring ingredients

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Abstract

The invention aims to improve the fruity degree and mellow fragrance of plum wine or plum wine-containing beverage. In the present invention, the contents of ethyl laurate and the weight ratio of ethyl laurate to the total content of diethyl malate and triethyl citrate in the ume liquor and the ume liquor-containing beverage are set to specific ranges.

Description

Plum wine or plum wine-containing beverage
Technical Field
The present invention relates to a plum wine or a plum wine-containing beverage having a specific composition and a related method.
Background
Plum wine is a beverage produced by adding plum fruits and saccharides to alcohol such as distilled liquor. Plum wine has been produced not only at home since ancient times, but also in recent years, brewers have been producing and selling lightly drunk plum wine, new plum wine having a specific flavor, and the like.
The method for producing plum wine is generally a method in which plum fruits, saccharides and alcohols are used in a certain proportion, the plum fruits are immersed in the alcohols, and then the plum fruits are taken out and further ripened. During the ripening period, plum wine is imparted with a strong and hierarchical aroma having an aromaticity such as esters, and has a unique ripening aroma different from the original aroma of plum.
Patent document 1 describes a plum wine containing hexyl acetate, which is fresh and has an enhanced fruity flavor.
Patent literature
Patent document 1: japanese patent laid-open publication No. 2019-77
Disclosure of Invention
Various types of plum wines have been produced so far, but as the times have shifted, the desirability of plum wines having different flavors has further developed.
Therefore, the present inventors have attempted to improve the fruity degree and/or the mellow aroma of plum in plum wine, and have obtained an unprecedented plum wine or plum-containing beverage having excellent flavor.
The invention aims to improve the fruity degree and/or mellow fragrance of plum in plum wine or plum wine-containing beverage.
The present inventors have found that when the weight ratio of the ethyl laurate content to the total content of diethyl malate and triethyl citrate in the plum wine is in a specific range, the plum-like fruity degree and/or rich aroma is improved, and thus have completed the present invention.
That is, the present invention relates to the following, but is not limited thereto.
[1] A plum wine or a plum wine-containing beverage characterized by containing (a) ethyl laurate and (b) diethyl malate and/or (c) triethyl citrate, wherein the content of (a) ethyl laurate is 10 to 50mg/L, and the weight ratio of the total content of (b) diethyl malate and (c) triethyl citrate to the content of (a) ethyl laurate, that is, (b + c)/a, is 2.7 or less.
[2] The Japanese apricot wine or the Japanese apricot wine-containing beverage according to [1], wherein the total content of diethyl malate and triethyl citrate is 80mg/L or less.
[3] The Japanese apricot wine or the Japanese apricot wine-containing beverage according to [1] or [2], wherein at least one of the following conditions (1) to (2) is satisfied:
(1) the content of the phenylethyl acetate is 11-27 mg/L, and,
(2) the content of the ethyl lactate is 2-10 mg/L.
[4] A method for improving a plum-like fruity degree and a rich aroma of a plum wine or a plum wine-containing beverage, comprising:
adjusting the content of ethyl laurate (a) in the plum wine or the plum wine-containing beverage to 10 to 50mg/L, and,
and (b + c)/a, which is the weight ratio of the total content of (b) diethyl malate and (c) triethyl citrate to the content of (a) ethyl laurate, is adjusted to 2.7 or less.
The present invention can improve the plum-like fruit taste and/or richness and aroma of plum wine or plum wine-containing beverage.
The "fruity degree like plum" in the present specification means a flavor having a strong fruity feeling of plum and an integrated feeling. In addition, "mellow fragrance" means a fragrance like a flower which is soft and elegant.
Detailed Description
The plum wine and the plum wine-containing beverage of the present invention and the related method will be explained below.
(plum wine and beverage containing plum wine)
The term "plum wine" as used herein refers to a beverage obtained by immersing a raw material plum fruit such as green plum or ripe plum in an alcohol-containing solution such as distilled liquor and extracting the component.
The plum variety for providing the plum fruit is not particularly limited as long as it is a variety generally used for producing plum wine, and typical varieties include south gao, white caragana, origami, and the like. Then, the plum fruit may be directly immersed in the alcohol-containing solution, or may be used in the immersion step after being pulverized or in a dried form.
The term "plum wine-containing beverage" as used herein means a beverage containing plum wine. Typical examples of the plum wine-containing beverage include a beverage obtained by diluting plum wine with water or carbonated water.
The content of the plum wine in the plum wine-containing beverage is preferably 1 to 99 v/v%, more preferably 5 to 99 v/v%, still more preferably 10 to 99 v/v%, and still more preferably 20 to 99 v/v%.
(Ethyl laurate, diethyl malate, triethyl citrate)
The plum wine or plum wine-containing beverage of the present invention contains ethyl laurate and diethyl malate and/or triethyl citrate.
The content of ethyl laurate in the plum wine or the plum wine-containing beverage of the present invention is 10 to 50mg/L, preferably 10 to 47mg/L, more preferably 10.3 to 46.1mg/L, more preferably 20 to 40mg/L, more preferably 28.2 to 37.1 mg/L. In the ume wine or the ume wine-containing beverage of the present invention, the weight ratio ((b + c)/a) of the total content of diethyl malate and triethyl citrate to the content of ethyl laurate is 2.7 or less, preferably 2.5 or less, more preferably 2.2 or less, more preferably 1.6 or less, and more preferably 1.2 or less. The lower limit of the weight ratio is not particularly limited, but is, for example, 0.1, 0.2, 0.3, 0.4, 0.5, 0.6, 0.7 or 0.8.
The total content of diethyl malate and triethyl citrate in the ume liquor or the ume liquor-containing beverage of the present invention is preferably 80mg/L or less, preferably 76mg/L or less, preferably 71mg/L or less, preferably 62.3mg/L or less, preferably 45mg/L or less, preferably 34.9mg/L or less. The lower limit of the content is not particularly limited, but is, for example, 2.6mg/L, 5.3mg/L, 7.9mg/L, 10.5mg/L, 13.1mg/L, 15.8mg/L, 18.4mg/L or 21.2 mg/L.
In order to adjust the contents and weight ratios of ethyl laurate, diethyl malate and triethyl citrate, for example, some or all of these components may be added from the outside, or a plurality of types of plum liquors or plum liquor beverages having different contents of these components may be mixed. The desired components may be added to the plum wine as they are, or may be added to the plum wine as a material such as plum juice, plum extract, or wine base containing a part or all of the components. Examples of such wine bases are whisky, brandy (e.g. cognac brandy). The liquor can be added as raw material, or the plum fruit can be soaked in the liquor. In addition, the aging time may be adjusted as necessary.
(other ingredients relating to plum wine or plum wine-containing beverage)
In one form, the plum wine or the plum wine-containing beverage of the present invention satisfies at least one of the following conditions (1) to (2):
(1) the content of the phenethyl acetate is 11-27 mg/L, more preferably 11.2-26.2 mg/L, more preferably 12-26.2 mg/L, more preferably 13.7-26.2 mg/L, more preferably 15-26.2 mg/L, more preferably 16.2-26.2 mg/L, and
(2) the content of the ethyl lactate is 2-10 mg/L, more preferably 3-10 mg/L, more preferably 3.4-10 mg/L, more preferably 4-10 mg/L, more preferably 4.7-10 mg/L.
The method for adjusting the contents of these components may be the same as the above-mentioned method relating to the contents and weight ratio of ethyl laurate, diethyl malate and triethyl citrate.
(analysis method)
The analysis of the components of the alcoholic liquors is not limited, and can be carried out by any known method.
For example, the content of ethyl laurate, phenethylacetate and ethyl lactate can be measured by Gas Chromatography (GC) under the following conditions.
Specifically, a liquid obtained by mixing 100. mu.l of an internal standard (methyl decanoate) with 1000. mu.l of a sample was used to calculate a quantitative value by an internal standard analysis method. The GC assay conditions were as follows.
Gas chromatograph: GC 6890N (Agilent technologies)
Column: HP-ULTRA2(Agilent J & W) had an inner diameter of 0.32mm, a length of 50m, and a film thickness of 0.52 μm
Mobile phase: helium (2.5mL/min)
The sample injection method comprises the following steps: shunting (Split)
The split ratio is as follows: 15:1
Sample inlet temperature: 250 deg.C
Temperature of the incubator: 40 ℃ (5min) → 10 ℃/min → 230 ℃ (10min)
A detector: FID
Detector temperature: 260 deg.C
Sample introduction amount: 2.0. mu.l
Further, the contents of diethyl malate and triethyl citrate can be measured by the following conditions using, for example, LCMS.
Specifically, the sample solution is diluted with ethanol to an appropriate ratio. Thereafter, the resulting dilution was filtered with a 0.2 μm membrane filter, and collected in a 2mL sample bottle as an assay sample. The measurement samples were subjected to LC/MS measurement, and then quantitative values were calculated by a standard curve method. The LC/MS measurement conditions are as follows.
LC Condition
A high performance liquid chromatograph: 1260Infinity II LC System (Agilent Technologies)
Column: COSMOCORE 2.6Cholester (Nacalai Tesque Co., Ltd., inner diameter 3.0mm, length 100mm)
Column temperature: 40 deg.C
Eluent A: water-acetonitrile (950: 50) solution containing 10mM ammonium acetate
Eluent B: water-acetonitrile (50: 950) solution containing 10mM ammonium acetate
Gradient conditions: eluent B linear gradient from 0% to 40% for 9 min
Flow rate: 0.5mL/min
Sample introduction amount: 2 μ LMS Condition
Mass spectrometry: G6135B (Agilent Technologies)
An ionization method: electrospray ionization (ESI) method
Capillary voltage: 3000V
Drying gas: 350 ℃ and 11L/min
A sprayer: 50psi
Measurement mode: SIM (subscriber identity Module)
Polarity: positive for
Ions used for quantification: m/z 191 (diethyl malate), m/z 277 (triethyl citrate)
(alcohol)
The plum wine or the plum wine-containing beverage of the present invention contains alcohol. The term "alcohol" as used herein means ethanol unless otherwise specified.
The alcohol content of the plum wine or the plum wine-containing beverage of the present invention is preferably 1.0 to 30 v/v%, more preferably 5.0 to 25.0 v/v%.
In the present specification, the alcohol content may be measured by any known method, for example, by a vibrating densitometer. Specifically, a sample from which carbon dioxide has been removed from a beverage by filtration or ultrasonic treatment is prepared, and the sample is distilled with direct fire, and the density of the resulting distillate at 15 ℃ is measured, and then the density is obtained by conversion using the Japanese national tax office's specified analysis method (Japanese national tax office's standard No. 6, revised 6.6.22.19 (2007)) attached table "2 nd table of conversion table of alcoholic strength, density (15 ℃) and specific gravity (15/15 ℃).
(other Components)
Other additives usually added to the plum wine or the plum wine-containing beverage of the present invention, such as sugars, flavors, vitamins, pigments, antioxidants, preservatives, seasonings, souring materials, extracts, pH adjusters, and quality stabilizers, may be added to the plum wine or the plum wine-containing beverage of the present invention as long as the unique flavor inherent to the plum wine is not impaired and the effect of the present invention is not impaired.
(beverage packaged in container)
The ume wine or the ume wine-containing beverage of the present invention may be provided in the form of a container. The form of the container includes a metal container such as a can, a PET bottle, a carton, a glass bottle, a flexible package, etc., but is not limited thereto.
(method)
On the other hand, the present invention is a method for improving the plum-like fruity degree and richness of the plum wine or the plum wine-containing beverage. The method includes the following steps.
Adjusting the content of ethyl laurate (a) in the plum wine or the plum wine-containing beverage to 10 to 50mg/L, and
and a step wherein the weight ratio ((b + c)/a) of the total content of (b) diethyl malate and (c) triethyl citrate to the content of (a) ethyl laurate is adjusted to 2.7 or less.
The method of adjusting the content and the weight ratio is as described above in relation to or evident from the plum wine or plum wine-containing beverage. The time point is also not limited. For example, the above steps may be performed simultaneously or separately, or the order of the steps may be alternated. As long as the final resulting beverage satisfies the above conditions. In addition, the contents and weight ratios of ethyl laurate, diethyl malate, and triethyl citrate, as well as specific examples or parts of other ingredients added, are as described above in relation to the plum wine or the plum wine-containing beverage.
(numerical value Range)
For clarity of description, the numerical ranges indicated by the lower limit and the upper limit in the present specification, i.e., "from the lower limit to the upper limit" include the lower limit and the upper limit. For example, the range represented by "1 to 2" includes 1 and 2.
Examples
The present invention will be described below based on examples, but the present invention is not limited to these examples.
In addition, in the following examples, "ppm" is synonymous with "mg/L".
(test example 1)
A plum wine-containing beverage A (comparative example 1-1) having a pH of 2.8 was prepared by diluting the own plum wine base of this company with water. The amounts of the respective components in the obtained plum wine-containing beverage a are shown in the following table.
[ Table 1]
Figure BDA0003556141970000071
Next, ethyl laurate was added to the beverage as comparative example 1-1 to prepare several beverages. The ethyl laurate content of the resulting beverage is shown in the table below.
[ Table 2]
Figure BDA0003556141970000072
The above beverages were subjected to sensory evaluation. Specifically, the fruity taste and the full aroma were evaluated by a trained professional panelist. Evaluation was performed in 7 grades according to the criteria shown below. The product is qualified when the score is more than 3. Unless otherwise specified, this evaluation method was also used in other test examples.
< evaluation Standard >
1: has no fruit taste.
2: there is no fruity taste.
3: has a slight fruity taste.
4: has fruity taste.
5: has fruity taste and can be used for providing mellow fragrance.
6: the fruit taste is strong, and the fruit can feel mellow and fragrant.
7: the fruit taste is strong, and the fruit can feel mellow and fragrant with lingering charm.
The results are shown in Table 2. When the content of ethyl laurate is in a certain range, the fruit taste and mellow fragrance are excellent.
(test example 2)
Further research into methods of improving fruity taste and/or richness and aroma.
Specifically, in examples 1 to 4 in test example 1, diethyl malate and triethyl citrate were further added to perform sensory evaluation. The amounts of ingredients in each beverage and the sensory evaluation results are shown in the following table.
When the total content of diethyl malate and triethyl citrate with respect to the ratio of ethyl laurate is in a specific range, excellent effects can be obtained.
[ Table 3]
Figure BDA0003556141970000081
(test example 3)
Further research into methods of improving fruity taste and/or richness and aroma.
Specifically, examples 1 to 4 in test example 1 and examples 2 to 3 in test example 2 were further added with ethyl lactate and phenethylacetate, and sensory evaluation was performed. The amounts of ingredients in each beverage and the results of sensory evaluation are shown in the following table.
When the contents of these components are in specific ranges, very excellent effects can be obtained.
[ Table 4]
Figure BDA0003556141970000091
(test example 4)
A similar test to that of test example 1 was carried out using a different wine base of ume wine from the wine base used in test example 1.
This raw liquor was diluted with water to prepare a plum wine-containing beverage B having a pH of 2.8 (comparative example 4-1). The amounts of the respective components in the obtained plum wine-containing beverage B are shown in the following table.
[ Table 5]
Figure BDA0003556141970000092
Next, ethyl laurate was added to the beverage as comparative example 4-1 to prepare several beverages. The contents of ingredients such as ethyl laurate in the obtained beverage are shown in the table below. In addition, the weight ratio of the total content of diethyl malate and triethyl citrate in these beverages to the content of ethyl laurate was 2.54 or less.
Sensory evaluation was performed on the resulting beverage. The results are also shown in the following table.
[ Table 6]
Figure BDA0003556141970000101
Even if the type of the wine base of ume wine was changed, the same tendency as in test example 1 was exhibited.
Next, a similar test to test example 3 was performed. Specifically, ethyl lactate and phenethyl acetate were further added to the plum wine-containing beverages of examples 4 to 3 to prepare two kinds of beverages.
The amounts of ingredients in these beverages and the sensory evaluation results are shown in the table below.
[ Table 7]
Figure BDA0003556141970000102
When ethyl lactate and phenethylacetate were added, very excellent effects were obtained.

Claims (4)

1. A plum wine or a plum wine-containing beverage characterized by containing (a) ethyl laurate and (b) diethyl malate and/or (c) triethyl citrate, wherein the content of (a) ethyl laurate is 10 to 50mg/L, and the weight ratio of the total content of (b) diethyl malate and (c) triethyl citrate to the content of (a) ethyl laurate, that is, (b + c)/a, is 2.7 or less.
2. The ume wine or the ume wine-containing beverage as set forth in claim 1, wherein the total content of diethyl malate and triethyl citrate is 80mg/L or less.
3. The ume wine or ume wine-containing beverage as claimed in claim 1 or 2, wherein at least one of the following conditions (1) to (2) is satisfied:
(1) the content of phenylethyl acetate is 11-27 mg/L, and,
(2) the content of the ethyl lactate is 2-10 mg/L.
4. A method for improving a plum-like fruity degree and a rich aroma of a plum wine or a plum wine-containing beverage, comprising:
adjusting the content of ethyl laurate (a) in the plum wine or the plum wine-containing beverage to 10 to 50mg/L, and,
and (b + c)/a, which is the weight ratio of the total content of (b) diethyl malate and (c) triethyl citrate to the content of (a) ethyl laurate, is adjusted to 2.7 or less.
CN202210276380.6A 2021-03-25 2022-03-21 Plum wine or plum wine-containing beverage Pending CN115125093A (en)

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JP6267039B2 (en) 2014-03-28 2018-01-24 サントリーホールディングス株式会社 Distilled plum wine
JP6641237B2 (en) 2016-06-20 2020-02-05 サントリーホールディングス株式会社 Plum wine or beverage containing plum wine

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