CN115121199A - Reaction unit for solid phase preparation based on calcium titanate - Google Patents
Reaction unit for solid phase preparation based on calcium titanate Download PDFInfo
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- CN115121199A CN115121199A CN202210813183.3A CN202210813183A CN115121199A CN 115121199 A CN115121199 A CN 115121199A CN 202210813183 A CN202210813183 A CN 202210813183A CN 115121199 A CN115121199 A CN 115121199A
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 28
- AOWKSNWVBZGMTJ-UHFFFAOYSA-N calcium titanate Chemical compound [Ca+2].[O-][Ti]([O-])=O AOWKSNWVBZGMTJ-UHFFFAOYSA-N 0.000 title claims abstract description 22
- 239000007790 solid phase Substances 0.000 title claims abstract description 20
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 88
- 239000000463 material Substances 0.000 claims abstract description 11
- 238000007789 sealing Methods 0.000 claims abstract description 9
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 27
- 238000003860 storage Methods 0.000 claims description 18
- 238000001914 filtration Methods 0.000 claims description 16
- 238000007667 floating Methods 0.000 claims description 13
- 238000010438 heat treatment Methods 0.000 claims description 12
- 229910052751 metal Inorganic materials 0.000 claims description 12
- 239000002184 metal Substances 0.000 claims description 12
- 239000012535 impurity Substances 0.000 claims description 10
- 239000007921 spray Substances 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 8
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 6
- 239000003381 stabilizer Substances 0.000 claims description 6
- 238000005485 electric heating Methods 0.000 claims description 5
- 238000000746 purification Methods 0.000 claims description 5
- 210000000056 organ Anatomy 0.000 claims description 4
- 238000005086 pumping Methods 0.000 claims description 4
- 238000005507 spraying Methods 0.000 claims description 4
- 230000008602 contraction Effects 0.000 claims description 3
- 238000011049 filling Methods 0.000 claims description 3
- 230000017525 heat dissipation Effects 0.000 claims description 3
- 229910052759 nickel Inorganic materials 0.000 claims description 3
- 238000004904 shortening Methods 0.000 claims description 3
- 238000005406 washing Methods 0.000 description 15
- 238000003756 stirring Methods 0.000 description 8
- 230000005540 biological transmission Effects 0.000 description 5
- 238000011010 flushing procedure Methods 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- 230000000149 penetrating effect Effects 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 3
- 230000003028 elevating effect Effects 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 229910002971 CaTiO3 Inorganic materials 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003985 ceramic capacitor Substances 0.000 description 1
- 238000004891 communication Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 239000003989 dielectric material Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 230000000087 stabilizing effect Effects 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000011144 upstream manufacturing Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Images
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/002—Avoiding undesirable reactions or side-effects, e.g. avoiding explosions, or improving the yield by suppressing side-reactions
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
- B01J4/002—Nozzle-type elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
- B01J4/007—Feed or outlet devices as such, e.g. feeding tubes provided with moving parts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/008—Feed or outlet control devices
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/003—Titanates
- C01G23/006—Alkaline earth titanates
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Inorganic Chemistry (AREA)
- Filtration Of Liquid (AREA)
Abstract
The invention discloses a reaction device for solid-phase preparation based on calcium titanate, which comprises a main body, a temperature control box, a first motor and an inclined plate, wherein the temperature control box is installed at the top of the main body, a first cavity is installed on the inner wall of the temperature control box, the first motor is installed on the outer wall of the main body, the output end of the first motor extends into the main body, and the inclined plate is installed on the inner wall of the main body. The water sprayer is installed on the feeding plate, materials are placed on the feeding plate, then the first water pump pumps the solution, the electric telescopic rod is shortened to drive the sealing block to leave the pipe orifice of the first telescopic pipe, so that the low-temperature solution in the first cavity and the high-temperature solution in the second cavity enter the water sprayer, the temperature sensor detects the temperature of the solution, when the temperature is too high or too low, the motor drives the cam to rotate, the lifting rod moves to drive the first spring to extend, the lifting rod is in contact with the conductive plate, and the conductive plate controls the first electric control valve and the second electric control valve, so that the temperature can be conveniently adjusted.
Description
Technical Field
The invention relates to the technical field of calcium titanate solid phase preparation, in particular to a reaction device for solid phase preparation based on calcium titanate.
Background
Calcium titanate is an inorganic substance, has a chemical formula of CaTiO3, belongs to a cubic crystal system, is a basic inorganic dielectric material with excellent dielectric property, temperature property, mechanical property and optical property, and is widely applied to the fields of ceramic capacitors, PTC thermistors, microwave antennas, filters, stainless steel welding rods and the like.
The existing calcium titanate preparation reaction equipment has the defects that:
1. patent document CN108211497A discloses a filter equipment that calcium titanate solid phase preparation in-process sparge water was used, the right item of protection "includes the main part, be equipped with in the main part and wash the chamber, filter chamber and control box, be equipped with first filtration guiding device in the filter chamber, second filtration guiding device and layering filter equipment, first filtration guiding device includes first main part, the top of first main part is equipped with receiving device, receiving device includes the main part of accepting to the indent, be equipped with the bulge loop on accepting the front of main part, accept first elevating gear of back connection of main part, pressure-sensitive device, first vibrations hammer, second filtration guiding device includes the second main part, a groove, second elevating gear connects, layering filter equipment includes layering filter screen and bottom plate. The filter device for flushing water in the solid-phase preparation process of calcium titanate has the advantages of reasonable structure, practical function, convenient and intelligent operation, capability of effectively collecting particles in wastewater and improving the effective utilization rate of resources, most of the conventional devices cannot control and detect the temperature of liquid, so that the temperature of the solution changes in the reaction process, and the production efficiency is reduced;
2. the patent document CN109454050A discloses a washing device in the process of preparing calcium titanate solid phase, the right of protection "comprises a main body, a cover plate and a control center, the control center is arranged at the side position below the bottom of the main body, the main body comprises a stirring device, a filtering device and a heating device, the stirring device is arranged below the cover plate and connected with the cover plate, the stirring device is transversely provided with a rotating shaft, the rotating shaft is connected with a first stirring motor, the tail part of the rotating shaft is provided with a pressure sensing device, the rotating shaft is provided with a stirring rod, a stirring bottom plate is arranged below the rotating shaft, the stirring bottom plate is a conical bottom plate, the two sides of the conical bottom plate form an included angle of 35-50 degrees with the ground, the central part of the conical bottom plate is a first layer of filter screen, the filtering device is arranged below the conical bottom plate, the bottom of the filtering device is provided with the heating device, and a heat insulation plate is arranged between the filtering device and the heating device, the heating device comprises an electric heater and a temperature sensor, the stirring device, the filtering device and the heating device are electrically connected with the control center, most of the existing devices lack warning structures and cannot remind workers when liquid is lacked or collected fully;
3. the patent document CN113522948A discloses a washing device and a washing system, the protection claim "the washing device is that the first transmission unit is provided, the first transmission unit is used to divide the housing into a washing area at the upper part of the housing and a collecting area at the lower part of the housing, and a plurality of gaps communicated with the washing area and the collecting area are arranged on the first transmission unit at intervals, so that the object to be washed is transported by the first transmission unit and passes through the washing area, and in the washing area, the object to be washed is washed by the washing component arranged on the side wall of the housing, the object to be washed is transported out of the washing area by the first transmission unit, the washed washing liquid enters the collecting area through the gaps and is collected for subsequent treatment, thus secondary pollution is not caused, the device has simple structure and simple and convenient construction process, and the washing device can be used for washing both sides by the first washing unit on the first side wall and the second washing unit on the second side wall, the device improves the removal effect and the working efficiency of pollutants on the surface of the object to be washed, and most of the existing devices lack a purification and filtration structure, so that the solution is changed into waste liquid with high probability, cannot be recycled and reused, and is not saved;
4. patent document CN111335453A discloses a flushing device, a flushing system and a flushing method, wherein the protection right "includes a storage room, a flow distribution room, a vacuum pumping device, an air inlet device, a first on-off device and a second on-off device; a first on-off device is arranged between the storage room and the flow dividing room and used for controlling the communication or the cut-off of the storage room and the flow dividing room, and when the first on-off device is closed, the storage room is a closed space; a water inlet and a water outlet are arranged on the wall body enclosing the flow splitting room, the water inlet is used for connecting with a drain pipe at the upstream of the flow splitting room, and the water outlet is used for connecting with a drain pipe at the downstream of the flow splitting room; the vacuumizing device is communicated with the storage room, and is used for vacuumizing the storage room when the first on-off equipment is closed; the wall body enclosing the storage room is provided with an air inlet device, and the air inlet device is used for communicating the atmosphere inside the storage room and the atmosphere outside the storage room to realize vacuum breaking between the storage rooms; the second on-off equipment sets up in being close to water inlet department for control water inlet switches on or ends, when current device was taken out mostly, needs the staff to manually pull out the feed plate, has increased staff's work burden, convenient and fast inadequately.
Disclosure of Invention
The present invention is directed to a reaction apparatus for solid-phase production based on calcium titanate, which solves the problems of the prior art.
In order to achieve the purpose, the invention provides the following technical scheme: a reaction device for solid phase preparation based on calcium titanate comprises a main body, a temperature control box, a first motor and an inclined plate, wherein the temperature control box is arranged at the top of the main body;
the display screen is installed at the top of the temperature control box, the first water pump is installed on the bottom wall inside the temperature control box, the water inlet pipe is installed at the input end of the first water pump, one end of the water inlet pipe extends out of the top of the temperature control box, the water outlet pipe is installed at the output end of the first water pump, and the first electric control valve and the second electric control valve are sequentially installed on the outer wall of the water outlet pipe;
the cavity is installed No. one to the inner wall of temperature control box, first motor is installed to the outer wall of main part, and the output of first motor extends into the inside of main part, the swash plate is installed to the inner wall of main part, the backup pad is installed to the inner wall of main part, and the backup pad is located the top of swash plate.
Preferably, the control screen is installed in the front of main part, and the outer wall of main part is equipped with the feed chute, and the inner wall of feed chute runs through and installs the feeding board, and the handle is installed to the outer wall of feeding board, and the bottom of feeding board is equipped with a plurality of holes that leak, and the filter screen is installed to the inner wall in the hole that leaks.
Preferably, No. two chambeies are installed to the inner wall of temperature control box, and the buckler is all installed to the inner wall in a chamber and No. two chambeies, and electric telescopic handle is installed to the inner wall of buckler, and electric telescopic handle's one end extends the outer wall of buckler, and sealed piece is installed to electric telescopic handle's one end, and the metal pole is installed to the nickel coin in No. two chambeies, and the heating wire is installed in encircleing of metal pole, and the bottom in a chamber and No. two chambeies all runs through and installs flexible pipe No. one.
Preferably, the output end of the first motor is provided with a reciprocating lead screw, the outer wall of the reciprocating lead screw is sleeved with a movable block, the bottom of the movable block is provided with a water sprayer, the inner wall of the main body is provided with a slide bar, the outer wall of the slide bar is provided with a slide block, the slide block and the movable block are connected with the inner wall of the main body and provided with a pressure pump, the output end of the pressure pump is provided with a second telescopic pipe, and one end of the second telescopic pipe extends into the water sprayer.
Preferably, the bottom of sprinkler is run through and is installed the spray pipe, the control valve is installed to the outer wall of spray pipe, the detector is installed to one side inner wall of sprinkler, temperature sensor is installed to the outer wall of detector, two sets of fixed plates are installed to the inner wall of detector, the top of fixed plate is run through and is installed the lifter, the outer wall of lifter encircles and installs first spring, the motor is installed to the inner wall of detector, the cam is installed to the output of motor, the current conducting plate is all installed to the inside roof and the inside diapire of detector, the gag lever post is installed to the opposite side inner wall of sprinkler.
Preferably, the montant is installed to the outer wall of gag lever post, and the elevator is installed to the outer wall of montant, and the floater is installed to the outer wall of elevator, and the attention device is installed to the outer wall of sprinkler, and the outer wall of attention device runs through installs the carriage release lever, and the one end of carriage release lever extends into the inside of sprinkler, and the outer wall of carriage release lever encircles installs the second spring, and two sets of buzzers are installed to the inner wall of attention device, and the switch is installed to the outer wall of buzzer.
Preferably, the filter is installed to the inside diapire of main part, and No. two water pumps are installed to the inner wall of filter, and the outer wall of filter is extended to the input of No. two water pumps, and the filter chamber is installed to the inner wall of filter, and the interception net outer wall is installed and is run through to install the inlet pipe to the inner wall of filter chamber, and the limiting plate is installed to the inner wall of inlet pipe, and the third spring is installed to the outer wall of limiting plate, and the drain pipe is installed to the outer wall of filter, and the bin is installed to the outer wall of main part, and electric putter is installed to the inner wall of bin, and the push pedal is installed to electric putter's one end.
Preferably, reset spring is installed to the inside back wall of main part, and the stabilizer plate is installed to the inside back wall of main part, and the hydraulic stem is installed to the bottom of stabilizer plate, and spacing post is installed to the bottom of hydraulic stem.
Preferably, the reaction device comprises the following working steps:
s1, firstly, putting the material on a feeding plate, then pumping the solution by a water pump, opening a first electric control valve and a second electric control valve, filling a first cavity and a second cavity, then electrifying a heating wire for heat dissipation, heating the solution by matching with a metal rod, shortening an electric telescopic rod to drive a sealing block to leave the pipe orifice of a first telescopic pipe, enabling the low-temperature solution in the first cavity and the high-temperature solution in the second cavity to enter the interior of a water sprayer, driving a reciprocating lead screw to rotate by a first motor, driving a moving block to rotate by the reciprocating lead screw, sliding a sliding block on a sliding rod to move the water sprayer, opening a control valve, pressurizing the water sprayer by a pressurizing pump, spraying the solution onto the material by the water sprayer through a water spraying pipe, and facilitating reaction, detecting the temperature of the solution by a temperature sensor, driving a cam to rotate by a motor when the temperature is too high or too low, extruding a lifting rod by the cam, driving a first spring to extend, the lifting rod is in contact with the current-conducting plate, and the current-conducting plate controls the first electric control valve and the second electric control valve, so that the temperature can be conveniently adjusted;
s2, when the content of the solution in the water sprayer is reduced or the water sprayer is full, the floating ball moves along with the liquid level, the floating ball drives the lifting block to slide on the outer wall of the vertical rod, the floating ball extrudes the movable rod, the movable rod moves to drive the second spring to extend, and the movable rod is in contact with the switch, so that the buzzer makes a sound to warn, and the warning function is realized;
s3, the inclined plate is a net plate, so that larger impurities can be filtered, the solution after reaction flows out through a water leakage hole and a filter screen, the solution is pumped into a filter cavity of the filter by a second water pump, then the electric push rod extends to drive the push plate to extrude the activated carbon in the storage box into the feed pipe, the activated carbon extrudes the limiting plate, the limiting plate rotates to drive the third spring to contract, the activated carbon enters the filter cavity to adsorb the impurities in the solution, the drain pipe is opened, the filtered solution is discharged and collected, and the purifying and filtering functions of the solution are realized;
s4 and the feeding plate are placed above the supporting plate, the feeding plate is pushed to enter the main body, the feeding plate extrudes a return spring, the return spring contracts to store energy, the hydraulic rod extends to drive the front end of the limit column to be inserted into the return spring, the return spring is in a contraction state, when the feeding plate needs to be popped out, the hydraulic rod contracts to enable the limit column to be not limited to the return spring any more, and the return spring extends to drive the feeding plate to pop out.
Compared with the prior art, the invention has the beneficial effects that:
1. the invention can realize the control function by installing a water sprayer, the material is placed on a feeding plate, then a first water pump pumps the solution, a first electric control valve and a second electric control valve are opened, a first cavity and a second cavity are filled, then an electric heating wire is electrified for heat dissipation, the solution is heated by matching with a metal rod, an electric telescopic rod shortens a pipe orifice for driving a sealing block to leave a first telescopic pipe, so that the low-temperature solution in the first cavity and the high-temperature solution in the second cavity enter the water sprayer, a first motor drives a reciprocating lead screw to rotate, the reciprocating lead screw rotates to drive a moving block to rotate, a sliding block slides on a sliding rod, the water sprayer moves, a control valve is opened, a pressurizing pump pressurizes the water sprayer, so that the water sprayer sprays the solution on the material through a water spraying pipe, the reaction is convenient, a temperature sensor detects the temperature of the solution, and when the temperature is too high or too low, a motor drives a cam to rotate, the cam extrudes the lifting rod, the lifting rod moves to drive the first spring to extend, the lifting rod is contacted with the current-conducting plate, and the current-conducting plate controls the first electric control valve and the second electric control valve, so that the temperature can be conveniently adjusted;
2. when the content of the solution in the water sprayer is reduced or the water sprayer is full, the floating ball moves along with the liquid level, the floating ball drives the lifting block to slide on the outer wall of the vertical rod, the floating ball extrudes the movable rod, the movable rod moves to drive the second spring to extend, and the movable rod is in contact with the switch, so that the buzzer makes a sound to warn, and the warning function is realized;
3. according to the invention, the purification and filtration functions can be realized by installing the filter cavity, the inclined plate is a net-shaped plate, larger impurities can be filtered, then, the solution after reaction flows out through the water leakage hole and the filter screen, the solution is pumped into the filter cavity in the filter by the second water pump, then, the electric push rod extends to drive the push plate to extrude active carbon in the storage box to enter the feeding pipe, the active carbon extrudes the limiting plate, the limiting plate rotates to drive the third spring to contract, the active carbon enters the filter cavity to adsorb the impurities in the solution, the drain pipe is opened, and the filtered solution is discharged and collected, so that the purification and filtration functions of the solution are realized;
4. the automatic ejection device can realize the automatic ejection function by installing the return spring, the feeding plate is placed above the supporting plate, then the feeding plate is pushed to enter the main body, the feeding plate extrudes the return spring, the return spring contracts to store energy, then the hydraulic rod extends to drive the limiting column to be inserted into the front end of the return spring, so that the return spring is in a contraction state, when the feeding plate needs to be ejected, the hydraulic rod contracts to enable the limiting column not to limit the return spring, and the return spring extends to drive the feeding plate to eject.
Drawings
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic front view of the present invention;
FIG. 3 is a schematic view of the sprinkler structure of the present invention;
FIG. 4 is a schematic view of the temperature control box according to the present invention;
FIG. 5 is a schematic side view of the present invention;
FIG. 6 is a schematic view of a filter portion according to the present invention;
fig. 7 is a schematic structural view of part a in fig. 6 according to the present invention.
In the figure: 1. a main body; 101. a control screen; 102. a feeding plate; 103. a handle; 104. a filter screen; 2. a temperature control box; 201. a display screen; 202. a water pump; 203. a first electrically controlled valve; 204. a second electrically controlled valve; 3. a first chamber; 301. a waterproof shell; 302. an electric telescopic rod; 303. a sealing block; 304. a second chamber; 305. a metal rod; 306. an electric heating wire; 307. a first telescopic pipe; 4. a first motor; 401. a reciprocating screw rod; 402. a moving block; 403. a slide bar; 404. a slider; 405. a pressure pump; 5. a water sprayer; 501. a water spray pipe; 502. a control valve; 503. a detector; 504. a temperature sensor; 505. a fixing plate; 506. a lifting rod; 507. a first spring; 508. a motor; 509. a cam; 510. a conductive plate; 6. a limiting rod; 601. a vertical rod; 602. a floating ball; 603. an alarm; 604. a travel bar; 605. a second spring; 606. a buzzer; 607. a switch; 7. a sloping plate; 701. a filter; 702. a second water pump; 703. an intercepting net; 704. a feeding pipe; 705. a limiting plate; 706. a third spring; 707. a drain pipe; 708. a storage tank; 709. an electric push rod; 710. pushing the plate; 711. a filter chamber; 8. a support plate; 801. a return spring; 802. a stabilizing plate; 803. a hydraulic lever; 804. a limiting column.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
In the description of the present invention, it should be noted that the terms "upper", "lower", "inner", "outer", "front", "rear", "both ends", "one end", "the other end", and the like indicate orientations or positional relationships based on orientations or positional relationships shown in the drawings, and are only for convenience of description and simplification of description, but do not indicate or imply that the device or element referred to must have a specific orientation, be configured in a specific orientation, and operate, and thus, should not be construed as limiting the present invention. Furthermore, the terms "first" and "second" are used for descriptive purposes only and are not to be construed as indicating or implying relative importance.
In the description of the present invention, it is to be noted that, unless otherwise explicitly specified or limited, the terms "mounted," "disposed," "connected," and the like are to be construed broadly, and for example, "connected" may be a fixed connection, a detachable connection, or an integral connection; can be mechanically or electrically connected; they may be connected directly or indirectly through intervening media, or they may be interconnected between two elements. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Referring to fig. 1, fig. 2, fig. 3 and fig. 4, an embodiment of the present invention: a reaction device for solid phase preparation based on calcium titanate comprises a main body 1, a temperature control box 2, a first motor 4 and an inclined plate 7, wherein the temperature control box 2 is installed at the top of the main body 1, a display screen 201 is installed at the top of the temperature control box 2, a first water pump 202 is installed at the bottom wall inside the temperature control box 2, a water inlet pipe is installed at the input end of the first water pump 202, one end of the water inlet pipe extends out of the top of the temperature control box 2, a water outlet pipe is installed at the output end of the first water pump 202, a first electric control valve 203 and a second electric control valve 204 are sequentially installed on the outer wall of the water outlet pipe, a first cavity 3 is installed on the inner wall of the temperature control box 2, the first motor 4 is installed on the outer wall of the main body 1, the output end of the first motor 4 extends into the main body 1, the inclined plate 7 is installed on the inner wall of the main body 1, a support plate 8 is installed on the inner wall of the main body 1, and the supporting plate 8 is located above the sloping plate 7, the front of the main body 1 is provided with the control screen 101, the outer wall of the main body 1 is provided with the feeding groove, the inner wall of the feeding groove is provided with the feeding plate 102 in a penetrating manner, the outer wall of the feeding plate 102 is provided with the handle 103, the bottom of the feeding plate 102 is provided with a plurality of water leakage holes, the inner wall of the water leakage holes is provided with the filter screen 104, the inner wall of the temperature control box 2 is provided with the second chamber 304, the inner walls of the first chamber 3 and the second chamber 304 are provided with the waterproof shell 301, the inner wall of the waterproof shell 301 is provided with the electric telescopic rod 302, one end of the electric telescopic rod 302 extends out of the outer wall of the waterproof shell 301, one end of the electric telescopic rod 302 is provided with the sealing block 303, the nickel coin in the second chamber 304 is provided with the metal rod 305, the metal rod 305 is surrounded by the electric heating wire 306, the bottoms of the first chamber 3 and the second chamber 304 are provided with the first telescopic pipe 307 in a penetrating manner, the output end of the first motor 4 is provided with the reciprocating screw rod 401, a moving block 402 is sleeved on the outer wall of the reciprocating screw 401, a water sprayer 5 is installed at the bottom of the moving block 402, a sliding rod 403 is installed on the inner wall of the main body 1, a sliding block 404 is installed on the outer wall of the sliding rod 403, the sliding block 404 and the moving block 402 are connected with the inner wall of the main body 1, a pressure pump 405 is installed on the inner wall of the pressure pump 405, one end of the second expansion pipe extends into the water sprayer 5, a water spray pipe 501 is installed at the bottom of the water sprayer 5 in a penetrating manner, a control valve 502 is installed on the outer wall of the water spray pipe 501, a detector 503 is installed on the inner wall of one side of the water sprayer 5, a temperature sensor 504 is installed on the outer wall of the detector 503, two fixing plates 505 are installed on the inner wall of the detector 503, a lifting rod 506 is installed on the top of the fixing plate 505 in a penetrating manner, a first spring 507 is installed on the outer wall of the lifting rod 506 in a surrounding manner, a motor 508 is installed on the inner wall of the detector 503, and a cam 509 is installed on the output end of the motor 508, the detector 503 has a conductive plate 510 mounted on both the inner top wall and the inner bottom wall, and a stopper 6 is mounted on the inner wall of the other side of the sprinkler 5.
Referring to fig. 3, an embodiment of the present invention: montant 601 is installed to the outer wall of gag lever post 6, the elevator is installed to the outer wall of montant 601, floater 602 is installed to the outer wall of elevator, alarm 603 is installed to the outer wall of sprinkler 5, the outer wall of alarm 603 runs through installs the carriage release lever 604, the inside of sprinkler 5 is extended into to the one end of carriage release lever 604, the outer wall of carriage release lever 604 encircles installs second spring 605, two sets of bee calling organ 606 are installed to the inner wall of alarm 603, switch 607 is installed to the outer wall of bee calling organ 606.
Referring to fig. 2, fig. 6 and fig. 7, an embodiment of the present invention: filter 701 is installed to main part 1's inside diapire, No. two water pump 702 are installed to filter 701's inner wall, No. two water pump 702's input extends filter 701's outer wall, filter chamber 711 is installed to filter 701's inner wall, the inner wall of filter chamber 711 is installed and is intercepted net 703 outer wall and run through and install inlet pipe 704, limiting plate 705 is installed to inlet pipe 704's inner wall, third spring 706 is installed to limiting plate 705's outer wall, drain pipe 707 is installed in filter 701's outer wall run through, storage box 708 is installed to main part 1's outer wall, electric putter 709 is installed to storage box 708's inner wall, push pedal 710 is installed to electric putter 709's one end.
Referring to fig. 5, an embodiment of the present invention: reset spring 801 is installed to the inside back wall of main part 1, and stabilizer plate 802 is installed to the inside back wall of main part 1, and hydraulic stem 803 is installed to the bottom of stabilizer plate 802, and spacing post 804 is installed to the bottom of hydraulic stem 803.
Further, the reaction device comprises the following working steps:
s1, firstly, putting the material on the feeding plate 102, pumping the solution by the first water pump 202, opening the first electric control valve 203 and the second electric control valve 204, filling the first cavity 3 and the second cavity 304, then, electrifying the heating wire 306 to dissipate heat, heating the solution by the cooperation with the metal rod 305, shortening the electric telescopic rod 302 to drive the sealing block 303 to leave the pipe orifice of the first telescopic pipe 307, leading the low-temperature solution in the first cavity 3 and the high-temperature solution in the second cavity 304 to enter the inside of the sprinkler 5, driving the reciprocating lead screw 401 to rotate by the first motor 4, driving the moving block 402 to rotate by the reciprocating lead screw 401, sliding the sliding block 404 on the sliding rod 403 to move the sprinkler 5, opening the control valve 502, pressurizing the sprinkler 5 by the pressurizing pump 405, leading the sprinkler 5 to spray the solution on the material through the sprinkler pipe 501, facilitating the reaction, detecting the temperature of the solution by the temperature sensor 504, when the temperature is too high or too low, the motor 508 drives the cam 509 to rotate, the cam 509 extrudes the lifting rod 506, the lifting rod 506 moves to drive the first spring 507 to extend, the lifting rod 506 is in contact with the conductive plate 510, and the conductive plate 510 controls the first electric control valve 203 and the second electric control valve 204, so that the temperature can be conveniently adjusted;
s2, when the content of the solution in the sprinkler 5 is reduced or is fully collected, the floating ball 602 moves along with the liquid level, the floating ball 602 drives the lifting block to slide on the outer wall of the vertical rod 601, the floating ball 602 extrudes the moving rod 604, the moving rod 604 moves to drive the second spring 605 to extend, and the moving rod 604 is in contact with the switch 607, so that the buzzer 606 gives out a sound to warn to realize a warning function;
s3, the inclined plate 7 is a net plate, so that larger impurities can be filtered, then, the reacted solution flows out through the water leakage holes and the filter screen 104, the second water pump 702 pumps the solution into the filter cavity 711 in the filter 701, then the electric push rod 709 extends to drive the push plate 710 to extrude the activated carbon in the storage tank 708 to enter the feed pipe 704, the activated carbon extrudes the limiting plate 705, the limiting plate 705 rotates to drive the third spring 706 to contract, the activated carbon enters the filter cavity 711 to adsorb the impurities in the solution, the drain pipe 707 is opened, the filtered solution is discharged and collected, and the purification and filtration functions of the solution are realized;
s4, the feeding plate 102 is placed above the supporting plate 8, then the feeding plate 102 is pushed to enter the main body 1, the feeding plate 102 extrudes the return spring 801, the return spring 801 contracts to store energy, then the hydraulic rod 803 extends to drive the limiting column 804 to be inserted into the front end of the return spring 801, so that the return spring 801 is in a contracted state, when the feeding plate 102 needs to be ejected, the hydraulic rod 803 contracts to enable the limiting column 804 to stop limiting the return spring 801, and the return spring 801 extends to drive the feeding plate 102 to eject.
The working principle is that firstly, a material is placed on the feeding plate 102, then the first water pump 202 pumps the solution, the first electric control valve 203 and the second electric control valve 204 are opened, the first cavity 3 and the second cavity 304 are filled, then the electric heating wire 306 is electrified to dissipate heat, the solution is heated by matching with the metal rod 305, the electric telescopic rod 302 shortens the pipe orifice for driving the sealing block 303 to leave the first telescopic pipe 307, so that the low-temperature solution in the first cavity 3 and the high-temperature solution in the second cavity 304 enter the inside of the sprinkler 5, the first motor 4 drives the reciprocating lead screw 401 to rotate, the reciprocating lead screw 401 rotates to drive the moving block 402 to rotate, the sliding block 404 slides on the sliding rod 403, the sprinkler 5 moves, the control valve 502 is opened, the pressure pump 405 pressurizes the sprinkler 5, so that the sprinkler 5 sprays the solution onto the material through the sprinkler pipe 501, the reaction is convenient, the temperature sensor 504 detects the temperature of the solution, when the temperature is too high or too low, the motor 508 drives the cam 509 to rotate, the cam 509 extrudes the lifting rod 506, the lifting rod 506 moves to drive the first spring 507 to extend, the lifting rod 506 is in contact with the conductive plate 510, and the conductive plate 510 controls the first electric control valve 203 and the second electric control valve 204, so that the temperature can be conveniently adjusted;
the inclined plate 7 is a mesh plate, so that larger impurities can be filtered, then, the reacted solution flows out through the water leakage holes and the filter screen 104, the second water pump 702 pumps the solution into the filter cavity 711 in the filter 701, then the electric push rod 709 extends to drive the push plate 710 to extrude the activated carbon in the storage tank 708 to enter the feed pipe 704, the activated carbon extrudes the limiting plate 705, the limiting plate 705 rotates to drive the third spring 706 to contract, the activated carbon enters the filter cavity 711, impurities in the solution are adsorbed, the drain pipe 707 is opened, the filtered solution is discharged and collected, and the purifying and filtering functions of the solution are realized;
the feeding plate 102 is placed above the supporting plate 8, then the feeding plate 102 is pushed to enter the main body 1, the feeding plate 102 extrudes the return spring 801, the return spring 801 contracts to store energy, then the hydraulic rod 803 extends to drive the limiting column 804 to be inserted into the front end of the return spring 801, so that the return spring 801 is in a contracted state, when the feeding plate 102 needs to be ejected, the hydraulic rod 803 contracts to enable the limiting column 804 to stop limiting the return spring 801, and the return spring 801 extends to drive the feeding plate 102 to eject.
It will be evident to those skilled in the art that the invention is not limited to the details of the foregoing illustrative embodiments, and that the present invention may be embodied in other specific forms without departing from the spirit or essential attributes thereof. The present embodiments are therefore to be considered in all respects as illustrative and not restrictive, the scope of the invention being indicated by the appended claims rather than by the foregoing description, and all changes which come within the meaning and range of equivalency of the claims are therefore intended to be embraced therein. Any reference sign in a claim should not be construed as limiting the claim concerned.
Claims (9)
1. The utility model provides a reaction unit that solid phase preparation used based on calcium titanate, includes main part (1), temperature control box (2), first motor (4) and swash plate (7), its characterized in that: the top of the main body (1) is provided with a temperature control box (2);
the display screen (201) is installed at the top of the temperature control box (2), the first water pump (202) is installed on the bottom wall inside the temperature control box (2), the water inlet pipe is installed at the input end of the first water pump (202), one end of the water inlet pipe extends out of the top of the temperature control box (2), the water outlet pipe is installed at the output end of the first water pump (202), and the first electric control valve (203) and the second electric control valve (204) are sequentially installed on the outer wall of the water outlet pipe;
chamber (3) are installed No. one to the inner wall of temperature control box (2), first motor (4) are installed to the outer wall of main part (1), and the output of first motor (4) extends into the inside of main part (1), swash plate (7) are installed to the inner wall of main part (1), backup pad (8) are installed to the inner wall of main part (1), and backup pad (8) are located the top of swash plate (7).
2. The reaction device for the solid-phase preparation based on calcium titanate according to claim 1, characterized in that: control screen (101) are installed in the front of main part (1), and the outer wall of main part (1) is equipped with the feed chute, and the inner wall of feed chute runs through and installs feed plate (102), and handle (103) are installed to the outer wall of feed plate (102), and the bottom of feed plate (102) is equipped with a plurality of holes that leak, and filter screen (104) are installed to the inner wall in the hole that leaks.
3. The reaction device for the solid-phase preparation based on calcium titanate according to claim 1, characterized in that: no. two chamber (304) are installed to the inner wall of temperature control box (2), waterproof case (301) are all installed to the inner wall in chamber (3) and No. two chamber (304), electric telescopic handle (302) are installed to the inner wall of waterproof case (301), and the one end of electric telescopic handle (302) extends the outer wall of waterproof case (301), sealing block (303) are installed to the one end of electric telescopic handle (302), metal pole (305) are installed to the nickel coin in No. two chamber (304), electric heating wire (306) are installed in encircleing of metal pole (305), the bottom in chamber (3) and No. two chamber (304) all runs through and installs one flexible pipe (307).
4. The reaction device for the solid-phase preparation based on calcium titanate according to claim 1, characterized in that: reciprocating screw rod (401) is installed to the output of first motor (4), the outer wall cover of reciprocating screw rod (401) is equipped with movable block (402), sprinkler (5) are installed to the bottom of movable block (402), slide bar (403) are installed to the inner wall of main part (1), slider (404) are installed to the outer wall of slide bar (403), and slider (404) and movable block (402) are connected the inner wall of main part (1) and are installed force (forcing) pump (405), flexible pipe No. two is installed to the output of force (forcing) pump (405), and the inside of sprinkler (5) is extended into to the one end of flexible pipe No. two.
5. The reaction device for the solid-phase preparation based on calcium titanate according to claim 4, characterized in that: the bottom of sprinkler (5) is run through and is installed spray pipe (501), control valve (502) are installed to the outer wall of spray pipe (501), detector (503) are installed to one side inner wall of sprinkler (5), temperature sensor (504) are installed to the outer wall of detector (503), two sets of fixed plates (505) are installed to the inner wall of detector (503), lifter (506) are run through and are installed at the top of fixed plate (505), first spring (507) are installed around to the outer wall of lifter (506), motor (508) are installed to the inner wall of detector (503), cam (509) are installed to the output of motor (508), electrically conductive plate (510) are all installed to the inside roof and the inside diapire of detector (503), gag lever post (6) are installed to the opposite side inner wall of sprinkler (5).
6. The reaction device for the solid-phase preparation based on calcium titanate according to claim 5, characterized in that: montant (601) are installed to the outer wall of gag lever post (6), the elevator is installed to the outer wall of montant (601), floater (602) are installed to the outer wall of elevator, alarm (603) are installed to the outer wall of sprinkler (5), the outer wall of alarm (603) runs through installs carriage release lever (604), the one end of carriage release lever (604) extends into the inside of sprinkler (5), the outer wall of carriage release lever (604) is encircleed and is installed second spring (605), two sets of bee calling organ (606) are installed to the inner wall of alarm (603), switch (607) is installed to the outer wall of bee calling organ (606).
7. The reaction device for the solid-phase preparation based on calcium titanate according to claim 1, characterized in that: filter (701) is installed to the inside diapire of main part (1), No. two water pump (702) are installed to the inner wall of filter (701), the outer wall of filter (701) is extended to the input of No. two water pump (702), filter chamber (711) are installed to the inner wall of filter (701), interception net (703) outer wall is installed to the inner wall of filter chamber (711) and is run through and install inlet pipe (704), limiting plate (705) are installed to the inner wall of inlet pipe (704), third spring (706) are installed to the outer wall of limiting plate (705), drain pipe (707) are installed to the outer wall of filter (701) through-mounting, bin (708) is installed to the outer wall of main part (1), electric putter (709) are installed to the inner wall of bin (708), push pedal (710) is installed to the one end of electric putter (709).
8. The reaction device for the solid-phase preparation based on calcium titanate according to claim 1, characterized in that: reset spring (801) are installed to the inside back wall of main part (1), and stabilizer plate (802) are installed to the inside back wall of main part (1), and hydraulic stem (803) are installed to the bottom of stabilizer plate (802), and spacing post (804) are installed to the bottom of hydraulic stem (803).
9. Reaction device for the solid phase preparation based on calcium titanate according to any one of claims 1 to 8, characterized in that it operates as follows:
s1, firstly, placing the material on a feeding plate (102), then pumping the solution by a first water pump (202), opening a first electric control valve (203) and a second electric control valve (204), filling a first cavity (3) and a second cavity (304), then electrifying a heating wire (306) for heat dissipation, matching with a metal rod (305) for heating the solution, shortening an electric telescopic rod (302) to drive a sealing block (303) to leave the pipe orifice of a first telescopic pipe (307), so that the low-temperature solution in the first cavity (3) and the high-temperature solution in the second cavity (304) enter the inside of a water sprayer (5), driving a reciprocating screw rod (401) to rotate by a first motor (4), driving a moving block (402) to rotate by the reciprocating screw rod (401), sliding a sliding block (404) on a sliding rod (403), moving the water sprayer (5), opening a control valve (502), and pressurizing pump (405) for pressurizing the water sprayer (5), the solution is sprayed onto the material through the water spraying pipe (501) by the water sprayer (5), reaction is convenient to carry out, the temperature of the solution is detected by the temperature sensor (504), when the temperature is too high or too low, the motor (508) drives the cam (509) to rotate, the cam (509) extrudes the lifting rod (506), the lifting rod (506) moves to drive the first spring (507) to extend, the lifting rod (506) is in contact with the conductive plate (510), and the conductive plate (510) controls the first electric control valve (203) and the second electric control valve (204), so that the temperature is convenient to adjust;
s2, when the content of the solution in the water sprayer (5) is reduced or is fully collected, the floating ball (602) moves along with the liquid level, the floating ball (602) drives the lifting block to slide on the outer wall of the vertical rod (601), the floating ball (602) extrudes the moving rod (604), the moving rod (604) moves to drive the second spring (605) to extend, and the moving rod (604) is in contact with the switch (607), so that the buzzer (606) gives out sound to warn and realize the warning function;
s3, the inclined plate (7) is a net plate, so that larger impurities can be filtered, the solution after reaction flows out through the water leakage holes and the filter screen (104), the second water pump (702) pumps the solution into the filter cavity (711) in the filter (701), the electric push rod (709) extends to drive the push plate (710) to extrude the activated carbon in the storage box (708) to enter the feeding pipe (704), the activated carbon extrudes the limiting plate (705), the limiting plate (705) rotates to drive the third spring (706) to contract, the activated carbon enters the filter cavity (711), the impurities in the solution are adsorbed, the drain pipe (707) is opened, the filtered solution is discharged and collected, and the purification and filtration functions of the solution are realized;
s4, the feeding plate (102) is placed above the supporting plate (8), then the feeding plate (102) is pushed to enter the main body (1), the feeding plate (102) extrudes the return spring (801), the return spring (801) contracts to store energy, then the hydraulic rod (803) extends to drive the limiting column (804) to be inserted into the front end of the return spring (801), the return spring (801) is in a contraction state, when the feeding plate (102) needs to be popped out, the hydraulic rod (803) contracts to enable the limiting column (804) not to limit the return spring (801), and the return spring (801) extends to drive the feeding plate (102) to pop out.
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| CN115121199B (en) | 2023-11-28 |
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