CN115054545B - Preparation process of skin care product containing truffle extract - Google Patents
Preparation process of skin care product containing truffle extract Download PDFInfo
- Publication number
- CN115054545B CN115054545B CN202210737931.4A CN202210737931A CN115054545B CN 115054545 B CN115054545 B CN 115054545B CN 202210737931 A CN202210737931 A CN 202210737931A CN 115054545 B CN115054545 B CN 115054545B
- Authority
- CN
- China
- Prior art keywords
- ring
- skin care
- care product
- wall
- tank body
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/90—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with paddles or arms
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F27/00—Mixers with rotary stirring devices in fixed receptacles; Kneaders
- B01F27/80—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis
- B01F27/91—Mixers with rotary stirring devices in fixed receptacles; Kneaders with stirrers rotating about a substantially vertical axis with propellers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/10—Maintenance of mixers
- B01F35/11—Maintenance of mixers using fluids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F35/00—Accessories for mixers; Auxiliary operations or auxiliary devices; Parts or details of general application
- B01F35/10—Maintenance of mixers
- B01F35/12—Maintenance of mixers using mechanical means
- B01F35/123—Maintenance of mixers using mechanical means using scrapers for cleaning mixers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
- B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
- B01F2101/21—Mixing of ingredients for cosmetic or perfume compositions
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Veterinary Medicine (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Chemical & Material Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Dermatology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Engineering & Computer Science (AREA)
- Biotechnology (AREA)
- Epidemiology (AREA)
- Gerontology & Geriatric Medicine (AREA)
- Birds (AREA)
- Botany (AREA)
- Mechanical Engineering (AREA)
- Cosmetics (AREA)
Abstract
The invention belongs to the technical field of cosmetics, and particularly relates to a process for preparing a skin care product containing a truffle extract, which comprises a tank body, a motor, a stirring rod, a paddle, a slip ring, an internal thread arc block, a cross arm and a telescopic sleeve rod; the motor drives the stirring rod to rotate to drive the paddle to rotate, and the mixed solution in the tank body is stirred and mixed to obtain a solution of the skin care product; after the solution of skin care products is discharged, a thicker layer of residual liquid is attached to the inner wall of the tank body, an operator meshes the internal thread arc-shaped block with a thread groove in the outer ring of the stirring rod, the motor drives the stirring rod to rotate, and the cross arm is guided by the telescopic sleeve rod to enable the internal thread arc-shaped block to be attached to the stirring rod to slide downwards and drive the cross arm to slide downwards, so that the telescopic sleeve rod is unfolded downwards to slide out, the inner wall of the tank body with the ring plate attached to the tank body is driven to slide, the residual liquid on the inner wall of the tank body is pushed to the bottom of the tank body to be discharged, the preparation amount of the skin care products solution is increased, and the waste rate of raw materials is reduced.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a preparation process of a skin care product containing a truffle extract.
Background
The skin care product is a product for protecting the skin, along with the continuous progress of social economy and the abundance of material life, people pay more and more attention to the maintenance of the skin per se, the skin care product has entered the daily life of people, and the skin care product plays a great role in improving the spirit and the image of people; the skin care product has the functions of beautifying, enhancing the elasticity and vitality of skin, enabling people to be light and beautiful in the year and improving the beautiful image of people.
A Chinese patent with publication number CN114043761B discloses a skin care product raw material mixing device containing plant extracts and a method thereof, which comprises a tank body, wherein a stirring and mixing mechanism is arranged in the bottom of the tank body, a primary squeezing mechanism is arranged outside the top of the tank body, the primary squeezing mechanism is used for preliminarily squeezing different plants, a secondary squeezing mechanism is arranged in the top of the tank body, the secondary squeezing mechanism is used for squeezing plant residues squeezed by the primary squeezing mechanism again, and the secondary squeezing mechanism comprises an outer filtering cylinder fixed in the top of the tank body and a squeezing piece coaxially rotating in the outer filtering cylinder; according to the invention, plant raw materials are premixed through the stirring and mixing mechanism, the plant raw materials are preliminarily squeezed through the primary squeezing mechanism, and squeezed residues are squeezed twice through the secondary squeezing mechanism and the tertiary squeezing mechanism, so that the squeezing effect on the plant raw materials is improved, the extracting solution contained in the squeezed plant residues is effectively reduced, and the waste of materials is avoided.
When the skin care product is prepared, various raw materials of the skin care product are subjected to mixing reaction in a mixing tank, after the skin care product finished product is discharged, a layer of thick residual liquid is attached to the inner wall of the mixing tank, workers are required to manually scrape the attached residual liquid, otherwise, great waste is caused, and the yield of the product is reduced.
Therefore, the invention provides a preparation process of a skin care product containing the truffle extract.
Disclosure of Invention
To remedy the deficiencies of the prior art, at least one of the technical problems set forth in the background is addressed.
The technical scheme adopted by the invention for solving the technical problems is as follows: the invention relates to a skin care product containing a truffle extract, which is characterized by comprising the following components in parts by weight: the skin care product is prepared from the following raw materials in parts by weight:
1-5 parts of truffle extract
43-96 parts of tremella extract
1-5 parts of glycerol;
the skin care product is an emulsion, and the added truffle extract improves the whitening and skin aging delaying effects of the skin care product; the tremella fuciformis extract has the effects of smoothing skin textures, super-strong water replenishing and moisturizing effects, and can condition the skin complexion and smooth the skin;
the skin care product prepared by matching various components, particularly the truffle extract, can effectively improve the skin whitening, delay the skin aging, relax and condition the skin, improve the skin vitality and enable the skin of a user to be vigorous.
A skin care product preparation process containing a truffle extract is suitable for the skin care product, and comprises the following steps:
s1: adding the truffle extract, the tremella extract and the glycerol into a mixing tank in proportion, heating to 70 ℃, and stirring and emulsifying;
s2: after stirring and emulsifying, continuing stirring, cooling and simultaneously extracting air in the mixing tank;
s3: stopping stirring when the temperature is reduced to 40 ℃, and standing and aging for more than 24 hours;
s4: and discharging the obtained skin care product stock solution out of the mixing tank, detecting, and filling after the detection is qualified to obtain a finished product.
Preferably, the preparation process of the truffle extract comprises the following steps:
s1: cleaning the white truffle by ultrasonic waves, and crushing and grinding the cleaned white truffle to obtain white truffle powder;
s2: mixing the white truffle powder into purified water, uniformly stirring, and simultaneously heating to 50 ℃ to obtain a mixed solution;
s3: filtering solid part in the mixed solution, and filtering the filtered solution through a nano filter membrane with pore diameter of 0.5-0.2 μm to obtain the truffle extract.
Preferably, the preparation process of the tremella extract comprises the following steps:
s1: washing tremella with water, drying the surface of the tremella, drying, grinding and extruding the tremella to obtain tremella powder;
s2: adding the tremella powder into an ethanol solution for soaking, and taking out insoluble substances in the solution;
s3: adding insoluble substances into theobromine water solution, freezing and centrifuging to obtain primary leaching solution, and adding water for leaching to obtain secondary leaching solution;
s4: taking the supernatant of the two leaching solutions, standing, and centrifugally separating to obtain a precipitate to obtain the tremella extract.
Preferably, the mixing tank comprises a tank body, a motor, a stirring rod and a blade; the top surface of the tank body is bolted with a motor, a rotating shaft of the motor is fixedly connected with a stirring rod, the stirring rod rotatably penetrates through the top wall of the tank body, the bottom end of the stirring rod is fixedly connected with a paddle, the outer wall of the stirring rod is provided with a threaded groove, the outer ring of the stirring rod is sleeved with a sliding ring, the inner ring of the sliding ring is provided with a plurality of internal thread arc-shaped blocks, the inner wall of each internal thread arc-shaped block is in threaded fit with the threaded groove, the outer ring of the sliding ring is fixedly connected with a plurality of transverse arms, the outer rings of the transverse arms are fixedly connected with a ring plate, the outer rings of the ring plate are in sliding fit with the inner wall of the tank body, the top surface of the tank body is fixedly connected with a plurality of telescopic sleeve rods, the inner rods of the telescopic sleeve rods slidably penetrate through the top wall of the tank body, and the bottom ends of the telescopic sleeve rods are fixedly connected with the top surfaces of the middle parts of the transverse arms; after the solution of the skin care product is prepared in the mixing tank, a layer of thick residual liquid is attached to the inner wall of the mixing tank after the solution of the skin care product is discharged; during operation, the motor drive puddler rotates, it is rotatory to drive the paddle, stir the mixed solution of internal portion of jar and mix, thereby obtain the solution of skin care products, after the solution of skin care products is discharged, thick one deck raffinate adheres to on the inner wall of jar body, the staff meshes the thread groove of internal thread arc piece and puddler outer lane, the motor rotates, it rotates to drive the puddler, because the xarm receives the direction that blocks of flexible loop bar, make internal thread arc piece laminating puddler slide down, drive the xarm and slide down, make flexible loop bar expand the roll-off downwards, it slides to drive the inner wall of the ring plate laminating jar body, push away the bottom of the jar body with adnexed raffinate on the internal wall of jar, thereby the preparation volume of skin care products solution has been improved, the unrestrained rate of raw materials has then been reduced.
Preferably, the inner ring of the slip ring is provided with a plurality of mounting grooves, the mounting grooves correspond to the cross arm one to one, the internal thread arc-shaped block is slidably mounted inside the mounting grooves, the middle of one end, close to the slip ring, of the cross arm is provided with a sliding hole, the sliding hole penetrates through the mounting grooves, the inner wall of the sliding hole is slidably provided with a push rod, the end head of the push rod is fixedly connected with the middle of the convex surface of the internal thread arc-shaped block, the other end of the push rod is fixedly connected with the sliding hole through a tension spring, the inside of the telescopic loop bar is provided with a water hole, the top end of the water hole is communicated with a high-pressure water pump, and the bottom end of the water hole is communicated with the sliding hole; the during operation, after skin care products solution preparation is accomplished, in the water hole was gone into through high pressure water pump high pressure water flow, the inside of slide opening is got into in the water hole at the flexible loop bar middle part of high pressure rivers, high pressure rivers promote the inside cunning of push rod from the slide opening to the inside of mounting groove, the push rod promotes the inside roll-off of internal thread arc piece from the mounting groove, make the thread groove meshing of internal thread arc piece and puddler outer lane, thereby staff's the operation difficulty degree has been reduced, the probability that the staff opened the jar body has been reduced simultaneously, the probability that skin care products solution takes place to pollute has been reduced.
Preferably, a sealing sheet is fixedly connected to one end, far away from the sliding ring, of the push rod, the outer ring of the sealing sheet is in sliding fit with the inner wall of the sliding hole, a plurality of connecting holes are formed between the convex surface of the internal thread arc-shaped block and the inner wall of the mounting groove, and a connecting rod is slidably mounted between the connecting holes at two ends; when the sealing piece is in work, when the push rod is pushed to slide by high-pressure water flow, the sealing piece is extruded by the high-pressure water flow, so that the outer ring of the sealing piece extrudes the inner wall of the sliding hole, a gap between the sliding hole and the push rod is sealed, and the probability of leakage of the high-pressure water flow is reduced; through connecting rod sliding connection internal thread arc piece and mounting groove to improved the driven intensity of the thread groove meshing of internal thread arc piece and puddler outer lane, reduced the probability that the internal thread arc piece takes place to break away from.
Preferably, an embedding ring is fixedly connected to the inner wall of the top of the tank body, an arc-shaped chamfer is arranged at the bottom of the inner ring of the embedding ring, an arc-shaped elastic plate is fixedly connected to the outer ring of the top of the ring plate, the outer wall of the arc-shaped elastic plate is in sliding fit with the inner wall of the embedding ring, an annular elastic scraper is fixedly connected to the bottom surface of the arc-shaped elastic plate, and the outer ring of the annular elastic scraper is in sliding fit with the inner wall of the tank body; when the skin care product liquid preparation device works, after the skin care product liquid is prepared, the motor drives the ring plate to slide downwards to drive the arc elastic plate to slide downwards to be separated from the inlaid ring, the arc elastic plate resets to drive the annular elastic scraper to be stretched completely, so that the annular elastic scraper is attached to the inner wall of the tank body, and the annular elastic scraper scrapes attached residual liquid; when the skin care product solution is prepared, the outer wall of the arc elastic plate is contacted with the inner wall of the inlaying ring, so that the arc elastic plate is stressed by bending towards the inner side, the annular plate is fixed on the inner ring of the inlaying ring, the probability that the inlaying ring and the cross arm slide downwards is reduced, and the influence on the preparation of the skin care product solution is reduced.
Preferably, a water pipe is embedded in the middle of one end, away from the slip ring, of the cross arm, one end of the water pipe is communicated with the slip ring, a water cavity is formed in the annular plate, the other end of the water pipe is communicated with the water cavity, a plurality of water spraying holes are formed in the outer ring of the annular plate and are communicated with the water cavity, and a remote control ball float is arranged in the middle of the water pipe; during operation, after the attached raffinate is discharged, the remote control ball-cock assembly is controlled to open for high-pressure rivers pass through the water pipe and get into the water cavity, and high-pressure rivers are followed the high-speed blowout of hole for water, and rivers erode the inside of the jar body, wash the inner wall of the jar body and the internal part of jar, thereby accomplish the cleaning work to the agitator tank, reduced staff's the washing degree of difficulty.
Preferably, a baffle is fixedly connected to the outer ring of the bottom end of the stirring rod, and an elastic rod is fixedly connected to the outer ring of the baffle; when the skin care product solution mixing device works, the motor drives the stirring rod to rotate and drives the blades to rotate, so that the elastic rod is unfolded and rotated outwards under the action of centrifugal force, and the mixing and stirring effects of the solution are further improved; when the skin care product solution is prepared and the ring plate slides downwards to clean the residual liquid, the baffle blocks the sliding ring from sliding downwards, so that the probability of impacting the blades is reduced, and the safety of cleaning the residual liquid is improved.
The invention has the following beneficial effects:
1. according to the skin care product containing the truffle extract and the preparation process thereof, the skin care product prepared by matching various components, particularly the truffle extract, improves the whitening and skin aging delaying effects of the skin care product, and the tremella extract has the effects of smoothing skin textures, superstrong water replenishing and moisturizing effects, can condition the complexion of the skin and smooth the skin feel;
2. the invention relates to a skin care product containing a truffle extract and a preparation process thereof, wherein the skin care product is prepared by arranging a slip ring, an internal thread arc block, a cross arm and a telescopic loop bar; after the solution of the skin care product is discharged, a thick layer of residual liquid is attached to the inner wall of the tank body, the inner thread arc-shaped block is meshed with a thread groove in the outer ring of the stirring rod by a worker, the motor rotates to drive the stirring rod to rotate, and the cross arm is blocked and guided by the telescopic sleeve rod, so that the inner thread arc-shaped block is attached to the stirring rod to slide downwards, the inner wall of the tank body attached to the ring plate is driven to slide, the residual liquid attached to the inner wall of the tank body is pushed to the bottom of the tank body, the preparation amount of the skin care product solution is increased, and the waste rate of raw materials is reduced.
Drawings
The invention will be further described with reference to the accompanying drawings.
FIG. 1 is a perspective view of a first embodiment of the present invention;
FIG. 2 is a cross-sectional view of a first embodiment of the present invention;
FIG. 3 is an enlarged view of a portion A of FIG. 2;
FIG. 4 is an enlarged view of a portion of FIG. 3 at B;
FIG. 5 is an enlarged view of a portion of FIG. 3 at C;
FIG. 6 is a cross-sectional view of a second embodiment of the present invention;
FIG. 7 is a flow chart of a skin care product manufacturing process of the present invention;
FIG. 8 is a flow chart of the preparation process of the truffle extract of the present invention;
fig. 9 is a flow chart of the tremella extract preparation process of the present invention;
in the figure: 1. a tank body; 2. a motor; 3. a stirring rod; 4. a paddle; 5. a thread groove; 6. a slip ring; 7. an inner thread arc block; 8. a cross arm; 9. a ring plate; 10. a telescopic loop bar; 11. mounting grooves; 12. a slide hole; 13. a push rod; 14. a tension spring; 15. a water pore; 16. sealing the sheet; 17. connecting holes; 18. a connecting rod; 19. inlaying a ring; 20. an arc-shaped elastic plate; 21. an annular elastic scraper; 22. a water pipe; 23. a water chamber; 24. a water spray hole; 25. remotely controlling the float valve; 26. a baffle plate; 27. an elastic rod.
Detailed Description
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further described with the specific embodiments.
Example one
The skin care product containing the truffle extract provided by the embodiment of the invention comprises the following raw materials in parts by weight:
1-5 parts of truffle extract
43-96 parts of tremella extract
1-5 parts of glycerol;
the skin care product is an emulsion liquid, and the added truffle extract improves the whitening and skin aging delaying effects of the skin care product; the tremella extract has the effects of smoothing skin textures, super-strong water-replenishing and moisture-preserving effects, and can condition skin complexion and smooth skin feeling;
the skin care product prepared by matching various components, particularly the truffle extract, can effectively improve the skin whitening, delay the skin aging, relax and condition the skin, improve the skin vitality and enable the skin of a user to be vigorous.
As shown in fig. 7, a process for preparing a skin care product containing a truffle extract is suitable for the skin care product, and comprises the following steps:
s1: adding the truffle extract, the tremella extract and the glycerol into a mixing tank in proportion, heating to 70 ℃, and stirring and emulsifying;
s2: after stirring and emulsifying, continuing stirring, cooling and simultaneously extracting air in the mixing tank;
s3: stopping stirring when the temperature is reduced to 40 ℃, and standing and aging for more than 24 hours;
s4: and discharging the obtained skin care product stock solution out of the mixing tank, detecting, and filling after the detection is qualified to obtain a finished product.
As shown in fig. 8, the preparation process of the truffle extract comprises the following steps:
s1: cleaning the white truffle by ultrasonic waves, and crushing and grinding the cleaned white truffle to obtain white truffle powder;
s2: mixing the white truffle powder into purified water, uniformly stirring, and simultaneously heating to 50 ℃ to obtain a mixed solution;
s3: filtering solid part in the mixed solution, and filtering the filtered solution through a nano-filtration membrane with pore diameter of 0.5-0.2 μm to obtain the truffle extract.
As shown in fig. 9, the preparation process of the tremella extract includes the following steps:
s1: washing tremella with water, drying the surface of the tremella, drying, grinding and extruding the tremella to obtain tremella powder;
s2: adding the tremella powder into an ethanol solution for soaking, and taking out insoluble substances in the solution;
s3: adding insoluble substances into theobromine water solution, freezing and centrifuging to obtain primary leaching solution, and adding water for leaching to obtain secondary leaching solution;
s4: taking the supernatant of the two leaching solutions, standing, and centrifugally separating to obtain a precipitate to obtain the tremella extract.
As shown in fig. 1 to 5, the mixing tank includes a tank body 1, a motor 2, a stirring rod 3 and a blade 4; a motor 2 is bolted on the top surface of the tank body 1, a stirring rod 3 is fixedly connected to a rotating shaft of the motor 2, the stirring rod 3 rotatably penetrates through the top wall of the tank body 1, a paddle 4 is fixedly connected to the bottom end of the stirring rod 3, a threaded groove 5 is formed in the outer wall of the stirring rod 3, a sliding ring 6 is sleeved on the outer ring of the stirring rod 3, a plurality of internal thread arc blocks 7 are arranged on the inner ring of the sliding ring 6, the inner wall of each internal thread arc block 7 is in threaded fit with the threaded groove 5, a plurality of transverse arms 8 are fixedly connected to the outer ring of the sliding ring 6, a ring plate 9 is fixedly connected to the outer rings of the transverse arms 8, the outer ring of the ring plate 9 is in sliding fit with the inner wall of the tank body 1, a plurality of telescopic sleeve rods 10 are fixedly connected to the top surface of the tank body 1, the inner rods of the telescopic sleeve rods 10 slidably penetrate through the top wall of the tank body 1, and the bottom ends of the transverse arms of the telescopic sleeve rods 10 are fixedly connected to the top wall of the middle part of the tank body 8; after the solution of the skin care product is manufactured in the mixing tank, a layer of thick residual liquid is attached to the inner wall of the mixing tank after the solution of the skin care product is discharged; during operation, motor 2 drive puddler 3 rotates, it is rotatory to drive paddle 4, stir the mixed solution of jar internal portion 1, thereby obtain the solution of skin care products, after the solution of skin care products is discharged, thick one deck raffinate adheres to on the inner wall of jar body 1, the staff meshes internal thread arc 7 with thread groove 5 of puddler 3 outer lane, motor 2 rotates, drive puddler 3 rotates, because xarm 8 receives the direction that blocks of flexible loop bar 10, make internal thread arc 7 laminate puddler 3 and slide downwards, drive xarm 8 and slide downwards, make flexible loop bar 10 expand the roll-off downwards, drive the inner wall of ring plate 9 laminating jar body 1 and slide, push the bottom of jar body 1 with the adnexed raffinate on jar body 1 inner wall, thereby the preparation volume of skin care products solution has been improved, the unrestrained rate of raw materials has been reduced then.
As shown in fig. 3 to 4, the inner ring of the slip ring 6 is provided with a plurality of mounting grooves 11, the mounting grooves 11 correspond to the cross arm 8 one to one, the internal thread arc block 7 is slidably mounted inside the mounting groove 11, a sliding hole 12 is formed in the middle of one end of the cross arm 8 close to the slip ring 6, the sliding hole 12 penetrates through the mounting groove 11, a push rod 13 is slidably mounted on the inner wall of the sliding hole 12, the end of the push rod 13 is fixedly connected with the middle of the convex surface of the internal thread arc block 7, a tension spring 14 is fixedly connected between the other end of the push rod 13 and the sliding hole 12, a water hole 15 is formed inside the telescopic loop bar 10, the top end of the water hole 15 is communicated with the high-pressure water pump, and the bottom end of the water hole 15 is communicated with the sliding hole 12; the during operation, after skin care products solution preparation is accomplished, in water hole 15 is gone into through high pressure water pump high pressure water flow, the water hole 15 at high pressure rivers telescopic sleeve pole 10 middle part gets into the inside of slide opening 12, high pressure rivers promote push rod 13 from the inside of slide opening 12 inside to mounting groove 11, push rod 13 promotes the inside roll-off of internal thread arc piece 7 from mounting groove 11, make the 5 meshing of thread groove of internal thread arc piece 7 and 3 outer lanes of puddler, thereby staff's the operation difficulty has been reduced, the probability that the staff opened jar body 1 has been reduced simultaneously, skin care products solution emergence pollution's probability has been reduced.
As shown in fig. 4, a sealing piece 16 is fixedly connected to one end of the push rod 13 away from the slip ring 6, an outer ring of the sealing piece 16 is in sliding fit with an inner wall of the sliding hole 12, a plurality of connecting holes 17 are formed between a convex surface of the internal thread arc block 7 and the inner wall of the mounting groove 11, and a connecting rod 18 is slidably mounted between the connecting holes 17 at two ends; when the high-pressure water flow sealing device works, when the push rod 13 is pushed to slide by the high-pressure water flow, the sealing sheet 16 is squeezed by the high-pressure water flow, so that the outer ring of the sealing sheet 16 squeezes the inner wall of the sliding hole 12, a gap between the sliding hole 12 and the push rod 13 is sealed, and the probability of leakage of the high-pressure water flow is reduced; through connecting rod 18 sliding connection internal thread arc piece 7 and mounting groove 11 to improved internal thread arc piece 7 and the driven intensity of the thread groove 5 meshing of puddler 3 outer lane, reduced the probability that internal thread arc piece 7 takes place to break away from.
As shown in fig. 3 and 5, an inlaid ring 19 is fixedly connected to the inner wall of the top of the tank body 1, an arc-shaped chamfer is arranged at the bottom of the inner ring of the inlaid ring 19, an arc-shaped elastic plate 20 is fixedly connected to the outer ring of the top of the ring plate 9, the outer wall of the arc-shaped elastic plate 20 is in sliding fit with the inner wall of the inlaid ring 19, an annular elastic scraper 21 is fixedly connected to the bottom surface of the arc-shaped elastic plate 20, and the outer ring of the annular elastic scraper 21 is in sliding fit with the inner wall of the tank body 1; when the skin care product liquid preparation device works, after the skin care product liquid is prepared, the motor 2 drives the ring plate 9 to slide downwards to drive the arc elastic plate 20 to slide downwards to be separated from the inlaid ring 19, the arc elastic plate 20 resets to drive the annular elastic scraper 21 to be stretched completely, so that the annular elastic scraper 21 is attached to the inner wall of the tank body 1, and the annular elastic scraper 21 scrapes off attached residual liquid; when the skin care product solution is prepared, the outer wall of the arc elastic plate 20 is in contact with the inner wall of the inlaid ring 19, so that the arc elastic plate 20 is subjected to inward bending stress, the ring plate 9 is fixed at the inner ring of the inlaid ring 19, the probability that the inlaid ring 19 and the cross arm 8 slide downwards is reduced, and the influence on the preparation of the skin care product solution is reduced.
As shown in fig. 5, a water pipe 22 is embedded in the middle of one end of the cross arm 8 far away from the slip ring 6, one end of the water pipe 22 is communicated with the slip hole 12, a water cavity 23 is formed inside the annular plate 9, the other end of the water pipe 22 is communicated with the water cavity 23, a plurality of water spray holes 24 are formed in the outer ring of the annular plate 9, the water spray holes 24 are communicated with the water cavity 23, and a remote control ball float 25 is arranged in the middle of the water pipe 22; during operation, after the discharge of adnexed raffinate, control remote control ball-cock assembly 25 is opened for high-pressure rivers pass through water pipe 22 and get into in the water cavity 23, and high-pressure rivers are followed the high-speed blowout of hole for water jet 24, and rivers wash the inside of jar body 1, wash the inner wall of jar body 1 and the inside part of jar body 1, thereby accomplish the cleaning work to the agitator tank, reduced staff's the washing degree of difficulty.
As shown in fig. 6, a baffle 26 is fixedly connected to an outer ring of a bottom end of the stirring rod 3, and an elastic rod 27 is fixedly connected to an outer ring of the baffle 26; when the skin care product solution mixing device works, the motor 2 drives the stirring rod 3 to rotate and drives the blades 4 to rotate, so that the elastic rod 27 is expanded and rotated outwards under the action of centrifugal force, and the mixing and stirring effects of the solution are further improved; when the ring plate 9 slides downwards to clean the residual liquid after the skin care product solution is prepared, the baffle 26 blocks the sliding ring 6 from sliding downwards, so that the probability of impacting the blades 4 is reduced, and the safety of cleaning the residual liquid is improved.
Example two
Comparative example one, wherein another embodiment of the present invention is: the skin care product containing the truffle extract is prepared from the following raw materials in parts by weight:
1 part of truffle extract
60 parts of tremella extract
3 parts of glycerol;
according to the formula, the manufacturing process of the skin care product in the second embodiment is the same as that in the first embodiment.
The obtained skin care product is uniformly divided into 5 parts, and the 5 parts are respectively provided for 5 volunteers to use; after 30 days, skin melanin of 5 volunteers was measured, and as a result, the value of skin melanin after use was reduced by 10% on average as compared with the value of skin melanin when not used.
EXAMPLE III
A first comparative example, wherein another embodiment of the present invention is: the skin care product containing the truffle extract is prepared from the following raw materials in parts by weight:
60 parts of tremella extract
3 parts of glycerol;
according to the formula, the manufacturing process of the skin care product in the third embodiment is the same as that in the first embodiment.
The obtained skin care product is uniformly divided into 5 parts, and the 5 parts are respectively provided for 5 volunteers to use; after 30 days, skin melanin of the skin of 5 volunteers was detected, and the value of skin melanin after use was reduced by 17% on average as compared with that of skin melanin when not used.
Example four
A first comparative example, wherein another embodiment of the present invention is: the skin care product containing the truffle extract is prepared from the following raw materials in parts by weight:
5 parts of truffle extract
60 parts of tremella extract
3 parts of glycerol;
according to the formula, the manufacturing process of the skin care product in the fourth embodiment is the same as that in the first embodiment.
The obtained skin care product is uniformly divided into 5 parts, and the 5 parts are respectively provided for 5 volunteers to use; after 30 days, skin melanin of the skin of 5 volunteers was detected, and the value of skin melanin after use was reduced by 25% on average as compared with the value of skin melanin when not used.
EXAMPLE five
Comparative example one, wherein another embodiment of the present invention is: the skin care product containing the truffle extract is prepared from the following raw materials in parts by weight:
10 parts of truffle extract
60 parts of tremella extract
3 parts of glycerol;
according to the formula, the manufacturing process of the skin care product in the fifth embodiment is the same as that in the first embodiment.
The obtained skin care product is uniformly divided into 5 parts, and the 5 parts are respectively provided for 5 volunteers to use; after 30 days, skin melanin of 5 volunteers was measured, and as a result, the value of skin melanin after use was reduced by 40% on average as compared with that of skin melanin when not used.
Through comparison of the second to fifth examples, it is known that the higher the content of the truffle extract in the skin care product is, the better the whitening effect of the skin care product is, but since the truffle is expensive, the higher the content of the truffle extract is, the higher the preparation cost of the skin care product is, the best weight part of the truffle extract in the skin care product is 1-5 parts.
When in work: adding the truffle extract, the tremella extract and the glycerol into a mixing tank in proportion; at this time, the tension spring 14 pulls the push rod 13 to be positioned inside the slide hole 12, so that the internal thread arc-shaped block 7 is positioned inside the mounting groove 11, and the internal thread arc-shaped block 7 is separated from the thread groove 5 on the outer ring of the stirring rod 3; meanwhile, the outer wall of the arc-shaped elastic plate 20 is in contact with the inner wall of the inlaid ring 19, so that the arc-shaped elastic plate 20 is bent inwards to bear force, the ring plate 9 is fixed on the inner ring of the inlaid ring 19, and the probability that the inlaid ring 19 and the cross arm 8 slide downwards is reduced; the motor 2 drives the stirring rod 3 to rotate, drives the paddle 4 to rotate, and stirs and mixes the mixed solution in the tank body 1, so that the solution of the skin care product is obtained;
after the skin care product liquid is discharged, a layer of thicker residual liquid is attached to the inner wall of the tank body 1; high-pressure water of the high-pressure water pump flows into the water hole 15, the water hole 15 in the middle of the high-pressure water flow telescopic sleeve rod 10 enters the inside of the sliding hole 12, the high-pressure water flow pushes the push rod 13 to slide from the inside of the sliding hole 12 to the inside of the mounting groove 11, so that the tension spring 14 is stretched, the push rod 13 pushes the internal thread arc-shaped block 7 to slide out from the inside of the mounting groove 11, and the internal thread arc-shaped block 7 is meshed with the thread groove 5 in the outer ring of the stirring rod 3;
the motor 2 drives the stirring rod 3 to rotate, and the cross arm 8 is blocked and guided by the telescopic loop bar 10, so that the internal thread arc-shaped block 7 is attached to the stirring rod 3 to slide downwards, the cross arm 8 is driven to slide downwards, the telescopic loop bar 10 is unfolded and slides downwards, the ring plate 9 is driven to slide downwards, the arc-shaped elastic plate 20 is driven to slide downwards to be separated from the embedded ring 19, the arc-shaped elastic plate 20 is reset, the annular elastic scraper 21 is driven to be completely stretched, the annular elastic scraper 21 is attached to the inner wall of the tank body 1, the annular elastic scraper 21 scrapes attached residual liquid, and the residual liquid attached to the inner wall of the tank body 1 is pushed to the bottom of the tank body 1, so that the preparation amount of the skin care product solution is increased, and the waste rate of raw materials is reduced;
when the attached residual liquid is discharged, the remote control ball float valve 25 is controlled to be opened, so that high-pressure water flow enters the water cavity 23 through the water pipe 22, the high-pressure water flow is sprayed out from the water spraying holes 24 at a high speed, the water flow washes the inside of the tank body 1, the inner wall of the tank body 1 and parts inside the tank body 1 are washed, the cleaning work of the stirring tank is completed, and the cleaning difficulty of workers is reduced.
The front, the back, the left, the right, the upper and the lower are all based on figure 1 in the attached drawings of the specification, according to the standard of the observation angle of a person, the side of the device facing an observer is defined as the front, the left side of the observer is defined as the left, and the like.
In the description of the present invention, it is to be understood that the terms "center", "longitudinal", "lateral", "front", "rear", "left", "right", "vertical", "horizontal", "top", "bottom", "inner", "outer", etc. indicate orientations or positional relationships based on those shown in the drawings, and are merely intended to facilitate the description of the present invention and to simplify the description, but do not indicate or imply that the device or element referred to must have a particular orientation, be constructed and operated in a particular orientation, and therefore should not be construed as limiting the scope of the present invention.
The foregoing shows and describes the general principles, principal features and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (5)
1. A manufacturing process of a skin care product containing a truffle extract is characterized in that: the skin care product is prepared from the following raw materials in parts by weight:
1-5 parts of truffle extractive
43-96 parts of tremella extract
1-5 parts of glycerol;
the manufacturing process of the skin care product comprises the following steps:
s1: adding the truffle extract, the tremella extract and the glycerol into a mixing tank in proportion, heating to 70 ℃, and stirring and emulsifying;
s2: after stirring and emulsifying, continuously stirring, cooling, and simultaneously extracting air in the mixing tank;
s3: stopping stirring when the temperature is reduced to 40 ℃, and standing and aging for more than 24 hours;
s4: discharging the obtained skin care product stock solution out of the mixing tank, detecting, and filling after the detection is qualified to obtain a finished product;
the preparation process of the truffle extract comprises the following steps:
s1: cleaning the white truffle by ultrasonic waves, and crushing and grinding the cleaned white truffle to obtain white truffle powder;
s2: mixing the white truffle powder into purified water, uniformly stirring, and simultaneously heating to 50 ℃ to obtain a mixed solution;
s3: filtering solid part in the mixed solution, and filtering the filtered solution through a nano filter membrane with pore diameter of 0.5-0.2 μm to obtain the truffle extract;
the preparation process of the tremella extract comprises the following steps:
s1: washing tremella, drying water on the surface of the tremella, drying, grinding and extruding the tremella to obtain tremella powder;
s2: adding tremella powder into ethanol solution for soaking, and taking out insoluble substances in the solution;
s3: adding insoluble substances into theobromine water solution, freezing and centrifuging to obtain primary leaching solution, and adding water for leaching to obtain secondary leaching solution;
s4: taking the supernatant of the two leaching solutions, standing, and centrifuging to obtain a precipitate to obtain a tremella extract;
the mixing tank comprises a tank body (1), a motor (2), a stirring rod (3) and a blade (4); the tank is characterized in that a motor (2) is bolted on the top surface of the tank body (1), a stirring rod (3) is fixedly connected to a rotating shaft of the motor (2), the stirring rod (3) rotates to penetrate through the top wall of the tank body (1), a paddle (4) is fixedly connected to the bottom end of the stirring rod (3), a thread groove (5) is formed in the outer wall of the stirring rod (3), a sliding ring (6) is sleeved on the outer ring of the stirring rod (3), a plurality of internal thread arc blocks (7) are arranged on the inner ring of the sliding ring (6), the inner wall of each internal thread arc block (7) is in threaded fit with the thread groove (5), a plurality of transverse arms (8) are fixedly connected to the outer ring of the sliding ring (8), a ring plate (9) is fixedly connected to the outer ring of the transverse arms (8), the outer ring of the ring plate (9) is in sliding fit with the inner wall of the tank body (1), a plurality of telescopic sleeve rods (10) are arranged on the top surface of the tank body (1), and the inner rods of the telescopic sleeve rods (10) slide to penetrate through the top wall of the tank body (1), and the bottom end of the transverse arms (8) is fixedly connected with the top surface of the middle of the top surface of the telescopic sleeve rod (8);
the inner ring of the slip ring (6) is provided with a plurality of mounting grooves (11), the mounting grooves (11) correspond to cross arms (8) one by one, the internal thread arc-shaped blocks (7) are slidably mounted inside the mounting grooves (11), the middle part of one end, close to the slip ring (6), of each cross arm (8) is provided with a sliding hole (12), each sliding hole (12) penetrates through the corresponding mounting groove (11), push rods (13) are slidably mounted on the inner walls of the corresponding sliding holes (12), the ends of the push rods (13) are fixedly connected with the middle parts of convex surfaces of the internal thread arc-shaped blocks (7), tension springs (14) are fixedly connected between the other ends of the push rods (13) and the sliding holes (12), water holes (15) are formed inside the telescopic sleeved rods (10), the top ends of the water holes (15) are communicated with a high-pressure water pump, and the bottom ends of the water holes (15) are communicated with the sliding holes (12);
2. the process for preparing a skin care product containing the truffle extract according to claim 1, wherein the process comprises the following steps: one end of the push rod (13) far away from the sliding ring (6) is fixedly connected with a sealing sheet (16), the outer ring of the sealing sheet (16) is in sliding fit with the inner wall of the sliding hole (12), a plurality of connecting holes (17) are formed between the convex surface of the internal thread arc-shaped block (7) and the inner wall of the mounting groove (11), and connecting rods (18) are slidably mounted between the connecting holes (17).
3. The process for preparing a skin care product containing the truffle extract according to claim 2, wherein the process comprises the following steps: the top inner wall rigid coupling of the jar body (1) has inlays ring (19), the inner circle bottom of inlaying ring (19) is provided with the arc chamfer, the top outer lane rigid coupling of crown plate (9) has arc diving board (20), the outer wall of arc diving board (20) and the inner wall sliding fit who inlays ring (19), the bottom surface rigid coupling of arc diving board (20) has annular elasticity scraper blade (21), the outer lane of annular elasticity scraper blade (21) and the inner wall sliding fit of the jar body (1).
4. The process for preparing a skin care product containing a truffle extract according to claim 1, wherein the process comprises the following steps: a water pipe (22) is buried in the middle of one end, far away from the slip ring (6), of the cross arm (8), one end of the water pipe (22) is communicated with the sliding hole (12), a water cavity (23) is formed in the inner portion of the ring plate (9), the other end of the water pipe (22) is communicated with the water cavity (23), a plurality of water spraying holes (24) are formed in the outer ring of the ring plate (9), the water spraying holes (24) are communicated with the water cavity (23), and a remote control ball float valve (25) is arranged in the middle of the water pipe (22).
5. The process for preparing a skin care product containing a truffle extract according to claim 1, wherein the process comprises the following steps: the bottom end outer ring of puddler (3) rigid coupling has baffle (26), the outer lane rigid coupling of baffle (26) has flexible pole (27).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210737931.4A CN115054545B (en) | 2022-06-27 | 2022-06-27 | Preparation process of skin care product containing truffle extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210737931.4A CN115054545B (en) | 2022-06-27 | 2022-06-27 | Preparation process of skin care product containing truffle extract |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN115054545A CN115054545A (en) | 2022-09-16 |
| CN115054545B true CN115054545B (en) | 2023-03-03 |
Family
ID=83201821
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210737931.4A Active CN115054545B (en) | 2022-06-27 | 2022-06-27 | Preparation process of skin care product containing truffle extract |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115054545B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117068581B (en) * | 2023-10-17 | 2024-02-20 | 广东圣蜜生物科技有限公司 | Microbial fermentation liquid flow stabilizing device and method for plant skin care products |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107320382A (en) * | 2017-07-31 | 2017-11-07 | 上海中翊日化有限公司 | A kind of composition containing dried tremella extract and the application in personal care articles |
| CN107961191A (en) * | 2017-12-28 | 2018-04-27 | 广州蜜妆生物科技有限公司 | A kind of kahikatea dew anti-aging is compacted eye mask and preparation method thereof |
| CN108721155A (en) * | 2017-04-14 | 2018-11-02 | Isp投资有限公司 | Reveal the cosmetics prepared product and its cosmetic method of extract containing kahikatea |
| CN110022850A (en) * | 2016-11-29 | 2019-07-16 | 莱雅公司 | Composition comprising truffle extract and neohesperidin dihydrochalcone |
| CN110179725A (en) * | 2018-04-04 | 2019-08-30 | 郭洪杰 | A kind of replenishing water and preserving moisture facial mask and preparation method thereof |
| CN111686027A (en) * | 2020-07-09 | 2020-09-22 | 刘赛 | Skin conditioning and caring product prepared from plant extract and preparation method thereof |
| CN113318029A (en) * | 2021-06-17 | 2021-08-31 | 广东柏俐臣生物科技有限公司 | Moisturizing lotion and preparation method thereof |
-
2022
- 2022-06-27 CN CN202210737931.4A patent/CN115054545B/en active Active
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110022850A (en) * | 2016-11-29 | 2019-07-16 | 莱雅公司 | Composition comprising truffle extract and neohesperidin dihydrochalcone |
| CN108721155A (en) * | 2017-04-14 | 2018-11-02 | Isp投资有限公司 | Reveal the cosmetics prepared product and its cosmetic method of extract containing kahikatea |
| CN107320382A (en) * | 2017-07-31 | 2017-11-07 | 上海中翊日化有限公司 | A kind of composition containing dried tremella extract and the application in personal care articles |
| CN107961191A (en) * | 2017-12-28 | 2018-04-27 | 广州蜜妆生物科技有限公司 | A kind of kahikatea dew anti-aging is compacted eye mask and preparation method thereof |
| CN110179725A (en) * | 2018-04-04 | 2019-08-30 | 郭洪杰 | A kind of replenishing water and preserving moisture facial mask and preparation method thereof |
| CN111686027A (en) * | 2020-07-09 | 2020-09-22 | 刘赛 | Skin conditioning and caring product prepared from plant extract and preparation method thereof |
| CN113318029A (en) * | 2021-06-17 | 2021-08-31 | 广东柏俐臣生物科技有限公司 | Moisturizing lotion and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN115054545A (en) | 2022-09-16 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN115054545B (en) | Preparation process of skin care product containing truffle extract | |
| CN209237421U (en) | A kind of decoloration kettle with cleaning function | |
| CN109968532A (en) | A kind of concrete batch plant having cleaning inside function and its operating method | |
| CN116396857B (en) | Enzymolysis device for extracting polypeptide skin care products and use method | |
| CN209193765U (en) | A kind of sludge treatment equipment | |
| CN205797107U (en) | A kind of agricultural yellow unit rice cracker quick paint device | |
| CN214683119U (en) | Spiral flushing device in mechanical automation field | |
| CN209669029U (en) | A kind of php slurry harmless treatment device | |
| CN216964450U (en) | Agitated kettle of skin care products production usefulness | |
| CN221179123U (en) | Dough kneading device with cleaning function for processing vermicelli | |
| CN219072127U (en) | Haematococcus pluvialis CO2 supercritical fluid extraction device | |
| CN212035887U (en) | Degritting device is used in laver production | |
| CN117926611B (en) | Slurry treatment device and treatment process for tissue production | |
| CN211754907U (en) | Energy-conserving reation kettle of acyl chloride production constant temperature | |
| CN218796320U (en) | Food synthetic colorant draws purification device | |
| CN213885884U (en) | Self-cleaning pigment mixing device | |
| CN219076070U (en) | Aggregate mixer | |
| CN217169053U (en) | Self-cleaning concrete mixing kettle | |
| CN220573202U (en) | Stirring filter | |
| CN212758431U (en) | Safe and energy-saving homogenizer for bean flour processing | |
| CN220216013U (en) | Artificial diamond elutriation device with good cleaning effect | |
| CN220918856U (en) | Water-based acrylic resin dispersing and stirring device convenient to clean | |
| CN212188777U (en) | Emulsifying tank for emulsifying methyl silicone oil | |
| CN219702152U (en) | Anthocyanin extraction element | |
| CN219765321U (en) | High-efficient reation kettle is used in production of nanometer zirconia powder |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |