CN114989664A - Rosin ink, preparation method, application and application method - Google Patents

Rosin ink, preparation method, application and application method Download PDF

Info

Publication number
CN114989664A
CN114989664A CN202210702614.9A CN202210702614A CN114989664A CN 114989664 A CN114989664 A CN 114989664A CN 202210702614 A CN202210702614 A CN 202210702614A CN 114989664 A CN114989664 A CN 114989664A
Authority
CN
China
Prior art keywords
ink
rosin
parts
pine
container
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN202210702614.9A
Other languages
Chinese (zh)
Other versions
CN114989664B (en
Inventor
马友谊
董昊
马俊杰
高慧
滕培国
李霞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jinan Friendship Gourd Culture Development Co ltd
Original Assignee
Jinan Friendship Gourd Culture Development Co ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jinan Friendship Gourd Culture Development Co ltd filed Critical Jinan Friendship Gourd Culture Development Co ltd
Priority to CN202210702614.9A priority Critical patent/CN114989664B/en
Publication of CN114989664A publication Critical patent/CN114989664A/en
Application granted granted Critical
Publication of CN114989664B publication Critical patent/CN114989664B/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/02Printing inks
    • C09D11/08Printing inks based on natural resins
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B44DECORATIVE ARTS
    • B44CPRODUCING DECORATIVE EFFECTS; MOSAICS; TARSIA WORK; PAPERHANGING
    • B44C1/00Processes, not specifically provided for elsewhere, for producing decorative surface effects
    • B44C1/22Removing surface-material, e.g. by engraving, by etching
    • B44C1/224Removing surface-material, e.g. by engraving, by etching manually
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/02Printing inks
    • C09D11/03Printing inks characterised by features other than the chemical nature of the binder
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D11/00Inks
    • C09D11/02Printing inks
    • C09D11/06Printing inks based on fatty oils

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inks, Pencil-Leads, Or Crayons (AREA)

Abstract

The invention belongs to the technical field of gourd carving, and particularly relates to rosin ink, a preparation method, application and an application method. The invention provides rosin ink which is characterized by comprising the following components in parts by weight: 4-6 of pine branches; 1-3 parts of pine needles; 1-3 parts of pine bark; 2-4 parts of lard oil; 1-3 parts of plant ash; 0.5-2% of brown sugar powder; 0.5-1.5% of honey; 0.5-1.5 of bait tea. The preparation method, the application in gourd carving and the application method of the rosin ink are also within the protection scope of the invention. When the gourd is carved, the matched turpentine ink is adopted for coloring, so that the product is simple and elegant, and the color retention time is longer.

Description

Rosin ink, preparation method, application and application method
Technical Field
The invention belongs to the technical field of gourd carving, and particularly relates to rosin ink, a preparation method, application and an application method.
Background
The gourd surface is either smooth or uneven, and has itself a shape of either a circle or a length. The calabash becomes a beautiful handicraft after being carved with characters or pictures, and is popular with people. When the calabash is carved, the calabash needs to be colored by ink. If the common commercial engraving ink is used for engraving the calabash, on one hand, the ink is easy to produce oil and is attached to the surface of the calabash; in addition, the water-soluble organic fertilizer is easy to seep and spill on the surface of the calabash when meeting moisture, and the attractiveness of the calabash handicraft is affected.
The rosin ink for gourd carving is disclosed in the literature.
Disclosure of Invention
In order to solve the above technical problems, the present invention provides a rosin ink which is excellent in coloring effect and is not discolored; in addition, the invention also provides a preparation method of the rosin ink and application of the rosin ink in gourd carving.
The invention provides rosin ink which comprises the following components in parts by weight:
4-6 of pine branches; 1-3 parts of pine needles; 1-3 parts of pine bark; 2-4 parts of lard oil; 1-3 parts of plant ash; 0.5-2% of brown sugar powder; 0.5-1.5% of honey; 0.5-1.5 of bait tea.
Preferably, the composition comprises the following components in parts by weight: pine branches 5; 2, pine needles; pine bark 2; 3, lard oil; 2 parts of plant ash; brown sugar powder 1; 1, honey; bait tea 1.
In the actual manufacturing process, the preparation method comprises the following steps: 5, two pine branches; 2, two pine needles; 2, two pine barks; 3, two lard oils; 2, two of plant ash; 1 part of brown sugar powder; 1, adding honey for two times; two kinds of bait tea 1.
The preparation method of the rosin ink comprises the following steps:
s1: preparing raw materials in parts by weight as follows: 4-6 of pine branches; 1-3 parts of pine needles; 1-3 parts of pine bark; 2-4 parts of lard oil; 1-3 parts of plant ash; 0.5-2% of brown sugar powder; 0.5-1.5% of honey; 0.5-1.5 parts of bait tea; grinding pine twigs, pine needles and pine barks by using a stone mill, drying the ground pine twigs, pine needles and pine barks, and burning the ground pine twigs, pine needles and pine barks by using fire to obtain a component containing rosin oil, wherein the component is black and is similar to a mixture of pot bottom ash and the rosin oil;
s2: smashing the components containing the turpentine oil in the step (1) by using a stone mortar;
s3: smashing the bait tea into fine powder by using a stone mortar;
s4: mixing the materials in the S2-S3 together, and stirring until the materials are completely stirred to obtain a mixture;
s5: pouring the mixture into an iron pan, placing the iron pan into a baking machine, adjusting the temperature of the baking machine to 380-400 ℃, and baking for 2.8-3.1 hours;
s6: grinding the baked materials by No. 100 fine sand paper to obtain fine powder;
s7: sieving the fine powder ground in the step S6 by using a fine-mesh basket sieve, grinding the slightly larger powder blocks obtained after sieving again, and repeating the steps until all fine powder is sieved;
s8: putting lard, plant ash, brown sugar powder and honey into a glass container, and stirring to uniformly mix the lard, the plant ash, the brown sugar powder and the honey;
s9: stirring the material in the S8 and the fine powder sieved in the S7 for multiple times to fully and uniformly mix the material and the fine powder, pouring the mixture into a glass sealed container for sealing and fermenting, wherein the sealing and fermenting time is 28-32 days;
s10: opening a cover of the sealed container, and drying the materials in the container in the shade for 6-8 days;
s11: and fully stirring the mixture in the container by using bamboo chopsticks, covering a container opening cover after uniformly stirring, and sealing and storing for 28-32 days again to obtain the rosin ink.
Preferably, in the above step, the fine powder in S2 is 40 to 100 mesh.
Preferably, in the above step, the fine powder in S3 is 40 to 100 mesh.
Preferably, in the above step, the temperature of the baker is adjusted to 390 ℃ and baked for 3 hours.
Preferably, in the above step, S9: stirring the material in the S8 and the fine powder sieved in the S7 for multiple times to fully and uniformly mix the materials, pouring the mixture into a glass sealed container, sealing and fermenting for 30 days;
s10: opening the cover of the sealed container, and drying the materials in the container in the shade for 7 days;
s11: and fully stirring the mixture in the container by using bamboo chopsticks, covering a container opening cover after uniformly stirring, and sealing and storing for 30 days again to obtain the rosin ink.
The rosin ink is obtained by adopting a specific formula and a specific process, can be used for engraving the calabash, can ensure that the calabash artware does not fade for many years, has long color retention time, and does not leak and spill due to absorbing moisture in the air in humid weather.
The method for applying the rosin ink to gourd carving, which is provided by the invention, specifically comprises the following steps:
(1) firstly, taking the rosin ink in a container out by using a small iron spoon, putting the rosin ink in a porcelain container (such as a porcelain plate), and fully and uniformly stirring the rosin ink with bamboo chopsticks for use in the step (2);
(2) when the gourd is carved, the carving knife is held by the right hand, the ink is rubbed by the thumb of the left hand, the ink is rubbed along with carving, the ink is rubbed to enable the ink color of the rosin ink to be blended into the carved texture, the operation is repeated in the process until the gourd is carved, and finally, after the gourd is carved, the rosin ink floating on the surface of the gourd is wiped clean after cotton cloth is soaked in water.
The pine resin ink blended into the carved texture has lasting color and luster without fading, and is called as follows in the field: the expression of 'carving the surface texture and cutting into three parts of bone' means that the gourd peel can also penetrate into the deep surface texture of the gourd peel even if the gourd peel is slightly carved by a knife and the pine resin ink is smeared, and plays an irreplaceable role in the lasting and preservation of the color of the carved gourd works.
In the invention, the carved gourd artwork is colored by the rosin ink, so that the color of the gourd artwork is simple and elegant and never fades, the defect that common ink is easy to seep and spill when meeting moisture is overcome, and meanwhile, the rosin ink disclosed by the invention cannot generate an oil phenomenon after carving is finished, so that the attractiveness of the surface of the gourd artwork is not influenced.
Drawings
FIG. 1 is a first photograph of turpentine ink applied to gourd carving;
FIG. 2 is a second photograph of rosin ink applied to gourd sculptures;
FIG. 3 is a third photograph of pine resin ink applied to gourd sculptures;
fig. 4 is a fourth photograph of rosin ink applied to gourd sculptures;
FIG. 5 is a fifth photograph of pine resin ink applied to gourd sculptures;
fig. 6 is a sixth photograph of rosin ink applied to gourd sculptures.
Detailed Description
The present invention will now be further described with reference to specific embodiments in order to enable those skilled in the art to better understand the present invention.
The apparatus, equipment and devices used in the invention are as follows:
no. 100 fine sandpaper, commercially available plain sandpaper;
pine branch: naturally occurring pine branches;
bait tea, honey, black sugar powder, a baking machine and a fine mesh basket sieve are all common commercial products.
Lard, namely common lard, is an oil product prepared by refining pork at high temperature.
Example 1
Preparing rosin ink:
taking the preparation of 1 kg of rosin ink as an example, the specific steps are as follows:
s1: preparing raw materials in parts by weight as follows: 5, two pine branches; 2, two pine needles; 2, two pine barks; 3, two lard oils; 2, two of plant ash; 1 part of brown sugar powder; 1, adding two kinds of honey; 1, two bait teas; grinding pine branch, pine needle and pine bark with stone roller, oven drying, and burning to obtain component containing oleum Pini (the two components are 50 g);
common turpentine oil is yellow brown, has clear texture and has intense pine fragrance; however, if the pine oil is contacted with strong light or air during storage, adverse reaction is easy to occur, and resin-like substances such as common commonly known pine oil (dried on pine trees, transparent and stuck together) are generated; meanwhile, the components containing the turpentine oil after being fired also contain plant ash, the color of the plant ash is black, and the basic ground color is provided for coloring;
s2: smashing the component containing the turpentine oil in the S1 with a stone mortar;
s3: smashing the bait tea into fine powder by using a stone mortar; about 40 mesh;
s4: mixing the powder in the S2-S3 together, and stirring until the mixture is completely stirred to obtain a mixture;
s5: pouring the mixed powder into an iron pan, placing the iron pan into a baking machine, adjusting the temperature of the baking machine to 390 ℃, and baking for 3 hours;
s6: grinding the baked materials by using No. 100 fine sand paper;
s7: sieving the fine powder ground in the step S6 by using a fine-mesh basket sieve, grinding the slightly larger powder blocks obtained after sieving again, and repeating the steps until all fine powder is sieved;
s8: placing lard, plant ash, brown sugar powder and honey into a glass container, and stirring to mix them uniformly;
s9: stirring the material in the S8 and the fine powder sieved in the S7 for multiple times to fully and uniformly mix the materials, pouring the mixture into a glass sealed container, sealing and fermenting for 30 days;
s10: opening the cover of the sealed container, and drying the materials in the container in the shade for 7 days;
s11: and fully stirring the mixture in the container by using bamboo chopsticks, covering a container opening cover after uniformly stirring, and sealing and storing for about 30 days to obtain the rosin ink.
The rosin ink can be stored for one month, and can be used within one month. When the bottle gourd ink is used, the rosin ink is taken out of the small bowl, is uniformly stirred, is rubbed with hands by the right thumb and the left thumb, and is rubbed with hands along with carving, so that the rosin ink enters the carved gourd patterns.
Example 2
Preparing rosin ink:
taking the preparation of 1 kg of rosin ink as an example, the specific steps are as follows:
s1: preparing raw materials in parts by weight as follows: 4.5 pine branches; 1.8 parts of pine needles; 2.2 of pine barks; 2.8 portions of lard oil; 2.2 parts of plant ash; 1.1 portions of brown sugar powder; 1.2 portions of honey; 1.2 portions of bait tea; grinding pine branch, pine needle and pine bark with stone roller, oven drying, and burning to obtain component containing oleum Pini (the two components are 50 g);
s2: smashing the components containing the turpentine oil in the S1 by using a stone mortar;
s3: smashing the bait tea into fine powder by using a stone mortar; about 40 mesh;
s4: mixing the powder in the S2-S3 together, and stirring until the mixture is completely stirred to obtain a mixture;
s5: pouring the mixed powder into an iron pan, placing the iron pan into a baking machine, adjusting the temperature of the baking machine to 390 ℃, and baking for 3 hours;
s6: grinding the baked materials by using No. 100 fine sand paper;
s7: sieving the fine powder ground in the step S6 by using a fine mesh basket sieve, grinding the slightly larger powder blocks obtained after sieving again, and repeating the steps until all the fine powder is sieved;
s8: placing lard, plant ash, brown sugar powder and honey into a glass container, and stirring to mix them uniformly;
s9: stirring the material in the S8 and the fine powder sieved in the S7 for multiple times to fully and uniformly mix the materials, pouring the mixture into a glass sealed container, sealing and fermenting for 30 days;
s10: opening the cover of the sealed container, and drying the materials in the container in shade for 7 days;
s11: and fully stirring the mixture in the container by using bamboo chopsticks, covering a container opening cover after uniformly stirring, and sealing and storing for about 30 days to obtain the rosin ink.
Example 3
Preparing rosin ink:
taking the preparation of 1 kg of rosin ink as an example, the specific steps are as follows:
s1: preparing raw materials in parts by weight as follows: 4.8 pine branches; 1.8 pine needles; 2.1 parts of pine bark; 2.6 portions of lard oil; 2.2 parts of plant ash; brown sugar powder 0.9; 0.9 part of honey; 1.1 portions of bait tea; grinding pine branch, pine needle and pine bark with stone roller, oven drying, and burning to obtain component containing oleum Pini (the two components are 50 g);
s2: smashing the component containing the turpentine oil in the S1 with a stone mortar;
s3: smashing the bait tea into fine powder by using a stone mortar; about 40 mesh;
s4: mixing the powder in the S2-S3 together, and stirring until the mixture is completely stirred to obtain a mixture;
s5: pouring the mixed powder into an iron pan, placing the iron pan into a baking machine, adjusting the temperature of the baking machine to 390 ℃, and baking for 3 hours;
s6: grinding the baked materials by using No. 100 fine sand paper;
s7: sieving the fine powder ground in the step S6 by using a fine-mesh basket sieve, grinding the slightly larger powder blocks obtained after sieving again, and repeating the steps until all fine powder is sieved;
s8: putting lard, plant ash, brown sugar powder and honey into a glass container, and stirring to uniformly mix the lard, the plant ash, the brown sugar powder and the honey;
s9: stirring the material in the S8 and the fine powder sieved in the S7 for multiple times to fully and uniformly mix the materials, pouring the mixture into a glass sealed container, sealing and fermenting for 30 days;
s10: opening the cover of the sealed container, and drying the materials in the container in the shade for 7 days;
s11: and fully stirring the mixture in the container by using bamboo chopsticks, covering a container opening cover after uniformly stirring, and sealing and storing for about 30 days to obtain the rosin ink.
Example 4
The method for applying the rosin ink to gourd carving specifically comprises the following steps:
(1) firstly, taking the rosin ink in a container out by using a small iron spoon, putting the rosin ink in a porcelain container, and fully and uniformly stirring the rosin ink with bamboo chopsticks for use in the step (2);
(2) when the gourd is carved, the carving knife is held by the right hand, the ink is rubbed by the thumb of the left hand, and the ink is rubbed along with the carving, so that the rosin ink enters the carved gourd patterns, the operation is repeated in the link until the gourd is carved, and after the work is finished, the rosin ink floating on the surface of the gourd is wiped clean after the cotton cloth is dipped in water.
Example 5
Regarding the durability of the time that can be maintained after the rosin ink of the present invention is applied to gourd carving, the present inventors conducted the following experiment:
the calabash handicraft in the attached fig. 2 is manufactured in 3 months in 2010, and the calabash handicraft does not fade until 4 middle days in 2022; the portion in which the color appears black is completed using the rosin ink of the present invention.
The calabash artware in the attached figures 3-6 is an artware which is manufactured for more than 8 years, and the engraved patterns on the calabash still keep the original color after being placed for a long time. The rosin ink is applied to gourd carving, does not fade for a long time, and does not generate oil; it will not spill in humid weather.
Comparative product 1: in the invention, the method is characterized in that: printer ink (common commercial ink-jet printer ink, namely dye ink, is formed by blending the dye ink and vegetable oil according to a certain proportion, for example, the printer ink is mixed with peanut oil which is commonly adopted in the industry at present, and can be blended with other oils, such as olive oil, soybean oil, corn oil, sunflower seed oil, castor oil, cottonseed oil and the like, and all plants which can lubricate and enable the dye ink to be adsorbed to the carved nicks of the gourd can be used);
TABLE 1 durability of rosin inks of the present invention compared to commercial conventional inks
Figure RE-GDA0003743084150000101
The above-mentioned rosin ink of the present invention is prepared by the method of the present invention, and the method is the same as in example 1.
(1) With respect to persistence
Because the formula and the method of the invention are ancestral methods, generation-by-generation, and regarding the durability, the product can completely reach no fading for 20 years (or no obvious fading observed by naked eyes), many of the products mentioned in the invention have been stored for more than 20 years, and the nicked part dyed by the rosin ink is still intact till now, and the ink is black like paint; products which are stored for more than 10 years are not faded from the date of carving, dyeing and drying; the product of the invention has good durability, because in the formula of the invention, the pine needles, pine branches and pine barks are used as raw materials to prepare the components containing the rosin oil (the mixture of burnt ash and the rosin oil, black and blocky structures), wherein the rosin oil component plays a role in lubrication and emulsification on one hand, and has harmonious property and permeability to enable various materials to be better mixed, diluted and dissolved; on the other hand, the turpentine oil has strong adhesion, so that the color of plant ash (or called as carbon black or carbon black) is tightly adsorbed in the engraved patterns on the surface of the gourd, so that the plant ash is firmly adhered in the lines of the patterns, and the falling off is avoided; the turpentine oil also has a function of being fully mixed with components such as plant ash and the like, and has a barrier function like a transparent cover outside the color of the plant ash to protect the color of the plant ash from being oxidized by the components in the outside air and being not washed by the outside moisture or rain water, so that the color is durable and not faded.
The lard oil has the effects of strong lubricity and good moisture retention performance, so that the turpentine ink is not easy to evaporate or dry, the humidity of the turpentine ink is kept, and the turpentine oil is assisted; the black color produced by hand making is easier to be absorbed in the lines of the carved patterns, the hand feeling is more moist when the color is rubbed, and the color rubbing is easier to succeed; and the rosin ink and the rosin oil have synergistic effect, so that the rosin ink has more adhesiveness, and a transparent protective layer is formed outside the color of the rosin ink, so that the carved product is durable and does not fade;
plant ash, which provides the color of black carbon black for dyeing, so that the final rosin ink presents black;
brown sugar powder: can blend the over-strong black of plant ash (grass carbon) to make the color of the plant ash black with light feeling;
the bait tea powder contains tea polyphenol which contains a large amount of phenolic hydroxyl, and the phenolic hydroxyl is combined with cellulose and other components in the cucurbit skin to form hydrogen bonds and hydrophobic bonds, so that the colored cucurbit artware is not easy to fade after being wetted, and the color is more durable; meanwhile, the black color rubbed by the rosin ink is softer and cannot be too strong due to the use of the bait tea powder;
the honey contains sugar which has excellent adhesion performance, so that various raw materials can be combined together more tightly, and a firm protective barrier is formed for the color of plant ash. And the honey and the rosin oil have brightness, so that the whole rosin ink presents a fine, smooth and bright appearance, and the rosin ink is rubbed on the gourd to form high unification with the smoothness of the gourd surface, thereby being beneficial to improving the visual aesthetic feeling.
The printer ink is also commercially available for coloring gourd sculptures, but the printer ink is very likely to fade with time when used for gourd sculptures. On the one hand, it is well known in the industry that the cause of ink fading is mainly the irregular distribution of the circumferential patterns and non-patterns of the plate cylinder, while the non-printing cylinder gap also has an effect and lateral cross-inking affects ink fading. The coloring object in the invention is a calabash handicraft article, which is a product carved by hand, colors are rubbed in the engraved grooves or nicks on the surface of the calabash, and the engraved grooves or nicks are sunken in the surface of the calabash.
On the other hand, dye ink is susceptible to fading due to ultraviolet rays, ozone, and other components in sunlight, which is why ordinary photographs are susceptible to yellowing and fading. Meanwhile, the dye ink also has the phenomena of ink seepage or fading and the like caused by moisture absorption and easy moisture absorption, so that the color fastness of the dye ink is also poor.
Therefore, compared with the common printer ink, the rosin ink product is derived from natural plant and animal grease, has no artificially synthesized chemical components in dye ink, and has stronger durability.
(2) With respect to oil-bleeding, spillage or leakage
The rosin ink is applied to gourd carving, so that the phenomenon that the pattern at the carving and dyeing position is leaked and spilled out of the nicks due to high moisture absorption or deliquescence of air in rainy days is avoided, the phenomenon of oil leakage is avoided, and the phenomenon of oil leakage or oil leakage can be observed by naked eyes.
The judgment of the phenomena of spilling and oil leakage is to adopt a common paper towel to wipe the carved part back and forth and observe whether the paper towel has black pollution or oil stain. The rosin ink prepared by the method is carved on the gourd and then dried, and after the rosin ink is placed for 30 days, the method is adopted to judge in rainy days, so that black pollution and oil stain are avoided, which shows that the rosin ink dyed in the method has no oil seepage and spilling phenomenon and oil seepage phenomenon in gourd carving.
Or the gourd handicraft article colored by the rosin ink is placed in a damp and dark basement, observed after being placed for 1 to 2 days, and the gourd carving and dyeing part is wiped by using a paper towel, and the result shows that the paper towel is not dyed with any black stain or oil stain, which also indicates that the rosin ink has strong adhesion and is tightly adhered to the carving groove of the gourd handicraft article.
(3) The inventors of the present invention judged that the stability was high if the ink was uniform without precipitation, and whether the ink had precipitation or not was judged to be stable. After the rosin ink is prepared, the rosin ink is placed for 30 days, ink on the uppermost layer, the middle layer and the bottommost layer of the rosin ink is scooped up by a long handle spoon and placed in a taste dish, and the taste dish is stirred by a glass rod to observe whether black granular matters are settled on the taste dish or not. Some of the common commercial inks are prone to precipitation due to their formulation or processing.
(4) Washing with clean water
Experiment one: taking the gourd handicraft article manufactured by the method in the embodiment 1, fully airing, respectively standing for 10 days, 20 days and 30 days, then rinsing the dyed carved pattern with 100mL of clear water, receiving the rinsing water by a white porcelain plate, wiping the carved pattern with a paper towel after rinsing, and observing the color of the paper towel, wherein the result shows that the color of the paper towel is unchanged in 3 samples; and meanwhile, observing the color of the shower water in the white porcelain plate, and finding that the water is colorless and is not stained by any ink. This shows that the rosin ink is not decolorized by rinsing with clear water, and the rosin ink has strong coloring power and is not decolorized for a long time after being dyed on the gourd, and can not be decolorized even by rinsing with water.
Experiment two: the gourd handicraft article prepared by the method in example 1 was completely dried in the air, and was left to stand for 10 days, 20 days, and 30 days, respectively, and was placed in a white plastic tray, and was soaked in a large amount of tap water, and during soaking, the gourd was pressed with a weight, and the dyed carved pattern was always in a state of being soaked in water. After soaking for 12 hours, wiping the engraved pattern with a paper towel, and observing the color of the paper towel, wherein the result shows that the color of the paper towel is unchanged in 3 samples; this shows that the carved cucurbit dyed with the rosin ink of the present invention does not fade whether rinsed or soaked.
(5) Degree of convenience in use
The rosin ink of the present invention can be used after being prepared, and the ink rubbing and dyeing are performed in the manner of example 1.
The product 1 sold on the market is dye ink, or is mixed with peanut oil when in use, and is used after being prepared, so that the convenience is poor. The dosage proportion of the dye ink to the peanut oil needs to be controlled in the preparation process, and if the peanut oil is excessive, the phenomenon of oil leakage after dyeing is easily caused; if the peanut oil is insufficient, the ideal lubricating effect is not achieved, the glossiness after coloring is influenced, and the product has a rough feeling. If the finished product is prepared, the solubility between the dye ink and the peanut oil is not ideal, so that the oil is likely to float on the upper layer.
Therefore, the rosin ink of the present invention is far superior to the commercial products in terms of convenience.
(6) Smell(s)
The rosin ink is prepared from rosin serving as a raw material, and has a unique rosin taste. The common dye ink has the ink smell of chemical products. The rosin ink disclosed by the invention has the effects of soothing the nerves and helping sleep, and is pleasant to smell.
Example 6
In this example, example 1 was compared with each comparative example, and it was confirmed that the formulation of the present invention has a more significant advantage than the formulation of the comparative example, demonstrating that the formulation of the rosin ink of the present invention as a whole is not indispensable. When certain raw materials are reduced, the product cannot achieve an ideal effect, and the color fastness, the color durability and the like of later carving and coloring are influenced.
Compared to example 1, the difference is that comparative example 1: lard is not used;
comparative example 2: black sugar powder is not adopted;
comparative example 3: honey is not adopted;
comparative example 4: bait tea is not adopted;
comparative example 5: the consumption of the raw materials of pine branches, pine needles and pine barks is greatly reduced;
comparative examples 1 to 5 are comparisons of the rosin ink products by the present inventors, and specifically are as follows:
TABLE 2 rosin ink product formulations (g) of example 1 and comparative examples 1 to 5
Example 1 Comparative example 1 Comparative example 2 Comparative example 3 Comparative example 4 Comparative example 5
Pine branch 250 250 250 250 250 120
Pine needle 100 100 100 100 100 50
Pine bark 100 100 100 100 100 50
Lard oil 150 / 150 150 150 150
Plant ash 100 100 100 100 100 100
Black sugar powder 50 50 / 50 50 50
Honey 50 50 50 / 50 50
Bait tea 50 50 50 50 / 50
TABLE 3 comparison of rosin ink products of example 1 with comparative examples 1 to 5
Figure RE-GDA0003743084150000161
From the description in the above table, the rosin ink product of the present invention, which is made of raw materials with a specific ratio, when one of the raw materials is reduced or absent, will cause the properties of the final product to change, thereby affecting the coloring effect of the gourd sculpture at a later stage.
The raw material of the rosin ink in the invention is derived from pure natural vegetable or animal oil, such as rosin oil with rosin; such as plant ash; even some edible raw materials such as honey, bait tea powder, lard and the like have no pollution; the printing ink of the printer especially contains antioxidant hydroquinone, adhesive polyvinylpyrrolidone, cosolvent N-methyl-2-pyrrolidone, diethylene glycol and the like, and the organic components have certain influence on the body of the engraver. The rosin ink of the present invention is clearly more safe.
From the analysis of the coloring power, durability, coloring effect and the like, it can be seen from table 1 that the effect of the rosin ink of the present invention is far superior to that of the printer ink.

Claims (9)

1. The rosin ink is characterized by comprising the following components in parts by weight:
4-6 of pine branches; 1-3 parts of pine needles; 1-3 parts of pine bark; 2-4 parts of lard oil; 1-3 parts of plant ash; 0.5-2% of brown sugar powder; 0.5-1.5% of honey; 0.5-1.5 of bait tea.
2. The rosin ink according to claim 1, comprising the following components in parts by weight: 5, pine branches; 2, pine needles; 2, pine bark; 3, lard oil; 2, plant ash; brown sugar powder 1; 1, honey; bait tea 1.
3. The preparation method of the rosin ink comprises the following steps:
s1: preparing raw materials in parts by weight as follows: 4-6 of pine branches; 1-3 parts of pine needles; 1-3 parts of pine bark; 2-4% of lard oil; 1-3 parts of plant ash; 0.5-2% of brown sugar powder; 0.5-1.5% of honey; 0.5-1.5 parts of bait tea;
grinding ramulus Pini Massonianae, folium Pini and cortex Pini with stone roller, oven drying, and baking with fire to obtain component containing oleum Pini;
s2: smashing the component containing the turpentine oil in the S1 with a stone mortar;
s3: smashing the bait tea into fine powder by using a stone mortar;
s4: mixing the materials in the S2-S3 together, and stirring until the materials are completely stirred to obtain a mixture;
s5: pouring the mixture into an iron pan, placing the iron pan into a baking machine, adjusting the temperature of the baking machine to 380-400 ℃, and baking for 2.8-3.1 hours;
s6: grinding the baked material by No. 100 fine sand paper to obtain fine powder;
s7: sieving the fine powder ground in the step S6 by using a fine-mesh basket sieve, grinding the slightly larger powder blocks obtained after sieving again, and repeating the steps until all fine powder is sieved;
s8: putting lard, plant ash, brown sugar powder and honey into a glass container, and stirring to uniformly mix the lard, the plant ash, the brown sugar powder and the honey;
s9: stirring the material in the S8 and the fine powder sieved in the S7 for multiple times to fully and uniformly mix the material and the fine powder, pouring the mixture into a glass sealed container for sealing and fermenting, wherein the sealing and fermenting time is 28-32 days;
s10: opening a cover of the sealed container, and drying the materials in the container in the shade for 6-8 days;
s11: and after drying in the shade, fully stirring the mixture in the container by using bamboo chopsticks, after uniformly stirring, covering a container opening cover for sealing, and sealing and storing for 28-32 days again to obtain the rosin ink.
4. The method of producing the rosin ink according to claim 3, wherein the fine powder in S2 is 40 to 100 mesh.
5. The method for producing the rosin ink as claimed in claim 3, wherein in S3, the fine powder is 40 to 100 mesh.
6. The method of preparing rosin ink according to claim 3, wherein in S5, the temperature of the baking machine is adjusted to 390 ℃ and baking is performed for 3 hours.
7. The method for producing a rosin ink according to claim 3, wherein the ratio of S9: stirring the material in the S8 and the fine powder sieved in the S7 for multiple times to fully and uniformly mix the materials, pouring the mixture into a glass sealed container, sealing and fermenting for 30 days;
s10: opening the cover of the sealed container, and drying the materials in the container in the shade for 7 days;
s11: and fully stirring the mixture in the container by using bamboo chopsticks, covering a container opening cover after uniformly stirring, and sealing and storing for 30 days again to obtain the rosin ink.
8. Use of the rosin ink of claim 1 in gourd engraving.
9. The method of application of claim 8, comprising the steps of:
(1) firstly, taking the rosin ink in a container out by using a small iron spoon, putting the rosin ink in a porcelain container, and fully and uniformly stirring the rosin ink with bamboo chopsticks for use in the step (2);
(2) when the gourd is carved, the carving knife is held by the right hand to carve, the ink is rubbed by the thumb of the left hand, the rubbing is carried out along with carving, the ink color of the turpentine ink is fused into the carved texture through the ink rubbing, the operation is repeated until the gourd is carved, and finally, after the work is finished, the turpentine ink floating on the surface of the gourd is wiped cleanly after the cotton cloth is dipped in water.
CN202210702614.9A 2022-06-21 2022-06-21 Rosin ink, preparation method, application and application method Active CN114989664B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202210702614.9A CN114989664B (en) 2022-06-21 2022-06-21 Rosin ink, preparation method, application and application method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202210702614.9A CN114989664B (en) 2022-06-21 2022-06-21 Rosin ink, preparation method, application and application method

Publications (2)

Publication Number Publication Date
CN114989664A true CN114989664A (en) 2022-09-02
CN114989664B CN114989664B (en) 2023-03-21

Family

ID=83037314

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202210702614.9A Active CN114989664B (en) 2022-06-21 2022-06-21 Rosin ink, preparation method, application and application method

Country Status (1)

Country Link
CN (1) CN114989664B (en)

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103183982A (en) * 2013-02-28 2013-07-03 扬州古籍线装产业有限公司 Pine-soot ink and preparation method thereof
CN104589886A (en) * 2015-01-07 2015-05-06 山东维多利食品科技有限公司 Process for carving poetry and print on surface of cucurbit
CN106581118A (en) * 2016-11-30 2017-04-26 杭州丰受堂制墨有限公司 Ointment of Chinese ink made from pine soot and preparation method therefor

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103183982A (en) * 2013-02-28 2013-07-03 扬州古籍线装产业有限公司 Pine-soot ink and preparation method thereof
CN104589886A (en) * 2015-01-07 2015-05-06 山东维多利食品科技有限公司 Process for carving poetry and print on surface of cucurbit
CN106581118A (en) * 2016-11-30 2017-04-26 杭州丰受堂制墨有限公司 Ointment of Chinese ink made from pine soot and preparation method therefor

Non-Patent Citations (5)

* Cited by examiner, † Cited by third party
Title
小鱼妈: "《零失败面包机教科书》", 31 May 2017, 北京联合出版社 *
纪立芳: "《江南建筑彩画研究》", 31 December 2017, 东南大学出版社 *
美J.I.达菲编 《小吃食品工艺》翻译组译: "《小吃食品工艺》", 31 July 1988, 轻工业出版社 *
郑万钟等: "《中国风物特产》", 31 July 2004, 中国商业出版社 *
高彦祥: "《食品添加剂》", 31 July 2019, 中国轻工业出版社 *

Also Published As

Publication number Publication date
CN114989664B (en) 2023-03-21

Similar Documents

Publication Publication Date Title
Doerner The materials of the artist and their use in painting, with notes on the techniques of the old masters
CN105382899A (en) Bamboo material dyeing method with edible amaranth as coloring agent
Stokes The Cabinet-Maker and Upholsterer's Companion
CN114989664B (en) Rosin ink, preparation method, application and application method
CN103333610B (en) A kind of protection maintaining agent of antiquated woodenware tool of new coating structure
KR101080877B1 (en) Leather dyeing method and products thereof
CN1195049A (en) Reversible wax printing technique and its product
WO2005004600A1 (en) Process for producing artificial flower with natural plant and finishing agent for use therein
CN113550159B (en) Layered dyeing silk fabric and preparation method thereof
KR101746355B1 (en) Conservation treatment method for seaweed.
CN109795249A (en) A kind of manufacture craft of perpendicular color carved lacquerware
Beltinger et al. Painting in Tempera, c. 1900
Gärtner Historical pigments, dyes and binders
Hill Traditional paint from Papua New Guinea: Context, materials and techniques, and their implications for conservation
CN110406304A (en) A kind of processing technology of colour wood carving
KR101904475B1 (en) Preservation liquid composition for manufacturing preserved flower and manufacturing method of preserved flower using the same that
KR960007177B1 (en) Process for the preparation of arts using waste paper
Williams The art of landscape painting in oil colours
CN115635553A (en) Wood carving color embedding process
Hoff Paint and Varnish Facts and Formulae: A Hand Book for the Maker, Dealer and User of Paints and Varnishes
Sheares The Batik Patterning Technique in Southeast Asia.
CN101890865B (en) Method for manufacturing chili patchwork
Larson The treatment and examination of polychrome Chinese sculpture at the Victoria and Albert Museum
Stokes The Complete Cabinetmaker, and Upholsterer's Guide... With... Engravings
New THE USE OF STAIN BY FURNITURE MAKERS 1660—1850

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant