CN114963700A - Dried silkworm chrysalis cordyceps sinensis and preparation process thereof - Google Patents

Dried silkworm chrysalis cordyceps sinensis and preparation process thereof Download PDF

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Publication number
CN114963700A
CN114963700A CN202210581189.2A CN202210581189A CN114963700A CN 114963700 A CN114963700 A CN 114963700A CN 202210581189 A CN202210581189 A CN 202210581189A CN 114963700 A CN114963700 A CN 114963700A
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drying
preparation
silkworm chrysalis
cordyceps
cordyceps militaris
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Inventor
杨敏忠
廉宁
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Sichuan Moving Sun Pharmaceutical Co ltd
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Sichuan Moving Sun Pharmaceutical Co ltd
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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B3/00Drying solid materials or objects by processes involving the application of heat
    • F26B3/32Drying solid materials or objects by processes involving the application of heat by development of heat within the materials or objects to be dried, e.g. by fermentation or other microbiological action
    • F26B3/34Drying solid materials or objects by processes involving the application of heat by development of heat within the materials or objects to be dried, e.g. by fermentation or other microbiological action by using electrical effects
    • F26B3/347Electromagnetic heating, e.g. induction heating or heating using microwave energy
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B25/00Details of general application not covered by group F26B21/00 or F26B23/00
    • F26B25/001Handling, e.g. loading or unloading arrangements
    • F26B25/002Handling, e.g. loading or unloading arrangements for bulk goods
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F26DRYING
    • F26BDRYING SOLID MATERIALS OR OBJECTS BY REMOVING LIQUID THEREFROM
    • F26B25/00Details of general application not covered by group F26B21/00 or F26B23/00
    • F26B25/22Controlling the drying process in dependence on liquid content of solid materials or objects
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P60/00Technologies relating to agriculture, livestock or agroalimentary industries
    • Y02P60/80Food processing, e.g. use of renewable energies or variable speed drives in handling, conveying or stacking
    • Y02P60/85Food storage or conservation, e.g. cooling or drying

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • General Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Microbiology (AREA)
  • Physics & Mathematics (AREA)
  • Electromagnetism (AREA)
  • Health & Medical Sciences (AREA)
  • Biomedical Technology (AREA)
  • Biotechnology (AREA)
  • Molecular Biology (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)

Abstract

The invention provides a dried cordyceps militaris and a preparation process thereof, belongs to the field of silkworm development, and aims at overcoming the defect that the conventional drying process of the cordyceps militaris cannot well retain two beneficial components, namely adenosine and cordycepin in the cordyceps militaris.

Description

Dried silkworm chrysalis cordyceps sinensis and preparation process thereof
Technical Field
The invention relates to silkworm industry development, in particular to a dried silkworm chrysalis cordyceps sinensis and a preparation process thereof.
Background
The silkworm chrysalis cordyceps is one of the most popular nutritional supplements in east Asia, the form and chemical components of the silkworm chrysalis cordyceps are balanced with those of the cordyceps, the silkworm chrysalis cordyceps can be artificially cultivated, and the large-scale production of the silkworm chrysalis cordyceps is realized by artificially cultivating silkworm larvae or chrysalis as hosts. The silkworm chrysalis cordyceps is rich in various bioactive substances, wherein nucleoside substances such as adenosine, cordycepin and the like are important medicinal active ingredients, and the content of the two active ingredients in the silkworm chrysalis cordyceps is an important index for evaluating the quality of the silkworm chrysalis cordyceps.
The drying process of the silkworm chrysalis cordyceps sinensis is a process which is convenient to store, process and sell after moisture of fresh artificially-cultivated products is removed, and currently, reference is mainly made to drying methods of edible fungi and partial fresh dragon products in production. However, the two effective components of adenosine and cordycepin in the silkworm chrysalis cordyceps can not be well preserved by the drying process.
Disclosure of Invention
Based on the problems, the invention aims to provide a drying process of cordyceps militaris, which maximally retains the effective components of adenosine and cordycepin in the cordyceps militaris by combining a sectional type microwave drying process and a polysaccharide film-forming protection mode.
In order to achieve the aim, the technical scheme of the invention provides a preparation method of cordyceps militaris, which comprises the following steps:
placing fresh silkworm chrysalis cordyceps in an oven for drying to obtain a material I;
soaking the material I in a arabic gum solution to obtain a material II;
and carrying out microwave drying on the material II to obtain a finished product.
Further, the drying temperature of the oven is 60-80 ℃, and the drying time is 4-6 h.
Further, the adding ratio of the first material to the Arabic gum solution is 1: (1-2).
Further, the mass fraction of the acacia gum solution is 20% -30%.
Further, the microwave drying process comprises drying the cordyceps militaris to constant weight at 700-900 w.
Further, after the finished product is obtained by drying, the finished product is preserved at the temperature of 5-8 ℃.
The application also discloses a dried silkworm chrysalis cordyceps prepared by the preparation method.
The invention has the following beneficial effects:
the utility model provides a defect to two kinds of useful compositions of adenosine and cordycepin in the unable fine reservation silkworm chrysalis worm grass of drying process of present conventional silkworm chrysalis worm grass, the mode that two sections drying combine arabic gum membrane formation has been adopted, go out fresh silkworm chrysalis worm grass surface and inside unnecessary moisture through oven low-temperature drying earlier, it soaks to put into arabic gum solution, it is that arabic gum forms membrane on silkworm chrysalis worm grass surface, later, the thorough drying of silkworm chrysalis worm grass is carried out to the mode of rethread microwave drying, make two kinds of useful compositions of adenosine and cordycepin in the obtained silkworm chrysalis worm grass fully keep the worm grass.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present disclosure more apparent, the technical solutions of the embodiments of the present disclosure are described below clearly and completely. It is to be understood that the described embodiments are only a few embodiments of the present disclosure, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the described embodiments of the disclosure without inventive step, are within the scope of protection of the disclosure.
Unless defined otherwise, technical or scientific terms used herein shall have the ordinary meaning as understood by one of ordinary skill in the art to which this disclosure belongs.
One embodiment of the application discloses a preparation process of dried silkworm chrysalis cordyceps sinensis, which comprises the following steps:
placing fresh silkworm chrysalis cordyceps in an oven for drying to obtain a material I;
soaking the material I in a arabic gum solution to obtain a material II;
and carrying out microwave drying on the material II to obtain a finished product.
In this embodiment, the preparation method of the gum arabic solution is as follows: adding water into the Arabic gum, heating and dissolving to prepare an Arabic gum solution with the mass fraction of 20-30%.
In some embodiments, the oven drying temperature is 60-80 ℃ and the drying time is 4-6 h.
In some embodiments, the ratio of the first material to the acacia gum solution is 1: (1-2).
In some embodiments, the gum arabic solution has a mass fraction of 20% to 30%.
In some embodiments, the microwave drying process is 700-900w for drying the cordyceps militaris to constant weight.
In some embodiments, after said drying to obtain said finished product, said finished product is stored at a temperature of 5-8 ℃.
The preparation method of the quick-frozen bamboo shoot of the application is disclosed by the following specific examples, and obviously, the described examples are part of the examples of the disclosure, but not all of the examples. All other embodiments, which can be derived by a person skilled in the art from the described embodiments of the disclosure without any inventive step, are within the scope of protection of the disclosure.
Example 1 preparation of dried Cordyceps militaris
(1) Cleaning fresh cordyceps militaris, putting into a drying oven, setting the drying temperature to be 70 ℃, and drying for 5 hours to obtain a material I;
(2) and (3) soaking the first material in 25% of Arabic gum solution for 30min to obtain a second material, wherein the weight ratio of the first material to the Arabic gum solution is 1: 1.
(3) And (5) drying the material II by using microwaves, setting the microwave intensity to be 800w, and drying until the weight of the material is constant to obtain a finished product.
(4) And storing the finished product at 6 ℃.
Example 2 preparation of dried Cordyceps militaris
(1) Cleaning fresh cordyceps militaris, putting into a drying oven, setting the drying temperature to be 60 ℃, and drying for 4 hours to obtain a material I;
(2) and (3) soaking the first material in a gum arabic solution with the mass fraction of 20% for 30min to obtain a second material, wherein the weight ratio of the first material to the gum arabic solution is 1: 2.
(3) And drying the material II by using microwaves, setting the microwave intensity to be 700w, and drying until the weight of the material is constant to obtain a finished product.
(4) And storing the finished product at 5 ℃.
Example 2 preparation of dried Cordyceps militaris
(1) Cleaning fresh cordyceps militaris, putting into a drying oven, setting the drying temperature to be 80 ℃, and drying for 6 hours to obtain a material I;
(2) and (3) soaking the first material in a gum arabic solution with the mass fraction of 30% for 30min to obtain a second material, wherein the weight ratio of the first material to the gum arabic solution is 1: 1.
(3) And (5) drying the material II by using microwaves, setting the microwave intensity to be 900w, and drying until the weight of the material is constant to obtain a finished product.
(4) And storing the finished product at 8 ℃.
Comparative example 1 preparation of dried silkworm chrysalis Cordyceps
The preparation method is the same as example 1 except that comparative example 1 does not perform the oven drying treatment.
Comparative example 2 preparation of dried silkworm chrysalis Cordyceps
The procedure is the same as in example 1 except that comparative example 2 is not soaked in the gum arabic solution.
Comparative example 3 preparation of dried silkworm chrysalis Cordyceps
The preparation method was the same as example 1 except that comparative example 3 was not subjected to oven drying treatment and gum arabic solution soaking.
Comparative example 4 preparation of dried Cordyceps militaris
The preparation method is the same as that of example 1, except that comparative example 4 does not carry out microwave drying treatment, and after soaking with arabic gum, drying treatment is carried out until the weight is constant.
Comparative example 5 preparation of dried Cordyceps militaris
The preparation method is the same as example 1 except that comparative example 5 does not perform direct baking to constant weight, and does not perform gum arabic soaking and microwave treatment.
Comparative example 6 preparation of dried Cordyceps militaris
The preparation method is the same as that of example 1, except that in comparative example 6, the silkworm chrysalis cordyceps is preserved at 20 ℃.
Comparative example 7 preparation of dried Cordyceps militaris
The preparation method is the same as that of example 1, except that in comparative example 7, the silkworm chrysalis cordyceps is preserved at 0 ℃.
Test examples active ingredient measurement
Adenosine, cordycepin and the like in the cordyceps militaris are important medicinal active ingredients, and the prepared cordyceps militaris is obtained by measuring different treatment methods.
The test method comprises the following steps: preserving the prepared finished product for 30 days, taking out, crushing, sieving with a 80-mesh sieve, and measuring by using a reversed-phase high performance liquid chromatography. Accurately weighing 0.1g of a cordyceps militaris sample, adding 1mL of distilled water, carrying out vortex flow for 1min, carrying out microwave extraction for 1min, standing to obtain a cordycepin and adenosine extracting solution, filtering through a 0.22-micron filter membrane to obtain a solution to be detected, and carrying out sample loading determination: the detection wavelength is 259nm, the mobile phase is tetrahydrofuran-0.1% methanol-phosphate buffer solution (volume ratio is 1:2: 0.97), the flow rate is 1.0mL/min, the sample injection amount is 20 mu L, and the content of the target component is analyzed and calculated by an external standard method.
The experimental results are as follows: see table 1.
And (4) analyzing results: as can be seen from the table 1, the cordycepin content and the adenosine content of the embodiment are relatively higher than those of the comparative example, and the fact that the dry silkworm chrysalis cordyceps prepared by the preparation method can well keep the content of the active ingredients in the silkworm chrysalis cordyceps is proved; compared with comparative examples 1-5 (respectively changing the drying process of the cordyceps militaris), cordycepin and adenosine in the cordyceps militaris with different treatment modes are reduced to different degrees, so that the effective components of the cordyceps militaris can be retained to the maximum extent only under the process conditions of drying treatment, gum arabic soaking and microwave drying; example 1 compared with comparative examples 6-7 (changing storage conditions), the content of cordycepin and adenosine in the dried cordyceps militaris is reduced to different degrees in the storage process after the storage conditions are changed, which shows that the storage time influences the attenuation of the active ingredients of the cordyceps militaris, and the active ingredients of the cordyceps militaris are retained to the maximum extent within the storage range specified in the application.
TABLE 1 results of the experiment
Figure DEST_PATH_IMAGE001
Finally, it should be noted that: the above embodiments are only used to illustrate the technical solution of the present invention, and not to limit the same; while the invention has been described in detail and with reference to the foregoing embodiments, those skilled in the art will appreciate that; the technical solutions described in the foregoing embodiments may still be modified, or some or all of the technical features may be equivalently replaced; and the modifications or the substitutions do not make the essence of the corresponding technical solutions depart from the scope of the technical solutions of the embodiments of the present invention.

Claims (7)

1. A preparation method of dried silkworm chrysalis cordyceps is characterized by comprising the following steps:
placing fresh silkworm chrysalis cordyceps in an oven for drying to obtain a material I;
soaking the material I in a arabic gum solution to obtain a material II;
and carrying out microwave drying on the material II to obtain a finished product.
2. The preparation method according to claim 1, wherein the oven drying temperature is 60-80 ℃ and the drying time is 4-6 h.
3. The preparation method of claim 1, wherein the first material and the acacia gum solution are added in a ratio of 1: (1-2).
4. The preparation method according to claim 1, wherein the mass fraction of the gum arabic solution is 20% to 30%.
5. The preparation method as claimed in claim 1, wherein the microwave drying process comprises 700-900w drying of Cordyceps militaris to constant weight.
6. The method of claim 1, wherein the finished product is stored at a temperature of 5-8 ℃ after drying to obtain the finished product.
7. A dried silkworm chrysalis cordyceps prepared by the preparation method according to claims 1-6.
CN202210581189.2A 2022-05-26 2022-05-26 Dried silkworm chrysalis cordyceps sinensis and preparation process thereof Pending CN114963700A (en)

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Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1075402A (en) * 1992-02-16 1993-08-25 陈顺志 Freshness-preserved cordyceps and food-processing method thereof
CN1137926A (en) * 1996-02-05 1996-12-18 杨满寿 Chinese caterpillar fungus with protective layer and its making method
CN101161133A (en) * 2007-05-16 2008-04-16 东莞市生物技术研究所 A method for drying cordyceps fresh sporophore
CN102232548A (en) * 2011-08-08 2011-11-09 浙江天使生物工程有限公司 Cordyceps militaris-American ginseng capsule health-care product and preparation process thereof
CN102793177A (en) * 2012-09-07 2012-11-28 广州安德生物科技有限公司 Biological adhesion type cordyceps militaris liposome and preparation method thereof
CN109810201A (en) * 2019-03-01 2019-05-28 江南大学 The ultrasonic wave combination of acidic water extracting method of Cordyceps sinensis polysaccharide and cordycepin in a kind of Cordyceps militaris
CN214792422U (en) * 2021-05-08 2021-11-19 江西虹景天药业有限公司 Drying and sterilizing equipment for refining cordyceps militaris protein powder
WO2022088284A1 (en) * 2020-10-27 2022-05-05 苏州家和蚕业生物科技有限公司 Method of preparing silkworm chrysalis-cultured cordyceps militaris tablet

Patent Citations (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1075402A (en) * 1992-02-16 1993-08-25 陈顺志 Freshness-preserved cordyceps and food-processing method thereof
CN1137926A (en) * 1996-02-05 1996-12-18 杨满寿 Chinese caterpillar fungus with protective layer and its making method
CN101161133A (en) * 2007-05-16 2008-04-16 东莞市生物技术研究所 A method for drying cordyceps fresh sporophore
CN102232548A (en) * 2011-08-08 2011-11-09 浙江天使生物工程有限公司 Cordyceps militaris-American ginseng capsule health-care product and preparation process thereof
CN102793177A (en) * 2012-09-07 2012-11-28 广州安德生物科技有限公司 Biological adhesion type cordyceps militaris liposome and preparation method thereof
CN109810201A (en) * 2019-03-01 2019-05-28 江南大学 The ultrasonic wave combination of acidic water extracting method of Cordyceps sinensis polysaccharide and cordycepin in a kind of Cordyceps militaris
WO2022088284A1 (en) * 2020-10-27 2022-05-05 苏州家和蚕业生物科技有限公司 Method of preparing silkworm chrysalis-cultured cordyceps militaris tablet
CN214792422U (en) * 2021-05-08 2021-11-19 江西虹景天药业有限公司 Drying and sterilizing equipment for refining cordyceps militaris protein powder

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* Cited by examiner, † Cited by third party
Title
中国科学院四川分院中医中药研究所: "《四川中药志》", 四川人民出版社, pages: 598 - 599 *

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