CN1149631A - Method for preparing ferro-phosphorus from corundum slag - Google Patents
Method for preparing ferro-phosphorus from corundum slag Download PDFInfo
- Publication number
- CN1149631A CN1149631A CN 95118506 CN95118506A CN1149631A CN 1149631 A CN1149631 A CN 1149631A CN 95118506 CN95118506 CN 95118506 CN 95118506 A CN95118506 A CN 95118506A CN 1149631 A CN1149631 A CN 1149631A
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- China
- Prior art keywords
- corundum slag
- phosphorus
- slag
- raw material
- corundum
- Prior art date
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Abstract
The present invention uses corundum slag and phosphate ore as raw material, addes fusing agent and adopts the metallurgical blast furnace and conventional method to smelt. Compared with the existent technologies, the advantages of said method are simple operation, easy control, low productive cost, and full utilizing the industrial waste slags. The productive cost is lowered by 20%-30% than that of the traditional Technologies and the practical value is very great.
Description
The invention belongs to a kind of method of producing kakoxene with iron slag.
Traditional ferrophosphorus production method is to adopt the melting and obtain ferrophosphorus in electric furnace or blast furnace of iron or iron ore and Rock Phosphate (72Min BPL), and this Technology difficulty is big, and the production cost height.And the corundum slag is generally all outwelled as waste residue as a kind of industrial residue.
The objective of the invention is to: a kind of method of utilizing industrial residue to produce the ferrophosphorus product is provided, thereby reduces product cost greatly, and made full use of industrial residue again, turn waste into wealth.
The present invention constitutes like this: it is to be raw material with corundum slag, Rock Phosphate (72Min BPL), adds flux, adopts the metallurgy high temperature stove to smelt with conventional smelting process.
The present invention compared with prior art, have simple to operate, be easy to control, production cost is low, has made full use of advantages such as industrial residue, its production cost reduces by 20%~30% than traditional technology, has great practical value.
Embodiments of the invention 1: adopt the melting of miniaturization iron furnace, main raw material composition (%): corundum slag Fe72.1, Si15.6, Al5.8, Ti4.2, Po7; Silica SiO298.6, when furnace temperature rises to more than 1400 ℃, begin to feed in raw material, its order and batch of material are: 10 kilograms in coke, 10 kilograms of phosphorus ores, 5 kilograms of corundum slags, 4 kilograms in silica, reinforced 10 batches altogether, 45.3 kilograms of output ferrophosphorus, ferrophosphorus composition (%): P22.8, Si2.3, C0.9, S0.2, Mn0.1, phosphorous recovery: 76.3%.
Embodiment 2: adopt crucible oven to handle, with corundum slag 200 grams, Rock Phosphate (72Min BPL) 400 grams, silica 120 grams, clay 80 grams, to expect to put into plumbago crucible behind the mixing, in 1450 ℃ of reactions 2 hours, come out of the stove after cooling, slag iron separate, get ferrophosphorus 168.6 grams, ferrophosphorus composition (%): P22.3, Si0.5, C1.0, S0.1, Mn0.05, phosphorous recovery: 88.06%.
Claims (1)
1, a kind of method with preparing ferro-phosphorus from corundum slag is characterized in that: it is to be raw material with corundum slag, Rock Phosphate (72Min BPL), adds flux, adopts the metallurgy high temperature stove to smelt with conventional smelting process.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN95118506A CN1042351C (en) | 1995-11-03 | 1995-11-03 | Method for preparing ferro-phosphorus from corundum slag |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN95118506A CN1042351C (en) | 1995-11-03 | 1995-11-03 | Method for preparing ferro-phosphorus from corundum slag |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1149631A true CN1149631A (en) | 1997-05-14 |
CN1042351C CN1042351C (en) | 1999-03-03 |
Family
ID=5081735
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN95118506A Expired - Fee Related CN1042351C (en) | 1995-11-03 | 1995-11-03 | Method for preparing ferro-phosphorus from corundum slag |
Country Status (1)
Country | Link |
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CN (1) | CN1042351C (en) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1060689C (en) * | 1997-12-31 | 2001-01-17 | 云南磷肥工业有限公司 | Sorting and processing of ferro-phosphorus, and method of application |
CN103397126A (en) * | 2013-08-01 | 2013-11-20 | 河南豫中铁合金有限公司 | Ferrophosphorous and preparation method thereof |
CN105399069A (en) * | 2015-11-25 | 2016-03-16 | 云南师范大学 | Ferrophosphorus recycle method |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
SU438714A1 (en) * | 1973-05-03 | 1974-08-05 | Институт Металлургии И Обогащения Академии Наук Казахской Сср | Method of refining electrothermal ferrophosphorus |
JPS6357738A (en) * | 1986-08-27 | 1988-03-12 | Nippon Chem Ind Co Ltd:The | Manufacture of high-purity phosphoric iron |
-
1995
- 1995-11-03 CN CN95118506A patent/CN1042351C/en not_active Expired - Fee Related
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1060689C (en) * | 1997-12-31 | 2001-01-17 | 云南磷肥工业有限公司 | Sorting and processing of ferro-phosphorus, and method of application |
CN103397126A (en) * | 2013-08-01 | 2013-11-20 | 河南豫中铁合金有限公司 | Ferrophosphorous and preparation method thereof |
CN103397126B (en) * | 2013-08-01 | 2016-01-20 | 河南豫中铁合金有限公司 | A kind of ferrophosphorus and preparation method thereof |
CN105399069A (en) * | 2015-11-25 | 2016-03-16 | 云南师范大学 | Ferrophosphorus recycle method |
Also Published As
Publication number | Publication date |
---|---|
CN1042351C (en) | 1999-03-03 |
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PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
C19 | Lapse of patent right due to non-payment of the annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |