CN114950272A - Automatic dropping equipment for phosphorus oxychloride - Google Patents

Automatic dropping equipment for phosphorus oxychloride Download PDF

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Publication number
CN114950272A
CN114950272A CN202210635181.XA CN202210635181A CN114950272A CN 114950272 A CN114950272 A CN 114950272A CN 202210635181 A CN202210635181 A CN 202210635181A CN 114950272 A CN114950272 A CN 114950272A
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CN
China
Prior art keywords
wall
fixedly connected
phosphorus oxychloride
sleeve
cylinder
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Granted
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CN202210635181.XA
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Chinese (zh)
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CN114950272B (en
Inventor
李虹毅
祖加夫
胡文影
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Suzhou Hantech Chemical Co ltd
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Suzhou Hantech Chemical Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • B01J4/007Feed or outlet devices as such, e.g. feeding tubes provided with moving parts
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2204/00Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices
    • B01J2204/002Aspects relating to feed or outlet devices; Regulating devices for feed or outlet devices the feeding side being of particular interest
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Feeding, Discharge, Calcimining, Fusing, And Gas-Generation Devices (AREA)

Abstract

The invention discloses automatic phosphorus oxychloride dripping equipment, which belongs to the technical field of chemical product production and comprises a base and an adjusting component arranged on the outer wall of the top of the base, wherein a feeding mechanism is arranged on the inner wall of one side of the adjusting component, the feeding mechanism comprises a material storage component and a protection component, the material storage component comprises a sleeve and a charging barrel fixedly connected to the inner wall of the sleeve, the outer wall of the bottom end of the charging barrel is fixedly connected with a chassis, the charging barrel is provided with six air passages which are arranged circumferentially, and the air passages are respectively communicated with the chassis and the inner wall of the sleeve. The device is provided with the feeding mechanism, wherein the feeding mechanism is composed of the material storage component and the protection component, the material storage component can be used for transferring materials, the phosphorus oxychloride liquid is stored in a closed mode, the contact of the rest of the phosphorus oxychloride liquid with the outside is avoided, the volatilization of the phosphorus oxychloride is avoided, and in addition, due to the volatilization characteristic of the phosphorus oxychloride, the possibility of volatilization and sputtering exists in the space stage that liquid drops are dripped into the solution from the device during dripping, and due to the fact that the phosphorus oxychloride is quite dangerous, the protection component can provide observation and protection.

Description

Automatic dropping equipment for phosphorus oxychloride
Technical Field
The invention relates to a chemical dropwise adding device, in particular to automatic phosphorus oxychloride dropwise adding equipment, and belongs to the technical field of chemical product production.
Background
Phosphorus oxychloride is an important chemical raw material, is colorless transparent fuming liquid, is widely applied to the production of pesticides, medicines, dyes, phosphate esters and flame retardants, is a raw material for manufacturing organophosphorus pesticides, herbicides, chlordimeform and the like, is also used for producing plastic plasticizers, can also be used for chlorination reaction of long-acting sulfanilamide medicines, and is an intermediate for producing dyes, an organically synthesized chlorinating agent and a catalyst, an extracting agent of uranium ore and the like.
Traditional dropwise add equipment, during dropwise add phosphorus oxychloride hazardous articles, lack corresponding protection mechanism, lead to there being the sputtering danger among the dropwise add process, and dropwise add equipment can't regard as the material transfer, can't play good storage effect, can't avoid it to volatilize and lead to environmental pollution.
How to research the automatic dropping equipment of phosphorus oxychloride is a problem to be solved urgently at present.
Disclosure of Invention
The invention mainly aims to solve the defects of the prior art and provides automatic dropping equipment for phosphorus oxychloride.
The purpose of the invention can be achieved by adopting the following technical scheme:
automatic dropwise add equipment of phosphorus oxychloride, including base and the adjusting part who sets up in its top outer wall, adjusting part one side inner wall is provided with feeding mechanism, feeding mechanism includes stock subassembly and protection component, the stock subassembly includes sleeve pipe and the feed cylinder of fixed connection in its inner wall, feed cylinder bottom outer wall fixedly connected with chassis, the feed cylinder is provided with six circumference range's air flue, the air flue respectively with chassis and sleeve pipe inner wall UNICOM, air flue bottom inner wall fixedly connected with filter plug, the protection component includes slide sleeve that slides in the feed cylinder outside and the pipe support of fixed connection in slide sleeve bottom outer wall, the slide sleeve inner wall is provided with the semicircle arch, the feed cylinder outer wall is provided with the recess of adaptation with it, the pipe support inner wall is provided with four circumference range's transparent plate, pipe support bottom outer wall fixedly connected with plectane, the outer wall of the bottom of the circular plate is provided with a plurality of floating pieces.
Preferably, the outer wall is provided with ejection of compact funnel in the middle of the chassis bottom, chassis bottom outer wall fixedly connected with two springback poles of symmetry installation, the outer wall fixedly connected with circular arc structure's of the piston rod of springback pole water conservancy diversion frame, the outer wall is provided with the plug in the middle of the water conservancy diversion frame, the plug in slide in ejection of compact funnel's export inner wall.
Preferably, the outer wall of the top of the sleeve is fixedly connected with a linking frame, the outer wall of the top of the linking frame is fixedly connected with an extrusion cylinder, the outer wall of a piston rod of the extrusion cylinder is fixedly connected with a movable plate, and the outer wall of the bottom of the movable plate is provided with a scale rod which slides on the inner wall of the top of the linking frame.
Preferably, the outer wall of the bottom of the movable plate is fixedly connected with a feeding cylinder, the outer wall of the bottom of the feeding cylinder is fixedly connected with a sliding pipe with a three-way structure, the inner wall of the sleeve is provided with a plug sleeve, and the outer wall of the sliding pipe slides on the inner wall of the plug sleeve.
Preferably, the outer wall of the bottom end of the sliding pipe is fixedly connected with a piston disc, and a sealing ring is arranged on the outer wall of the piston disc.
Preferably, the inner wall of the bottom end of the sliding pipe is fixedly connected with a plug plate, a plurality of leakage holes are formed in the inner wall of the circumference of the plug plate, a sliding shaft of an I-shaped structure is connected to the inner wall of the middle of the plug plate in a sliding mode, and a communicating groove is formed in the outer wall of the sliding shaft.
Preferably, the outer wall of the piston rod of the feeding cylinder is fixedly connected with an inner shaft which slides on the inner wall of the sliding pipe, the inner wall of the inner shaft is provided with an L-shaped channel, and the wall of the inner shaft covers the outer wall of the top of the leak hole.
Preferably, the adjusting assembly comprises an adjusting cylinder fixedly connected to the outer wall of the top of the base and an adjusting rod arranged on the inner wall of the adjusting cylinder, a knob is arranged on the outer wall of one side of the adjusting cylinder, and a locking ring is fixedly connected to the outer wall of the top end of the adjusting rod.
Preferably, the outer wall in the middle of the locking ring is rotatably connected with a connecting arm, an extension plate is arranged on the inner wall in the middle of the connecting arm, and the outer wall of the sleeve is fixedly connected to the inner wall at one end of the connecting arm.
Preferably, the inner wall of the base is provided with magnetic sheets, the outer wall of one side of the base is provided with a rotating handle, the outer wall of the other side of the base is provided with a nitrogen pump box, the outer wall of the bottom of the base is provided with rollers, and the outlet end of the nitrogen pump box is communicated with the sleeve through a hose.
The invention has the beneficial technical effects that: according to the automatic dropping equipment of phosphorus oxychloride provided by the invention, the feeding mechanism is arranged, wherein the feeding mechanism consists of the material storage component and the protection component, the material storage component can be used for transferring materials, the phosphorus oxychloride liquid is stored in a closed manner, the contact of other outside is avoided, the volatilization of phosphorus oxychloride is avoided, and in addition, due to the volatilization characteristic of phosphorus oxychloride, the possibility of volatilization and sputtering exists in the space stage that liquid drops are dropped from the device into the solution during dropping, and due to the considerable danger of phosphorus oxychloride, the protection component can provide observation and protection; the whole feeding mechanism is fed into a dripping area, after the protection assembly is contacted with the liquid level, the circular plate and the floating sheet support the pipe frame above the liquid level, the charging barrel is pulled upwards, a negative pressure space is generated between the charging barrel and the inner wall of the pipe frame, the possibility of upward overflow of solution exists, the charging barrel, the chassis and the sleeve balance air pressure through an air passage, the overflow of the solution is avoided, the filter plug can avoid liquid diversion from being carried out in the air passage, meanwhile, the sliding sleeve depends on the semicircular bulge and the groove in the outer wall of the charging barrel, the rotation of the pipe frame can be avoided, further, the transparent plate can conveniently observe the dripping condition, and meanwhile, the overflow of sputtered liquid is avoided; the material storage assembly is arranged, when the feeding cylinder is in the original position, the L-shaped channel of the inner shaft is communicated with the inlet of the sliding pipe, the inlet end of the sliding pipe is communicated with an external pipeline, the material is conveniently filled, the sliding shaft is communicated with the plug plate, liquid bubbles are filtered by the plug plate and enter the inner wall of the charging barrel, after the filling is finished, the feeding cylinder is started to drive the inner shaft to move, so that the L-shaped channel is communicated with the inlet of the sliding pipe and is cut off, then the extrusion cylinder is started to drive the piston disc to descend, the material is pushed to pass through the base plate and is pushed to open the middle plug, and the circular arc structure of the flow guide frame can prevent the liquid from flowing upwards to corrode the rebound rod and release the material to enter a dripping area; through setting up adjusting part, linking up the arm and can rely on the extension of extension board, realize the regional extension of dropwise add, the height that feeding mechanism can be adjusted to knob, regulation section of thick bamboo and regulation pole simultaneously, the lock solid ring can conveniently link up the arm and rotate, and when the rotatory handle of base rotated, the gyro wheel stretched out, and the device can remove, and when the rotatory handle of base resets, its inside magnetic sheet can adsorb on agitated vessel surface, optimizes fixed effect.
Drawings
FIG. 1 is a schematic view of the overall structure of a preferred embodiment of the automatic dropping device of phosphorus oxychloride according to the invention;
FIG. 2 is a schematic structural view of a feeding mechanism of a preferred embodiment of the automatic dropping device of phosphorus oxychloride according to the invention;
FIG. 3 is a schematic view of a barrel structure of a preferred embodiment of the automatic dropping device of phosphorus oxychloride according to the invention;
FIG. 4 is a schematic structural view of a guide frame of a preferred embodiment of the automatic dropping device of phosphorus oxychloride according to the invention;
FIG. 5 is a schematic structural view of a sliding tube of a preferred embodiment of the automatic dropping device of phosphorus oxychloride according to the invention;
FIG. 6 is a schematic structural diagram of a stopper plate of a preferred embodiment of the automatic dropping device of phosphorus oxychloride according to the invention;
FIG. 7 is a schematic structural view of a pipe frame of a preferred embodiment of the automatic dropping device of phosphorus oxychloride according to the invention;
fig. 8 is a schematic structural view of an adjusting component of a preferred embodiment of the automatic phosphorus oxychloride dripping device according to the invention.
In the figure: 1-base, 2-connecting arm, 3-sliding sleeve, 4-sleeve, 5-extruding cylinder, 6-scale rod, 7-movable plate, 8-feeding cylinder, 9-floating plate, 10-charging barrel, 11-filter plug, 12-rebound rod, 13-flow guide frame, 14-base plate, 15-middle plug, 16-sliding tube, 17-inner shaft, 18-piston disc, 19-plug plate, 20-sealing ring, 21-sliding shaft, 22-pipe frame, 23-transparent plate, 24-adjusting cylinder, 25-knob, 26-extension plate, 27-locking ring, 28-nitrogen pump box and 29-roller.
Detailed Description
In order to make the technical solutions of the present invention more clear and definite, the present invention is further described in detail below with reference to the examples and the accompanying drawings, but the embodiments of the present invention are not limited thereto.
As shown in fig. 1-8, the automatic dropping device of phosphorus oxychloride provided in this embodiment comprises a base 1 and an adjusting assembly disposed on the top outer wall thereof, a feeding mechanism disposed on the inner wall of one side of the adjusting assembly, the feeding mechanism including a material storage assembly and a protection assembly, the material storage assembly including a sleeve 4 and a material cylinder 10 fixedly connected to the inner wall thereof, a chassis 14 fixedly connected to the bottom outer wall of the material cylinder 10, the material cylinder 10 having six air passages arranged circumferentially, the air passages respectively communicating with the chassis 14 and the inner wall of the sleeve 4, a filter plug 11 fixedly connected to the bottom inner wall of the air passage, the protection assembly including a sliding sleeve 3 sliding on the outer side of the material cylinder 10 and a pipe frame 22 fixedly connected to the bottom outer wall of the sliding sleeve 3, a semicircular protrusion disposed on the inner wall of the sliding sleeve 3, a groove adapted to the outer wall of the material cylinder 10, four transparent plates 23 arranged circumferentially disposed on the inner wall of the pipe frame 22, and a circular plate fixedly connected to the bottom outer wall of the pipe frame 22, the outer wall of the bottom of the circular plate is provided with a plurality of floating sheets 9.
The feeding mechanism is arranged, wherein the feeding mechanism is composed of a material storage component and a protection component, the material storage component can be used for transferring materials, the phosphorus oxychloride liquid is stored in a closed mode, the contact of the rest of the phosphorus oxychloride liquid with the outside is avoided, the volatilization of the phosphorus oxychloride is avoided, and the possibility of volatilization and sputtering exists in a space stage that liquid drops are dripped into a solution from a device due to the volatilization characteristic of the phosphorus oxychloride during dripping, and the protection component can provide observation and protection due to the fact that the phosphorus oxychloride is quite dangerous; wherein feeding mechanism is whole sends into the dropwise add region, after protection subassembly and liquid level contact, the plectane supports pipe support 22 in the liquid level top with superficial piece 9, then feed cylinder 10 upwards pull, its negative pressure space that produces with pipe support 22 inner wall, there is the upwards excessive possibility of solution, feed cylinder 10, chassis 14 and sleeve pipe 4 pass through air flue balanced atmospheric pressure, avoid solution to overflow, strain stopper 11 and can avoid liquid water conservancy diversion to carry out in the air flue, 3 recesses that rely on semicircle arch and feed cylinder 10 outer wall of sliding sleeve simultaneously, can avoid pipe support 22 to rotate, it is further, the dropwise add condition can conveniently be observed to transparent plate 23, avoid sputtering liquid excessive simultaneously.
In this embodiment, as shown in fig. 1 to 6, a discharge funnel is disposed on the outer wall of the middle of the bottom of the chassis 14, two symmetrically installed rebound rods 12 are fixedly connected to the outer wall of the bottom of the chassis 14, a diversion frame 13 with an arc structure is fixedly connected to the outer wall of a piston rod of the rebound rod 12, a middle plug 15 is disposed on the outer wall of the middle of the diversion frame 13, and the middle plug 15 slides on the inner wall of an outlet of the discharge funnel; the outer wall of the top of the sleeve 4 is fixedly connected with a connecting frame, the outer wall of the top of the connecting frame is fixedly connected with a squeezing cylinder 5, the outer wall of a piston rod of the squeezing cylinder 5 is fixedly connected with a movable plate 7, and the outer wall of the bottom of the movable plate 7 is provided with a scale rod 6 sliding on the inner wall of the top of the connecting frame; the outer wall of the bottom of the movable plate 7 is fixedly connected with a feeding cylinder 8, the outer wall of the bottom of the feeding cylinder 8 is fixedly connected with a sliding pipe 16 with a three-way structure, the inner wall of the sleeve 4 is provided with a plug sleeve, and the outer wall of the sliding pipe 16 slides on the inner wall of the plug sleeve; the outer wall of the bottom end of the sliding pipe 16 is fixedly connected with a piston disc 18, and the outer wall of the piston disc 18 is provided with a sealing ring 20; a plug plate 19 is fixedly connected to the inner wall of the bottom end of the sliding pipe 16, a plurality of leakage holes are formed in the circumferential inner wall of the plug plate 19, a sliding shaft 21 with an I-shaped structure is connected to the inner wall of the middle of the plug plate 19 in a sliding mode, and a communicating groove is formed in the outer wall of the sliding shaft 21; an inner shaft 17 sliding on the inner wall of the sliding pipe 16 is fixedly connected to the outer wall of a piston rod of the feeding cylinder 8, an L-shaped channel is arranged on the inner wall of the inner shaft 17, and the pipe wall of the inner shaft 17 covers the outer wall of the top of the leak hole.
Through arranging the material storage assembly, when the feeding cylinder 8 is in the original position, the L-shaped channel of the inner shaft 17 is communicated with the inlet of the sliding pipe 16, the inlet of the sliding pipe 16 is communicated with an external pipeline, so that materials can be conveniently filled, the sliding shaft 21 is communicated with the plug plate 19, liquid bubbles are filtered by the plug plate 19 and enter the inner wall of the charging barrel 10, after filling is finished, the feeding cylinder 8 is started to drive the inner shaft 17 to move, so that the communication between the L-shaped channel and the inlet of the sliding pipe 16 is cut off, then the extrusion cylinder 5 is started to drive the piston disc 18 to descend, push the materials to pass through the chassis 14 and push the middle plug 15 to be opened, and the circular arc structure of the guide frame 13 can prevent the rebound rod 12 from being corroded due to the upward flow of liquid and release the materials to enter a dripping area, and meanwhile, when the piston disc 18 is pressed downwards, the bottom of the sliding shaft 21 is reversely acted by the materials upwards to seal the middle of the plug plate 19, so as to prevent backflow of the liquids during dripping and dripping.
In this embodiment, as shown in fig. 1 and 8, the adjusting assembly includes an adjusting cylinder 24 fixedly connected to the outer wall of the top of the base 1 and an adjusting rod disposed on the inner wall thereof, the outer wall of one side of the adjusting cylinder 24 is provided with a knob 25, and the outer wall of the top end of the adjusting rod is fixedly connected with a locking ring 27; the middle outer wall of the locking ring 27 is rotatably connected with a connecting arm 2, the middle inner wall of the connecting arm 2 is provided with an extension plate 26, and the outer wall of the sleeve 4 is fixedly connected with the inner wall of one end of the connecting arm 2; the inner wall of the base 1 is provided with a magnetic sheet, the outer wall of one side of the base 1 is provided with a rotating handle, the outer wall of the other side of the base 1 is provided with a nitrogen pump box 28, the outer wall of the bottom of the base 1 is provided with a roller 29, and the outlet end of the nitrogen pump box 28 is communicated with the sleeve 4 through a hose.
Through setting up adjusting part, join in marriage arm 2 and can rely on extension plate 26 extension, realize the regional extension of dropwise add, the height that feeding mechanism can be adjusted to knob 25, regulation section of thick bamboo 24 and regulation pole simultaneously, lock ring 27 can conveniently join in marriage arm 2 and rotate, and when the rotatory handle of base 1 rotated, gyro wheel 29 stretched out, and the device can remove, and when the rotatory handle of base 1 resets, its inside magnetic sheet can adsorb on agitated vessel surface, optimizes fixed effect.
In this embodiment, as shown in fig. 1 to fig. 8, the working process of the automatic phosphorus oxychloride dropwise adding device provided in this embodiment is as follows:
step 1: when the feeding cylinder 8 is in the original position, the L-shaped channel of the inner shaft 17 is communicated with the inlet of the sliding pipe 16, the inlet end of the sliding pipe 16 is communicated with an external pipeline, so that the material is conveniently filled, the sliding shaft 21 is communicated with the plug plate 19, and the plug plate 19 is used for filtering vacuoles and entering the inner wall of the charging barrel 10;
step 2: after filling, the feeding cylinder 8 is started to drive the inner shaft 17 to move, so that the L-shaped channel is communicated with and cut off from the inlet of the sliding pipe 16, then the extrusion cylinder 5 is started to drive the piston disc 18 to descend, so that materials are pushed to pass through the base plate 14, and the middle plug 15 is pushed to be opened;
and step 3: the charging barrel 10, the chassis 14 and the sleeve 4 balance air pressure through an air passage to avoid overflow of solution, and the filter plug 11 can avoid liquid diversion to be carried out in the air passage.
In summary, in the present embodiment, according to the automatic dropping device of phosphorus oxychloride of the present embodiment, by providing the feeding mechanism, wherein the feeding mechanism is composed of the material storage component and the protection component, the material storage component can be used as a material transfer to store the liquid of phosphorus oxychloride in a sealed manner, thereby avoiding contact between the remaining external environment and volatilization of phosphorus oxychloride, and during dropping, due to the volatilization characteristic of phosphorus oxychloride, the possibility of volatilization and sputtering exists at the spatial stage when liquid drops are dropped from the device into the solution, and due to the considerable danger of phosphorus oxychloride, the protection component can provide observation and protection; the whole feeding mechanism is fed into a dripping area, after a protection assembly is contacted with a liquid level, a circular plate and a floating sheet 9 support a pipe frame 22 above the liquid level, then a charging barrel 10 is pulled upwards and is pulled upwards, a negative pressure space is formed between the charging barrel 10 and the inner wall of the pipe frame 22, the possibility of solution overflowing upwards exists, the charging barrel 10, a chassis 14 and a sleeve 4 balance air pressure through an air channel to avoid the solution overflowing, a filter plug 11 can avoid liquid diversion from being carried out in the air channel, meanwhile, a sliding sleeve 3 depends on a semicircular bulge and a groove in the outer wall of the charging barrel 10, the rotation of the pipe frame 22 can be avoided, further, a transparent plate 23 can facilitate observation of the dripping condition, and simultaneously avoid the overflowing of sputtered liquid; by arranging the material storage assembly, when the feeding cylinder 8 is in the original position, the L-shaped channel of the inner shaft 17 is communicated with the inlet of the sliding pipe 16, the inlet of the sliding pipe 16 is communicated with an external pipeline, so that materials can be conveniently filled, the sliding shaft 21 is communicated with the plug plate 19, liquid bubbles are filtered by the plug plate 19 and enter the inner wall of the charging barrel 10, after filling is finished, the feeding cylinder 8 is started to drive the inner shaft 17 to move, so that the communication between the L-shaped channel and the inlet of the sliding pipe 16 is cut off, then the extrusion cylinder 5 is started to drive the piston disc 18 to descend, push the materials to pass through the chassis 14 and push the middle plug 15 to be opened, and the arc structure of the guide frame 13 can prevent the rebound rod 12 from being corroded due to the upward flow of liquid and release the materials to enter a dripping area, and simultaneously when the piston disc 18 is pressed downwards, the bottom of the sliding shaft 21 is reversely acted due to the upward materials to seal the middle of the plug plate 19, so as to prevent backflow of the liquid during dripping and dripping; through setting up adjusting part, join in marriage arm 2 and can rely on extension plate 26 extension, realize the regional extension of dropwise add, the height that feeding mechanism can be adjusted to knob 25, regulation section of thick bamboo 24 and regulation pole simultaneously, lock ring 27 can conveniently join in marriage arm 2 and rotate, and when the rotatory handle of base 1 rotated, gyro wheel 29 stretched out, and the device can remove, and when the rotatory handle of base 1 resets, its inside magnetic sheet can adsorb on agitated vessel surface, optimizes fixed effect.
The above are only further embodiments of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can substitute or change the technical solution of the present invention and its concept within the scope of the present invention.

Claims (10)

1. Automatic dropwise add equipment of phosphorus oxychloride, its characterized in that, including base (1) and the adjusting part who sets up in its top outer wall, adjusting part one side inner wall is provided with feeding mechanism, feeding mechanism includes stock subassembly and protection component, the stock subassembly includes sleeve pipe (4) and fixed connection in feed cylinder (10) of its inner wall, feed cylinder (10) bottom outer wall fixedly connected with chassis (14), feed cylinder (10) are provided with the air flue of six circumference arrangements, the air flue respectively with chassis (14) with sleeve pipe (4) inner wall UNICOM, air flue bottom inner wall fixedly connected with filter plug (11), the protection component includes slide in slide sleeve (3) in the feed cylinder (10) outside and fixed connection in pipe support (22) of slide sleeve (3) bottom outer wall, slide sleeve (3) inner wall is provided with the semicircle arch, the feed cylinder (10) outer wall is provided with the recess of adaptation with it, and pipe support (22) inner wall is provided with transparent plate (23) that four circumferences were arranged, pipe support (22) bottom outer wall fixedly connected with plectane, plectane bottom outer wall is provided with a plurality of superficial pieces (9).
2. The automatic dropping device of phosphorus oxychloride as claimed in claim 1, wherein a discharging funnel is arranged on the bottom middle outer wall of the bottom plate (14), two symmetrically-installed rebound rods (12) are fixedly connected to the bottom outer wall of the bottom plate (14), a guide frame (13) with a circular arc structure is fixedly connected to the outer wall of the piston rod of the rebound rod (12), a middle plug (15) is arranged on the middle outer wall of the guide frame (13), and the middle plug (15) slides on the outlet inner wall of the discharging funnel.
3. The automatic phosphorus oxychloride dropwise adding equipment according to claim 2, wherein the top outer wall of the sleeve (4) is fixedly connected with a connecting frame, the top outer wall of the connecting frame is fixedly connected with a squeezing cylinder (5), the outer wall of a piston rod of the squeezing cylinder (5) is fixedly connected with a movable plate (7), and the outer wall of the bottom of the movable plate (7) is provided with a scale rod (6) sliding on the inner wall of the top of the connecting frame.
4. The automatic dropping device of phosphorus oxychloride as claimed in claim 3, wherein the outer wall of the bottom of the movable plate (7) is fixedly connected with a feeding cylinder (8), the outer wall of the bottom of the feeding cylinder (8) is fixedly connected with a sliding tube (16) with a three-way structure, the inner wall of the sleeve (4) is provided with a plug sleeve, and the outer wall of the sliding tube (16) slides on the inner wall of the plug sleeve.
5. The automatic dropping device of phosphorus oxychloride as claimed in claim 4, characterized in that a piston disc (18) is fixedly connected to the outer wall of the bottom end of the sliding tube (16), and a sealing ring (20) is arranged on the outer wall of the piston disc (18).
6. The automatic dropping device of phosphorus oxychloride as claimed in claim 4, wherein the inner wall of the bottom end of the sliding tube (16) is fixedly connected with a plug plate (19), the inner wall of the circumference of the plug plate (19) is provided with a plurality of leakage holes, the inner wall of the middle of the plug plate (19) is slidably connected with a sliding shaft (21) with an I-shaped structure, and the outer wall of the sliding shaft (21) is provided with a communicating groove.
7. The automatic dropping device of phosphorus oxychloride as claimed in claim 5, wherein the outer wall of the piston rod of the feeding cylinder (8) is fixedly connected with an inner shaft (17) sliding on the inner wall of the sliding tube (16), the inner wall of the inner shaft (17) is provided with an L-shaped channel, and the wall of the inner shaft (17) covers the outer wall of the top of the leak hole.
8. The automatic dropping device of phosphorus oxychloride as claimed in claim 1, wherein the adjusting assembly comprises an adjusting cylinder (24) fixedly connected to the outer wall of the top of the base (1) and an adjusting rod arranged on the inner wall of the adjusting cylinder, the outer wall of one side of the adjusting cylinder (24) is provided with a knob (25), and the outer wall of the top end of the adjusting rod is fixedly connected with a locking ring (27).
9. The automatic dropping device of phosphorus oxychloride as claimed in claim 8, characterized in that the locking ring (27) is rotatably connected with the connecting arm (2) at the middle outer wall, the connecting arm (2) is provided with an extension plate (26) at the middle inner wall, and the outer wall of the sleeve (4) is fixedly connected with the inner wall at one end of the connecting arm (2).
10. The automatic dropping device of phosphorus oxychloride as claimed in claim 1, wherein the inner wall of the base (1) is provided with magnetic sheets, the outer wall of one side of the base (1) is provided with a rotating handle, the outer wall of the other side of the base (1) is provided with a nitrogen pump box (28), the outer wall of the bottom of the base (1) is provided with rollers (29), and the outlet end of the nitrogen pump box (28) is communicated with the sleeve (4) through a hose.
CN202210635181.XA 2022-06-06 2022-06-06 Automatic phosphorus oxychloride dripping equipment Active CN114950272B (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202210635181.XA CN114950272B (en) 2022-06-06 2022-06-06 Automatic phosphorus oxychloride dripping equipment

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202210635181.XA CN114950272B (en) 2022-06-06 2022-06-06 Automatic phosphorus oxychloride dripping equipment

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Publication Number Publication Date
CN114950272A true CN114950272A (en) 2022-08-30
CN114950272B CN114950272B (en) 2023-06-16

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107674240A (en) * 2017-10-09 2018-02-09 常州建轩纺织品有限公司 A kind of preparation method of compound phosphonium flame retardant
CN212215447U (en) * 2020-05-13 2020-12-25 宿州汉泰化工有限公司 Automatic filling device of electronic grade phosphorus oxychloride
CN215923691U (en) * 2021-08-23 2022-03-01 惠州市恒德信精密科技有限公司 Full-automatic watchcase feeding device
CN114572718A (en) * 2022-03-14 2022-06-03 安徽惠泽农业科技有限公司 Fertilizer production dosing equipment

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107674240A (en) * 2017-10-09 2018-02-09 常州建轩纺织品有限公司 A kind of preparation method of compound phosphonium flame retardant
CN212215447U (en) * 2020-05-13 2020-12-25 宿州汉泰化工有限公司 Automatic filling device of electronic grade phosphorus oxychloride
CN215923691U (en) * 2021-08-23 2022-03-01 惠州市恒德信精密科技有限公司 Full-automatic watchcase feeding device
CN114572718A (en) * 2022-03-14 2022-06-03 安徽惠泽农业科技有限公司 Fertilizer production dosing equipment

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