CN114941061A - Heat treatment method for steel forging of hot-working die with ultra-thick section - Google Patents

Heat treatment method for steel forging of hot-working die with ultra-thick section Download PDF

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CN114941061A
CN114941061A CN202210527075.XA CN202210527075A CN114941061A CN 114941061 A CN114941061 A CN 114941061A CN 202210527075 A CN202210527075 A CN 202210527075A CN 114941061 A CN114941061 A CN 114941061A
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forging
forging blank
cooling
heat treatment
blank
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CN114941061B (en
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禹兴胜
石如星
元亚莎
武川
汪雨昌
李昌义
殷立涛
王九花
张玉栋
刘旺
陈朝阳
黄志恒
梁贤淑
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Citic Corp Of China
Luoyang Recasting Forging Co ltd
CITIC Heavy Industries Co Ltd
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Luoyang Recasting Forging Co ltd
CITIC Heavy Industries Co Ltd
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    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/26Methods of annealing
    • C21D1/28Normalising
    • CCHEMISTRY; METALLURGY
    • C21METALLURGY OF IRON
    • C21DMODIFYING THE PHYSICAL STRUCTURE OF FERROUS METALS; GENERAL DEVICES FOR HEAT TREATMENT OF FERROUS OR NON-FERROUS METALS OR ALLOYS; MAKING METAL MALLEABLE, e.g. BY DECARBURISATION OR TEMPERING
    • C21D1/00General methods or devices for heat treatment, e.g. annealing, hardening, quenching or tempering
    • C21D1/26Methods of annealing
    • C21D1/32Soft annealing, e.g. spheroidising
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

Abstract

A heat treatment method for a steel forging of a hot working die with an extra-thick section comprises the steps of normalizing a forging blank by a heating furnace, cooling the forging blank by blowing strong air by an industrial fan, spheroidizing annealing the forging blank by the heating furnace, performing oil cooling on the forging blank, and finally performing air cooling to room temperature. The air cooling rate of the forced air cooling can reach 2-4 ℃/min and is far higher than the air cooling rate, and the oil cooling rate after spheroidizing annealing is also far higher than the air cooling rate, so that the cooling rate is greatly improved, the cooling time is reduced, the formation of an upper bainite structure can be effectively avoided, the coarsening of carbide is inhibited, the temperature gradient in the thickness direction of the forge piece can be obviously reduced by improving the normalizing treatment and the spheroidizing annealing cooling rate, the temperature difference between the forge piece core and the surface layer area is reduced, the tissue difference between the forge piece core and the surface layer area is reduced, and the microstructure distribution uniformity is improved.

Description

Heat treatment method for steel forging of hot working die with ultra-thick section
Technical Field
The invention relates to the field of hot-work die steel forgings, in particular to a heat treatment method of an extra-thick section hot-work die steel forging.
Background
The hot die steel forging plays an important role in the field of industrial manufacturing, and is a necessary equipment material for forming various products. The service environment of the hot die steel forging is harsh, and the hot die steel forging is required to bear the tests of high temperature, high pressure and abrasion for a long time. Therefore, the industrial field has high requirements on the macroscopic mechanical property and the microstructure characteristic of the hot die steel forging. In order to meet the industrial requirements, the hot die steel forging is subjected to a heat treatment process of normalizing and annealing after forging so as to improve the comprehensive mechanical properties of the material.
However, when the thickness dimension of the hot-work die steel forging is larger than 700mm (an extra-thick section), a large temperature gradient can occur in the thickness direction of the forging in the normalizing air cooling process, and the core temperature is 300-400 ℃ higher than the surface temperature, so that the microstructure type and the grain size of the core are greatly different from the surface region; similarly, in the annealing and air cooling process of the forging, the core temperature in the thickness direction is still higher than the surface temperature by 200-300 ℃, so that the center region and the surface region of the forging after annealing have great differences in carbide nodularity, precipitate morphology size, strength, plasticity and toughness, and the microstructure and mechanical property homogeneity of the super-thick section hot work die steel forging are poor, and the performance requirements of the hot work die steel forging are difficult to meet. Therefore, how to improve the uniform distribution of the microstructure and the mechanical property of the super-thick section forging by improving the heat treatment process is a technical problem to be solved urgently by hot work die steel production enterprises.
Disclosure of Invention
The invention provides a heat treatment method of an extra-thick section hot work die steel forging, aiming at solving the problem of poor homogeneity of microstructure and mechanical property of the extra-thick section hot work die steel forging after heat treatment.
The technical scheme adopted by the invention for solving the technical problems is as follows: a heat treatment method of a hot work die steel forging with an ultra-thick section is used for carrying out heat treatment on a hot work die steel forging blank with the section thickness of more than 700mm, and comprises the following steps:
normalizing the forging blank by a heating furnace at a normalizing temperature Ac3+ (10-50 ℃), and keeping the temperature for 10-12 h and then discharging the forging blank out of the furnace;
secondly, cooling the forging blank by blowing strong wind through an industrial fan, wherein the wind cooling rate is controlled to be 2-4 ℃/min;
when the section thickness of the forging blank is 700-850 mm, the forging blank is cooled to 400-450 ℃ by air, and then the forging blank is placed into a heating furnace;
when the section thickness of the forging blank is larger than 850mm, air-cooling the forging blank to 500 +/-30 ℃, then putting the forging blank into a heating furnace, and continuously cooling the forging blank to 400-450 ℃ in the heating furnace;
and step three, spheroidizing annealing the forging blank by a heating furnace, heating the forging blank to 600-650 ℃, preserving heat for 8-10 h, then continuously heating the forging blank to Ac1+ (10-30 ℃), preserving heat for 25-27 h, discharging the forging blank out of the furnace, cooling oil to 350-400 ℃, and then cooling air to room temperature to complete the heat treatment of the hot-work die steel forging.
Preferably, the air volume of the industrial fan used in the step two is not less than 12000m 3 The rotation speed is not lower than 1400r/min, the voltage is 380V, and the power is 0.2 KW.
According to the technical scheme, the invention has the beneficial effects that:
the process improves the normalizing treatment and spheroidizing annealing cooling process of the hot-work die steel forging with the extra-thick section, a pure natural air cooling mode is not adopted any more, an industrial fan is adopted for cooling by blowing strong air after the normalizing treatment, and the air cooling rate of the cooling by blowing strong air can reach 2-4 ℃/min and is far higher than the cooling rate of air cooling, so that the cooling rate of the hot-work die steel forging with the extra-thick section is greatly improved, and the cooling time is reduced; the cooling speed of oil cooling after spheroidizing annealing is also far higher than that of air cooling, so that the cooling rate is greatly improved, the cooling time is shortened, the formation of an upper bainite structure can be effectively avoided, and simultaneously the coarsening of carbide is inhibited. Therefore, the cooling speed of normalizing treatment and spheroidizing annealing is increased, the temperature gradient in the thickness direction of the forging can be obviously reduced, and the temperature difference between the center of the forging and the surface layer area is reduced, so that the tissue difference between the center of the forging and the surface layer area is reduced, and the uniformity of microstructure distribution is improved.
Drawings
FIG. 1 is a shape and size diagram of a hot-work die steel forging of the first embodiment;
FIG. 2 is a schematic view of a heat treatment process flow according to the first embodiment;
FIG. 3 is a shape and size diagram of the hot work die steel forging of the second embodiment;
FIG. 4 is a schematic view of a heat treatment process flow of the second embodiment.
Detailed Description
A heat treatment method of a hot-work die steel forging with an ultra-thick section is used for carrying out heat treatment on a hot-work die steel forging blank with the section thickness of more than 700mm and comprises the following steps.
Normalizing the forging blank by a heating furnace at a normalizing temperature Ac3+ (10-50 ℃), and discharging after heat preservation for 10-12 h.
Secondly, strong air blowing cooling is carried out on the forging blank through an industrial fan, and the air volume of the industrial fan is not less than 12000m 3 The rotation speed is not lower than 1400r/min, the voltage is 380V, the power is 0.2KW, and the air cooling rate is controlled to be 2-4 ℃/min.
When the section thickness of the forging blank is 700-850 mm, the forging blank is air-cooled to 400-450 ℃, and then the forging blank is placed into a heating furnace.
And when the section thickness of the forging blank is larger than 850mm, air-cooling the forging blank to 500 +/-30 ℃, then putting the forging blank into a heating furnace, and continuously cooling the forging blank to 400-450 ℃ in the heating furnace.
And step three, spheroidizing annealing the forging blank by a heating furnace, heating the forging blank to 600-650 ℃, preserving heat for 8-10 h, then continuously heating the forging blank to Ac1+ (10-30 ℃), preserving heat for 25-27 h, discharging the forging blank out of the furnace, cooling oil to 350-400 ℃, and then cooling air to room temperature to complete the heat treatment of the hot-work die steel forging.
The first embodiment is as follows: the hot work die steel forging blank which is made of 55NiCrMoV7 and has the size specification of 4500mm multiplied by 2500mm multiplied by 900mm is subjected to heat treatment, the shape and the size of the forging blank are shown in figure 1, the thickness of the forging blank is 900mm, the forging blank belongs to an extra-thick section hot work die steel forging, and the heat treatment process flow is shown in figure 2.
Step 1, normalizing the forging blank by a heating furnace at a normalizing temperature Ac3+ (10-50 ℃), and discharging the forging blank after heat preservation for 10-12 h.
Step 2, performing strong air blowing cooling on the forging blank through an industrial fan, wherein the air volume of the industrial fan is not less than 12000m 3 The rotating speed is not lower than 1400r/min, the voltage is 380V, the power is 0.2KW, the air cooling speed is controlled to be 2-4 ℃/min, the forging blank is cooled to 400-450 ℃, and then the forging blank is placed into a heating furnace.
And 3, spheroidizing annealing the forging blank by using a heating furnace, heating the forging blank to 600-650 ℃, preserving heat for 8-10 h, then continuously heating the forging blank to Ac1+ (10-30 ℃), preserving heat for 25-27 h, discharging the forging blank out of the furnace, cooling oil to 350-400 ℃, and then cooling air to room temperature to complete the heat treatment of the hot-work die steel forging.
Example two: the hot work die steel forging blank which is made of 55NiCrMoV7 and has the size specification of 4500mm multiplied by 2650mm multiplied by 800mm is subjected to heat treatment, the shape and the size of the forging blank are shown in figure 3, the thickness of the forging blank is 800mm, the forging blank belongs to an extra-thick section hot work die steel forging, and the heat treatment process flow is shown in figure 4.
Step 1, normalizing the forging blank by a heating furnace at a normalizing temperature Ac3+ (10-50 ℃), and discharging the forging blank after heat preservation for 10-12 h.
Step 2, performing strong air blowing cooling on the forging blank through an industrial fan, wherein the air volume of the industrial fan is not less than 12000m 3 The rotating speed is not lower than 1400r/min, the voltage is 380V, the power is 0.2KW, the air cooling speed is controlled to be 2-4 ℃/min, the forging blank is cooled to 500 +/-30 ℃, and then the forging blank is placed into a heating furnace, and the forging blank is continuously cooled to 400-450 ℃ in the heating furnace.
And 3, spheroidizing annealing the forging blank by using a heating furnace, heating the forging blank to 600-650 ℃, preserving heat for 8-10 h, then continuously heating the forging blank to Ac1+ (10-30 ℃), preserving heat for 25-27 h, discharging, cooling oil to 350-400 ℃, and then cooling air to room temperature to complete the heat treatment of the hot-work die steel forging.
And (4) machining the forging blank, and removing the surface oxide layer and the surface stress concentration cracking part to obtain the hot-work die steel forging with the standard size. The hot-work die steel forgings in the first embodiment and the second embodiment are respectively taken at different positions in the thickness direction, microstructure metallographic observation and mechanical property comparison are carried out, the grain sizes and microstructure types of the forgings at different positions tend to be consistent, mechanical property indexes are respectively shown in tables 1 and 2, and the mechanical properties at different positions in the thickness direction are almost not different.
TABLE 1 mechanical properties of different thickness positions of a forged piece
Figure DEST_PATH_IMAGE001
TABLE 2 mechanical properties of the second forging at different thickness positions
Figure DEST_PATH_IMAGE002
Therefore, the cooling speed of normalizing treatment and spheroidizing annealing is increased, the temperature gradient in the thickness direction of the forging can be obviously reduced, and the temperature difference between the center of the forging and the surface layer area is reduced, so that the tissue difference between the center of the forging and the surface layer area is reduced, the uniformity of microstructure distribution is improved, and the comprehensive mechanical property of the hot-work die steel forging with the ultra-thick section is finally improved.

Claims (2)

1. A heat treatment method of a hot work die steel forging with an ultra-thick section is used for carrying out heat treatment on a hot work die steel forging blank with the section thickness of more than 700mm, and is characterized by comprising the following steps:
normalizing the forging blank by a heating furnace at a normalizing temperature Ac3+ (10-50 ℃), keeping the temperature for 10-12 h, and discharging;
secondly, cooling the forging blank by blowing strong wind through an industrial fan, wherein the wind cooling rate is controlled to be 2-4 ℃/min;
when the section thickness of the forging blank is 700-850 mm, the forging blank is air-cooled to 400-450 ℃, and then the forging blank is placed into a heating furnace;
when the section thickness of the forging blank is larger than 850mm, air-cooling the forging blank to 500 +/-30 ℃, then putting the forging blank into a heating furnace, and continuously cooling the forging blank to 400-450 ℃ in the heating furnace;
and step three, spheroidizing annealing the forging blank by a heating furnace, heating the forging blank to 600-650 ℃, preserving heat for 8-10 h, then continuously heating the forging blank to Ac1+ (10-30 ℃), preserving heat for 25-27 h, discharging the forging blank out of the furnace, cooling oil to 350-400 ℃, and then cooling air to room temperature to complete the heat treatment of the hot-work die steel forging.
2. The heat treatment method for the hot work die steel forging with the extra thick section as claimed in claim 1, wherein the heat treatment method comprises the following steps: the air volume of the industrial fan used in the second step is not less than 12000m 3 The rotation speed is not lower than 1400r/min, the voltage is 380V, and the power is 0.2 KW.
CN202210527075.XA 2022-05-16 Heat treatment method for super-thick section hot work die steel forging Active CN114941061B (en)

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Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101591727A (en) * 2009-06-17 2009-12-02 江苏森威精锻有限公司 A kind of heat treating method of low-carbon alloy steel forging blank
CN101709365A (en) * 2009-11-13 2010-05-19 中原特钢股份有限公司 Heating processing process in production of high -carbon chromium bearing steel
CN103468889A (en) * 2013-08-30 2013-12-25 马鞍山市晨旭机械制造有限公司 After-forged heat treatment technique of 9Cr2MoV chilled roll steel
CN104259801A (en) * 2014-09-19 2015-01-07 马鞍山邦斯科自动化科技有限公司 Manufacturing method of high-toughness reamer
CN106521106A (en) * 2016-11-24 2017-03-22 通裕重工股份有限公司 Heat treatment technology capable of improving mechanical property of forged piece after forging
CN106811580A (en) * 2017-02-13 2017-06-09 钢铁研究总院 A kind of annealing process of H13 hot die steels
WO2017206552A1 (en) * 2016-06-03 2017-12-07 上海新闵(东台)重型锻造有限公司 Monoblock forging of nuclear power steam generator housing and method for molding same by forging
CN107686878A (en) * 2017-03-30 2018-02-13 山西同航特钢有限公司 A kind of manufacturing process of hot-work die steel forgings
CN108823381A (en) * 2018-07-12 2018-11-16 河钢股份有限公司 A kind of heat treatment process improving H13 hot-work die steel forging material structural homogenity
CN110405121A (en) * 2019-06-26 2019-11-05 中信重工机械股份有限公司 A kind of forging method of Heavy Back-Up Roll forging
CN113862434A (en) * 2021-09-18 2021-12-31 河南中原特钢装备制造有限公司 Heat treatment process of 35CrNi3MoVR material for thick-wall ultrahigh-pressure container
CN114351042A (en) * 2021-11-26 2022-04-15 河北工程大学 Die steel and preheating treatment method for carbide dispersion in die steel
CN114411043A (en) * 2021-12-24 2022-04-29 钢铁研究总院 Preparation method of large hot forging hot work die steel

Patent Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101591727A (en) * 2009-06-17 2009-12-02 江苏森威精锻有限公司 A kind of heat treating method of low-carbon alloy steel forging blank
CN101709365A (en) * 2009-11-13 2010-05-19 中原特钢股份有限公司 Heating processing process in production of high -carbon chromium bearing steel
CN103468889A (en) * 2013-08-30 2013-12-25 马鞍山市晨旭机械制造有限公司 After-forged heat treatment technique of 9Cr2MoV chilled roll steel
CN104259801A (en) * 2014-09-19 2015-01-07 马鞍山邦斯科自动化科技有限公司 Manufacturing method of high-toughness reamer
WO2017206552A1 (en) * 2016-06-03 2017-12-07 上海新闵(东台)重型锻造有限公司 Monoblock forging of nuclear power steam generator housing and method for molding same by forging
CN106521106A (en) * 2016-11-24 2017-03-22 通裕重工股份有限公司 Heat treatment technology capable of improving mechanical property of forged piece after forging
CN106811580A (en) * 2017-02-13 2017-06-09 钢铁研究总院 A kind of annealing process of H13 hot die steels
CN107686878A (en) * 2017-03-30 2018-02-13 山西同航特钢有限公司 A kind of manufacturing process of hot-work die steel forgings
CN108823381A (en) * 2018-07-12 2018-11-16 河钢股份有限公司 A kind of heat treatment process improving H13 hot-work die steel forging material structural homogenity
CN110405121A (en) * 2019-06-26 2019-11-05 中信重工机械股份有限公司 A kind of forging method of Heavy Back-Up Roll forging
CN113862434A (en) * 2021-09-18 2021-12-31 河南中原特钢装备制造有限公司 Heat treatment process of 35CrNi3MoVR material for thick-wall ultrahigh-pressure container
CN114351042A (en) * 2021-11-26 2022-04-15 河北工程大学 Die steel and preheating treatment method for carbide dispersion in die steel
CN114411043A (en) * 2021-12-24 2022-04-29 钢铁研究总院 Preparation method of large hot forging hot work die steel

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