CN114904477A - Conical preheating chemical solution reaction container - Google Patents
Conical preheating chemical solution reaction container Download PDFInfo
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- CN114904477A CN114904477A CN202210692294.3A CN202210692294A CN114904477A CN 114904477 A CN114904477 A CN 114904477A CN 202210692294 A CN202210692294 A CN 202210692294A CN 114904477 A CN114904477 A CN 114904477A
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- pipe
- gas transmission
- reaction tank
- fixed mounting
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- 238000006243 chemical reaction Methods 0.000 title claims abstract description 95
- 239000000126 substance Substances 0.000 title claims abstract description 21
- 230000007246 mechanism Effects 0.000 claims abstract description 123
- 238000007789 sealing Methods 0.000 claims abstract description 37
- 238000003860 storage Methods 0.000 claims abstract description 28
- 230000000149 penetrating effect Effects 0.000 claims abstract description 10
- 230000005540 biological transmission Effects 0.000 claims description 61
- 239000007788 liquid Substances 0.000 claims description 60
- 238000007790 scraping Methods 0.000 claims description 35
- 239000000706 filtrate Substances 0.000 claims description 21
- 238000004140 cleaning Methods 0.000 claims description 20
- 239000000463 material Substances 0.000 claims description 11
- 238000009434 installation Methods 0.000 claims description 9
- 238000001914 filtration Methods 0.000 claims description 8
- 230000003139 buffering effect Effects 0.000 claims description 5
- 241001233242 Lontra Species 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 abstract description 3
- 238000005265 energy consumption Methods 0.000 abstract 1
- 239000002994 raw material Substances 0.000 description 8
- 239000007787 solid Substances 0.000 description 8
- 238000000034 method Methods 0.000 description 5
- 238000003756 stirring Methods 0.000 description 4
- 230000008569 process Effects 0.000 description 3
- 230000000694 effects Effects 0.000 description 2
- 238000010030 laminating Methods 0.000 description 2
- 230000036632 reaction speed Effects 0.000 description 2
- 239000002910 solid waste Substances 0.000 description 2
- 230000009471 action Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000009172 bursting Effects 0.000 description 1
- 238000012824 chemical production Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000010926 purge Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000009923 sugaring Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/01—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
- B01D29/03—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements self-supporting
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D29/00—Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
- B01D29/62—Regenerating the filter material in the filter
- B01D29/64—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element
- B01D29/6469—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element scrapers
- B01D29/6476—Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element scrapers with a rotary movement with respect to the filtering element
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/087—Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Organic Chemistry (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
Abstract
The invention relates to the field of chemical reaction, in particular to a conical preheating chemical solution reaction vessel, which comprises a reaction tank and a supporting base, wherein the supporting base is fixedly arranged at the bottom of the reaction tank, a sealing mechanism is fixedly arranged at the upper end of the reaction tank, a first gas conveying mechanism is arranged at the upper end of the sealing mechanism in a penetrating way, the other end of the first gas conveying mechanism is fixedly connected with a rotating mechanism, the rotating mechanism is fixedly arranged at the upper end of the sealing mechanism, a rotating mechanism is rotatably arranged in the reaction tank and is rotatably arranged in the sealing mechanism, the rotating mechanism is fixedly connected with the rotating mechanism, the other end of the rotating mechanism is fixedly connected with a second gas conveying mechanism, the other end of the second gas conveying mechanism is fixedly arranged on a gas storage tank, the gas storage tank is fixedly arranged outside the reaction tank, a third gas conveying mechanism is fixedly arranged at the lower end of the reaction tank, and the other end of the third gas conveying mechanism is fixedly connected with a preheating mechanism, and preheat mechanism fixed mounting on the retort, not only can reduce energy consumption, can improve production efficiency moreover.
Description
Technical Field
The invention relates to the field of chemical reactions, in particular to a conical preheating chemical solution reaction container.
Background
The chemical reactions in chemical production can be divided into endothermic reactions and exothermic reactions according to reaction heat effects, the temperature has important influence on the reactions in the chemical reaction process, solid and liquid participate in the reactions and the chemical reactions with gas generation, some gas generated by the reactions belongs to pollutant gas, so the gas cannot be directly discharged, and certain heat is carried by the gas generated in the reaction process to be heated, if the heat is directly ignored, energy waste to a certain extent can be caused, in addition, in the solid-liquid reaction process, some crystals can be influenced by the gas generated in the reactions, so that bubbles are attached to the surface of the solid, the contact area of the solid and the liquid is prevented to a certain extent, and the reaction rate is reduced.
Disclosure of Invention
Aiming at the problems in the prior art, the invention provides a conical preheating chemical solution reaction vessel.
The technical scheme adopted by the invention for solving the technical problems is as follows: a conical preheating chemical solution reaction vessel comprises a reaction tank and a supporting base, wherein the supporting base is fixedly arranged at the bottom of the reaction tank, a sealing mechanism is fixedly arranged at the upper end of the reaction tank, a moving arm is rotatably arranged at one side of the sealing mechanism, the other end of the moving arm is fixedly arranged on the supporting base, a first gas conveying mechanism is arranged at the upper end of the sealing mechanism in a penetrating way, a rotating mechanism 7 is fixedly connected at the other end of the first gas conveying mechanism, the rotating mechanism is fixedly arranged at the upper end of the sealing mechanism, a rotating mechanism is rotatably arranged in the reaction tank, the rotating mechanism is rotatably arranged in the sealing mechanism and is fixedly connected with the rotating mechanism, a second gas conveying mechanism is fixedly connected at the other end of the rotating mechanism, the other end of the second gas conveying mechanism is fixedly arranged on a gas storage tank, the gas storage tank is fixedly arranged at the outer side of the reaction tank, a third gas conveying mechanism is fixedly arranged at the lower end of the reaction tank, and a preheating mechanism is fixedly connected at the other end of the third gas conveying mechanism, and the preheating mechanism is fixedly arranged on the reaction tank.
Specifically, sealing mechanism includes the top cap, and the seal cover, locking is detained and is carried the gas port, and the gas port link up and fixed the setting in top cap one side, and top cap lower extreme fixed mounting has the seal cover, and the seal cover can make top cap and retort seal installation, and the top cap lower extreme outside is fixed to be provided with a plurality of locking and detains, and locks to detain and to make top cap and retort fixed closely the installation.
Specifically, first gas transmission mechanism includes first gas-supply pipe and compressor, and first gas-supply pipe fixed mounting is on the compressor, and the first gas-supply pipe other end can be with gas transmission port through connection.
Specifically, slewing mechanism includes the wind wheel, seal box and axis of rotation, and the wind wheel rotates to be installed inside the seal box, and seal box fixed mounting is in the top cap upper end, and the first gas-supply pipe other end through connection seal box, and the axis of rotation rotates to be installed on the top cap.
Specifically, the second gas transmission mechanism comprises a second gas transmission pipe and a second control valve, the second control valve is fixedly mounted on the second gas transmission pipe, one end of the second gas transmission pipe is communicated with the seal box, and the other end of the second gas transmission pipe is communicated with the gas storage tank.
The preheating mechanism comprises an air inlet, a gas collecting cavity, a heater and an air outlet pipe, the air inlet is fixedly arranged at the upper end of the reaction tank, the gas collecting cavity is arranged inside the reaction tank, the air inlet is in through connection with the gas collecting cavity, the heater is fixedly arranged on the reaction tank outside the air inlet, the air outlet pipe is fixedly arranged at the lower end of the other side of the reaction tank, and the air outlet pipe is in through connection with the gas collecting cavity.
Specifically, the third gas transmission mechanism comprises a third control valve and a third gas transmission pipe, the third control valve is fixedly installed on the third gas transmission pipe, one end of the third gas transmission pipe is fixedly installed on the gas storage tank, the other end of the third gas transmission pipe is fixedly installed on the heater, and the other end of the third gas transmission pipe is communicated with the gas inlet.
Concretely, retort lower extreme fixed mounting has a liquid mechanism, and goes out liquid mechanism and include filter component, goes out liquid control valve and drain pipe, and the drain pipe is fixed to be set up at the retort lower extreme, and drain pipe and retort through connection, goes out liquid control valve fixed mounting at the drain pipe other end, and filter component fixed mounting at the drain pipe middle part.
Specifically, rotary mechanism includes swiveling wheel, swivel mount, rotation axis and cleaning brush, and the swiveling wheel rotates to be installed inside the top cap, and rotation axis lower extreme fixed mounting is in the centre of a circle position of swiveling wheel, the non-centre of a circle position fixed mounting rotation axis of swiveling wheel downside, rotation axis lower extreme fixed connection swivel mount, cleaning brush fixed mounting is in the swivel mount outside, and cleaning brush and retort inner wall closely laminate.
Concretely, the filtering component includes the filtrating component, scrape material component and gentle liquid component, the filtrating component rotates and installs on the drain pipe, and filtrating component and the installation of slow liquid component rotation, and scrape material component and the closely laminating of filtrating component, the filtrating component includes driven bevel gear and filtrating board, the filtrating board rotates and installs on the drain pipe, and filtrating board outside fixed mounting has driven bevel gear, driven bevel gear rotates and installs on the drain pipe, the slow liquid mechanism includes initiative bevel gear and rotating fan, rotating fan rotates and installs on the drain pipe, and rotating fan other end fixed mounting has initiative bevel gear, the initiative bevel gear rotates and installs on the drain pipe, and initiative bevel gear and driven bevel gear meshing installation.
Specifically, scrape material mechanism including scraping magazine and clearance piece, scrape magazine and clearance piece fixed mounting, scrape the magazine including scraping the flitch, stock chest and weeping otter board, the stock chest setting is scraping the magazine inside, and scrape magazine bottom fixed mounting have the weeping otter board, scrape magazine right side fixed mounting and scrape the flitch, and scrape flitch and closely laminate with the filtrating board, the clearance piece includes the connecting rod, spring and closing plate, clearance box upper end fixed mounting connecting rod, and the connecting rod removes and installs on the drain pipe, connecting rod upper end fixed mounting has the closing plate.
Specifically, the fourth gas transmission mechanism comprises a fourth gas transmission pipe and a fourth control valve, the fourth control valve is fixedly installed on the fourth gas transmission pipe, and one end of the fourth gas transmission pipe is fixedly installed on the gas storage tank.
The invention has the beneficial effects that:
according to the conical preheating chemical solution reaction container, the wind wheel, the rotating shaft, the rotating wheel and the rotating frame are matched for use, the rotating shaft is driven by the wind wheel to rotate with the rotating wheel in the circle center, the rotating wheel drives the rotating frame to rotate and stir in the reaction tank through the rotating shaft, the attachment time of bubbles on solid raw materials is reduced, the reaction speed is accelerated, the production efficiency is improved, the rotating frame drives the cleaning brush to scrape and clean the molten (similar to sugaring) solid raw materials on the inner wall of the reaction tank, and the raw materials are prevented from being left and adhering to the inner wall of the reaction tank.
According to the conical preheating chemical solution reaction vessel, the driven bevel gear, the scraper plate, the scraper box, the rotary fan and the driving gear are used in a matched mode, the rotary fan performs buffering and speed reduction on the flowing liquid when rotating, hidden danger of liquid outlet pipe bursting is reduced, the rotary fan enables the driven bevel gear to drive the filter liquid plate and the scraper plate to perform rotary scraping through rotation of the driving bevel gear, rotary scraping cleaning is performed on the surface of the filter liquid plate, solid waste materials remained after reaction are prevented from being adhered and blocked on the filter liquid plate, and the filtering efficiency of the filter liquid plate is improved.
Drawings
The invention is further illustrated with reference to the following figures and examples.
FIG. 1 is a schematic view of the overall structure of the present invention;
FIG. 2 is a schematic cross-sectional view of section A-A of FIG. 1 according to the present invention;
FIG. 3 is a schematic cross-sectional view of section B-B of FIG. 1 according to the present invention;
FIG. 4 is a schematic view of the wind wheel and the seal box of FIG. 1 according to the present invention;
FIG. 5 is a schematic structural view of the scraper box of FIG. 2 according to the present invention;
in the figure: 1. a reaction tank; 2. a support base; 3. a sealing mechanism; 301. a top cover; 302. sealing sleeves; 303. a locking buckle; 304. a gas transmission port; 4. a preheating mechanism; 411. an air inlet; 412. a gas collection cavity; 413. a heater; 414. an air outlet pipe; 6. a first gas delivery mechanism; 611. a first gas delivery pipe; 613. a compressor; 7. a rotating mechanism; 711. a wind wheel; 712. a sealing box; 713. a rotating shaft; 10. a second gas transmission mechanism; 101. a second control valve; 102. a second gas delivery pipe; 11. a moving arm; 12. a third gas transmission mechanism; 121. a third control valve; 122. a third gas delivery pipe; 13. a gas storage tank; 14. a fourth gas transmission mechanism; 141. a fourth control valve; 142. a fourth gas delivery pipe; 15. a liquid outlet mechanism; 151. a filter member; 152. a liquid outlet control valve; 153. a liquid outlet pipe; 17. a rotation mechanism; 171. a rotating wheel; 172. a rotating frame; 173. a rotating shaft; 174. cleaning a brush; 18. a filtrate member; 181. a driven bevel gear; 182. a filtrate plate; 19. a scraping member; 191. scraping the material box; 1911. a scraping plate; 1912. a storage tank; 1913. a liquid leakage screen plate; 192. cleaning the workpiece; 1921. a connecting rod; 1923. a sealing plate; 20. a buffer mechanism; 201. a drive bevel gear; 202. the fan is rotated.
Detailed Description
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further described with the specific embodiments.
As shown in fig. 1-5, the conical preheating chemical solution reaction vessel according to the present invention comprises a reaction tank 1 and a supporting base 2, the supporting base 2 is fixedly installed at the bottom of the reaction tank 1, a sealing mechanism 3 is fixedly installed at the upper end of the reaction tank 1, a moving arm 11 is rotatably installed at one side of the sealing mechanism 3, the other end of the moving arm 11 is fixedly installed on the supporting base 2, a first gas transmission mechanism 6 is installed at the upper end of the sealing mechanism 3 in a penetrating manner, the other end of the first gas transmission mechanism 6 is fixedly connected with a rotating mechanism 77, the rotating mechanism 7 is fixedly installed at the upper end of the sealing mechanism 3, a rotating mechanism 17 is rotatably installed inside the reaction tank 1, the rotating mechanism 17 is rotatably installed inside the sealing mechanism 3, the rotating mechanism 17 is fixedly connected with the rotating mechanism 7, the other end of the rotating mechanism 7 is fixedly connected with a second gas transmission mechanism 10, the other end of the second gas transmission mechanism 10 is fixedly installed on a gas storage tank 13, and the gas storage tank 13 is fixedly arranged at the outer side of the reaction tank 1, the lower end of the reaction tank 1 is fixedly provided with a third gas transmission mechanism 12, the other end of the third gas transmission mechanism 12 is fixedly connected with a preheating mechanism 4, and the preheating mechanism 4 is fixedly arranged on the reaction tank 1.
Specifically, sealing mechanism 3 includes top cap 301, seal cover 302, 303 and gas transmission mouth 304 are detained in the locking, gas transmission mouth 304 link up and fixed the setting in top cap 301 one side, top cap 301 lower extreme fixed mounting has seal cover 302, and seal cover 302 can make top cap 301 and retort 1 seal installation, the fixed a plurality of locking that is provided with in top cap 301 lower extreme outside detains 303, and locking detains 303 can make top cap 301 and retort 1 fixed inseparable installation, and then provide a closed environment to the chemical reaction in retort 1, prevent that foreign matter from participating in the reaction, and prevent that the polluting product that produces from drifting about in the air in the reaction, cause the pollution to reveal.
Specifically, the first gas transmission mechanism 6 includes a first gas transmission pipe 611 and a compressor, the first gas transmission pipe 611 is fixedly installed on the compressor, and the other end of the first gas transmission pipe 611 can be communicated with the gas transmission port 304 to compress and transmit gas generated by the reaction, so that the gas generation rate is prevented from being slow, and high-speed gas flow can still be provided for subsequent movement.
Specifically, the rotating mechanism 7 comprises a wind wheel 711, a seal box 712 and a rotating shaft 713, the wind wheel 711 is rotatably installed inside the seal box 712, the seal box 712 is fixedly installed at the upper end of the top cover 301, the other end of the first air pipe 611 is connected with the seal box 712 in a penetrating manner, the rotating shaft 713 is rotatably installed on the top cover 301, and the wind wheel 711 provides power for high-speed circulating air flow for stirring movement, so that the utilization of air is enhanced, and a positive feedback path is formed, wherein the more air is generated and the faster stirring is performed.
Specifically, the second gas transmission mechanism 10 includes a second gas transmission pipe 102 and a second control valve 101, the second control valve 101 is fixedly installed on the second gas transmission pipe 102, one end of the second gas transmission pipe 102 is installed on the seal box 712 in a penetrating manner, and the other end of the second gas transmission pipe 102 is connected with the gas storage tank 13 in a penetrating manner, so that the gas is stored in the gas storage tank 13.
Specifically, preheat mechanism 4 and include air inlet 411, gas collecting chamber 412, heat generator 413 and outlet duct 414, air inlet 411 is fixed to be set up in retort 1 upper end, gas collecting chamber 412 sets up in retort 1's jar internal portion, and air inlet 411 and gas collecting chamber 412 through connection, heat generator 413 is fixed to be set up on retort 1 in the air inlet 411 outside, outlet duct 414 is fixed to be set up at retort 1 opposite side lower extreme, and outlet duct 414 and gas collecting chamber 412 through connection, make the gaseous preheating heat supply raw materials for the reaction that produces, reduce the searching for the utilization to other heat sources.
Specifically, the third gas transmission mechanism 12 includes a third control valve 121 and a third gas transmission pipe 122, the third control valve 121 is fixedly mounted on the third gas transmission pipe 122, one end of the third gas transmission pipe 122 is fixedly mounted on the gas storage tank 13, the other end of the third gas transmission pipe 122 is fixedly mounted on the heater 413, and the other end of the third gas transmission pipe 122 is connected to the gas inlet 411 in a penetrating manner.
Specifically, a liquid outlet mechanism 15 is fixedly mounted at the lower end of the reaction tank 1, the liquid outlet mechanism 15 comprises a filtering member 151, a liquid outlet control valve 152 and a liquid outlet pipe 153, the liquid outlet pipe 153 is fixedly arranged at the lower end of the reaction tank 1, the liquid outlet pipe 153 is communicated with the reaction tank 1, the liquid outlet control valve 152 is fixedly mounted at the other end of the liquid outlet pipe 153, and the filtering member 151 is fixedly mounted in the middle of the liquid outlet pipe 153.
Specifically, rotary mechanism 17 includes swiveling wheel 171, swivel mount 172, rotation axis 173 and cleaning brush 174, and swiveling wheel 171 rotates and installs inside top cap 301, and rotation axis 713 lower extreme fixed mounting is in the centre of a circle position of swiveling wheel 171, and the non-centre of a circle position fixed mounting rotation axis 173 of swiveling wheel 171 downside, rotation axis 173 lower extreme fixed connection swivel mount 172, cleaning brush 174 fixed mounting is in the swivel mount 172 outside, and cleaning brush 174 closely laminates with retort 1 inner wall for swivel mount 172 stirs the internal reaction, improves reaction rate.
In particular, the filtering member 151 comprises a filtrate member 18, a scraping member 19 and a buffer member, the filtrate member 18 is rotatably mounted on the liquid outlet pipe 153, the filtrate member 18 and the buffer member are rotatably mounted, the scraping member 19 is tightly attached to the filtrate member 18, the filtrate member 18 comprises a driven bevel gear 181 and a filtrate plate 182, the filtrate plate 182 is rotatably mounted on the liquid outlet pipe 153, and the outer side of the filtrate plate 182 is fixedly provided with a driven bevel gear 181, the driven bevel gear 181 is rotatably arranged on the liquid outlet pipe 153, the buffer mechanism 20 comprises a driving bevel gear 201 and a rotating fan 202, the rotating fan 202 is rotatably arranged on the liquid outlet pipe 153, and the other end of the rotating fan 202 is fixedly provided with a driving bevel gear 201, the driving bevel gear 201 is rotatably arranged on the liquid outlet pipe 153, and the driving bevel gear 201 and the driven bevel gear 181 are engaged with each other, the power is provided by the effluent water flow, so that the rotating fan 202 can slow down the effluent speed and perform rotary filtration at the same time.
Specifically, the scraping mechanism comprises a scraping box 191 and a cleaning piece 192, the scraping box 191 and the cleaning piece 192 are fixedly installed, the scraping box 191 comprises a scraping plate 1911, a storage groove 1912 and a leakage net plate 1913, the storage groove 1912 is arranged inside the scraping box 191, the leakage net plate 1913 is fixedly installed at the bottom of the scraping box 191, the scraping plate 1911 is fixedly installed on the right side of the scraping box 191, the scraping plate 1911 is tightly attached to the filtrate plate 182, the cleaning piece 192 comprises a connecting rod 1921, a spring and a sealing plate 1923, the connecting rod 1921 is fixedly installed at the upper end of the cleaning box, the connecting rod 1921 is movably installed on the outlet pipe 153, the sealing plate 1923 is fixedly installed at the upper end of the connecting rod 1921, so that the scraping and cleaning can be conveniently performed on the filtrate plate 182 in rotation, and the scraped residual materials are collected and removed.
Specifically, the fourth air delivery mechanism 14 includes a fourth air delivery pipe 142 and a fourth control valve 141, the fourth control valve 141 is fixedly installed on the fourth air delivery pipe 142, and one end of the fourth air delivery pipe 142 is fixedly installed on the air storage tank 13, so as to enter the air storage tank 13 for the first time of preheating air at the beginning of the reaction.
The working principle is as follows: when solid-liquid chemical reaction with solid participation and gas generation is carried out in the reaction tank 1, firstly, the top cover 301 is opened through the moving arm 11, reaction raw materials are added into the reaction tank 1, then, the top cover 301 is closed through the moving arm 11, the top cover 301 is hermetically installed on the reaction tank 1 through the locking buckle 303 and the sealing sleeve 302, then, the third control valve 121 on the third gas pipe 122 is opened, gas in the gas storage tank 13 is made to flow into the heat generator 413 through the third gas pipe 122, at this time, the gas in the gas storage tank 13 is the gas generated in the previous chemical reaction, and carries certain heat in the gas, so that the heat required when the gas is heated again is reduced, the gas heated by the heat generator 413 flows into the gas collection cavity 412 through the gas inlet 411, the heated gas collected in the gas collection cavity 412 preheats the chemical reaction in the reaction tank 1, and the heated gas flows out from the gas outlet pipe 414, the subsequent purge process is performed, and when the preheating process is completed, the third control valve 121 is closed.
The preheated reaction tank 1 is subjected to chemical reaction, gas generated during the reaction flows into the first gas conveying pipe 611 through the gas conveying port 304, the gas in the first gas conveying pipe 611 is compressed by the compressor 613 and then flows into the seal box 712, the wind wheel 711 rotatably mounted in the seal box 712 rotates under the action of gas flow, and then the second control valve 101 on the second gas conveying pipe 102 is opened, so that the gas in the seal box 712 flows into the gas storage tank 13 through the second gas conveying pipe 102 to be stored, and the preheated gas can be provided for the next preheating treatment.
When the wind wheel 711 rotates, the wind wheel 711 drives the rotating wheel 171 fixedly installed with the rotating shaft 173 to rotate in the center of a circle through the rotating shaft 713 fixedly installed with the wind wheel 711, the rotating wheel 171 drives the rotating shaft 173 fixedly installed with the non-center position of the rotating wheel to rotate in the non-center position of the rotating wheel, the rotating shaft 173 drives the rotating frame 172 fixedly installed with the rotating frame 173 to rotate in the reaction tank 1 in the circumferential direction, solid-liquid reaction in the reaction tank 1 is stirred, attachment time of bubbles on solid raw materials is reduced, reaction speed is increased, production efficiency is improved, the rotating frame 172 drives the cleaning brush 174 fixedly installed with the outer side of the rotating frame 172 in the rotating process to rotate, the cleaning brush 174 scrapes and cleans the solid raw materials which are molten and similar to sugared on the inner wall of the reaction tank 1, and bubbles generated by the raw materials and the reaction are prevented from being adhered to the inner wall of the reaction tank 1.
After the reaction is completed, when the reacted liquid is extracted and flows out, the liquid outlet control valve 152 fixedly mounted on the liquid outlet pipe 153 is opened, the liquid flows out through the liquid outlet pipe 153, and because the pressure at the bottom of the reaction tank 1 is too high, when the liquid flows out from the bottom of the reaction tank 1, the liquid has the situation that the liquid outlet pipe 153 bursts due to the too high pressure, therefore, when the liquid flows out, the liquid enables the rotating fan 202 rotatably mounted in the filter pipe to rotate, when the rotating fan 202 rotates, the buffer deceleration is carried out on the flowing-out liquid, and the hidden danger that the liquid outlet pipe 153 bursts is reduced.
Rotatory fan 202 is at the in-process of rotatory buffering, rotatory fan 202 drives rather than fixed mounting's driving gear rotatory in the filter tube, the rotatory driven bevel gear 181 that drives rather than the meshing installation of drive bevel gear 201 is rotatory, driven gear drives rather than inboard fixed mounting filtrating board 182 and rotates, filtrating board 182 makes the scraping plate 1911 rather than closely laminating rotatory scraping the material clearance to filtrating board 182 surface at rotatory in-process, prevent that the remaining solid waste adhesion of reaction from blockking up on filtrating board 182, improve filtrating board 182's filtration efficiency.
And the scraping plate 1911 scrapes the residual materials on the filtrate plate 182 and stores them into the storage trough 1912 of the scraping box 191, when the storage trough 1912 is full of residual materials, the liquid outlet control valve 152 is closed, the sealing plate 1923 on the upper side of the filter pipe is opened, so that the sealing plate 1923 moves upwards and extends, the sealing plate 1923 drives the scraping box 191 to move upwards and extend through the connecting rod 1921 fixedly mounted with the sealing plate 1923, and simultaneously the liquid left in the scraping box 191 flows out through the liquid leakage mesh plate 1913 at the bottom of the scraping box 191, so that the scraping box 191 is taken out upwards, and the plate materials in the scraping box 191 are cleaned conveniently.
The foregoing illustrates and describes the principles, general features, and advantages of the present invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, and the embodiments and descriptions given above are only illustrative of the principles of the present invention, and various changes and modifications may be made without departing from the spirit and scope of the invention, which fall within the scope of the claims. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (12)
1. The utility model provides a chemical industry solution reaction vessel is preheated to tapered, includes retort (1) and supporting base (2), its characterized in that: the supporting base (2) is fixedly arranged at the bottom of the reaction tank (1), the upper end of the reaction tank (1) is fixedly provided with a sealing mechanism (3), one side of the sealing mechanism (3) is rotatably provided with a moving arm (11), the other end of the moving arm (11) is fixedly arranged on the supporting base (2), the upper end of the sealing mechanism (3) is provided with a first gas transmission mechanism (6) in a penetrating way, the other end of the first gas transmission mechanism (6) is fixedly connected with a rotating mechanism (7), the rotating mechanism (7) is fixedly arranged at the upper end of the sealing mechanism (3), the reaction tank (1) is internally and rotatably provided with a rotating mechanism (17), the rotating mechanism (17) is rotatably arranged inside the sealing mechanism (3), the rotating mechanism (17) is fixedly connected with the rotating mechanism (7), the other side of the rotating mechanism (7) is fixedly connected with a second gas transmission mechanism (10), the other end of the second gas transmission mechanism (10) is fixedly arranged on a gas storage tank (13), and the gas storage tank (13) is fixedly arranged on the outer side of the reaction tank (1), the lower end of the reaction tank (1) is fixedly provided with a third gas transmission mechanism (12), the other end of the third gas transmission mechanism (12) is fixedly connected with a preheating mechanism (4), and the preheating mechanism (4) is fixedly arranged on the reaction tank (1).
2. The conical preheating chemical solution reactor vessel of claim 1, wherein: sealing mechanism (3) are including top cap (301), seal cover (302), locking is detained (303) and is carried gas port (304), it is in top cap (301) one side just to link up and fixed the setting in to carry gas port (304), top cap (301) lower extreme fixed mounting has seal cover (302), and seal cover (302) can make top cap (301) and retort (1) seal installation, top cap (301) lower extreme outside is fixed to be provided with a plurality of locking and detains (303), and locking detains (303) and can make top cap (301) and retort (1) fixed inseparable installation.
3. The conical preheating chemical solution reactor vessel of claim 2, wherein: the first air delivery mechanism (6) comprises a first air delivery pipe (611) and a compressor, the first air delivery pipe (611) is fixedly arranged on the compressor, and the other end of the first air delivery pipe (611) can be communicated with the air delivery port (304).
4. The conical preheating chemical solution reactor vessel of claim 3, wherein: the rotating mechanism (7) comprises a wind wheel (711), a sealing box (712) and a rotating shaft (713), the wind wheel (711) is rotatably installed inside the sealing box (712), the sealing box (712) is fixedly installed at the upper end of the top cover (301), the other end of the first air conveying pipe (611) is communicated with the sealing box (712), and the rotating shaft (713) is rotatably installed on the top cover (301).
5. The conical preheating chemical solution reactor vessel of claim 4, wherein: the second air delivery mechanism (10) comprises a second air delivery pipe (102) and a second control valve (101), the second control valve (101) is fixedly installed on the second air delivery pipe (102), one end of the second air delivery pipe (102) is installed on the seal box (712) in a penetrating mode, and the other end of the second air delivery pipe (102) is connected with the air storage tank (13) in a penetrating mode.
6. The conical preheating chemical solution reactor vessel of claim 5, wherein: preheating mechanism (4) include air inlet (411), gas collection chamber (412), heat generator (413) and outlet duct (414), air inlet (411) are fixed to be set up in retort (1) upper end, gas collection chamber (412) set up in the internal portion of jar of retort (1), and air inlet (411) and gas collection chamber (412) through connection, heat generator (413) are fixed to be set up on retort (1) in air inlet (411) outside, outlet duct (414) are fixed to be set up at retort (1) opposite side lower extreme, and outlet duct (414) and gas collection chamber (412) through connection.
7. The conical preheating chemical solution reactor vessel of claim 6, wherein: the third gas transmission mechanism (12) comprises a third control valve (121) and a third gas transmission pipe (122), the third control valve (121) is fixedly installed on the third gas transmission pipe (122), one end of the third gas transmission pipe (122) is fixedly installed on the gas storage tank (13), the other end of the third gas transmission pipe (122) is fixedly installed on the heat generator (413), and the other end of the third gas transmission pipe (122) is communicated with the gas inlet (411).
8. The conical pre-heated chemical solution reactor vessel of claim 7, wherein: reaction tank (1) lower extreme fixed mounting has out liquid mechanism (15), and goes out liquid mechanism (15) and include filter member (151), goes out liquid control valve (152) and drain pipe (153), and drain pipe (153) are fixed to be set up at reaction tank (1) lower extreme, and drain pipe (153) and reaction tank (1) through connection, goes out liquid control valve (152) fixed mounting at the drain pipe (153) other end, and filter member (151) fixed mounting at drain pipe (153) middle part.
9. The conical pre-heated chemical solution reactor vessel of claim 8, wherein: rotary mechanism (17) are including swiveling wheel (171), swivel mount (172), rotation axis (173) and cleaning brush (174), swiveling wheel (171) rotate and install inside top cap (301), and axis of rotation (713) lower extreme fixed mounting is in the centre of a circle position of swiveling wheel (171), non-centre of a circle position fixed mounting rotation axis (173) of swiveling wheel (171) downside, rotation axis (173) lower extreme fixed connection swivel mount (172), cleaning brush (174) fixed mounting is in the swivel mount (172) outside, and cleaning brush (174) and retort (1) inner wall closely laminate.
10. The conical pre-heated chemical solution reactor vessel of claim 9, wherein: the filtering member (151) comprises a filtrate member (18), a scraping member (19) and a buffering member, the filtrate member (18) is rotatably installed on the liquid outlet pipe (153), the filtrate member (18) and the buffering member are rotatably installed, the scraping member (19) is tightly attached to the filtrate member (18), the filtrate member (18) comprises a driven bevel gear (181) and a filtrate plate (182), the filtrate plate (182) is rotatably installed on the liquid outlet pipe (153), the driven bevel gear (181) is fixedly installed on the outer side of the filtrate plate (182), the driven bevel gear (181) is rotatably installed on the liquid outlet pipe (153), the buffering mechanism (20) comprises a driving bevel gear (201) and a rotating fan (202), the rotating fan (202) is rotatably installed on the liquid outlet pipe (153), the other end of the rotating fan (202) is fixedly installed with the driving bevel gear (201), the driving bevel gear (201) is rotatably installed on the liquid outlet pipe (153), and the drive bevel gear (201) and the driven bevel gear (181) are installed in mesh.
11. The conical pre-heated chemical solution reactor vessel of claim 10, wherein: scrape material mechanism including scraping magazine (191) and clearance piece (192), scrape magazine (191) and clearance piece (192) fixed mounting, scrape magazine (191) including scraping flitch (1911), stock chest (1912) and weeping otter board (1913), stock chest (1912) set up inside scraping magazine (191), and scrape magazine (191) bottom fixed mounting have weeping otter board (1913), scrape magazine (191) right side fixed mounting scrape flitch (1911), and scrape flitch (1911) and closely laminate with weeping board (182), clearance piece (192) include connecting rod (1921), spring and closing plate (1923), clearance magazine upper end fixed mounting connecting rod (1921), and connecting rod (1921) movable mounting is on drain pipe (153), connecting rod (1921) upper end fixed mounting has closing plate (1923).
12. The conical pre-heated chemical solution reactor vessel as defined in claim 11, wherein: the fourth gas transmission mechanism (14) comprises a fourth gas transmission pipe (142) and a fourth control valve (141), the fourth control valve (141) is fixedly installed on the fourth gas transmission pipe (142), and one end of the fourth gas transmission pipe (142) is fixedly installed on the gas storage tank (13).
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN202210692294.3A CN114904477A (en) | 2022-06-17 | 2022-06-17 | Conical preheating chemical solution reaction container |
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CN202210692294.3A CN114904477A (en) | 2022-06-17 | 2022-06-17 | Conical preheating chemical solution reaction container |
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CN202210692294.3A Withdrawn CN114904477A (en) | 2022-06-17 | 2022-06-17 | Conical preheating chemical solution reaction container |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115518408A (en) * | 2022-11-08 | 2022-12-27 | 山东坤宝新材料集团股份有限公司 | Scraper catcher for anhydrous aluminum trichloride production and method |
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2022
- 2022-06-17 CN CN202210692294.3A patent/CN114904477A/en not_active Withdrawn
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN115518408A (en) * | 2022-11-08 | 2022-12-27 | 山东坤宝新材料集团股份有限公司 | Scraper catcher for anhydrous aluminum trichloride production and method |
CN115518408B (en) * | 2022-11-08 | 2024-04-26 | 山东坤宝新材料集团股份有限公司 | Scraper catcher and method for anhydrous aluminum trichloride production |
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