CN114870774B - Vertical hydrothermal kettle - Google Patents

Vertical hydrothermal kettle Download PDF

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Publication number
CN114870774B
CN114870774B CN202210424593.9A CN202210424593A CN114870774B CN 114870774 B CN114870774 B CN 114870774B CN 202210424593 A CN202210424593 A CN 202210424593A CN 114870774 B CN114870774 B CN 114870774B
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hydrothermal kettle
fixed
arc
hydrothermal
shell
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CN114870774A (en
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冯磊
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Jiangsu Siyao New Energy Equipment Manufacturing Co ltd
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Jiangsu Siyao New Energy Equipment Manufacturing Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/01Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements
    • B01D29/03Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements self-supporting
    • B01D29/035Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with flat filtering elements self-supporting with curved filtering elements
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/62Regenerating the filter material in the filter
    • B01D29/64Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element
    • B01D29/6407Regenerating the filter material in the filter by scrapers, brushes, nozzles, or the like, acting on the cake side of the filtering element brushes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • B01J19/0013Controlling the temperature of the process
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/04Pressure vessels, e.g. autoclaves
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00Feed or outlet devices; Feed or outlet control devices
    • B01J4/001Feed or outlet devices as such, e.g. feeding tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/185Details relating to the spatial orientation of the reactor vertical

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention relates to the technical field of hydrothermal kettles, in particular to a vertical hydrothermal kettle, which further comprises: the temperature measuring meter is inserted into one side of the top of the hydrothermal kettle shell in a penetrating manner; the baffle is inserted and fixed in the first fixing frames; the stirring device is arranged between the hydrothermal kettle shell and the cover body; and the precipitation guiding device is arranged between the inside of the hydrothermal kettle shell and the stirring device. This device is through setting up of precipitation guiding device, and the liquid that flows makes the sediment that the reaction produced after passing through precipitation guiding device is filtered and is stayed in precipitation guiding device's inside to make precipitation and the liquid separation of reaction, be favorable to avoiding the sediment to cause the hindrance to the mixed reaction of liquid, make the sediment can be convenient after the reaction is accomplished by the discharge, thereby be favorable to avoiding the sediment to scatter everywhere inside the hydrothermal kettle casing and be difficult to clean the discharge.

Description

Vertical hydrothermal kettle
Technical Field
The invention relates to the field of hydrothermal kettles, in particular to a vertical type hydrothermal kettle.
Background
The hydrothermal reactor is also called a hydrothermal reaction vessel and is a sealed container capable of decomposing refractory substances.
The prior art discloses a part of the invention patent in the aspect of hydrothermal kettles, and the Chinese patent with the application number of CN201510155534.6 discloses a screen type hydrothermal kettle capable of separating solid from liquid, which is characterized in that a kettle body with an opening at the top and a bracket are arranged on a base, an adjusting knob and an adjusting rod are arranged on the bracket, the adjusting knob is connected with a rotating gear through a rotating shaft, straight teeth meshed with the rotating gear are arranged on the side wall of the adjusting rod, an outer magnetic fixing plate is arranged at the lower end of the adjusting rod, a top cover and an inner cavity are arranged on an opening of the kettle body, an inner magnetic fixing plate fixed by the magnetic force of the outer magnetic fixing plate is arranged in the inner cavity, and at least one screen is arranged on the inner magnetic fixing plate.
In the prior art, the hydrothermal kettle can generate a large amount of precipitates for some reactions which can generate precipitates in the reaction process, and the generated precipitates can be accumulated in the hydrothermal kettle, so that the precipitates can be accumulated at all corners of the reaction kettle when the internal part of the hydrothermal kettle is subjected to stirring reaction, reaction liquid and the precipitates generated by the reaction are inconvenient to discharge after the reaction is finished, and meanwhile, the internal part of the hydrothermal kettle after the reaction is inconvenient to clean. Therefore, the invention provides a vertical type hydrothermal kettle for solving the problems.
Disclosure of Invention
The invention aims to solve the defects in the prior art and provides a vertical type hydrothermal kettle.
In order to achieve the above purpose, the invention adopts the following technical scheme: the utility model provides a vertical hydrothermal kettle, includes hydrothermal kettle casing, the lid is installed at the top of hydrothermal kettle casing, the top of lid is provided with main feed inlet, the top array of lid is provided with a plurality of auxiliary feed inlets, the bottom of hydrothermal kettle casing is provided with the discharge gate, still includes:
the temperature measuring meter penetrates through and is inserted into one side of the top of the hydrothermal kettle shell, and the bottom end of the temperature measuring meter extends to the inside of the hydrothermal kettle shell;
the first fixing frames are fixed on the side wall of the hydrothermal kettle shell in an array mode;
the baffle is inserted and fixed in the first fixing frames;
the hydrothermal device is arranged on the outer wall of the hydrothermal kettle shell;
the stirring device is arranged between the hydrothermal kettle shell and the cover body;
the sedimentation guide device is arranged between the inside of the hydrothermal kettle shell and the stirring device;
the hydrothermal device is used for heating the whole hydrothermal kettle, the stirring device is used for stirring the inside of the shell of the hydrothermal kettle, and the stirring device drives the sediment guiding device to start to guide the sediment generated by the reaction to flow towards the inside of the sediment guiding device to collect when stirring, and the sediment is separated from the liquid.
Preferably, the hydrothermal device comprises a water heat pipe, the water heat pipe is spirally wound on the outer wall of the shell of the hydrothermal kettle, a water inlet connecting pipe is fixedly connected with the end part of the top of the water heat pipe, and a water outlet connecting pipe is fixedly connected with the end part of the bottom of the water heat pipe.
Preferably, the stirring device comprises a mounting frame, the mounting frame is fixed at the top of the cover body, a motor is fixed at the top of the mounting frame through a screw, an output shaft of the motor penetrates through the mounting frame and the cover body and then extends to the inside of the hydrothermal kettle shell, a rotating shaft is fixed at the end part of the output shaft of the motor, and a plurality of stirring blades are coaxially fixed on the outer wall of the rotating shaft.
Preferably, the precipitation guiding device comprises a threaded opening and a spiral blade, the threaded opening is formed in the bottom of the hydrothermal kettle shell, a precipitation box is inserted in the threaded opening, the precipitation box is provided with an annular screen plate and a bottom plate, an external thread sleeve is fixed on the outer annular surface of the bottom plate, the external thread sleeve is in threaded fit with the threaded opening, the spiral blade is movably inserted in the precipitation box, the spiral blade is connected to the surface of the rotating shaft in a sliding mode in the vertical direction, an elastic supporting mechanism is connected between the top of the spiral blade and the surface of the rotating shaft, and a backflow mechanism for guiding liquid to flow towards the top of the hydrothermal kettle shell is installed between two sides of the precipitation box and the inside of the hydrothermal kettle shell.
Preferably, the elastic supporting mechanism comprises a first fixing plate and a first sliding groove, the first fixing plate is fixed on the outer wall of the rotating shaft, a first spring is fixed at the bottom of the first fixing plate, the first spring is sleeved on the outer ring of the rotating shaft, a lifting disc is fixed at the bottom of the first spring, a sliding opening is formed in the inner ring of the lifting disc, a first sliding groove array is formed in the outer wall of the rotating shaft, and the first sliding groove is in sliding fit with the sliding opening.
Preferably, the reflux mechanism includes two second mounts, two second mounts symmetry is fixed in on the inner wall of hydrothermal kettle casing, two the inside of second mount all is fixed with the pipeline, the pipeline is fixed with the casing, two intermeshing's first gear is installed in the inside rotation of casing, one of them first gear with install between the first fixed plate be used for driving first gear pivoted link gear, two the top of pipeline all is fixed with the return bend.
Preferably, the linkage mechanism comprises two connecting frames and a second bevel gear, the two connecting frames are symmetrically fixed on two sides of the first fixing plate, the bottoms of the two connecting frames are jointly fixed with an annular porous sleeve, the annular porous sleeve is movably sleeved on the outer ring of the settling tank, an annular bevel gear is coaxially fixed at the bottom of the annular porous sleeve, the second bevel gear is rotatably mounted on the outer wall of the shell, and a rotating shaft of the second bevel gear penetrates through the shell and then is coaxially fixed with one of the first bevel gears, and the second bevel gear is meshed with the annular bevel gear.
Preferably, an arc filter plate is fixed on the inner wall of the hydrothermal kettle shell, the arc filter plate is sleeved on the outer wall of the pipeline, through holes corresponding to the thermometer, the baffle and the pipeline are formed in the side wall of the arc filter plate, a plurality of arc rods are fixed on the top circumference array of the arc filter plate, all the two sides of the arc rods are hinged with a plurality of overturning brush heads, all the overturning brush heads and the outer ring of a rotating shaft at the hinged position of the arc rods are sleeved with torsion springs, two ends of each torsion spring are fixedly connected with the arc rods and the overturning brush heads respectively, a plurality of pushing plates corresponding to the overturning brush heads are slidably connected with the outer wall of each arc rod, all the pushing plates are connected with the arc rods and the connecting frames through pulling mechanisms, and the pulling mechanisms are used for driving the pushing plates to reciprocate.
Preferably, the pulling mechanism comprises a plurality of second sliding grooves and a plurality of second fixing plates, all the second sliding grooves are respectively formed in the top of the arc-shaped rod, the second sliding grooves are internally and slidably connected with a plurality of sliding blocks corresponding to the pushing plates, pulling ropes are fixedly connected between all the sliding blocks in the same second sliding grooves together, all the pulling ropes face one end of the connecting frame and a winding mechanism for winding the pulling ropes is arranged between the connecting frame, the pulling ropes face away from one end of the connecting frame, second springs are fixed at one ends of the connecting frame, all the second fixing plates are respectively fixed at one ends of the arc-shaped rod face away from the connecting frame, and one ends of the second springs face away from the pulling ropes are fixedly connected with the second fixing plates.
Preferably, the winding mechanism comprises a plurality of winding drums, a plurality of openings and two arc racks, all the winding drum arrays are rotatably installed on the side wall of the arc filter plate, the openings are formed in the end parts of the arc rods, the pulling ropes face to one end parts of the connecting frames penetrate through the openings and then fixedly wind the outside of the winding drums, a third gear is coaxially fixed at the top of the winding drums, the two arc racks are symmetrically fixed on the side wall of the connecting frames, and the arc center of each arc rack is located on the axis of the corresponding rotating shaft and matched with the corresponding arc rack.
Compared with the prior art, the invention has the following beneficial effects:
1. according to the invention, through the arrangement of the precipitation guiding device, the flowing liquid is filtered and left in the precipitation guiding device after passing through the precipitation guiding device, so that the precipitation is separated from the reacted liquid, the blocking of the precipitation on the mixed reaction of the liquid is avoided, and the precipitation separated from the liquid can be conveniently discharged after the reaction is finished, so that the precipitation is prevented from being scattered in various positions in the hydrothermal kettle shell and difficult to clean and discharge.
2. According to the invention, through the arrangement of the reflux mechanism, the liquid above the hydrothermal kettle shell flows downwards after the liquid at the bottom of the hydrothermal kettle shell flows away, so that the up-and-down circulation flow of the liquid in the hydrothermal kettle shell is promoted, the reaction is promoted by the flow mixing of the liquid, and the flowing liquid drives the sediment to flow and collect towards the inside of the sedimentation tank.
3. According to the invention, through the arrangement of the arc-shaped filter plate and the turnover brush head, the arc-shaped filter plate can drain liquid flowing from top to bottom, so that the liquid can flow into the sedimentation tank in a concentrated manner when flowing downwards, and the turnover brush head brushes the surface of the arc-shaped filter plate after being turned over, so that sediments accumulated on the surface of the arc-shaped filter plate are brushed, the sediments are collected along with flowing liquid entering the sedimentation tank, the sedimentation is facilitated to be collected into the sedimentation tank, and the phenomenon that the sediments are difficult to clear due to accumulation of the sediments at the bottom of the hydrothermal kettle shell is avoided.
Drawings
FIG. 1 is a schematic diagram of the overall structure of the present invention;
FIG. 2 is a schematic view of the structure of the present invention in an overall section;
FIG. 3 is a schematic view of the structure of the present invention shown in FIG. 2A with a partial enlargement;
FIG. 4 is a partially enlarged schematic illustration of the structure of FIG. 2B in accordance with the present invention;
FIG. 5 is a partially enlarged schematic illustration of the structure of FIG. 2 according to the present invention;
FIG. 6 is a partially enlarged schematic illustration of the structure of FIG. 5D in accordance with the present invention;
FIG. 7 is a schematic view of the structure of the present invention in further overall section;
FIG. 8 is a partially enlarged schematic illustration of the structure of FIG. 7E in accordance with the present invention;
FIG. 9 is a partially enlarged schematic illustration of the structure of FIG. 7 according to the present invention;
FIG. 10 is a schematic view of a settling tank and surrounding connection structure according to the present invention;
FIG. 11 is a partially enlarged schematic illustration of the structure of FIG. 10 according to the present invention;
FIG. 12 is a schematic view of an arc-shaped filter plate and a connecting structure according to the present invention;
FIG. 13 is a partially enlarged schematic illustration of the structure of FIG. 12 at H in accordance with the present invention;
FIG. 14 is a partially enlarged schematic illustration of the structure of FIG. 13 according to the present invention;
fig. 15 is a partially enlarged schematic view of the structure of fig. 13 according to the present invention.
In the figure: 1. a hydrothermal kettle shell; 2. a cover body; 3. a main feed inlet; 4. an auxiliary feed port; 5. a mounting frame; 6. a motor; 7. a rotating shaft; 8. stirring the leaves; 9. a water heat pipe; 10. a water inlet connecting pipe; 11. a water outlet connecting pipe; 12. a thermometer; 13. a first fixing frame; 14. a baffle plate; 15. a threaded port; 16. a sedimentation tank; 1601. an annular screen plate; 17. an external thread sleeve; 18. a bottom plate; 19. a discharge port; 20. a first fixing plate; 21. a first spring; 22. a lifting disc; 23. a first chute; 24. a sliding port; 25. spiral leaves; 26. a pipe; 27. a housing; 28. a first gear; 29. a second helical gear; 30. an annular helical rack; 31. an annular porous sleeve; 32. a connecting frame; 33. bending the pipe; 34. arc-shaped filter plates; 35. an arc-shaped rod; 36. turning over the brush head; 37. a torsion spring; 38. a second chute; 39. a slide block; 40. pulling the rope; 41. a pushing plate; 42. an opening; 43. a second fixing plate; 44. a second spring; 45. a third gear; 46. a reel; 47. an arc-shaped rack; 48. a through hole; 49. and the second fixing frame.
Detailed Description
The following description is presented to enable one of ordinary skill in the art to make and use the invention. The preferred embodiments in the following description are by way of example only and other obvious variations will occur to those skilled in the art.
The utility model provides a vertical hydrothermal kettle as shown in fig. 1 through 15, includes hydrothermal kettle casing 1, lid 2 is installed at the top of hydrothermal kettle casing 1, and the top of lid 2 is provided with main feed inlet 3, and the top array of lid 2 is provided with a plurality of auxiliary feed inlets 4, and the bottom of hydrothermal kettle casing 1 is provided with discharge gate 19, its characterized in that still includes:
the temperature detector 12, the temperature detector 12 is inserted into one side of the top of the hydrothermal kettle shell 1, and the bottom end of the temperature detector 12 extends to the inside of the hydrothermal kettle shell 1;
the first fixing frames 13 are fixed on the side wall of the hydrothermal kettle shell 1 in an array manner;
the baffle plates 14, the baffle plates 14 are inserted and fixed in the first fixing frames 13;
the hydrothermal device is arranged on the outer wall of the hydrothermal kettle shell 1;
the stirring device is arranged between the hydrothermal kettle shell 1 and the cover body 2;
the precipitation guiding device is arranged between the interior of the hydrothermal kettle shell 1 and the stirring device;
the hydrothermal device is used for heating the whole hydrothermal kettle, the stirring device is used for stirring the inside of the hydrothermal kettle shell 1, and the stirring device drives the precipitation guiding device to start to guide precipitation generated by reaction to flow to the inside of the precipitation guiding device for collection when stirring, and the precipitation is separated from the liquid; during operation, in the reaction process of the hydrothermal kettle in the prior art, for some reactions which can generate precipitates, a large amount of precipitates can be generated in the reaction process, the generated precipitates can be accumulated in the hydrothermal kettle, so that the precipitates can be accumulated at all corners of the reaction kettle when the internal parts of the hydrothermal kettle are subjected to stirring reaction, reaction liquid and the precipitates generated by the reaction are inconvenient to discharge after the reaction is finished, and meanwhile, the internal parts of the hydrothermal kettle after the reaction are inconvenient to clean. The auxiliary feeding port 4 can conveniently add other auxiliary materials, the hydrothermal device can heat the liquid reacted in the hydrothermal kettle shell 1, the thermometer 12 can detect the temperature in the hydrothermal kettle shell 1, thereby facilitating the operator to control the temperature in the hydrothermal kettle shell 1, the stirring device can stir the inside of the hydrothermal kettle shell 1, the reaction liquid in the hydrothermal kettle shell 1 is mixed, the first fixing frame 13 can fixedly mount the baffle plate 14, the baffle plate 14 can obstruct the liquid stirred in the hydrothermal kettle shell 1, the liquid is blocked to generate resistance reverse reflux after encountering the baffle plate 14, thereby being beneficial to fully mixing the liquid in the hydrothermal kettle shell 1, promoting the reaction speed, the discharge port 19 can discharge the reacted liquid, the stirring device can drive the flow of the liquid in the stirring process, the flowing liquid passes through the precipitation guiding device to enable the precipitate generated by the reaction to be filtered and left in the precipitation guiding device, so that the precipitate is separated from the reacted liquid, the obstruction of the mixed reaction of the precipitate to the liquid is avoided, the precipitate separated from the liquid can be conveniently discharged after the reaction is completed, and the precipitate is prevented from being scattered in various positions in the hydrothermal kettle shell 1 and difficult to clean and discharge.
As one embodiment of the invention, the hydrothermal device comprises a water heat pipe 9, wherein the water heat pipe 9 is spirally wound on the outer wall of the hydrothermal kettle shell 1, a water inlet connecting pipe 10 is fixedly connected with the end part of the top of the water heat pipe 9, and a water outlet connecting pipe 11 is fixedly connected with the end part of the bottom of the water heat pipe 9; during operation, in the process of carrying out the reaction in the interior of the hydrothermal kettle shell 1, an operator inputs external high-temperature water into the interior of the hydrothermal pipe 9 through the water inlet connecting pipe 10, the hydrothermal pipe 9 is spirally wound on the outer wall of the hydrothermal kettle shell 1, so that the interior of the hydrothermal kettle shell 1 is heated through water flow of the hydrothermal pipe 9, and flowing water flowing through the hydrothermal pipe 9 is discharged through the water outlet connecting pipe 11 and collected, so that the interior of the hydrothermal kettle shell 1 can be subjected to temperature control by controlling the flow speed of the water flow in the interior of the hydrothermal pipe 9 during reaction, and different temperatures can be regulated in the process of carrying out different reactions in the interior of the hydrothermal kettle shell 1.
As one embodiment of the invention, the stirring device comprises a mounting frame 5, wherein the mounting frame 5 is fixed at the top of the cover body 2, a motor 6 is fixed at the top of the mounting frame 5 through screws, an output shaft of the motor 6 penetrates through the mounting frame 5 and the cover body 2 and then extends into the hydrothermal kettle shell 1, a rotating shaft 7 is fixed at the end part of the output shaft of the motor 6, and a plurality of stirring blades 8 are coaxially fixed on the outer wall of the rotating shaft 7; during operation, the mounting bracket 5 can carry out fixed mounting to the motor 6, and the motor 6 can drive the pivot 7 through the output shaft after starting and rotate, drives stirring leaf 8 after the pivot 7 rotates and rotates, drives the inside liquid flow of hydrothermal kettle casing 1 after stirring leaf 8 rotates to promote the mixing of liquid through strengthening the flow of the inside liquid of hydrothermal kettle casing 1, thereby be favorable to promoting the going on of reaction.
As one embodiment of the invention, the sedimentation guiding device comprises a threaded opening 15 and a spiral blade 25, wherein the threaded opening 15 is arranged at the bottom of the hydrothermal kettle shell 1, a sedimentation tank 16 is inserted in the threaded opening 15, the sedimentation tank 16 is provided with an annular screen 1601 and a bottom plate 18, an external thread sleeve 17 is fixed on the outer annular surface of the bottom plate 18, the external thread sleeve 17 is in threaded fit with the threaded opening 15, the spiral blade 25 is movably inserted in the sedimentation tank 16, the spiral blade 25 is connected onto the surface of the rotating shaft 7 in a sliding manner in the vertical direction, an elastic supporting mechanism is connected between the top of the spiral blade 25 and the surface of the rotating shaft 7, and a reflux mechanism for guiding liquid to flow towards the top of the hydrothermal kettle shell 1 is arranged between two sides of the sedimentation tank 16 and the inside of the hydrothermal kettle shell 1; during operation, screw thread mouth 15 can make things convenient for the dismouting of rose box 16, screw thread mouth 15 and external screw thread cover 17 screw thread fit back can make the inside of rose box 16 sealed mounting in screw thread mouth 15, bottom plate 18 can seal the bottom of rose box 16, the effect that can pass through elastic support mechanism when pivot 7 rotates drives spiral leaf 25 and rotates, spiral leaf 25 rotates the back and can promote the inside of rose box 16 gradually with the sediment, the sediment is piled up the bottom at the rose box 16 along with spiral leaf 25 downwardly flowing back, mixed liquid is discharged along with the filtration pore of rose box 16 lateral wall in the sediment, elastic support mechanism rotates the compaction to the sediment of piling up in the inside of rose box 16 in the rotation process, make the sediment pile up the inside of collecting at the rose box 16, the liquid of following the rose box 16 lateral wall discharge is discharged to the top of hydrothermal kettle shell 1 under the effect of reflux mechanism, thereby the liquid of making the bottom is by the liquid flow to the bottom after the evacuation, be favorable to promoting the upper and lower flow of liquid, make the flow of liquid promote the mixing of reactant, and be favorable to promoting the reaction along with the flow of liquid from the top to the rose box to the inside by the rose box 16 to promote the flow of the sediment to the sediment by the flow of the sediment 16.
As an embodiment of the invention, the elastic supporting mechanism comprises a first fixed plate 20 and a first sliding groove 23, wherein the first fixed plate 20 is fixed on the outer wall of the rotating shaft 7, a first spring 21 is fixed at the bottom of the first fixed plate 20, the first spring 21 is sleeved on the outer ring of the rotating shaft 7, a lifting disc 22 is fixed at the bottom of the first spring 21, a sliding opening 24 is formed in the inner ring of the lifting disc 22, a first sliding groove 23 array is formed on the outer wall of the rotating shaft 7, and the first sliding groove 23 is in sliding fit with the sliding opening 24; during operation, the rotating shaft 7 rotates to drive the first fixed plate 20 and the first sliding groove 23 to rotate, the first sliding groove 23 rotates to drive the lifting disc 22 to rotate through the sliding opening 24, the lifting disc 22 rotates to drive the spiral blade 25 to rotate, the first spring 21 pushes the lifting disc 22 downwards through elastic force, the lifting disc 22 drives the spiral blade 25 to have a trend of pushing down to push precipitation in the rotating process, when the internal precipitation of the precipitation tank 16 is piled up, the internal precipitation pushes the spiral blade 25 upwards, the spiral blade 25 pushes the lifting disc 22 upwards, the lifting disc 22 pushes the first spring 21 upwards, the elastic force is increased after the first spring 21 is compressed and deformed, thereby being beneficial to extruding and compacting the precipitation inside the precipitation tank 16, and being beneficial to adjusting the height of the spiral blade 25 according to the internal piled precipitation height of the precipitation tank 16 when pushing the precipitation to collect the precipitation, and being beneficial to piling up and collecting the precipitation.
As one embodiment of the invention, the reflux mechanism comprises two second fixing frames 49, the two second fixing frames 49 are symmetrically fixed on the inner wall of the hydrothermal kettle shell 1, the inner parts of the two second fixing frames 49 are respectively fixed with a pipeline 26, the pipeline 26 is fixed with a shell 27, two first gears 28 meshed with each other are rotatably arranged in the shell 27, a linkage mechanism for driving the first gears 28 to rotate is arranged between one first gear 28 and the first fixing plate 20, and bent pipes 33 are respectively fixed at the top parts of the two pipelines 26; during operation, the second fixing frame 49 can be fixedly installed on the pipeline 26, the first fixing plate 20 rotates and then drives the first gears 28 to rotate under the action of the linkage mechanism, the two first gears 28 rotate and then play a role of a gear pump to drive the liquid to flow, so that the liquid enters the inside of the shell 27 along with the rotation of the first gears 28, then flows upwards along the pipeline 26 after passing through the inside of the shell 27, flows out of the top of the inside of the hydrothermal kettle shell 1 along the bent pipe 33 through the liquid of the pipeline 26, the liquid above the hydrothermal kettle shell 1 flows downwards after the liquid at the bottom of the hydrothermal kettle shell 1 flows, the up-down circulation flow of the liquid in the inside of the hydrothermal kettle shell 1 is promoted, the reaction is promoted by the flow mixing of the liquid, and the flowing liquid drives the sediment to flow and collect in the sedimentation tank 16.
As an embodiment of the invention, the linkage mechanism comprises two connecting frames 32 and a second bevel gear 29, the two connecting frames 32 are symmetrically fixed on two sides of the first fixing plate 20, the bottoms of the two connecting frames 32 are jointly fixed with an annular porous sleeve 31, the annular porous sleeve 31 is movably sleeved on the outer ring of the sedimentation tank 16, the bottom of the annular porous sleeve 31 is coaxially fixed with an annular bevel rack 30, the second bevel gear 29 is rotatably arranged on the outer wall of the shell 27, a rotating shaft of the second bevel gear 29 penetrates through the shell 27 and is coaxially fixed with one of the first gears 28, and the second bevel gear 29 is meshed with the annular bevel rack 30; during operation, the first fixing plate 20 rotates to drive the connecting frame 32 to rotate, the connecting frame 32 rotates to drive the annular porous sleeve 31 to rotate, the annular porous sleeve 31 rotates to drive the annular helical rack 30 to rotate, the annular helical rack 30 rotates to drive the second helical gear 29 meshed with the annular helical rack 30 to rotate, and the second helical gear 29 rotates to drive the first gear 28 coaxially fixed with the second helical gear 29 to rotate, so that liquid in the hydrothermal kettle shell 1 can drive the first gear 28 to rotate while stirring, gear pumping is formed, and the liquid is driven to flow along the pipeline 26 to circulate up and down.
As one implementation mode of the invention, an arc-shaped filter plate 34 is fixed on the inner wall of the hydrothermal kettle shell 1, the arc-shaped filter plate 34 is sleeved on the outer wall of the pipeline 26, through holes 48 corresponding to the thermometer 12, the baffle 14 and the pipeline 26 are formed in the side wall of the arc-shaped filter plate 34, a plurality of arc-shaped rods 35 are fixed on the top circumferential array of the arc-shaped filter plate 34, a plurality of turnover brush heads 36 are hinged to two sides of all the arc-shaped rods 35, torsion springs 37 are sleeved on the outer ring of a rotating shaft at the hinged position of all the turnover brush heads 36 and the arc-shaped rods 35, two ends of the torsion springs 37 are fixedly connected with the arc-shaped rods 35 and the turnover brush heads 36 respectively, a plurality of pushing plates 41 corresponding to the turnover brush heads 36 are connected with the outer wall of all the arc-shaped rods 35 in a sliding manner, and all pushing plates 41 are connected with the arc-shaped rods 35 and the connecting frames 32 through pulling mechanisms, and the pulling mechanisms are used for driving the pushing plates 41 to reciprocate; when the sedimentation tank 16 is used for collecting sediment generated by reaction, when liquid flows back upwards along with a pipeline 26, the sediment flows downwards to the bottom of the hydrothermal kettle shell 1 along with the liquid flow, so that the sediment is scattered at the corner of the outside of the sedimentation tank 16 at the bottom of the hydrothermal kettle shell 1, the sediment is difficult to be completely recovered to the inside of the sedimentation tank 16, thereby being unfavorable for fully collecting the sediment, the embodiment of the invention can solve the problems, the specific implementation mode is as follows, the arc-shaped filter plate 34 is fixed on the inner wall of the hydrothermal kettle shell 1, the through holes 48 can facilitate the installation of the arc-shaped filter plate 34 and then leave a space for the installation of the thermometer 12, the baffle plate 14 and the pipeline 26, the arc-shaped filter plate 34 can drain the liquid flowing downwards along with the liquid flow, the inside of the sedimentation tank 16 can be concentrated, the arc-shaped rod 35 can hinge and fix the turnover brush head 36, when the connecting frame 32 rotates, the connecting frame 32 pushes the pushing plate 41 to move through the pushing plate 41 to the arc-shaped rod 35, the pushing plate 41 to move, the turnover brush head 36 is pushed by the pushing the turnover brush head 36 to rotate to the surface of the sedimentation tank 36 to rotate along with the rotation of the sedimentation tank, thereby the sedimentation tank is driven by the surface of the sedimentation tank 36 to rotate, the sedimentation tank is driven by the turnover brush head 36 to rotate, the surface of the sedimentation tank is driven by the turnover brush 34 to rotate, thereby the surface of the sedimentation tank is driven to rotate, the sedimentation tank is turned to rotate, and the surface is favorable to rotate and the sedimentation tank is turned to rotate, and the sedimentation tank is turned to be opposite to the inside by the sedimentation tank is subjected to the sedimentation tank and has a high, and has a high quality. And is beneficial to avoiding the difficult removal of the sediment caused by the sediment accumulated at the bottom of the hydrothermal kettle shell 1.
As an embodiment of the present invention, the pulling mechanism includes a plurality of second sliding grooves 38 and a plurality of second fixing plates 43, all the second sliding grooves 38 are respectively opened at the top of the arc-shaped rod 35, the inside of the second sliding grooves 38 is slidably connected with a plurality of sliding blocks 39 corresponding to the pushing plates 41, a pulling rope 40 is fixedly connected between all the sliding blocks 39 in the same second sliding groove 38, a winding mechanism for winding the pulling rope 40 is installed between one end of all the pulling ropes 40 facing the connecting frame 32 and the connecting frame 32, one end of the pulling rope 40 facing away from the connecting frame 32 is fixed with a second spring 44, all the second fixing plates 43 are respectively fixed at one end of the arc-shaped rod 35 facing away from the connecting frame 32, and one end of the second spring 44 facing away from the pulling rope 40 is fixedly connected with the second fixing plates 43; when the connecting frame 32 rotates and passes through, the pulling rope 40 is pulled through the winding mechanism, the sliding block 39 is pulled after the pulling rope 40 is pulled, the sliding block 39 slides in the second sliding groove 38 after being pulled, the sliding block 39 slides and pulls the second spring 44 to extend, the extending second spring 44 generates pulling force through deformation, the sliding block 39 is pulled and drives the pushing plate 41 fixed with the sliding block to move, so that the turnover brush head 36 is pushed to turn and spread through the movement of the pushing plate 41, after the connecting frame 32 rotates and passes through, the sliding block 39 is pulled to reset by the pulling force of the second spring 44, the second fixing plate 43 can fixedly mount the second spring 44, and the sliding block 39 is reset and then the pushing plate 41 is pulled to reset, so that the connecting frame 32 can drive the reciprocating brushing of the turnover brush head 36 through brushing, and the accumulation of the turnover brush head 36 on the arc-shaped filter plate 34 is reduced through brushing.
As one embodiment of the present invention, the winding mechanism includes a plurality of winding discs 46, a plurality of openings 42, and two arc racks 47, all the winding discs 46 are rotatably installed on the side wall of the arc filter plate 34, the openings 42 are opened at the ends of the arc rods 35, the pulling rope 40 passes through the openings 42 towards one end of the connecting frame 32 and then is fixedly wound on the outside of the winding disc 46, the top of the winding disc 46 is coaxially fixed with a third gear 45, the two arc racks 47 are symmetrically fixed on the side walls of the two connecting frames 32, the arc centers of the arc racks 47 are located on the axis of the rotating shaft 7, and the third gear 45 is matched with the arc racks 47; in operation, the connecting frame 32 rotates to drive the arc-shaped rack 47 to rotate, the arc-shaped rack 47 rotates to drive the third gear 45 in threaded connection with the arc-shaped rack 47 to rotate, the third gear 45 rotates to drive the rolling disc 46 to rotate, the rolling disc 46 rotates to wind the pulling rope 40, the free length of the pulling rope 40 is shortened after being rolled, thereby the pulling slide block 39 moves, the opening 42 can facilitate the pulling rope 40 to wind on the outer ring rolling of the rolling disc 46 through the opening 42, pulling of the pulling rope 40 is facilitated when the connecting frame 32 rotates to pass through the third gear 45, and pulling of the pulling rope 40 can be lost after the connecting frame 32 passes through, so that the turnover brush head 36 is turned over by rigid force pulling when the connecting frame 32 passes through, and automatic resetting of the turnover brush head 36 is facilitated after the connecting frame 32 passes through.
The working principle of the invention is as follows: in the prior art, for some reactions which can generate precipitates, a large amount of precipitates can be generated in the reaction process, the generated precipitates can be accumulated in the hydrothermal kettle, so that the precipitates can be accumulated to all corners of the reaction kettle when the internal parts of the hydrothermal kettle are subjected to stirring reaction, so that reaction liquid and the precipitates generated by the reaction are inconvenient to discharge after the reaction is finished, and meanwhile, the internal parts of the hydrothermal kettle after the reaction are inconvenient to clean, the embodiment of the invention can solve the problems, in particular embodiments, the internal parts of the hydrothermal kettle shell 1 can provide a container for the reaction, the cover body 2 can form a sealed container with the hydrothermal kettle shell 1 to perform the reaction, the main feed port 3 can facilitate the operator to add raw materials required by the reaction into the internal parts of the hydrothermal kettle shell 1, the auxiliary feed port 4 can facilitate the addition of other auxiliary materials, the hydrothermal device can heat the liquid for the internal reaction of the hydrothermal kettle shell 1, the thermometer 12 can detect the temperature of the internal parts of the hydrothermal kettle shell 1, so that the operator can conveniently clean the internal parts of the hydrothermal kettle shell 1, the internal parts of the hydrothermal kettle shell 1 can be conveniently cleaned, the stirring device can control the internal parts of the hydrothermal kettle shell 1, the water can be prevented from flowing through the internal parts of the reaction shell 1, the stirring device can be completely, the water can be prevented from flowing through the internal parts of the reaction shell 1, the internal parts of the hydrothermal kettle can be completely, the reaction can be prevented from flowing through the internal parts of the reaction shell 1, the reaction can be completely, the internal parts of the reaction can be prevented from being completely, and the internal part of the reaction can be separated from being filled into the internal part of the reaction shell 1, and the reaction shell is required is a reaction tank is filled, and a reaction tank is used for the required raw material is heated, the flowing liquid passes through the precipitation guiding device to enable the precipitate generated by the reaction to be filtered and left in the precipitation guiding device, so that the precipitate is separated from the reacted liquid, the obstruction of the mixed reaction of the precipitate to the liquid is avoided, the precipitate separated from the liquid can be conveniently discharged after the reaction is completed, and the precipitate is prevented from being scattered in various positions in the hydrothermal kettle shell 1 and difficult to clean and discharge.
The foregoing has shown and described the basic principles, principal features and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the foregoing embodiments, but rather, the foregoing embodiments and description illustrate the principles of the invention, and that various changes and modifications may be effected therein without departing from the spirit and scope of the invention as defined by the appended claims and their equivalents.

Claims (4)

1. The utility model provides a vertical hydrothermal kettle, includes hydrothermal kettle casing (1), lid (2) are installed at the top of hydrothermal kettle casing (1), the top of lid (2) is provided with main feed inlet (3), the top array of lid (2) is provided with a plurality of auxiliary feed inlets (4), the bottom of hydrothermal kettle casing (1) is provided with discharge gate (19), its characterized in that still includes:
the temperature detector (12) is inserted into one side of the top of the hydrothermal kettle shell (1) in a penetrating way, and the bottom end of the temperature detector (12) extends to the inside of the hydrothermal kettle shell (1);
the first fixing frames (13) are fixed on the side wall of the hydrothermal kettle shell (1) in an array manner;
the baffle plates (14) are inserted and fixed in the first fixing frames (13);
the hydrothermal device is arranged on the outer wall of the hydrothermal kettle shell (1);
the stirring device is arranged between the hydrothermal kettle shell (1) and the cover body (2);
the sedimentation guide device is arranged between the inside of the hydrothermal kettle shell (1) and the stirring device;
the stirring device is used for stirring the inside of the hydrothermal kettle shell (1), and the stirring device drives the sediment guiding device to start guiding reaction to generate sediment, flow to the inside of the sediment guiding device and collect the sediment, and the sediment is separated from liquid;
the stirring device comprises a mounting frame (5), the mounting frame (5) is fixed at the top of the cover body (2), a motor (6) is fixed at the top of the mounting frame (5) through screws, an output shaft of the motor (6) penetrates through the mounting frame (5) and the cover body (2) and then extends to the inside of the hydrothermal kettle shell (1), a rotating shaft (7) is fixed at the end part of the output shaft of the motor (6), and a plurality of stirring blades (8) are coaxially fixed on the outer wall of the rotating shaft (7);
the sedimentation guide device comprises a threaded opening (15) and a spiral blade (25), the threaded opening (15) is formed in the bottom of the hydrothermal kettle shell (1), a sedimentation tank (16) is inserted into the threaded opening (15), the sedimentation tank (16) is provided with an annular screen plate (1601) and a bottom plate (18), an external thread sleeve (17) is fixed on the outer annular surface of the bottom plate (18), the external thread sleeve (17) is in threaded fit with the threaded opening (15), the spiral blade (25) is movably inserted into the sedimentation tank (16), the spiral blade (25) is connected onto the surface of the rotating shaft (7) in a sliding mode in the vertical direction, an elastic supporting mechanism is connected between the top of the spiral blade (25) and the surface of the rotating shaft (7), and a backflow mechanism for guiding liquid to flow towards the top of the hydrothermal kettle shell (1) is arranged between two sides of the sedimentation tank (16) and the inside of the hydrothermal kettle shell (1);
the elastic supporting mechanism comprises a first fixing plate (20) and a first sliding groove (23), the first fixing plate (20) is fixed on the outer wall of the rotating shaft (7), a first spring (21) is fixed at the bottom of the first fixing plate (20), the first spring (21) is sleeved on the outer ring of the rotating shaft (7), a lifting disc (22) is fixed at the bottom of the first spring (21), a sliding opening (24) is formed in the inner ring of the lifting disc (22), the first sliding groove (23) is formed in the outer wall of the rotating shaft (7) in an array mode, and the first sliding groove (23) is in sliding fit with the sliding opening (24);
the backflow mechanism comprises two second fixing frames (49), the two second fixing frames (49) are symmetrically fixed on the inner wall of the hydrothermal kettle shell (1), pipelines (26) are fixed in the two second fixing frames (49), a shell (27) is fixed in the pipelines (26), two first gears (28) meshed with each other are rotatably installed in the shell (27), a linkage mechanism used for driving the first gears (28) to rotate is installed between one first gear (28) and the first fixing plate (20), and bent pipes (33) are fixed at the tops of the two pipelines (26);
the linkage mechanism comprises two connecting frames (32) and a second bevel gear (29), wherein the two connecting frames (32) are symmetrically fixed on two sides of the first fixing plate (20), annular porous sleeves (31) are jointly fixed at the bottoms of the two connecting frames (32), the annular porous sleeves (31) are movably sleeved on the outer ring of the settling tank (16), annular bevel racks (30) are coaxially fixed at the bottoms of the annular porous sleeves (31), the second bevel gear (29) is rotatably installed on the outer wall of the shell (27), a rotating shaft of the second bevel gear (29) penetrates through the shell (27) and then is coaxially fixed with one of the first bevel gears (28), and the second bevel gear (29) is meshed with the annular bevel racks (30);
the utility model provides a hydrothermal kettle shell (1) is fixed with arc filter (34) on the inner wall of casing (1), arc filter (34) cup joint on the outer wall of pipeline (26), offer on the lateral wall of arc filter (34) with thermometer (12) baffle (14) through-hole (48) corresponding in pipeline (26), the top circumference array of arc filter (34) is fixed with a plurality of arc poles (35), all the both sides of arc pole (35) all articulate have a plurality of upset brush heads (36), all upset brush heads (36) with the articulated department pivot outer lane of arc pole (35) all overlaps torsion spring (37), torsion spring (37) both ends respectively with arc pole (35) with upset brush head (36) fixed connection, all the outer wall sliding connection of arc pole (35) have a plurality of with thrust plate (41) corresponding with upset brush heads (36), all thrust plate (41) with thrust plate (32) link are connected through pulling mechanism between the pulling mechanism for driving reciprocating movement board (41).
2. The vertical type hydrothermal kettle according to claim 1, wherein the hydrothermal device comprises a hydrothermal pipe (9), the hydrothermal pipe (9) is spirally wound on the outer wall of the hydrothermal kettle shell (1), a water inlet connecting pipe (10) is fixedly connected to the end part of the top of the hydrothermal pipe (9), and a water outlet connecting pipe (11) is fixedly connected to the end part of the bottom of the hydrothermal pipe (9).
3. The vertical type hydrothermal kettle according to claim 1, wherein the pulling mechanism comprises a plurality of second sliding grooves (38) and a plurality of second fixing plates (43), all the second sliding grooves (38) are respectively formed in the top of the arc-shaped rod (35), sliding blocks (39) corresponding to the pushing plates (41) are slidingly connected in the second sliding grooves (38), pulling ropes (40) are fixedly connected between all the sliding blocks (39) in the same second sliding grooves (38), a winding mechanism for pulling the pulling ropes (40) is arranged between one end, facing towards the connecting frame (32), of all the pulling ropes (40), and one end, facing away from the connecting frame (32), of all the pulling ropes (40) is fixedly provided with second springs (44), all the second fixing plates (43) are respectively fixed on one end, facing away from the connecting frame (32), of the arc-shaped rod (35), and all the second springs (44) are respectively fixed on one end, facing away from the second fixing plates (43).
4. A vertical hydrothermal kettle according to claim 3, wherein the winding mechanism comprises a plurality of winding discs (46) and a plurality of openings (42), two arc racks (47), all the winding discs (46) are rotatably installed on the side wall of the arc filter plate (34), the openings (42) are formed in the end parts of the arc rods (35), the pulling ropes (40) penetrate through the openings (42) towards one end part of the connecting frame (32) and then fixedly wind the outer parts of the winding discs (46), a third gear (45) is coaxially fixed at the top of each winding disc (46), the two arc racks (47) are symmetrically fixed on the side walls of the two connecting frames (32), the arc centers of the arc racks (47) are located on the axis of the rotating shaft (7), and the third gear (45) is matched with the arc racks (47).
CN202210424593.9A 2022-04-21 2022-04-21 Vertical hydrothermal kettle Active CN114870774B (en)

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