CN114832928A - Pulsed intelligent breaker of high-purity phosphorus - Google Patents

Pulsed intelligent breaker of high-purity phosphorus Download PDF

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Publication number
CN114832928A
CN114832928A CN202210770825.6A CN202210770825A CN114832928A CN 114832928 A CN114832928 A CN 114832928A CN 202210770825 A CN202210770825 A CN 202210770825A CN 114832928 A CN114832928 A CN 114832928A
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China
Prior art keywords
raw material
crushing
phosphorus
vortex
turbulence
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CN202210770825.6A
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CN114832928B (en
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邓拥军
何建军
张浩鹏
沈丹丹
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Jiangsu Qinene New Materials Co ltd
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Jiangsu Qinene New Materials Co ltd
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C19/00Other disintegrating devices or methods
    • B02C19/18Use of auxiliary physical effects, e.g. ultrasonics, irradiation, for disintegrating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B02CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
    • B02CCRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
    • B02C23/00Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
    • B02C23/18Adding fluid, other than for crushing or disintegrating by fluid energy
    • B02C23/36Adding fluid, other than for crushing or disintegrating by fluid energy the crushing or disintegrating zone being submerged in liquid

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  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Health & Medical Sciences (AREA)
  • Toxicology (AREA)
  • Disintegrating Or Milling (AREA)

Abstract

The invention discloses a pulse type intelligent crushing device for high-purity phosphorus, which is provided with a crushing cylinder body, a pulse type crushing component and a flow disturbance mechanism, wherein the crushing cylinder body is used for placing a solid phosphorus raw material, water is filled in the crushing cylinder body, the flow disturbance mechanism is arranged in the crushing cylinder body, pool water is stirred, so that crushed phosphorus powder is separated from the solid phosphorus raw material, the pulse type crushing component comprises an electromagnetic pulse generator and a pulse reflector, the output end of the electromagnetic pulse generator is right opposite to the solid phosphorus raw material and used for generating electromagnetic pulse waves and crushing the solid phosphorus raw material in a shock wave mode, the pulse reflector is opposite to the electromagnetic pulse generator and used for receiving and reflecting electromagnetic pulses sent by the electromagnetic pulse generator, the electromagnetic pulses reflected by the pulse reflector are right opposite to the solid phosphorus raw material, so that the electromagnetic pulse waves are used for crushing the solid phosphorus raw material in the shock wave mode, and the crushing process of the solid phosphorus raw material has no physical contact, thereby avoiding the risk of collision with spontaneous combustion.

Description

Pulsed intelligent breaker of high-purity phosphorus
Technical Field
The invention relates to the technical field of crushing machinery, in particular to a pulse type intelligent crushing device for high-purity phosphorus.
Background
White phosphorus is a simple substance of phosphorus and has a chemical formula of P 4 . The appearance was white or pale yellow translucent solid. Soft, brittle and deep in color when cold. Green phosphorescence and white smoke are generated in the dark in the exposed air. The fire was about 40 ℃ in humid air and slightly higher in dry air. The white phosphorus can directly react with halogen, sulfur, metal, etc., react with nitric acid to generate phosphoric acid, and react with sodium hydroxide or potassium hydroxide to generate phosphine and sodium hypophosphite or potassium phosphate. Contact with potassium chlorate, potassium permanganate, peroxides and other oxides should be avoided.
Most of crushing mechanisms in the prior art use a physical contact mode to crush raw materials through collision, but due to the physical characteristics of phosphorus, when massive high-purity phosphorus is crushed, firstly, a crushing environment needs to be placed in water to avoid spontaneous combustion caused by the fact that phosphorus raw materials contact air, but the instant of contact collision of the crushing mechanism and the massive phosphorus raw materials can generate heat, the phosphorus can be spontaneously combusted after the heat is accumulated, and the crushing cannot be carried out.
Disclosure of Invention
The invention aims to provide a pulse type intelligent crushing device for high-purity phosphorus, which aims to solve the problem that in the prior art, most of crushing mechanisms are in physical contact, raw materials are crushed through collision, phosphorus is spontaneously combusted when the phosphorus raw materials are crushed, and the crushing cannot be carried out.
In order to solve the technical problems, the invention specifically provides the following technical scheme:
the utility model provides an intelligent breaker of pulsed of high-purity phosphorus, possesses:
the crushing cylinder body is used for placing a solid phosphorus raw material, water is filled in the crushing cylinder body, and the solid phosphorus raw material is located in the water;
the pulse type crushing component is arranged on the crushing cylinder body and used for generating electromagnetic pulse waves and crushing the solid phosphorus raw material in a shock wave mode;
the turbulence mechanism is arranged in the crushing cylinder body and stirs pool water to separate crushed phosphorus powder from the solid phosphorus raw material;
the pulse type crushing component comprises an electromagnetic pulse generator and a pulse reflector, the electromagnetic pulse generator and the pulse reflector are fixed on the crushing cylinder body, the output end of the electromagnetic pulse generator faces the solid phosphorus raw material and is used for generating electromagnetic pulse waves and shattering the solid phosphorus raw material in the form of shock waves, the pulse reflector is opposite to the electromagnetic pulse generator and is used for receiving and reflecting the electromagnetic pulses sent by the electromagnetic pulse generator, and the electromagnetic pulses reflected by the pulse reflector face the solid phosphorus raw material.
As a preferable scheme of the present invention, the turbulent flow mechanism is an agitation type turbulent flow structure, the water liquid is agitated by adopting a direct contact manner, so that the crushed phosphorus powder is separated from the solid phosphorus raw material, and the turbulent flow mechanism comprises a turbulent flow plate and an agitation turbulent flow component for driving the turbulent flow plate to move in the crushing cylinder body.
As a preferable scheme of the present invention, an output end of the turbulence-stirring member is connected to the spoiler, and the turbulence-stirring member drives the spoiler to move transversely back and forth;
the stirring and turbulent flow component comprises a stirring sliding groove arranged outside the crushing cylinder body, a stirring sliding seat and a stirring driving component for driving the stirring sliding seat to move in a reciprocating mode are arranged in the stirring sliding groove, the stirring sliding seat is connected with an inverted U-shaped support, one end of the inverted U-shaped support is connected with the stirring sliding seat, the other end of the inverted U-shaped support extends into the crushing cylinder body, and the end of the inverted U-shaped support is connected with the turbulent flow plate.
As a preferred scheme of the present invention, the turbulent flow mechanism is a jet type turbulent flow structure, and the solid phosphorus raw material is impacted by water flow to separate the crushed phosphorus powder and phosphorus lumps from the solid phosphorus raw material, the turbulent flow mechanism comprises a turbulent flow nozzle and a turbulent flow pump connected with the turbulent flow nozzle, and the water flow output by the turbulent flow nozzle faces the solid phosphorus raw material.
As a preferable scheme of the invention, an inlet of the turbulent flow pump is arranged below the liquid level, and the turbulent flow nozzle is arranged below the liquid level and directly faces the solid phosphorus raw material.
As a preferable scheme of the invention, the turbulent flow spray head is positioned above the liquid level and faces the solid phosphorus raw material.
As a preferred scheme of the invention, the turbulent flow mechanism further comprises a displacement component of which the output end is connected with the turbulent flow nozzle, and the displacement component drives the turbulent flow nozzle to move above the liquid level, so that water flow sprayed by the turbulent flow nozzle falls on different areas of the solid phosphorus raw material;
the aversion part is including setting up the annular mounting panel in the liquid level top, the annular mounting panel pass through the support with broken cylinder body links to each other, be provided with annular aversion spout on the annular mounting panel, it is provided with aversion slide and drive to slide in the aversion spout aversion slide gliding drive assembly, the aversion slide is connected with the jib, the terminal vertical downwards of jib and with the vortex shower nozzle links to each other.
As a preferred scheme of the present invention, the turbulent flow mechanism is an eddy flow type turbulent flow structure, which generates an eddy and attracts the phosphorus powder by using the eddy, so that the crushed phosphorus powder is separated from the solid phosphorus raw material.
As a preferable scheme of the invention, the turbulence mechanism comprises a plurality of turbulence plates and a turbulence assembly for driving the turbulence plates to horizontally rotate, and the vortexes formed by the rotation of the turbulence plates are positioned around the solid phosphorus raw material.
As a preferable scheme of the invention, the turbulence mechanism comprises a vortex nozzle and a vortex pump connected with the vortex nozzle, an inlet of the vortex pump is installed at the upper part of the vortex, a liquid pumping direction of the vortex pump is arranged along the tangential direction of the vortex, the crushing cylinder body is in a cylindrical tubular structure, the vortex nozzle is tightly attached to the inner wall of the crushing cylinder body, and an injection direction of the vortex nozzle is arranged along the tangential direction of the crushing cylinder body.
Compared with the prior art, the invention has the following beneficial effects:
(1) according to the invention, the pulse type crushing component is arranged to crush the solid phosphorus raw material, the pulse type crushing component generates electromagnetic pulse waves through the electromagnetic pulse generator, so that the electromagnetic pulse waves crush the solid phosphorus raw material in a shock wave mode, and the solid phosphorus raw material is not physically contacted in the crushing process, so that the risk of collision and spontaneous combustion is avoided;
(2) according to the invention, the flow disturbing mechanism is arranged, has good phosphorus raw material stripping performance, can stir pool water, enables crushed phosphorus powder to be separated from solid phosphorus raw materials, can enable the phosphorus raw materials to sink to the bottom, and avoids the phosphorus raw materials from floating to the liquid level to cause spontaneous combustion, meanwhile, the phosphorus raw materials cannot be contacted and collided with other components in the whole crushing process, and the risk of spontaneous combustion caused by heating the phosphorus due to the contact with the phosphorus is avoided, so that the crushing efficiency is enhanced, the risk of spontaneous combustion in the crushing process is reduced, and the safety performance is improved.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below. It should be apparent that the drawings in the following description are merely exemplary and that other implementation drawings may be derived from the provided drawings by those of ordinary skill in the art without inventive effort.
FIG. 1 is an overall schematic view of the present invention;
FIG. 2 is a schematic diagram of an agitated turbulator structure according to an embodiment of the present invention;
FIG. 3 is a schematic diagram of a jet-based turbulator structure according to an embodiment of the present invention;
FIG. 4 is a schematic structural diagram of a displacement member provided in accordance with an embodiment of the present invention;
FIG. 5 provides a bottom view of the displacement member for an embodiment of the present invention;
FIG. 6 is a schematic diagram of a vortex spoiler structure according to an embodiment of the present invention;
FIG. 7 is a schematic view of a vortex nozzle provided in accordance with an embodiment of the present invention;
FIG. 8 is a schematic top view of a vortex nozzle according to an embodiment of the present invention.
The reference numerals in the drawings denote the following, respectively:
1-crushing a cylinder body; 2-a pulse type crushing component; 3-a flow disturbing mechanism;
201-an electromagnetic pulse generator; 202-a pulse reflector;
311-spoiler; 312-agitating the spoiler;
3121-a stirring chute; 3122-an agitation slide; 3123-agitation drive assembly; 3124-inverted U-shaped support;
321-a turbulent flow nozzle; 322-a turbulent flow pump; 323-a displacement member;
3231-annular mounting plate; 3232-shifting chute; 3233-shift slide; 3234-a shift drive assembly; 3235-a boom;
331-a whirl plate; 332-a vortex spoiler assembly; 333-vortex nozzle; 334-vortex pump.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
As shown in fig. 1 to 8, the present invention provides a pulsed intelligent high-purity phosphorus crushing apparatus, comprising:
the device comprises a crushing cylinder body 1, wherein the crushing cylinder body 1 is used for placing a solid phosphorus raw material, water is filled in the crushing cylinder body 1, and the solid phosphorus raw material is located in the water;
the pulse type crushing component 2 is arranged on the crushing cylinder body 1 and used for generating electromagnetic pulse waves and crushing the solid phosphorus raw material in a shock wave mode;
the turbulence mechanism 3 is arranged in the crushing cylinder body 1, and pool water is stirred to separate crushed phosphorus powder from solid phosphorus raw materials;
the pulse type crushing component 2 comprises an electromagnetic pulse generator 201 and a pulse reflector 202, wherein the electromagnetic pulse generator 201 and the pulse reflector 202 are fixed on the crushing cylinder body 1, the output end of the electromagnetic pulse generator 201 faces the solid phosphorus raw material and is used for generating electromagnetic pulse waves and crushing the solid phosphorus raw material in the form of shock waves, the pulse reflector 202 is opposite to the electromagnetic pulse generator 201 and is used for receiving and reflecting the electromagnetic pulses sent by the electromagnetic pulse generator 201, and the electromagnetic pulses reflected by the pulse reflector 202 face the solid phosphorus raw material.
The phosphorus should be kept in water and the white phosphorus cannot be stored in kerosene or wax, because the white phosphorus has a very low ignition point, only 40 ℃ and (melting point 44.1 ℃ and boiling point 280.5 ℃) and can spontaneously ignite when exposed to air, and therefore the white phosphorus must be kept in a substance with a higher boiling point by isolating air. And the white phosphorus is insoluble in water, slightly soluble in benzene and chloroform, and easily soluble in nonpolar solvents such as carbon disulfide, kerosene, paraffin and the like to form a white phosphorus solution. Since the solution is homogeneous, the solute white phosphorus remains in contact with air in the upper layer of the solution, and there is still a risk of spontaneous combustion. And the solvent kerosene or paraffin is inflammable, the spontaneous combustion of the white phosphorus can ignite the kerosene or paraffin to cause more serious accidents, and the density (the density is 1.82g/cm < SP > 3 </SP >) of the white phosphorus is higher than that of water and can sink underwater, so the white phosphorus is stored by adopting water.
Therefore, in the present embodiment, the crushing cylinder 1 is filled with water, and the solid phosphorus raw material is placed in water to be crushed, so as to avoid the solid phosphorus raw material from contacting with air in the crushing process, thereby avoiding the risk of spontaneous combustion of the raw material.
Similarly, if the solid phosphorus material is crushed by mechanical impact, the solid phosphorus material will heat up during impact, and thus the solid phosphorus material will be heated, which may cause spontaneous combustion, since the ignition point of phosphorus is low. In the embodiment, the pulse type crushing component 2 is arranged to crush the solid phosphorus raw material, the pulse type crushing component 2 generates electromagnetic pulse waves through the electromagnetic pulse generator 201, the electromagnetic pulse waves are used for crushing the solid phosphorus raw material in a shock wave mode, and the solid phosphorus raw material is not physically contacted in the crushing process, so that the risk of collision and spontaneous combustion is avoided.
Further, in the present embodiment, the pulse crushing member 2 further includes a pulse reflector 202, the pulse reflector 202 is opposite to the electromagnetic pulse generator 201, and receives and reflects the electromagnetic pulse emitted by the electromagnetic pulse generator 201, the electromagnetic pulse reflected by the pulse reflector 202 faces the solid phosphorus raw material, the electromagnetic pulse generator 201 and the pulse reflector 202 are respectively disposed on two sides of the solid phosphorus raw material, and the electromagnetic pulse wave oscillates the solid phosphorus raw material back and forth in the crushing cylinder 1, so as to achieve a better crushing effect.
It should be noted that, in the present embodiment, the turbulence mechanism 3 is provided, and can stir the pool water to make the pool water fluctuate, so as to drop the crushed phosphorus from the solid phosphorus raw material and fall on the bottom of the tank, so that the remaining solid phosphorus raw material which is not crushed continues to be shocked by the shock wave, thereby improving the crushing effect.
As shown in fig. 2, the turbulence mechanism 3 is a stirring turbulence structure, and the water liquid is stirred by direct contact, so that the crushed phosphorus powder is separated from the solid phosphorus material, and the turbulence mechanism 3 includes a turbulence plate 311 and a stirring turbulence member 312 for driving the turbulence plate 311 to move in the crushing cylinder 1.
Specifically, the output end of the turbulence stirring member 312 is connected to the spoiler 311, and the turbulence stirring member 312 drives the spoiler 311 to move transversely in a reciprocating manner, the turbulence stirring member 312 includes a stirring chute 3121 disposed outside the crushing cylinder 1, a stirring slide 3122 and a stirring driving assembly 3123 for driving the stirring slide 3122 to move reciprocally are disposed in the stirring chute 3121, the stirring driving assembly 3123 may adopt a linear motor, the stirring slide 3122 is connected to an inverted U-shaped support 3124, one end of the inverted U-shaped support 3124 is connected to the stirring slide 3122, the other end of the inverted U-shaped support 3124 extends into the crushing cylinder 1, and the end is connected to the spoiler 311.
When the turbulence stirring member 312 operates, the stirring driving unit 3123 drives the stirring slide 3122 to reciprocate in the stirring chute 3121, and drives the turbulence plate 311 to reciprocate in the crushing cylinder 1 through the inverted U-shaped support 3124, thereby stirring the water.
Through the setting, the water liquid can be stirred by the turbulence mechanism 3 to enable the pool water to fluctuate, so that the crushed phosphorus falls off from the solid phosphorus raw material, and the crushing effect is improved. However, the generated water liquid is stirred a little and the broken massive phosphorus raw material is difficult to fall off from the solid phosphorus raw material, so the effect of peeling the phosphorus raw material is poor.
Meanwhile, in the embodiment, the water liquid is stirred in a direct contact mode, and the water liquid contains phosphorus powder, so that phosphorus is likely to be touched during stirring, and the phosphorus is heated during collision, so that the risk of spontaneous combustion of the phosphorus is increased.
Further, this embodiment adopts stirring formula vortex structure, and water liquid is constantly undulant in broken cylinder body 1, and the phosphorus powder then wanders in broken cylinder body 1 along with the fluctuation of water liquid, if the phosphorus powder moves to the liquid level, has the risk of spontaneous combustion with the contact of air.
In another embodiment, as shown in fig. 3, the turbulent flow mechanism 3 is a jet turbulent flow structure, and the solid phosphorus raw material is impacted by water flow, so that the crushed phosphorus powder and phosphorus lumps are separated from the solid phosphorus raw material, the turbulent flow mechanism 3 includes a turbulent flow nozzle 321 and a turbulent flow pump 322 connected to the turbulent flow nozzle 321, the water flow output by the turbulent flow nozzle 321 faces the solid phosphorus raw material, an inlet of the turbulent flow pump 322 is installed below the liquid level and is close to the area of the liquid level, so as to avoid sucking the powder at the bottom of the pool, and the turbulent flow nozzle 321 is arranged below the liquid level and faces the solid phosphorus raw material.
Through the above arrangement, the turbulent flow mechanism 3 can jet water liquid by aiming at the position of the solid phosphorus raw material to impact the solid phosphorus raw material, so that the crushed phosphorus powder and the massive phosphorus raw material fall off from the solid phosphorus raw material, and compared with the previous embodiment, the effect of stripping the phosphorus raw material is better.
However, in this embodiment, a jet-type turbulent flow structure is adopted, the water liquid continuously fluctuates in the crushing cylinder 1 under the impact of the jet liquid, the phosphorus powder fluctuates in the crushing cylinder 1 along with the fluctuation of the water liquid, and there is still a risk that the phosphorus powder moves to the liquid surface and contacts with air to spontaneously ignite.
In order to further improve the effect of stripping the phosphorus raw material by the turbulence mechanism 3 in this embodiment, the turbulence mechanism 3 further includes a displacement component 323 having an output end connected to the turbulence nozzle 321, the displacement component 323 drives the turbulence nozzle 321 to move above the liquid surface, so that water ejected from the turbulence nozzle 321 falls on different areas of the solid phosphorus raw material, the displacement component 323 includes an annular mounting plate 3231 disposed above the liquid surface, the annular mounting plate 3231 is connected to the crushing cylinder 1 through a bracket, an annular displacement chute 3232 is disposed on the annular mounting plate 3231, a displacement slide 3233 and a displacement drive component 3234 for driving the displacement slide 3233 to slide are slidably disposed in the displacement chute 3232, the displacement drive component 3234 may be a rack-and-pinion drive structure, the displacement slide 3233 is connected to a boom 3235, and a tail end of the boom 3235 is vertically downward and connected to the turbulence nozzle 321.
Through setting up shift unit 323, it can drive vortex shower nozzle 321 and remove, changes vortex shower nozzle 321 blowout rivers and falls on the position of solid phosphorus raw materials, promotes its effect of peeling off the phosphorus raw materials, nevertheless because vortex shower nozzle 321 removes and is located under the liquid level, and contains the phosphorus powder in the water liquid, at its removal in-process, very probably touches the phosphorus, can make the phosphorus be heated when the collision to the risk of phosphorus spontaneous combustion has been increased.
To avoid this risk, the turbulator nozzle 321 may be positioned above the liquid surface and against the solid phosphorus feedstock, avoiding contact with the powder in the aqueous liquid when agitated.
However, in general, this embodiment has better effect of stripping the phosphorus material than the previous embodiment, and avoids the natural risk caused by touching the phosphorus powder, but the risk of spontaneous combustion caused by the phosphorus powder moving to the liquid surface by itself and contacting with air still exists.
In another embodiment, the turbulent flow mechanism 3 is an eddy flow type turbulent flow structure which generates eddy and attracts the phosphorus powder by the eddy to separate the crushed phosphorus powder from the solid phosphorus raw material.
The turbulence mechanism 3 comprises a plurality of turbulence plates 331 and a turbulence component 332 for driving the turbulence plates 331 to horizontally rotate, the displacement driving component 3234 is a motor, and the turbulence plates 331 are provided with a plurality of vortexes which are formed when the turbulence plates 331 rotate and are positioned around the solid phosphorus raw material. The displacement driving component 3234 drives the vortex plate 331 to rotate, so that the water in the crushing cylinder 1 can form a vortex, and the attraction of the vortex center to surrounding substances is utilized to make the vortex center outside the solid phosphorus raw material and attract the crushed powdery phosphorus raw material of the solid phosphorus raw material.
And because the characteristic of the vortex can drag surrounding substances and make the substances deposit to the bottom, the vortex type turbulent flow structure can attract broken phosphorus raw materials, and the phosphorus raw materials deposit at the bottom of the cylinder to avoid moving to the liquid level, thereby reducing the risk of spontaneous combustion caused by the contact of the phosphorus raw materials and air.
It should be noted that, the vortex-type turbulent flow structure agitates the water liquid by direct contact to generate a vortex, and the turbulence is likely to contact with the phosphor, which heats the phosphor during collision, thereby increasing the risk of spontaneous combustion of the phosphor.
For this purpose, the present embodiment provides a further embodiment, in which the turbulence mechanism 3 is still an eddy current type turbulence structure, but the turbulence mechanism 3 includes an eddy current nozzle 333 and an eddy current pump 334 connected to the eddy current nozzle 333, an inlet of the eddy current pump 334 is installed on the upper portion of the eddy current, a liquid pumping direction of the eddy current pump 334 is arranged along a tangential direction of the eddy current, the crushing cylinder 1 is a cylindrical tubular structure, the eddy current nozzle 333 is tightly attached to an inner wall of the crushing cylinder 1, and an injection direction of the eddy current nozzle 333 is arranged along the tangential direction of the crushing cylinder 1.
In the vortex-type turbulent flow structure, the vortex nozzle 333 is used for jetting water flow along the tangential direction of the crushing cylinder body 1, the water flow is translated along the inner wall of the cylinder body, and a rotating force is applied to the water liquid in the crushing cylinder body 1, so that the water liquid in the crushing cylinder body 1 integrally rotates together, and a vortex is formed at the center of the water liquid.
Above-mentioned embodiment, can exert suction to the phosphorus raw materials after the breakage, make it drop from solid phosphorus raw materials, have good phosphorus raw materials stripping performance, and the phosphorus raw materials can sink along the swirl after getting into the swirl, can avoid the phosphorus raw materials come-up to the liquid level and spontaneous combustion, and simultaneously, whole crushing process phosphorus raw materials can not collide with other part contact, avoided because touch phosphorus, make the phosphorus be heated and the risk of spontaneous combustion, therefore, this embodiment can strengthen crushing efficiency well, reduce the risk of spontaneous combustion in the crushing process, promote the security performance.
The above embodiments are only exemplary embodiments of the present application, and are not intended to limit the present application, and the protection scope of the present application is defined by the claims. Various modifications and equivalents may be made by those skilled in the art within the spirit and scope of the present application and such modifications and equivalents should also be considered to be within the scope of the present application.

Claims (10)

1. The utility model provides an intelligent breaker of pulsed of high-purity phosphorus which characterized in that possesses:
the device comprises a crushing cylinder body (1), wherein the crushing cylinder body (1) is used for placing a solid phosphorus raw material, water is filled in the crushing cylinder body (1), and the solid phosphorus raw material is located in the water;
the pulse type crushing component (2) is arranged on the crushing cylinder body (1) and is used for generating electromagnetic pulse waves and crushing the solid phosphorus raw material in a shock wave mode;
the turbulence mechanism (3) is arranged in the crushing cylinder body (1), and pool water is stirred to separate crushed phosphorus powder from the solid phosphorus raw material;
the pulse type crushing component (2) comprises an electromagnetic pulse generator (201) and a pulse reflector (202), the electromagnetic pulse generator (201) and the pulse reflector (202) are fixed on the crushing cylinder body (1), the output end of the electromagnetic pulse generator (201) is opposite to the solid phosphorus raw material and used for generating electromagnetic pulse waves and crushing the solid phosphorus raw material in the form of shock waves, the pulse reflector (202) is opposite to the electromagnetic pulse generator (201) and used for receiving and reflecting the electromagnetic pulses emitted by the electromagnetic pulse generator (201), and the electromagnetic pulses reflected by the pulse reflector (202) are opposite to the solid phosphorus raw material.
2. The pulsed intelligent crushing device of high-purity phosphorus according to claim 1, characterized in that: the turbulence mechanism (3) is a stirring type turbulence structure, adopts a direct contact mode to stir water liquid, and enables the broken phosphorus powder to be separated from the solid phosphorus raw material, and the turbulence mechanism (3) comprises a turbulence plate (311) and a stirring turbulence component (312) for driving the turbulence plate (311) to move in the breaking cylinder body (1).
3. The pulsed intelligent crushing device of high-purity phosphorus according to claim 2, characterized in that: the output end of the turbulence stirring component (312) is connected with the spoiler (311), and the turbulence stirring component (312) drives the spoiler (311) to transversely reciprocate;
the stirring and turbulent flow component (312) comprises a stirring chute (3121) arranged outside the crushing cylinder body (1), a stirring slide seat (3122) and a stirring driving component (3123) for driving the stirring slide seat (3122) to reciprocate are arranged in the stirring chute (3121), an inverted U-shaped support (3124) is connected to the stirring slide seat (3122), one end of the inverted U-shaped support (3124) is connected to the stirring slide seat (3122), the other end of the inverted U-shaped support (3124) extends into the crushing cylinder body (1), and the end is connected to the turbulent flow plate (311).
4. The pulsed intelligent crushing device of high-purity phosphorus according to claim 1, characterized in that: the turbulence mechanism (3) is an injection type turbulence structure, utilizes water flow to impact solid phosphorus raw materials, and makes broken phosphorus powder and phosphorus blocks break away from the solid phosphorus raw materials, the turbulence mechanism (3) comprises a turbulence sprayer (321) and a turbulence pump (322) connected with the turbulence sprayer (321), and the water flow output by the turbulence sprayer (321) faces the solid phosphorus raw materials.
5. The pulsed intelligent crushing device of high-purity phosphorus according to claim 4, characterized in that: the inlet of the turbulent flow pump (322) is arranged below the liquid level, and the turbulent flow nozzle (321) is arranged below the liquid level and faces the solid phosphorus raw material.
6. The pulsed intelligent crushing device of high-purity phosphorus according to claim 4, characterized in that: the turbulent flow spray head (321) is positioned above the liquid level and faces the solid phosphorus raw material.
7. The pulsed intelligent crushing device of high-purity phosphorus according to claim 6, characterized in that: the turbulent flow mechanism (3) further comprises a displacement component (323) of which the output end is connected with the turbulent flow nozzle (321), and the displacement component (323) drives the turbulent flow nozzle (321) to move above the liquid level, so that water flow sprayed by the turbulent flow nozzle (321) falls on different areas of the solid phosphorus raw material;
the shift part (323) including setting up annular mounting panel (3231) in the liquid level top, annular mounting panel (3231) through the support with broken cylinder body (1) links to each other, be provided with annular aversion spout (3232) on annular mounting panel (3231), it is provided with aversion slide (3233) and drive to slide in aversion spout (3232) the gliding aversion drive assembly (3234) of aversion slide (3233), aversion slide (3233) are connected with jib (3235), the end of jib (3235) vertical downwards and with vortex shower nozzle (321) link to each other.
8. The pulsed intelligent crushing device for high-purity phosphorus according to claim 1, characterized in that: the flow disturbing mechanism (3) is of a vortex flow type flow disturbing structure, generates vortex and attracts phosphorus powder by utilizing the vortex, so that the crushed phosphorus powder is separated from the solid phosphorus raw material.
9. The pulsed intelligent crushing device of high-purity phosphorus according to claim 8, characterized in that: the vortex mechanism (3) comprises a vortex plate (331) and a vortex turbulence assembly (332) driven by the vortex plate (331) to rotate horizontally, the vortex plate (331) is provided with a plurality of vortex plates, and the vortex plates (331) form a plurality of vortex plates which are positioned around the solid phosphorus raw material when rotating.
10. The pulsed intelligent crushing device of high-purity phosphorus according to claim 8, characterized in that: vortex mechanism (3) include vortex nozzle (333) and with vortex pump (334) that vortex nozzle (333) link to each other, the upper portion at the swirl is installed to the import of vortex pump (334), just the tangential setting of swirl is followed to the drawing liquid direction of vortex pump (334), broken cylinder body (1) is cylinder tubular structure, vortex nozzle (333) hugs closely on the inner wall of broken cylinder body (1), just the injection direction of vortex nozzle (333) is followed the tangential setting of broken cylinder body (1).
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* Cited by examiner, † Cited by third party
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RU216450U1 (en) * 2022-10-10 2023-02-06 Валентин Алексеевич Голубев Device for shock-cavitational crushing of a substance

Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB905555A (en) * 1959-09-03 1962-09-12 Thomas Haden A process for the shattering of ores and rocks by high frequency electro-magnetic fields
CN1054728A (en) * 1989-04-04 1991-09-25 梅若特雷斯·弗尼特伦彻中心“英波尔斯” The accelerated method of liquid and discrete material and device for carrying out said thereof
JPH11131968A (en) * 1997-10-30 1999-05-18 Komatsu Ltd Electric crushing method and device
CN102172853A (en) * 2011-01-17 2011-09-07 任保林 Method for descaling cold stainless steel/carbon steel by utilizing ultrasonic pulse jet flow
US20120132732A1 (en) * 2009-02-13 2012-05-31 Abdelaziz Bentaj Method and system for reusing materials and/or products by pulsed power
CN203591728U (en) * 2013-12-02 2014-05-14 青海晶和新材料研究所 Ultrasonic wave solid-liquid mixing device
CN105534565A (en) * 2015-12-07 2016-05-04 沈阳彼得康医疗科技有限公司 High-voltage pulse generating device for calculus smashing
CN105776193A (en) * 2016-02-29 2016-07-20 成都新柯力化工科技有限公司 Method for preparing graphene nanoplatelets with pulsed high pressure water jet mill
CN106824506A (en) * 2016-11-14 2017-06-13 中国科学院地质与地球物理研究所 A kind of method and system of utilization separation by shaking table apatite
CN206906319U (en) * 2017-05-11 2018-01-19 湖南财经工业职业技术学院 A kind of inside failure detector for mould processing
CN112452497A (en) * 2020-11-02 2021-03-09 昆明理工大学 Method and device for preparing tailing nano-particles by using high-power electromagnetic pulses
CN113769864A (en) * 2021-09-14 2021-12-10 福州大学 Ore metal mineral content prediction method based on high-voltage electric pulse crushing
CN113976290A (en) * 2021-11-30 2022-01-28 青岛阿莫斯资源科技有限公司 Preparation method of high-purity quartz sand

Patent Citations (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB905555A (en) * 1959-09-03 1962-09-12 Thomas Haden A process for the shattering of ores and rocks by high frequency electro-magnetic fields
CN1054728A (en) * 1989-04-04 1991-09-25 梅若特雷斯·弗尼特伦彻中心“英波尔斯” The accelerated method of liquid and discrete material and device for carrying out said thereof
JPH11131968A (en) * 1997-10-30 1999-05-18 Komatsu Ltd Electric crushing method and device
US20120132732A1 (en) * 2009-02-13 2012-05-31 Abdelaziz Bentaj Method and system for reusing materials and/or products by pulsed power
CN102172853A (en) * 2011-01-17 2011-09-07 任保林 Method for descaling cold stainless steel/carbon steel by utilizing ultrasonic pulse jet flow
CN203591728U (en) * 2013-12-02 2014-05-14 青海晶和新材料研究所 Ultrasonic wave solid-liquid mixing device
CN105534565A (en) * 2015-12-07 2016-05-04 沈阳彼得康医疗科技有限公司 High-voltage pulse generating device for calculus smashing
CN105776193A (en) * 2016-02-29 2016-07-20 成都新柯力化工科技有限公司 Method for preparing graphene nanoplatelets with pulsed high pressure water jet mill
CN106824506A (en) * 2016-11-14 2017-06-13 中国科学院地质与地球物理研究所 A kind of method and system of utilization separation by shaking table apatite
CN206906319U (en) * 2017-05-11 2018-01-19 湖南财经工业职业技术学院 A kind of inside failure detector for mould processing
CN112452497A (en) * 2020-11-02 2021-03-09 昆明理工大学 Method and device for preparing tailing nano-particles by using high-power electromagnetic pulses
CN113769864A (en) * 2021-09-14 2021-12-10 福州大学 Ore metal mineral content prediction method based on high-voltage electric pulse crushing
CN113976290A (en) * 2021-11-30 2022-01-28 青岛阿莫斯资源科技有限公司 Preparation method of high-purity quartz sand

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU216450U1 (en) * 2022-10-10 2023-02-06 Валентин Алексеевич Голубев Device for shock-cavitational crushing of a substance

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