CN114806719A - Concentration method of low-power natural plant water-based spice - Google Patents
Concentration method of low-power natural plant water-based spice Download PDFInfo
- Publication number
- CN114806719A CN114806719A CN202210399167.4A CN202210399167A CN114806719A CN 114806719 A CN114806719 A CN 114806719A CN 202210399167 A CN202210399167 A CN 202210399167A CN 114806719 A CN114806719 A CN 114806719A
- Authority
- CN
- China
- Prior art keywords
- natural plant
- low
- resin
- spice
- power
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
- B01D15/08—Selective adsorption, e.g. chromatography
- B01D15/10—Selective adsorption, e.g. chromatography characterised by constructional or operational features
- B01D15/20—Selective adsorption, e.g. chromatography characterised by constructional or operational features relating to the conditioning of the sorbent material
- B01D15/203—Equilibration or regeneration
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D36/00—Filter circuits or combinations of filters with other separating devices
- B01D36/003—Filters in combination with devices for the removal of liquids
- B01D36/006—Purge means
Abstract
The invention provides a concentration method of low-power natural plant water-based perfume, which is characterized in that the natural plant perfume is used as the only raw material, redundant water is removed, impurities are removed by filtration, the adsorption is carried out by specific resin, and then the resin which is adsorbed with the perfume till saturation is heated to obtain the distillate which becomes the natural plant perfume essential oil; the method has the advantages of one-time concentration, multiple collection modes, simple process and easy operation, fractions collected step by step can be used as raw materials of a high-end essence formula to further improve the added value of products, meanwhile, the fractions can be blended into products with different flavors and fragrance characteristics according to market demands according to the essence formula, and the products or intermediate products can be directly sold as spice products or mixed with unprocessed raw materials to improve the concentration multiple of the raw materials or products to be adjusted with less cost or used as base materials or formula modifying components of the high-end essence formula.
Description
Technical Field
The invention relates to the technical field of perfume concentration, in particular to a method for concentrating low-power natural plant water-based perfume.
Background
The natural plant spice is a primary product formed by condensing the aroma of natural plants in the production and processing process, including but not limited to various fruit juices, tea leaves and fruit peel residues, through collecting the volatilized aroma and recovering the evaporated water concentrated in the aroma in the concentration process of the fruit juices or tea extract. Is a byproduct of large-scale industrial deep processing of natural plants. Because the aroma at this stage belongs to the aroma components in the plant aroma slow-release process, the concentration is not very high, and the aroma belongs to single-time or low-time products, the products with higher times can be formed after moisture or other components are removed and can be used in the market.
Through retrieval, the Chinese patent with publication number CN113201403A discloses a production device and a method for preparing spices by a distillation method, black tea leaves are put into a closed extraction tank with a steam heating and condensing device, steam is introduced for distillation, the pressure of the steam is 300-800 KPa, condensate is collected, the outflow temperature of the condensate is controlled to be 30-40 ℃, and the outflow speed of the condensate is 0.5-2.0L/min, so that black tea distillate A is obtained. Stopping collecting when the weight of the tea raw material reaches 2-6 times of the weight of the tea raw material, and refrigerating for later use. Then extracting by using a rotating cone distillation tower method, and adjusting extraction parameters as follows: the flow rate of the black tea distillate A is 400-800L/H, the feeding temperature of the black tea distillate A is 90-98 ℃, the temperature difference between the feeding temperature of the black tea distillate A and the system is-2-10 ℃, the temperature of a rotary cone distillation tower system is 100 ℃, the external extraction rate of the black tea distillate A is 1.5-3.0%, and the natural high-concentration black tea essence B is obtained.
In the above patent, a device and a method for preparing perfume by distillation method have the following disadvantages: the production method of the perfume is basically the same as the traditional process for preparing the perfume by evaporating and condensing water vapor, the concentration multiple of the perfume obtained by the evaporating and condensing process of the water vapor is not very high, and most of volatile matters such as water, ethanol, methanol and the like account for the main proportion, so that the transportation and the use of the product are influenced.
Therefore, a method for concentrating the low-power natural plant water-based spice is provided.
Disclosure of Invention
The invention aims to provide a method for concentrating low-power natural plant water-based perfume, which aims to realize one-time concentration and output of products by taking natural plant perfume as a raw material through the following process.
In order to achieve the purpose, the invention adopts the following technical scheme:
a method for concentrating low-power natural plant water-based spice comprises the following steps:
SA 1: taking low-power plant spice as a raw material;
SA 2: removing visible impurities possibly introduced in the packaging or transportation engineering by filtering and removing impurities;
SA 3: adsorbing main aroma components in the low-power natural plant spice by using resin until the resin adsorption reaches a saturated state;
SA 4: directly heating the saturated resin, wherein the heating temperature of the resin is kept below the maximum use temperature value of the resin;
SA 5: finally, all possible fractions of the product are obtained at one time through cooling recovery to become the natural plant perfume essential oil mixture.
Preferably, the SA3 process produces an effluent that is discharged directly when it cannot be recovered for reuse.
Preferably, in the SA4 step, the resin is heated by a heating device having a stirring or rotating function.
Preferably, the low-power plant spice is aroma-containing condensed water obtained by concentrating the fruit and vegetable juice in a pre-concentration stage.
According to a further technical scheme of the invention, a direct heating process of the resin is replaced by a medium heating process, and a concentration method comprises the following steps:
SB 1: taking low-power plant spice as a raw material;
SB 2: removing visible impurities possibly introduced in the packaging or transportation engineering by filtering and removing impurities;
SB 3: adsorbing main aroma components in the low-power natural plant spice by using resin until the resin adsorption reaches a saturated state;
SB 4: the saturated resin is heated by using gases at different temperature sections as heating media, and fractions at different temperature sections are collected by circulating condensation heating;
SB 5: the natural plant essential oil can be obtained after the fractions at different temperature sections are mixed and prepared according to a proportion.
Preferably, the heating medium is filtered air, high purity nitrogen or an inexpensive inert gas.
Preferably, the heating medium is maintained at a level below one atmosphere of pressure.
Preferably, the temperature sections of the heating medium in the SB4 step are 45-65C °, 70-95C ° and 100-115C °, respectively.
Due to the adoption of the technical scheme, the embodiment of the invention has the following advantages:
1. a method for concentrating natural plant water-based perfume adopts resin as an intermediate adsorption medium, and the resin saturated in adsorption is concentrated at one time, can be collected in various ways, and has simple process and easy operation.
2. The method for concentrating the low-power natural plant water-based spice has the advantages of low investment, small occupied area, low operating cost and high added value.
3. A method for concentrating low-power natural plant water-based spice can be used as a raw material of a high-end essence formula by collecting fractions step by step, and further improves the added value of products.
4. A method for concentrating natural plant water-based perfume with different fragrance and fragrance characteristics can be prepared according to the formula of the perfume and the market demand.
5. A method for concentrating natural plant water-based perfume with low concentration can be adjusted at will, and meets the requirements of different markets and levels.
6. The effluent liquid of the low-power natural plant water-based spice after being processed by the process can be further treated to be used as high-grade drinking water to further excavate product potential, and the value of resources is maximized.
The foregoing summary is provided for the purpose of description only and is not intended to be limiting in any way. In addition to the illustrative aspects, embodiments, and features described above, further aspects, embodiments, and features of the present invention will be readily apparent by reference to the drawings and following detailed description.
Drawings
In order to more clearly illustrate the embodiments of the present application or the technical solutions in the prior art, the drawings needed to be used in the embodiments or technical descriptions will be briefly described below, it is obvious that the drawings in the following description are only some embodiments of the present application, and for those skilled in the art, other drawings can be obtained according to the drawings without creative efforts.
FIG. 1 is a schematic flow chart of a process for concentrating natural plant perfume according to the present invention;
FIG. 2 is a schematic diagram of a process flow of the natural plant spice concentration process according to the present invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
Example 1:
as shown in figure 1, a method for concentrating low-power natural plant water-based spice comprises the following steps:
SA 1: taking low-power plant spices as raw materials, wherein the low-power plant spices comprise but are not limited to various fruit juices, tea leaves and fruit peel residues, and are primary products formed by condensing evaporated water which collects volatilized aroma and is concentrated in the concentration process of recovered fruit juice or tea extract; in the preferred embodiment, the low-power plant spice is aroma-containing condensed water obtained by pre-concentrating the concentrated fruit and vegetable juice;
SA 2: removing visible impurities possibly introduced in the packaging or transportation engineering by filtering and removing impurities;
SA 3: adsorbing main aroma components in the low-power natural plant spice by using resin until the resin adsorption reaches a saturated state;
SA 4: directly heating the saturated resin; wherein the heating temperature of the resin is kept below the maximum use temperature value of the resin, so that the resin component can not overflow or be mixed into the product by heating; the resin is heated by a heating device with stirring or rotating function; thereby being capable of maintaining the uniformity of heating;
SA 5: and (3) carrying out reduced pressure distillation and condensation on steam generated by heating the resin to obtain all possible fractions of the product at one time to become the natural plant spice and essential oil mixture.
Wherein, in the SA3 step, the produced effluent is directly discharged when the effluent cannot be recycled.
The product or intermediate product produced in the above steps can be directly sold as a spice product or mixed with raw materials, the concentration multiple of the raw materials or products to be adjusted is increased with less cost, or the product or the intermediate product is used as a base material or formula modifying component of a high-end essence formula.
Example 2:
as shown in FIG. 2, a method for concentrating low-power natural plant water-based perfume comprises the following steps:
SB 1: taking low-power plant spice as a raw material;
SB 2: removing visible impurities possibly introduced in the packaging or transportation engineering by filtering and removing impurities;
SB 3: adsorbing main aroma components in the low-power natural plant spice by using resin until the resin adsorption reaches a saturated state;
SB 4: the saturated resin is heated by using gases at different temperature sections as heating media, and fractions at different temperature sections are collected by circulating condensation heating;
SB 5: the natural plant essential oil can be obtained after the fractions at different temperature sections are mixed and prepared according to a proportion.
In this embodiment, the heating medium is not limited and may be filtered air, high purity nitrogen or other inexpensive inert gas, and the heating medium is maintained at a level below one atmosphere, thereby achieving a balance of indirect heating and reduced pressure effective distillation
Wherein, in the SB3 step, the effluent produced is directly discharged when the effluent cannot be recovered and reused.
Wherein, in the step of SB4, the temperature sections of the heating medium are respectively 45-65 ℃, 70-95 ℃ and 100-115 ℃.
The product or intermediate product of the steps can be directly sold as a spice product or mixed with raw materials, the concentration multiple of the raw materials or products to be adjusted is increased with less cost, or the product or the intermediate product is used as a base material or formula modifying component of a high-end essence formula.
The above description is only for the specific embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art can easily conceive various changes or substitutions within the technical scope of the present invention, and these should be covered by the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the appended claims.
Claims (8)
1. A method for concentrating low-power natural plant water-based spice is characterized by comprising the following steps: the method comprises the following steps:
SA 1: taking low-power plant spice as a raw material;
SA 2: removing visible impurities possibly introduced in the packaging or transportation engineering by filtering and removing impurities;
SA 3: adsorbing main aroma components in the low-power natural plant spice by using resin until the resin adsorption reaches a saturated state;
SA 4: directly heating the saturated resin, and keeping the heating temperature of the resin below the maximum use temperature value of the resin;
SA 5: finally, all possible fractions of the product are obtained at one time through cooling recovery to become the natural plant perfume essential oil mixture.
2. The method for concentrating low-power natural plant water-based spice according to claim 1, wherein the method comprises the following steps: in the SA3 process, the effluent produced is discharged directly when it cannot be recovered for reuse.
3. The method for concentrating low-power natural plant water-based spice according to claim 2, wherein the method comprises the following steps: in the SA4 step, the resin is heated by a heating device having a stirring or rotating function.
4. The method for concentrating low-power natural plant water-based spice according to claim 3, wherein the method comprises the following steps: the low-power plant spice is fragrant condensate water obtained by concentrating fruit and vegetable juice in a pre-concentration stage.
5. The method for concentrating low-power natural plant water-based spice according to claim 1, wherein the method comprises the following steps: the direct heating process of the resin is replaced by a medium heating process, and the concentration method comprises the following steps:
SB 1: taking low-power plant spice as a raw material;
SB 2: removing visible impurities possibly introduced in the packaging or transportation engineering by filtering and removing impurities;
SB 3: adsorbing main aroma components in the low-power natural plant spice by using resin until the resin adsorption reaches a saturated state;
SB 4: the saturated resin is heated by using gases at different temperature sections as heating media, and fractions at different temperature sections are collected by circulating condensation heating;
SB 5: the natural plant essential oil can be obtained after the fractions at different temperature sections are mixed and prepared according to a proportion.
6. The method for concentrating low-power natural plant water-based spice according to claim 5, wherein the method comprises the following steps: the heating medium is filtered air, high-purity nitrogen or cheap inert gas.
7. The method for concentrating low-power natural plant water-based spice according to claim 6, wherein the method comprises the following steps: the heating medium is maintained at a level below one atmosphere of pressure.
8. The method for concentrating low-power natural plant water-based spice according to claim 5, wherein the method comprises the following steps:
the temperature sections of the heating medium in the SB4 step are respectively 45-65 ℃, 70-95 ℃ and 100-115 ℃.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210399167.4A CN114806719A (en) | 2022-04-13 | 2022-04-13 | Concentration method of low-power natural plant water-based spice |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210399167.4A CN114806719A (en) | 2022-04-13 | 2022-04-13 | Concentration method of low-power natural plant water-based spice |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN114806719A true CN114806719A (en) | 2022-07-29 |
Family
ID=82537205
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210399167.4A Pending CN114806719A (en) | 2022-04-13 | 2022-04-13 | Concentration method of low-power natural plant water-based spice |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114806719A (en) |
Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2089639A (en) * | 1980-12-19 | 1982-06-30 | Gen Foods Corp | Process for recovery of aroma volatiles |
| JPH1077496A (en) * | 1996-09-02 | 1998-03-24 | T Hasegawa Co Ltd | Preparation of fragrant concentrate |
| CN1428408A (en) * | 2002-12-09 | 2003-07-09 | 广州合诚三先生物科技有限公司 | New method for extracting jasmine oil |
| JP2011092044A (en) * | 2009-10-28 | 2011-05-12 | Sanei Gen Ffi Inc | Method for producing natural flavor |
| CN105581313A (en) * | 2016-01-13 | 2016-05-18 | 山东鲁菱果汁有限公司 | Highly-concentrated essence and preparation method |
| CN109180848A (en) * | 2018-09-10 | 2019-01-11 | 西安金沃泰环保科技有限公司 | A kind of high stability hydrogen bonds hydrophily macroporous absorbent resin and the method for handling hydrogen peroxide tail gas exhaust |
| WO2021131636A1 (en) * | 2019-12-24 | 2021-07-01 | サントリーホールディングス株式会社 | Method for producing de-alcoholized beverage, method for producing alcoholic beverage, and method for producing aroma component derived from alcohol-containing beverage |
| CN214635194U (en) * | 2021-04-07 | 2021-11-09 | 德州绿霸精细化工有限公司 | Tail gas treatment device for reducing tail gas Vocs of pesticide production workshop |
-
2022
- 2022-04-13 CN CN202210399167.4A patent/CN114806719A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2089639A (en) * | 1980-12-19 | 1982-06-30 | Gen Foods Corp | Process for recovery of aroma volatiles |
| JPH1077496A (en) * | 1996-09-02 | 1998-03-24 | T Hasegawa Co Ltd | Preparation of fragrant concentrate |
| CN1428408A (en) * | 2002-12-09 | 2003-07-09 | 广州合诚三先生物科技有限公司 | New method for extracting jasmine oil |
| JP2011092044A (en) * | 2009-10-28 | 2011-05-12 | Sanei Gen Ffi Inc | Method for producing natural flavor |
| CN105581313A (en) * | 2016-01-13 | 2016-05-18 | 山东鲁菱果汁有限公司 | Highly-concentrated essence and preparation method |
| CN109180848A (en) * | 2018-09-10 | 2019-01-11 | 西安金沃泰环保科技有限公司 | A kind of high stability hydrogen bonds hydrophily macroporous absorbent resin and the method for handling hydrogen peroxide tail gas exhaust |
| WO2021131636A1 (en) * | 2019-12-24 | 2021-07-01 | サントリーホールディングス株式会社 | Method for producing de-alcoholized beverage, method for producing alcoholic beverage, and method for producing aroma component derived from alcohol-containing beverage |
| CN214635194U (en) * | 2021-04-07 | 2021-11-09 | 德州绿霸精细化工有限公司 | Tail gas treatment device for reducing tail gas Vocs of pesticide production workshop |
Non-Patent Citations (1)
| Title |
|---|
| 尹卓容: "利用吸附-洗脱方法分离酒精", 酿酒科技, no. 03, pages 36 * |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN101928639B (en) | Natural tea essence prepared by using tea and preparation method thereof | |
| CN105802738B (en) | Extraction method of wild chrysanthemum flower volatile oil | |
| CN105852189B (en) | A kind of method that utilization waste/hypo-tobacco leaf prepares tobacco extract | |
| CN102250689A (en) | Equipment and method for extracting perfume plant essential oil by reduced pressure steam distillation | |
| JP2011508034A (en) | Method for recovering aroma components from tea | |
| CN105296163A (en) | Extraction equipment for fragrant plant essential oil and headspace volatile | |
| CN103215135B (en) | Method for synchronously extracting sage clary essential oil and sclareol from sage clary | |
| CN112679314A (en) | Preparation process of sclareol | |
| CN111588758A (en) | Extraction method of rose extract | |
| CN112753831B (en) | Tea extract and preparation method and application thereof | |
| CN114806719A (en) | Concentration method of low-power natural plant water-based spice | |
| CN104164248A (en) | Preparation method of refined bamboo vinegar | |
| CN103805340A (en) | Method for extracting saffron crocus essential oil | |
| CN101096614A (en) | Rose essential oil vacuum water diffusing flushing steaming subcritical abstraction technology | |
| CN113088400A (en) | Device for extracting aroma substances from aromatic plants | |
| CN106316816A (en) | Method for preparing natural citral | |
| CN105272824A (en) | Preparation method of natural cinnamomum camphora aromatic material | |
| WO2020203720A1 (en) | Method for manufacturing tea aroma composition | |
| CN107927282A (en) | A kind of processing method of green tea extract | |
| CN107879913A (en) | The preparation method of natural benzaldehyde | |
| CN113197935A (en) | Extraction method of high-purity magnolia bark extract | |
| CN113973955A (en) | Tea concentrated solution and preparation method thereof | |
| CN109602065B (en) | Essence recovered from waste gas discharged in reconstituted tobacco concentration process and recovery method and application thereof | |
| CN110540895A (en) | Extraction method of perilla oil | |
| CN108060015A (en) | A kind of method for extracting natural perfume material from fragrant plant using tetraethylene glycol dimethyl ether |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination |