CN114673009A - Antistatic textile composite fabric and preparation process thereof - Google Patents
Antistatic textile composite fabric and preparation process thereof Download PDFInfo
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- CN114673009A CN114673009A CN202210409774.4A CN202210409774A CN114673009A CN 114673009 A CN114673009 A CN 114673009A CN 202210409774 A CN202210409774 A CN 202210409774A CN 114673009 A CN114673009 A CN 114673009A
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/04—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D06N3/047—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds with fluoropolymers
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/20—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads
- D03D15/208—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads cellulose-based
- D03D15/217—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads cellulose-based natural from plants, e.g. cotton
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- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/20—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads
- D03D15/208—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads cellulose-based
- D03D15/225—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads cellulose-based artificial, e.g. viscose
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- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/20—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads
- D03D15/283—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the material of the fibres or filaments constituting the yarns or threads synthetic polymer-based, e.g. polyamide or polyester fibres
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- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D15/00—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used
- D03D15/40—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the structure of the yarns or threads
- D03D15/47—Woven fabrics characterised by the material, structure or properties of the fibres, filaments, yarns, threads or other warp or weft elements used characterised by the structure of the yarns or threads multicomponent, e.g. blended yarns or threads
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/10—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M16/00—Biochemical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. enzymatic
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/0056—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the compounding ingredients of the macro-molecular coating
- D06N3/0061—Organic fillers or organic fibrous fillers, e.g. ground leather waste, wood bark, cork powder, vegetable flour; Other organic compounding ingredients; Post-treatment with organic compounds
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06N—WALL, FLOOR, OR LIKE COVERING MATERIALS, e.g. LINOLEUM, OILCLOTH, ARTIFICIAL LEATHER, ROOFING FELT, CONSISTING OF A FIBROUS WEB COATED WITH A LAYER OF MACROMOLECULAR MATERIAL; FLEXIBLE SHEET MATERIAL NOT OTHERWISE PROVIDED FOR
- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/0056—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the compounding ingredients of the macro-molecular coating
- D06N3/0063—Inorganic compounding ingredients, e.g. metals, carbon fibres, Na2CO3, metal layers; Post-treatment with inorganic compounds
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- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/0086—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the application technique
- D06N3/0088—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof characterised by the application technique by directly applying the resin
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- D06N3/00—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof
- D06N3/04—Artificial leather, oilcloth or other material obtained by covering fibrous webs with macromolecular material, e.g. resins, rubber or derivatives thereof with macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
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- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/02—Natural fibres, other than mineral fibres
- D06M2101/04—Vegetal fibres
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- D06M2101/00—Chemical constitution of the fibres, threads, yarns, fabrics or fibrous goods made from such materials, to be treated
- D06M2101/16—Synthetic fibres, other than mineral fibres
- D06M2101/30—Synthetic polymers consisting of macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D06M2101/32—Polyesters
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- D10—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B—INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
- D10B2201/01—Natural vegetable fibres
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- D10B2201/00—Cellulose-based fibres, e.g. vegetable fibres
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- D10B2201/24—Viscose
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- D10B2331/00—Fibres made from polymers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds, e.g. polycondensation products
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Abstract
The invention discloses an antistatic textile composite fabric and a preparation process thereof, wherein the antistatic textile composite fabric comprises a fabric base layer and an antistatic layer, wherein the fabric base layer is formed by weaving warps and wefts, the warps are formed by blending copper ammonia fibers and polyester fibers, and the wefts are formed by blending aloe fibers, modal fibers and cotton fibers; the antistatic layer is prepared from the following raw materials in percentage by weight: 40-50 parts of methyl acrylate; 5-8 parts of polytetrafluoroethylene; 1-3 parts of a surfactant; 10-15 parts of polyvinyl alcohol; 5-10 parts of nano silver; 10-20 parts of polyethylene glycol. The antistatic textile composite fabric prepared by the invention overcomes the defects of poor humidity, low moisture regain, easy static generation and the like of unmodified polyester fibers, and has good water absorption, moisture absorption, antistatic and antibacterial effects.
Description
Technical Field
The invention belongs to the technical field of textile fabrics, and particularly relates to an antistatic textile composite fabric, and a preparation process thereof.
Background
With the improvement of quality of life, more and more people are aware of the importance of health, and therefore, the requirements of people on clothes are higher and higher, such as clothes with an antibacterial function, the purpose of the antibacterial function is to enable fiber fabrics to have the function of killing or inhibiting pathogenic bacteria, prevent microorganisms from spreading through textiles and protect users from the attack of the microorganisms.
The functional protective textile has the use value of the textile, and also has other functions of antibiosis, flame retardance, mildew resistance, acid and alkali resistance, water and oil repellency, ultraviolet resistance, static resistance and the like. With the continuous development of industrial technology, people inevitably face threats in fire, static electricity, strong acid, strong alkali, virus and the like in work and life, and the functional protective textiles are widely applied to related special industries for resisting the threats. In recent years, with the continuous development of functional textiles, the original single function is gradually developed into multifunctional compounding, the modification treatment of fibers is developed through simple auxiliary agent finishing, and the process and the technology are continuously improved.
The flame-retardant, antistatic and acid and alkali resistant multifunctional fabric is a composite functional fabric integrating multiple functions, which is required by special industries, and the single-function functional protective fabric in the market at present cannot meet the requirements. Most of the acid and alkali resistant fabrics are subjected to special water and oil repellent and acid and alkali resistant after-treatment on the basis of common dyed fabrics, but the flame retardant effect of the flame retardant fabrics is affected by the general acid and alkali resistant agent applied to the surface of the flame retardant fabrics, so that the acid and alkali resistant effect needs to be further realized on the basis of ensuring the flame retardant and antistatic effects.
Disclosure of Invention
The purpose of the invention is as follows: the invention provides an antistatic textile composite fabric, a preparation process thereof and a preparation process thereof aiming at the defects in the prior art.
The technical scheme is as follows: the antistatic textile composite fabric comprises a fabric base layer and an antistatic layer, wherein the fabric base layer is formed by weaving warps and wefts, the warps are formed by blending cuprammonium fibers and polyester fibers, and the wefts are formed by blending aloe fibers, modal fibers and cotton fibers; the antistatic layer is prepared from the following raw materials in parts by weight: 40-50 parts of methyl acrylate; 5-8 parts of polytetrafluoroethylene; 1-3 parts of a surfactant; 10-15 parts of polyvinyl alcohol; 5-10 parts of nano silver; 10-20 parts of polyethylene glycol.
The invention also discloses a preparation process of the antistatic textile composite fabric and the preparation process thereof, wherein the preparation process comprises the following steps:
s11, antibacterial treatment: sequentially putting the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber into a soaking device, injecting a mixed solution added with a mite-proofing agent and an antibacterial agent and an extracting solution into the soaking device to ensure that the mixed solution completely submerges the copper ammonia fiber, the polyester fiber, the antibacterial fiber, the modal fiber and the cotton fiber, respectively taking out the fibers after soaking, and drying the fibers by using a drying device;
s12 spinning: blending the dried copper ammonia fiber and the dried polyester fiber into warp yarn, and then blending the dried aloe fiber, the dried modal fiber and the dried cotton fiber into weft yarn;
s13, weaving: weaving the warp yarns and the weft yarns prepared in the step S12 into grey cloth by using an air jet type weaving machine, and then trimming and rolling the grey cloth;
s14, treating the gray cloth: conveying the gray cloth prepared in the step S13 to a cleaning pool, washing at high temperature, drying after washing, putting the gray cloth into a dip dyeing pool for dyeing after fully drying, and drying and shaping after dyeing to obtain a fabric base layer;
s15, taking 40-50 parts of methyl acrylate in parts by weight; 5-8 parts of polytetrafluoroethylene; 1-3 parts of a surfactant; 10-15 parts of polyvinyl alcohol; 5-10 parts of nano silver; 10-20 parts of polyethylene glycol to prepare an antistatic coating, and then directly coating the antistatic coating on the surface of the fabric substrate, and drying.
Further, in the step S11, heating equipment is used for heating the soaking equipment, the heating temperature is controlled to be 45-65 ℃, and the soaking is carried out for 5-8 hours in a heat preservation mode.
Further, the preparation method of the extracting solution in the step S11 is as follows:
s21, selecting fresh roses, wormwood, murraya paniculata, mozzie buster and mint leaves without diseases and insect pests, and cleaning the roses, the wormwood, the murraya paniculata, the mint leaves by using cleaning equipment;
s22, sequentially putting the cleaned rose, wormwood, murraya paniculata, mozzie buster and mint leaves into drying equipment for drying, controlling the temperature of the drying equipment to be 85-140 ℃, taking out the dried rose, wormwood, murraya paniculata and mint leaves, and placing the dried rose, mugwort, murraya paniculata, mozzie buster and mint leaves in a shade place;
s23, sequentially putting the dried rose, the dried wormwood, the dried murraya paniculata, the dried mozzie buster and the dried mint leaves into crushing equipment, adjusting the rotating speed of the crushing equipment to 150r/min, continuously grinding for 5min, and taking out the crushed materials after full crushing to obtain raw material powder;
s24, putting the raw material powder prepared in the step S23 and deionized water into a reaction kettle according to the weight ratio of 2:10 for fully mixing and reacting, controlling the temperature of the reaction kettle to be 50-95 ℃, and moving the reaction kettle into a vacuum distillation kettle after fully reacting to obtain distillate, namely the extracting solution.
Further, the mass ratio of the anti-mite agent to the antibacterial agent in the mixed liquid medicine is 1: 1.5.
further, the content of the mite-proofing agent and the antibacterial agent in the mixed solution of S11 is not less than 5%.
Further, the diameter of the polyester fiber in the warp yarn is 16-21 μm, the diameter of the cuprammonium rayon fiber is 28-32 μm, the diameter of the aloe fiber in the weft yarn is 2.5-3.6 μm, the diameter of the modal fiber is 4-7 μm, and the diameter of the cotton fiber is 15-16 μm.
Further, before S11, the cuprammonium fibers, the polyester fibers, the aloe fibers, the modal fibers, and the cotton fibers are soaked in deionized water added with sodium hydroxide, then stirred for 1-1.5 hours by using a stirring device, added with a penetrant while stirring, kept at 55 ℃ for reaction for 1 hour, repeatedly washed for 4-8 times by using deionized water after the reaction is complete, and finally dried.
Further, the mass of the deionized water is 10-15 times of the total mass of the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber, the mass of the sodium hydroxide is 1-5% of the total mass of the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber, and the mass of the penetrating agent is 0.1-0.4% of the total mass of the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber.
Further, the drying condition in S15 is 120-.
Has the advantages that: the antistatic textile composite fabric prepared by the invention overcomes the defects of poor humidity, low moisture regain, easy static generation and the like of unmodified polyester fibers, and has good water absorption, moisture absorption, antistatic and antibacterial effects.
Detailed Description
The invention will be further illustrated with reference to specific examples:
example 1
The antistatic textile composite fabric comprises a fabric base layer and an antistatic layer, wherein the fabric base layer is formed by weaving warps and wefts, the warps are formed by blending cuprammonium fibers and polyester fibers, and the wefts are formed by blending aloe fibers, modal fibers and cotton fibers; the antistatic layer is prepared from the following raw materials in percentage by weight: 40 parts of methyl acrylate; 5 parts of polytetrafluoroethylene; 1 part of a surfactant; 10 parts of polyvinyl alcohol; 5 parts of nano silver; 10 parts of polyethylene glycol.
In the embodiment, the diameters of the nano titanium dioxide, the nano zinc oxide and the nano silicon-based oxide are 2-10 nm.
The preparation process of the antistatic textile composite fabric and the preparation process thereof comprises the following steps:
s11, antibacterial treatment: sequentially putting the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber into a soaking device, injecting a mixed solution added with a mite-proofing agent and an antibacterial agent and an extracting solution into the soaking device to enable the mixed solution to completely submerge the copper ammonia fiber, the polyester fiber, the antibacterial fiber, the modal fiber and the cotton fiber, heating the soaking device by using heating equipment, controlling the heating temperature to be 45 ℃, preserving heat and soaking for 5 hours, respectively taking out the fibers after soaking, and drying by using drying equipment;
wherein the mass ratio of the anti-mite agent to the antibacterial agent in the mixed liquid medicine is 1: 1.5; the content of the anti-mite agent and the antibacterial agent in the mixed solution is not lower than 5%;
s12 spinning: blending the dried copper ammonia fiber and the dried polyester fiber into warp yarn, and then blending the dried aloe fiber, the dried modal fiber and the dried cotton fiber into weft yarn;
s13, weaving: weaving the warp yarns and the weft yarns prepared in the step S12 into grey cloth by using an air jet type weaving machine, and then trimming and rolling the grey cloth;
s14, treating the gray cloth: conveying the gray cloth prepared in the step S13 to a cleaning pool, washing at high temperature, drying after washing, putting the gray cloth into a dip dyeing pool for dyeing after fully drying, and drying and shaping after dyeing to obtain a fabric base layer;
s15, taking 40 parts of methyl acrylate in parts by weight; 5 parts of polytetrafluoroethylene; 1 part of a surfactant; 10 parts of polyvinyl alcohol; 5 parts of nano silver; 10 parts of polyethylene glycol to prepare an antistatic coating, and then directly coating the antistatic coating on the surface of the fabric base layer and drying; the drying condition is 120 deg.C, 1.5 min, and the setting condition is 180 deg.C baking for 1.6 min.
In this example, the preparation method of the extract liquid in S11 is as follows:
s21, selecting fresh roses, wormwood, murraya paniculata, mozzie buster and mint leaves without diseases and insect pests, and cleaning the roses, the wormwood, the murraya paniculata, the mint leaves by using cleaning equipment;
s22, sequentially putting the cleaned rose, wormwood, murraya paniculata, mozzie buster and mint leaves into drying equipment for drying, controlling the temperature of the drying equipment to be 85 ℃, taking out the dried rose, wormwood, murraya paniculata and mint leaves, and putting the dried rose, wormwood, murraya paniculata and mint leaves in a shade;
s23, sequentially putting the dried rose, the dried wormwood, the dried murraya paniculata, the dried mozzie buster and the dried mint leaves into crushing equipment, adjusting the rotating speed of the crushing equipment to 150r/min, continuously grinding for 5min, and taking out the crushed materials after full crushing to obtain raw material powder;
s24, putting the raw material powder prepared in the step S23 and deionized water into a reaction kettle according to the weight ratio of 2:10 for fully mixing and reacting, controlling the temperature of the reaction kettle at 50 ℃, and moving the reaction kettle into a vacuum distillation kettle after fully reacting to obtain a distillate, namely an extracting solution.
In this embodiment, the diameter of the polyester fiber in the warp yarn is 16-21 μm, the diameter of the cuprammonium fiber is 28-32 μm, the diameter of the aloe fiber in the weft yarn is 2.5-3.6 μm, the diameter of the modal fiber is 4-7 μm, and the diameter of the cotton fiber is 15-16 μm.
In this embodiment, before S11, the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber, and the cotton fiber are soaked in deionized water added with sodium hydroxide, and then stirred for 1 hour by using a stirring device, a penetrant is added while stirring, the mixture is kept at 55 ℃ for reacting for 1 hour, and after the reaction is complete, the mixture is repeatedly washed for 4 times by using deionized water, and finally dried.
In this embodiment, the mass of the deionized water is 10 times of the total mass of the cuprammonium fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber, the mass of the sodium hydroxide is 1% of the total mass of the cuprammonium fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber, and the mass of the penetrating agent is 0.1% of the total mass of the cuprammonium fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber.
Example 2
The antistatic textile composite fabric comprises a fabric base layer and an antistatic layer, wherein the fabric base layer is formed by weaving warps and wefts, the warps are formed by blending cuprammonium fibers and polyester fibers, and the wefts are formed by blending aloe fibers, modal fibers and cotton fibers; the antistatic layer is prepared from the following raw materials in percentage by weight: 42 parts of methyl acrylate; 6 parts of polytetrafluoroethylene; 2 parts of a surfactant; 12 parts of polyvinyl alcohol; 6 parts of nano silver; 12 parts of polyethylene glycol.
In the embodiment, the diameters of the nano titanium dioxide, the nano zinc oxide and the nano silicon-based oxide are 2-10 nm.
The preparation process of the antistatic textile composite fabric and the preparation process thereof comprises the following steps:
s11, antibacterial treatment: sequentially putting the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber into a soaking device, injecting a mixed solution added with a mite preventing agent and an antibacterial agent and an extracting solution into the soaking device to enable the mixed solution to completely submerge the copper ammonia fiber, the polyester fiber, the antibacterial fiber, the modal fiber and the cotton fiber, heating the soaking device by using heating equipment, controlling the heating temperature to be 50 ℃, preserving heat and soaking for 6 hours, respectively taking out the fibers after soaking, and drying by using drying equipment;
wherein the mass ratio of the anti-mite agent to the antibacterial agent in the mixed liquid medicine is 1: 1.5; the content of the anti-mite agent and the antibacterial agent in the mixed solution is not less than 5%.
S12 spinning: blending the dried copper ammonia fiber and the dried polyester fiber into warp yarn, and then blending the dried aloe fiber, the dried modal fiber and the dried cotton fiber into weft yarn;
s13, weaving: weaving the warp yarns and the weft yarns prepared in the step S12 into grey cloth by using an air jet type weaving machine, and then trimming and rolling the grey cloth;
s14, treating the gray cloth: conveying the gray cloth prepared in the step S13 to a cleaning pool, washing at high temperature, drying after washing, putting the gray cloth into a dip dyeing pool for dyeing after fully drying, and drying and shaping after dyeing to obtain a fabric base layer;
s15, taking 42 parts of methyl acrylate in parts by weight; 6 parts of polytetrafluoroethylene; 2 parts of a surfactant; 12 parts of polyvinyl alcohol; 6 parts of nano silver; 12 parts of polyethylene glycol to prepare an antistatic coating, and then directly coating the antistatic coating on the surface of the fabric substrate and drying; the drying condition is 125 deg.C, 1.6min, and the setting condition is 190 deg.C baking for 1.7 min.
In this example, the preparation method of the extract liquid in S11 is as follows:
s21, selecting fresh roses, wormwood, murraya paniculata, mozzie buster and mint leaves without diseases and insect pests, and cleaning the roses, the wormwood, the murraya paniculata, the mint leaves by using cleaning equipment;
s22, sequentially putting the cleaned rose, wormwood, murraya paniculata, mozzie buster and mint leaves into drying equipment for drying, controlling the temperature of the drying equipment to be 95 ℃, taking out the dried rose, wormwood, murraya paniculata and mint leaves, and putting the dried rose, wormwood, murraya paniculata and mint leaves in a shade;
s23, sequentially putting the dried rose, the dried wormwood, the dried murraya paniculata, the dried mozzie buster and the dried mint leaves into crushing equipment, adjusting the rotating speed of the crushing equipment to 150r/min, continuously grinding for 5min, and taking out the crushed materials after full crushing to obtain raw material powder;
s24, putting the raw material powder prepared in the step S23 and deionized water into a reaction kettle according to the weight ratio of 2:10 for fully mixing and reacting, controlling the temperature of the reaction kettle at 60 ℃, and moving the reaction kettle into a vacuum distillation kettle after fully reacting to obtain a distillate, namely an extracting solution.
In this embodiment, the diameter of the polyester fiber in the warp yarn is 16-21 μm, the diameter of the cuprammonium fiber is 28-32 μm, the diameter of the aloe fiber in the weft yarn is 2.5-3.6 μm, the diameter of the modal fiber is 4-7 μm, and the diameter of the cotton fiber is 15-16 μm.
In this embodiment, before S11, the cuprammonium fibers, the polyester fibers, the aloe fibers, the modal fibers, and the cotton fibers are soaked in deionized water added with sodium hydroxide, and then stirred with a stirring device for 1.2 hours, while stirring, a penetrant is added, the mixture is reacted for 1 hour at 55 ℃, and after the reaction is completed, the mixture is repeatedly washed with deionized water for 6 times, and finally dried.
In this embodiment, the mass of the deionized water is 12 times of the total mass of the cuprammonium fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber, the mass of the sodium hydroxide is 3% of the total mass of the cuprammonium fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber, and the mass of the penetrating agent is 0.2% of the total mass of the cuprammonium fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber.
Example 3
The antistatic textile composite fabric comprises a fabric base layer and an antistatic layer, wherein the fabric base layer is formed by weaving warps and wefts, the warps are formed by blending cuprammonium fibers and polyester fibers, and the wefts are formed by blending aloe fibers, modal fibers and cotton fibers; the antistatic layer is prepared from the following raw materials in percentage by weight: 43 parts of methyl acrylate; 7 parts of polytetrafluoroethylene; 2 parts of a surfactant; 13 parts of polyvinyl alcohol; 7 parts of nano silver; 15 parts of polyethylene glycol.
In the embodiment, the diameters of the nano titanium dioxide, the nano zinc oxide and the nano silicon-based oxide are 2-10 nm.
The preparation process of the antistatic textile composite fabric and the preparation process thereof comprises the following steps:
s11, antibacterial treatment: sequentially putting the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber into a soaking device, injecting a mixed solution added with a mite-proofing agent and an antibacterial agent and an extracting solution into the soaking device to enable the mixed solution to completely submerge the copper ammonia fiber, the polyester fiber, the antibacterial fiber, the modal fiber and the cotton fiber, heating the soaking device by using heating equipment, controlling the heating temperature to be 60 ℃, preserving heat and soaking for 7 hours, respectively taking out the fibers after soaking, and drying by using drying equipment;
wherein the mass ratio of the anti-mite agent to the antibacterial agent in the mixed liquid medicine is 1: 1.5; the content of the anti-mite agent and the antibacterial agent in the mixed solution is not less than 5%.
S12 spinning: blending the dried copper ammonia fiber and the dried polyester fiber into warp yarn, and then blending the dried aloe fiber, the dried modal fiber and the dried cotton fiber into weft yarn;
s13, weaving: weaving the warp yarns and the weft yarns prepared in the step S12 into grey cloth by using an air jet type weaving machine, and then trimming and rolling the grey cloth;
s14, treating the gray cloth: conveying the gray cloth prepared in the step S13 to a cleaning pool, washing at high temperature, drying after washing, putting the gray cloth into a dip dyeing pool for dyeing after fully drying, and drying and shaping after dyeing to obtain a fabric base layer;
s15, taking 43 parts of methyl acrylate in parts by weight; 7 parts of polytetrafluoroethylene; 2 parts of a surfactant; 13 parts of polyvinyl alcohol; 7 parts of nano silver; 15 parts of polyethylene glycol to prepare an antistatic coating, and then directly coating the antistatic coating on the surface of the fabric base layer and drying; the drying condition is 130 deg.C, 1.7min, and the setting condition is 190 deg.C baking for 2.0 min.
In this example, the preparation method of the extract liquid in S11 is as follows:
s21, selecting fresh roses, wormwood, murraya paniculata, mozzie buster and mint leaves without diseases and insect pests, and cleaning the roses, the wormwood, the murraya paniculata, the mint leaves by using cleaning equipment;
s22, sequentially putting the cleaned rose, wormwood, murraya paniculata, mozzie buster and mint leaves into drying equipment for drying, controlling the temperature of the drying equipment to be 110 ℃, taking out the dried rose, wormwood, murraya paniculata and mint leaves, and putting the dried rose, wormwood, murraya paniculata and mint leaves in a shade;
s23, sequentially putting the dried rose, the dried wormwood, the dried murraya paniculata, the dried mozzie buster and the dried mint leaves into crushing equipment, adjusting the rotating speed of the crushing equipment to 150r/min, continuously grinding for 5min, and taking out the crushed materials after full crushing to obtain raw material powder;
s24, putting the raw material powder prepared in the step S23 and deionized water into a reaction kettle according to the weight ratio of 2:10 for fully mixing and reacting, controlling the temperature of the reaction kettle at 75 ℃, and moving the reaction kettle into a vacuum distillation kettle after fully reacting to obtain a distillate, namely an extracting solution.
In this embodiment, the diameter of the polyester fiber in the warp yarn is 16-21 μm, the diameter of the cuprammonium fiber is 28-32 μm, the diameter of the aloe fiber in the weft yarn is 2.5-3.6 μm, the diameter of the modal fiber is 4-7 μm, and the diameter of the cotton fiber is 15-16 μm.
In this embodiment, before S11, the cuprammonium fibers, the polyester fibers, the aloe fibers, the modal fibers, and the cotton fibers are soaked in deionized water added with sodium hydroxide, and then stirred with a stirring device for 1.3 hours, while stirring, a penetrant is added, the mixture is reacted for 1 hour at 55 ℃, and after the reaction is completed, the mixture is repeatedly washed with deionized water for 7 times, and finally dried.
In this embodiment, the mass of the deionized water is 14 times of the total mass of the cuprammonium fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber, the mass of the sodium hydroxide is 4% of the total mass of the cuprammonium fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber, and the mass of the penetrating agent is 0.3% of the total mass of the cuprammonium fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber.
Example 4
The antistatic textile composite fabric comprises a fabric base layer and an antistatic layer, wherein the fabric base layer is formed by weaving warps and wefts, the warps are formed by blending cuprammonium fibers and polyester fibers, and the wefts are formed by blending aloe fibers, modal fibers and cotton fibers; the antistatic layer is prepared from the following raw materials in percentage by weight: 50 parts of methyl acrylate; 8 parts of polytetrafluoroethylene; 3 parts of a surfactant; 15 parts of polyvinyl alcohol; 10 parts of nano silver; 20 parts of polyethylene glycol.
In the embodiment, the diameters of the nano titanium dioxide, the nano zinc oxide and the nano silicon-based oxide are 2-10 nm.
The preparation process of the antistatic textile composite fabric and the preparation process thereof comprises the following steps:
s11, antibacterial treatment: sequentially putting the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber into a soaking device, injecting a mixed solution added with a mite-proofing agent and an antibacterial agent and an extracting solution into the soaking device to enable the mixed solution to completely submerge the copper ammonia fiber, the polyester fiber, the antibacterial fiber, the modal fiber and the cotton fiber, heating the soaking device by using heating equipment, controlling the heating temperature to be 65 ℃, preserving heat and soaking for 8 hours, respectively taking out the fibers after soaking, and drying by using drying equipment;
wherein the mass ratio of the anti-mite agent to the antibacterial agent in the mixed liquid medicine is 1: 1.5; the content of the anti-mite agent and the antibacterial agent in the mixed solution is not less than 5%.
S12 spinning: blending the dried copper ammonia fiber and the dried polyester fiber into warp yarn, and then blending the dried aloe fiber, the dried modal fiber and the dried cotton fiber into weft yarn;
s13, weaving: weaving the warp yarns and the weft yarns prepared in the step S12 into grey cloth by using an air jet type weaving machine, and then trimming and rolling the grey cloth;
s14, treating the gray cloth: conveying the gray cloth prepared in the step S13 to a cleaning pool, washing at high temperature, drying after washing, putting the gray cloth into a dip dyeing pool for dyeing after fully drying, and drying and shaping after dyeing to obtain a fabric base layer;
s15, taking 50 parts of methyl acrylate in parts by weight; 8 parts of polytetrafluoroethylene; 3 parts of a surfactant; 15 parts of polyvinyl alcohol; 10 parts of nano silver; 20 parts of polyethylene glycol to prepare an antistatic coating, and then directly coating the antistatic coating on the surface of the fabric base layer and drying; the drying condition is 140 deg.C for 2min, and the setting condition is 200 deg.C for 2.1 min.
In this example, the preparation method of the extract liquid in S11 is as follows:
s21, selecting fresh roses, wormwood, murraya paniculata, mozzie buster and mint leaves without diseases and insect pests, and cleaning the roses, the wormwood, the murraya paniculata, the mint leaves by using cleaning equipment;
s22, sequentially putting the cleaned rose, wormwood, murraya paniculata, mozzie buster and mint leaves into drying equipment for drying, controlling the temperature of the drying equipment to be 140 ℃, taking out the dried rose, wormwood, murraya paniculata and mint leaves, and putting the dried rose, wormwood, murraya paniculata and mint leaves in a shade;
s23, sequentially putting the roses, the wormwood, the murraya paniculata, the mozzie buster and the mint leaves which are dried in the step S22 into a crushing device, adjusting the rotating speed of the crushing device to be 150r/min, continuously grinding for 5min, and taking out the crushed materials to obtain raw material powder;
s24, putting the raw material powder prepared in the step S23 and deionized water into a reaction kettle according to the weight ratio of 2:10 for fully mixing and reacting, controlling the temperature of the reaction kettle at 95 ℃, and moving the reaction kettle into a vacuum distillation kettle after fully reacting to obtain a distillate, namely an extracting solution.
In this embodiment, the diameter of the polyester fiber in the warp yarn is 16-21 μm, the diameter of the cuprammonium fiber is 28-32 μm, the diameter of the aloe fiber in the weft yarn is 2.5-3.6 μm, the diameter of the modal fiber is 4-7 μm, and the diameter of the cotton fiber is 15-16 μm.
In this embodiment, before S11, the cuprammonium fibers, the polyester fibers, the aloe fibers, the modal fibers, and the cotton fibers are soaked in deionized water added with sodium hydroxide, and then stirred with a stirring device for 1.5 hours, while stirring, a penetrant is added, the mixture is reacted for 1 hour at 55 ℃, and after the reaction is completed, the mixture is repeatedly washed with deionized water for 8 times, and finally dried.
In this embodiment, the mass of the deionized water is 15 times of the total mass of the cuprammonium fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber, the mass of the sodium hydroxide is 5% of the total mass of the cuprammonium fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber, and the mass of the penetrating agent is 0.4% of the total mass of the cuprammonium fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber.
Although the present invention has been described with reference to a preferred embodiment, it should be understood that various changes, substitutions and alterations can be made herein without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (10)
1. An antistatic textile composite fabric and a preparation process thereof are characterized in that: the fabric comprises a fabric base layer and an antistatic layer, wherein the fabric base layer is formed by weaving warps and wefts, the warps are formed by blending cuprammonium fibers and polyester fibers, and the wefts are formed by blending aloe fibers, modal fibers and cotton fibers; the antistatic layer is prepared from the following raw materials in parts by weight: 40-50 parts of methyl acrylate; 5-8 parts of polytetrafluoroethylene; 1-3 parts of a surfactant; 10-15 parts of polyvinyl alcohol; 5-10 parts of nano silver; 10-20 parts of polyethylene glycol.
2. The antistatic textile composite fabric and the preparation process thereof according to claim 1, wherein the preparation process comprises the following steps: the method comprises the following steps:
s11, antibacterial treatment: sequentially putting the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber into soaking equipment, injecting a mixed solution added with a mite preventing agent and an antibacterial agent and an extracting solution into the soaking equipment to ensure that the mixed solution completely submerges the copper ammonia fiber, the polyester fiber, the antibacterial fiber, the modal fiber and the cotton fiber, respectively taking out the fibers after soaking, and drying the fibers by using drying equipment;
s12 spinning: blending the dried copper ammonia fiber and the dried polyester fiber into warp yarn, and then blending the dried aloe fiber, the dried modal fiber and the dried cotton fiber into weft yarn;
s13, weaving: weaving the warp yarns and the weft yarns prepared in the step S12 into grey cloth by using an air jet type weaving machine, and then trimming and rolling the grey cloth;
s14, treating the gray cloth: conveying the gray cloth prepared in the step S13 to a cleaning pool, washing at high temperature, drying after washing, putting the gray cloth into a dip dyeing pool for dyeing after fully drying, and drying and shaping after dyeing to obtain a fabric base layer;
s15, taking 40-50 parts of methyl acrylate in parts by weight; 5-8 parts of polytetrafluoroethylene; 1-3 parts of a surfactant; 10-15 parts of polyvinyl alcohol; 5-10 parts of nano silver; 10-20 parts of polyethylene glycol to prepare an antistatic coating, and then directly coating the antistatic coating on the surface of the fabric substrate, and drying.
3. The antistatic textile composite fabric and the preparation process thereof according to claim 2, wherein the preparation process comprises the following steps: and in the step S11, heating the soaking equipment by using heating equipment, controlling the heating temperature to be 45-65 ℃, and soaking for 5-8h under heat preservation.
4. The antistatic textile composite fabric and the preparation process thereof according to claim 2, wherein the preparation process comprises the following steps: the preparation method of the extracting solution in the S11 comprises the following steps:
s21, selecting fresh roses, wormwood, murraya paniculata, mozzie buster and mint leaves without diseases and insect pests, and cleaning the roses, the wormwood, the murraya paniculata, the mint leaves by using cleaning equipment;
s22, sequentially putting the cleaned rose, wormwood, murraya paniculata, mozzie buster and mint leaves into drying equipment for drying, controlling the temperature of the drying equipment to be 85-140 ℃, taking out the dried rose, wormwood, murraya paniculata and mint leaves, and placing the dried rose, mugwort, murraya paniculata, mozzie buster and mint leaves in a shade place;
s23, sequentially putting the dried rose, the dried wormwood, the dried murraya paniculata, the dried mozzie buster and the dried mint leaves into crushing equipment, adjusting the rotating speed of the crushing equipment to 150r/min, continuously grinding for 5min, and taking out the crushed materials after full crushing to obtain raw material powder;
s24, putting the raw material powder prepared in the step S23 and deionized water into a reaction kettle according to the weight ratio of 2:10 for fully mixing and reacting, controlling the temperature of the reaction kettle to be 50-95 ℃, and moving the reaction kettle into a vacuum distillation kettle after fully reacting to obtain distillate, namely the extracting solution.
5. The antistatic textile composite fabric and the preparation process thereof according to claim 2, wherein the preparation process comprises the following steps: the mass ratio of the anti-mite agent to the antibacterial agent in the mixed liquid medicine is 1: 1.5.
6. the antistatic textile composite fabric and the preparation process thereof according to claim 2, wherein the preparation process comprises the following steps: the content of the mite-proofing agent and the antibacterial agent in the mixed solution of S11 is not less than 5%.
7. The antistatic textile composite fabric and the preparation process thereof according to claim 2, wherein the preparation process comprises the following steps: the diameter of the polyester fiber in the warp yarn is 16-21 mu m, the diameter of the cuprammonium rayon fiber is 28-32 mu m, the diameter of the aloe fiber in the weft yarn is 2.5-3.6 mu m, the diameter of the modal fiber is 4-7 mu m, and the diameter of the cotton fiber is 15-16 mu m.
8. The antistatic textile composite fabric and the preparation process thereof according to claim 2, wherein the preparation process comprises the following steps: before S11, soaking the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber in deionized water added with sodium hydroxide, stirring for 1-1.5 h by using stirring equipment, adding a penetrant while stirring, keeping the temperature at 55 ℃ for reaction for 1h, repeatedly washing for 4-8 times by using deionized water after the reaction is fully performed, and finally drying.
9. The antistatic textile composite fabric and the preparation process thereof according to claim 8, wherein the preparation process comprises the following steps: the deionized water is 10-15 times of the total mass of the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber, the sodium hydroxide is 1-5% of the total mass of the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber, and the penetrating agent is 0.1-0.4% of the total mass of the copper ammonia fiber, the polyester fiber, the aloe fiber, the modal fiber and the cotton fiber.
10. The antistatic textile composite fabric and the preparation process thereof according to claim 2, wherein the preparation process comprises the following steps: the drying condition in S15 is 120-140 ℃ for 1.5-2 min, and the setting condition is 180-200 ℃ for 1.6-2.1 min.
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