CN114601004A - DHA algae oil pressure tablet candy capable of reducing oxidation and preparation method thereof - Google Patents
DHA algae oil pressure tablet candy capable of reducing oxidation and preparation method thereof Download PDFInfo
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- CN114601004A CN114601004A CN202210299811.0A CN202210299811A CN114601004A CN 114601004 A CN114601004 A CN 114601004A CN 202210299811 A CN202210299811 A CN 202210299811A CN 114601004 A CN114601004 A CN 114601004A
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- 238000004806 packaging method and process Methods 0.000 claims description 4
- GUBGYTABKSRVRQ-XLOQQCSPSA-N Alpha-Lactose Chemical compound O[C@@H]1[C@@H](O)[C@@H](O)[C@@H](CO)O[C@H]1O[C@@H]1[C@@H](CO)O[C@H](O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-XLOQQCSPSA-N 0.000 claims description 3
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- 239000011786 L-ascorbyl-6-palmitate Substances 0.000 claims description 3
- GUBGYTABKSRVRQ-QKKXKWKRSA-N Lactose Natural products OC[C@H]1O[C@@H](O[C@H]2[C@H](O)[C@@H](O)C(O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@H]1O GUBGYTABKSRVRQ-QKKXKWKRSA-N 0.000 claims description 3
- 229930003427 Vitamin E Natural products 0.000 claims description 3
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- 229960005055 sodium ascorbate Drugs 0.000 claims description 3
- 239000001509 sodium citrate Substances 0.000 claims description 3
- NLJMYIDDQXHKNR-UHFFFAOYSA-K sodium citrate Chemical compound O.O.[Na+].[Na+].[Na+].[O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O NLJMYIDDQXHKNR-UHFFFAOYSA-K 0.000 claims description 3
- PPASLZSBLFJQEF-RXSVEWSESA-M sodium-L-ascorbate Chemical compound [Na+].OC[C@H](O)[C@H]1OC(=O)C(O)=C1[O-] PPASLZSBLFJQEF-RXSVEWSESA-M 0.000 claims description 3
- 238000012546 transfer Methods 0.000 claims description 3
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims description 3
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- SBJKKFFYIZUCET-JLAZNSOCSA-N Dehydro-L-ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(=O)C1=O SBJKKFFYIZUCET-JLAZNSOCSA-N 0.000 claims 1
- 235000013305 food Nutrition 0.000 abstract description 5
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- 235000020669 docosahexaenoic acid Nutrition 0.000 description 50
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- 239000003826 tablet Substances 0.000 description 13
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- DVSZKTAMJJTWFG-SKCDLICFSA-N (2e,4e,6e,8e,10e,12e)-docosa-2,4,6,8,10,12-hexaenoic acid Chemical compound CCCCCCCCC\C=C\C=C\C=C\C=C\C=C\C=C\C(O)=O DVSZKTAMJJTWFG-SKCDLICFSA-N 0.000 description 1
- GZJLLYHBALOKEX-UHFFFAOYSA-N 6-Ketone, O18-Me-Ussuriedine Natural products CC=CCC=CCC=CCC=CCC=CCC=CCCCC(O)=O GZJLLYHBALOKEX-UHFFFAOYSA-N 0.000 description 1
- 108010010803 Gelatin Proteins 0.000 description 1
- 241000598397 Schizochytrium sp. Species 0.000 description 1
- 230000001133 acceleration Effects 0.000 description 1
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- 239000007891 compressed tablet Substances 0.000 description 1
- KAUVQQXNCKESLC-UHFFFAOYSA-N docosahexaenoic acid (DHA) Natural products COC(=O)C(C)NOCC1=CC=CC=C1 KAUVQQXNCKESLC-UHFFFAOYSA-N 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
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- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
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- 235000020777 polyunsaturated fatty acids Nutrition 0.000 description 1
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- 150000004670 unsaturated fatty acids Chemical class 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/40—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds characterised by the fats used
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/42—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds characterised by the carbohydrates used, e.g. polysaccharides
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23G—COCOA; COCOA PRODUCTS, e.g. CHOCOLATE; SUBSTITUTES FOR COCOA OR COCOA PRODUCTS; CONFECTIONERY; CHEWING GUM; ICE-CREAM; PREPARATION THEREOF
- A23G3/00—Sweetmeats; Confectionery; Marzipan; Coated or filled products
- A23G3/34—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof
- A23G3/36—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds
- A23G3/48—Sweetmeats, confectionery or marzipan; Processes for the preparation thereof characterised by the composition containing organic or inorganic compounds containing plants or parts thereof, e.g. fruits, seeds, extracts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
- B01J13/02—Making microcapsules or microballoons
- B01J13/04—Making microcapsules or microballoons by physical processes, e.g. drying, spraying
- B01J13/043—Drying and spraying
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Organic Chemistry (AREA)
- Botany (AREA)
- Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Preparation (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention relates to the field of foods, in particular to DHA algae oil pressure candy tablets capable of reducing oxidation and a preparation method thereof, wherein the DHA algae oil pressure candy tablets are prepared from the following components in parts by mass: 50-800 parts of DHA algae oil powder, 0-800 parts of white granulated sugar, 100-800 parts of isomaltulose, 100-800 parts of fruit powder, 1-10 parts of sodium carboxymethylcellulose, 0-200 parts of sorbitol, 0-100 parts of magnesium stearate and 0-100 parts of microcrystalline cellulose. The candy disclosed by the invention has the advantages of convenience in carrying, better mouthfeel, reduction in oxidation and the like.
Description
Technical Field
The invention relates to the field of foods, in particular to DHA algae oil pressure tablet candies capable of reducing oxidation and a preparation method thereof.
Background
DHA: docosahexaenoic acid (DHA), commonly known as NAOHUANGJIN, is a major polyunsaturated fatty acid in human organs and tissues such as brain and retina, and DHA algae oil is prepared from marine microalgae by fermenting, separating, and purifying with Schizochytrium sp. The DHA grease is treated by the microcapsule technology and then is sprayed by the dry process to prepare powder, so that the storage stability is improved, and the bad smell of the grease is reduced.
The tablet is one of dry-process forming of candy or tablet, and can be prepared by tabletting one or more substances by special tabletting equipment. Gel candy (soft capsule): is a capsule product prepared by processing and sealing liquid raw materials or liquid solid raw materials in a soft capsule material. The soft capsule wall material is prepared from gelatin, glycerol or other suitable adjuvants alone or in combination.
The major products of DHA on the market are now in the form of gel candies (or soft capsules), and the main disadvantages of these products are: 1. the food is inconvenient to eat, and consumers need to open capsule shells and suck contents when eating the food, and the food is especially inconvenient for children; 2. the algae oil DHA has unpleasant smell such as fishy smell, and is a greasy product when being eaten, so the algae oil DHA tastes greasy and has unpleasant smell; 3. is easy to oxidize, and as the DHA in the algae oil belongs to unsaturated fatty acid, the DHA is easy to oxidize. The gel candy (or soft capsule) product is easy to be oxidized in shelf life. Therefore, it is urgently needed to provide a product which is convenient to carry and has better taste.
Disclosure of Invention
In order to solve the technical problems, the invention provides the DHA algae oil tabletting candy capable of reducing oxidation, which has the advantages of convenience in carrying, good taste, reduction of oxidation and the like.
The technical scheme provided by the invention is as follows:
the DHA algae oil tablet candy capable of reducing oxidation is prepared from the following components in parts by mass: 50-800 parts of DHA algae oil powder (20% of Anhui Kjeldahl DHA algae oil microcrystalline embedding powder), 0-800 parts of white granulated sugar, 100-800 parts of isomaltulose, 100-800 parts of fruit powder, 1-10 parts of sodium carboxymethylcellulose, 0-200 parts of sorbitol, 0-100 parts of magnesium stearate and 0-100 parts of microcrystalline cellulose.
The DHA algae oil powder is DHA algae oil microcrystal embedding powder, wherein the mass ratio of DHA (docosahexaenoic acid) in the total powder is 20%, and the DHA algae oil powder also comprises whey protein powder (whey protein concentrate, whey protein isolate), lactose, sodium citrate, sodium ascorbate, DHA essential oil, mono-diglycerol fatty acid ester, phospholipid, ascorbyl palmitate, vitamin E and tricalcium phosphate.
The invention also provides a preparation method of the DHA algae oil tabletting candies capable of reducing oxidation, which comprises the steps of mechanically pulverizing and sieving granular raw materials, transferring the granular raw materials into a raw material transfer bag, weighing the raw materials according to the formula amount, putting the raw materials into a mixer in sequence, fully mixing to obtain a semi-finished product, sampling and detecting the semi-finished product, putting the semi-finished product into a feed hopper after the semi-finished product meets the standard, tabletting, and packaging to obtain the DHA algae oil tabletting candies capable of reducing oxidation.
Further, the finished product is prepared into granules which can be used for tabletting.
Further, the raw materials were put into a blender in order and mixed thoroughly for 20 minutes.
Further, the semi-finished product detection indexes comprise moisture and microorganisms.
Further, the granular raw materials are mechanically pulverized and then sieved by a 80-mesh sieve.
Further, the preparation method of the DHA algae oil powder comprises the following steps: the raw materials comprise a packaging material, an antioxidant, a pH value regulator, primary water, DHA algae oil and an emulsifier, the raw materials of an oil phase and a water phase are independently blended and dissolved, the raw materials are pasteurized, mixed and sheared at a high speed, then homogenized, the homogenized emulsion is spray-dried to obtain microcapsule powder, and an anticaking agent is added and premixed to obtain algae oil powder.
Furthermore, the mass ratio of the DHA in the DHA algae oil powder in the total powder is 20%,
furthermore, the DHA algae oil powder also comprises whey protein powder, lactose, sodium citrate, sodium ascorbate, DHA essential oil, mono-diglycerol fatty acid ester, phospholipid, ascorbyl palmitate, vitamin E and tricalcium phosphate.
Further, the whey protein powder comprises whey protein concentrate and whey protein isolate.
Advantageous effects
The tablet (candy or tablet) can be directly chewed and taken, and is very convenient to eat; the DHA algae oil is made into powder by a microcapsule technology, so that the DHA algae oil has no greasy and greasy feeling and greatly reduces the bad smell; the sugar and the fruit powder are added in the tabletting process, so that the taste is sour, sweet and delicious, and the fruit taste is rich. DHA algae oil is prevented from contacting with air by a microcapsule technology, and the oxidation probability is reduced; the coating is coated on the outer layer after tabletting, so that the contact of the contents and air is effectively prevented, the double protection is realized, and the oxidation is avoided. Meanwhile, the tablet (candy or tablet) of the invention can adopt different packaging forms and is convenient to carry.
The application of the DHA algae oil in tabletting (candy and tablet) is not precedent at present, and the technical scheme of the invention realizes that the DHA algae oil can be directly chewed for eating, improves the unpleasant feeling of consumers in the original eating process, and enables the eaters to achieve the effect of both health and delicious taste.
Drawings
FIG. 1 shows the comparative results of the accelerated test of DHA grease and DHA powder;
figure 2 shows the process steps of the microencapsulation technique.
Detailed Description
Example 1
A DHA algae oil tablet candy capable of reducing oxidation has the following formula:
the preparation method of the DHA algal oil tablet candy capable of reducing oxidation comprises the following steps:
process flow
Raw material acceptance → powdering → sieving → mixing → inspection → granulation (optional) → tabletting → external packing
(II) concrete step
1. Raw material entry inspection: the quality standard of the corresponding raw materials is met;
2. powdering: mechanically powdering granular raw materials
3. Sieving: all the raw materials are respectively transferred into a raw material transfer bag after being respectively sieved by a 80-mesh vibrating screen;
4. weighing and matching: accurately weighing the raw materials in the formula amount;
5. premixing raw materials: the raw materials are sequentially put into a mixing barrel and stirred and mixed for 20 minutes;
6. mixing: the mixing machine is debugged to enter a preset working state, and the raw materials are fully mixed for 30 minutes to ensure that the raw materials are uniformly mixed;
7. sampling and detecting a semi-finished product: sampling the semi-finished product, and reserving a sample to detect moisture, microorganisms and the like:
8. and (3) granulation: making the mixed powder raw materials into granules which can be used for tabletting; (optional in this step)
9. Tabletting: debugging a tablet press, after the machine is preheated and stabilized, putting the mixed powder obtained in the step 6 (or 8) into a feed hopper, and tabletting;
10. and (4) inspecting a finished product: randomly extracting a sample, and inspecting to meet the finished product quality standard of the product;
11. outsourcing: and (5) packaging the finished products and warehousing the finished products.
The preparation method (microcapsule technology) of the DHA algae oil powder comprises the following steps: the raw materials comprise a packaging material, an antioxidant, a pH value regulator, primary water, DHA algae oil and an emulsifier, the raw materials of a water phase (the packaging material, the antioxidant, the pH value regulator and the primary water) and an oil phase (the DHA algae oil and the emulsifier) are independently mixed and dissolved, the raw materials are pasteurized, mixed and sheared at a high speed, homogenized, the emulsion after homogenization is spray-dried to obtain microcapsule powder, and an anticaking agent is added and premixed to obtain a finished product.
Example 2
The DHA algae oil and the DHA microcrystal embedding powder are respectively adopted for carrying out an acceleration test, and the results are as follows:
comparison of DHA algal oil with DHA microcrystalline embedding powder in accelerated test (results are shown in FIG. 1)
Note: the accelerated test conditions of the protein formula and the starch formula powder are 65 ℃ open; the DHA algal oil is subjected to accelerated test conditions by filling 62 ℃ with nitrogen.
The results show that: the antioxidant effect of the DHA microcrystalline embedded powder is far higher than that of DHA algae oil.
Example 3
The product performances of the microcrystalline embedding technology and the product without the microcrystalline embedding technology are mutually compared
Note: the method does not adopt a microcrystalline embedding technology, namely adding starch into DHA algae oil and directly spraying powder
The odor and mouthfeel of the product were compared, and the final sensory evaluation was scored by 20 sensory evaluation panelists, referring to the data standards of the following several tables.
Sensory analysis strength scoring scale table
Scale for scoring like degree of sensory analysis
The results of the intensity and preference of the sensory analysis indicate that: the compressed tablet candy prepared by adding the DHA microcrystalline embedding powder has better feeling after eating and is more popular.
Claims (10)
1. The DHA algae oil tabletting candy capable of reducing oxidation is characterized by being prepared from the following components in parts by mass: 50-800 parts of DHA algae oil powder, 0-800 parts of white granulated sugar, 100-800 parts of isomaltulose, 100-800 parts of fruit powder, 1-10 parts of sodium carboxymethylcellulose, 0-200 parts of sorbitol, 0-100 parts of magnesium stearate and 0-100 parts of microcrystalline cellulose.
2. The preparation method of the DHA algae oil tablet candy capable of reducing oxidation according to claim 1, wherein the granular raw materials are mechanically pulverized and sieved, and then transferred into a raw material transfer bag, the raw materials with the formula amount are weighed, and the raw materials are sequentially put into a mixer to be fully mixed to obtain a semi-finished product, the semi-finished product is sampled and detected, and after the semi-finished product meets the standard, the semi-finished product is put into a feed hopper to be tabletted, and the DHA algae oil tablet candy capable of reducing oxidation is obtained after packaging.
3. The method for preparing tablets and candies containing DHA and algal oil capable of reducing oxidation according to claim 2, wherein the finished product is made into granules for tabletting.
4. The method for preparing tablets and candies containing DHA and algal oil capable of reducing oxidation according to claim 2, wherein the raw materials are sequentially put into a blender and fully mixed for 20 minutes.
5. The method for preparing a DHA algal oil tablet candy capable of reducing oxidation according to claim 2, wherein the semi-finished product detection indexes include moisture and microorganism.
6. The method for preparing DHA algal oil tablet candy capable of reducing oxidation according to claim 2, wherein the granular raw material is mechanically pulverized and then sieved with 80 mesh sieve.
7. The preparation method of the DHA algal oil tablet candy capable of reducing oxidation according to claim 2, wherein the preparation method of the DHA algal oil powder is as follows: the raw materials comprise a packaging material, an antioxidant, a pH value regulator, primary water, DHA algae oil and an emulsifier, the raw materials of an oil phase and a water phase are independently blended and dissolved, the raw materials are pasteurized, mixed and sheared at a high speed, then homogenized, the homogenized emulsion is spray-dried to obtain microcapsule powder, and an anticaking agent is added and premixed to obtain algae oil powder.
8. The method for preparing DHA algal oil tablet candy capable of reducing oxidation according to claim 2, wherein the DHA algal oil powder has a DHA content of 20% by mass in the total powder.
9. The method for preparing DHA algal oil tablet candy capable of reducing oxidation according to claim 2, wherein the DHA algal oil powder further comprises whey protein powder, lactose, sodium citrate, sodium ascorbate, DHA essential oil, mono-and di-glyceride fatty acid ester, phospholipid, ascorbyl palmitate, vitamin E, and tricalcium phosphate.
10. The method for preparing a DHA algal oil tablet candy capable of reducing oxidation according to claim 2, wherein the whey protein powder comprises whey protein concentrate and whey protein isolate.
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105707894A (en) * | 2016-04-01 | 2016-06-29 | 广东润科生物工程有限公司 | Preparation method of high-temperature-resistant microalgae DHA (docosahexenoic acid) oil microcapsule powder |
| CN108541859A (en) * | 2018-02-12 | 2018-09-18 | 广州富诺健康科技股份有限公司 | A kind of DHA algal oil solid beverage |
| CN110074191A (en) * | 2019-06-11 | 2019-08-02 | 广东新乐食品有限公司 | A kind of nutrition chewing milk tablet and preparation method thereof for adding DHA algal oil microcapsule powder |
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Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105707894A (en) * | 2016-04-01 | 2016-06-29 | 广东润科生物工程有限公司 | Preparation method of high-temperature-resistant microalgae DHA (docosahexenoic acid) oil microcapsule powder |
| CN108541859A (en) * | 2018-02-12 | 2018-09-18 | 广州富诺健康科技股份有限公司 | A kind of DHA algal oil solid beverage |
| CN110074191A (en) * | 2019-06-11 | 2019-08-02 | 广东新乐食品有限公司 | A kind of nutrition chewing milk tablet and preparation method thereof for adding DHA algal oil microcapsule powder |
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