CN114588858A - Solid solution reaction vessel for processing rare earth element yttrium - Google Patents

Solid solution reaction vessel for processing rare earth element yttrium Download PDF

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Publication number
CN114588858A
CN114588858A CN202210165671.8A CN202210165671A CN114588858A CN 114588858 A CN114588858 A CN 114588858A CN 202210165671 A CN202210165671 A CN 202210165671A CN 114588858 A CN114588858 A CN 114588858A
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CN
China
Prior art keywords
solid solution
reaction vessel
fixedly connected
rare earth
earth element
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Pending
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CN202210165671.8A
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Chinese (zh)
Inventor
陈天晓
肖兆发
周细凌
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Ganzhou Ruike Alloy Material Co ltd
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Ganzhou Ruike Alloy Material Co ltd
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Priority to CN202210165671.8A priority Critical patent/CN114588858A/en
Publication of CN114588858A publication Critical patent/CN114588858A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006Controlling or regulating processes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053Details of the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/002Component parts of these vessels not mentioned in B01J3/004, B01J3/006, B01J3/02 - B01J3/08; Measures taken in conjunction with the process to be carried out, e.g. safety measures
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J3/00Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
    • B01J3/006Processes utilising sub-atmospheric pressure; Apparatus therefor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002Chemical plants
    • B01J2219/00018Construction aspects
    • B01J2219/00022Plants mounted on pallets or skids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00162Controlling or regulating processes controlling the pressure
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention provides a solid solution reaction vessel for processing rare earth element yttrium, and relates to the technical field of reaction vessels. The solid solution reaction vessel for processing rare earth element yttrium comprises a reactor shell, wherein a reactor cover is arranged at the top of the reactor shell, a power mechanism is arranged at the top end of a stirring rod, a plurality of piston cylinders are fixedly connected to the edge of the reactor cover, and piston heads are slidably connected to the inside of the piston cylinders. Make the adjustable ring go up and down through the pneumatic cylinder, and then make the regulation pole can go up and down, further make the piston head slide from top to bottom in the piston cylinder, the bottom of piston head rotates through the pivot and is connected with the connecting rod, utilizes the connecting rod to drive the bent axle and rotate at the inboard of reactor shell, can make disturbance pole and disturbance leaf rotate, can acutely stir solid solution, makes the intermolecular fully fuse, increases intermolecular collision and contact probability, makes the reaction more abundant, improves the quality of product.

Description

Solid solution reaction vessel for processing rare earth element yttrium
Technical Field
The invention relates to the technical field of reaction vessels, in particular to a solid solution reaction vessel for processing rare earth element yttrium.
Background
Yttrium is used in a wide range of industries as yttrium phosphor for producing red colors on television screens, as well as for filters for certain rays, superconductors and superalloys and specialty glasses. The yttrium is high temperature resistant and corrosion resistant, and can be used as a cladding material of nuclear fuel. Yttrium and various aminocarboxylic complexing agents can generate stable chelate; yttrium aluminum garnet containing neodymium is an excellent laser material, yttrium iron garnet is an excellent laser material, and yttrium iron garnet and yttrium aluminum garnet are novel magnetic materials.
In the processing process of the rare earth element yttrium, the solid solution reaction vessel has low mixing efficiency on two components, so that the components are not sufficiently dissolved, and the solid phase formed by the components is not uniform enough.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides a solid solution reaction vessel for processing rare earth element yttrium, which solves the problem of low mixing efficiency of the solid solution reaction vessel on components.
In order to achieve the purpose, the invention is realized by the following technical scheme: a solid solution reaction vessel for processing rare earth element yttrium comprises a reactor shell, wherein a reactor cover is arranged at the top of the reactor shell, a stirring rod is rotatably connected to the middle of the reactor cover, stirring blades are arranged on the outer side of the stirring rod, a power mechanism is arranged at the top end of the stirring rod, a plurality of piston cylinders are fixedly connected to the edge of the reactor cover, a piston head is slidably connected to the inside of each piston cylinder, a shaft pin is fixedly connected to the bottom of the piston head, a connecting rod is rotatably connected to the middle of the shaft pin, a crankshaft is rotatably connected to the bottom end of the connecting rod, one end of the crankshaft is rotatably connected to the inner side of the reactor shell, a disturbance blade is fixedly connected to the other end of the crankshaft, a regulation rod is arranged on the outer side of the disturbance blade, a regulation rod is fixedly connected to the top of the piston head, a regulation ring is arranged at the top end of the regulation rod, the upper surface fixed connection of adjustable ring has the pneumatic cylinder, the top fixed connection of pneumatic cylinder has the support frame.
Preferably, power unit includes fixed disk and motor, the top fixed connection of fixed disk is in the middle part of support frame, the bottom fixed connection of fixed disk is in the outside of motor, the output fixedly connected with output rod of motor, the bottom of output rod is connected in the top middle part of puddler.
Preferably, the bottom fixedly connected with inserted block of output lever, the top middle part of puddler is provided with the slot, the bottom of inserted block is connected in the slot, puddler and inserted block pass through fitting pin through connection.
Preferably, the number of the piston cylinders is three to six, the length of a connecting rod positioned at the bottom of the piston cylinder is sequentially increased, and the disturbance blades and the stirring blades are staggered.
Preferably, be provided with the adjustment tank in the middle part of adjustable ring, the adjustment tank is run through on the top of adjusting the pole, one side of adjustable ring is provided with the locking bolt, the outside through connection adjustable ring and the regulation pole of locking bolt.
Preferably, the two ends of the bottom of the support frame are fixedly connected with sliding blocks, and the bottoms of the sliding blocks are connected with tracks in a sliding mode.
Preferably, a manhole cover is arranged in one side of the reactor cover, and a connecting pipe is arranged in the other side of the reactor cover.
The working principle is as follows: the reaction vessel is convenient to clean and overhaul and maintain by utilizing a manhole cover, the reaction vessel is vacuumized by utilizing a connecting pipe to facilitate adding materials or introducing protective gas and the like, the vacuumized reaction vessel is sealed, a stirring rod is driven to rotate by a power mechanism to enable a stirring blade to stir and mix the rare earth element yttrium and the acid-base mixture, a hydraulic cylinder is utilized to enable an adjusting ring to lift, and further the adjusting rod can lift, a piston head further slides up and down in a piston cylinder, the bottom of the piston head is rotatably connected with a connecting rod through a shaft pin, a crankshaft is driven to rotate at the inner side of a reactor shell by the connecting rod, a disturbance rod and a disturbance blade can rotate, solid solution can be vigorously stirred, the molecules are fully fused, the collision and contact probability among the molecules is increased, the reaction is more sufficient, the quality of a product is improved, and the piston cylinders are distributed in a reactor cover, connecting rods with different heights are used for connecting the crankshafts, so that the crankshafts can be distributed at different heights of the reaction vessel, the stirring effect is further increased, disturbance blades are prevented from interfering the stirring blades, disturbing the solid solution at different heights to fully fuse the molecules, placing the insert blocks through the slots, penetrating the slots of the stirring rod and the insert blocks of the output rod by using the locking pins, can lock delivery pole and puddler, be convenient for utilize the motor drive puddler to rotate, place the regulation pole through the adjustment tank, recycle the locking bolt and insert the regulation pole from the adjustable ring, the locking bolt can be connected regulation ring and regulation pole, easy to assemble dismantlement, the convenience is maintained and is repaired reaction vessel, the convenience is maintained the repair to reaction vessel, the later stage operation of being convenient for, utilize the track to be convenient for remove pneumatic cylinder and fixed disk, be convenient for remove installation and dismantlement, time saving and labor saving.
The invention provides a solid solution reaction vessel for processing rare earth element yttrium. The method has the following beneficial effects:
1. according to the invention, the stirring rod is driven by the power mechanism to rotate, so that the stirring blade stirs and mixes the rare earth element yttrium and the acid-base mixture, the adjusting ring is lifted by the hydraulic cylinder, the adjusting rod can be lifted, the piston head can further slide up and down in the piston cylinder, the bottom of the piston head is rotatably connected with the connecting rod through the shaft pin, the crankshaft is driven by the connecting rod to rotate on the inner side of the reactor shell, the disturbance rod and the disturbance blade can rotate, the solid solution can be stirred vigorously, the molecules are fused fully, the collision and contact probability among the molecules is increased, the reaction is more sufficient, and the quality of the product is improved.
2. According to the invention, the insertion block is placed through the insertion slot, the locking pin penetrates through the insertion slot of the stirring rod and the insertion block of the output rod, the output rod and the stirring rod can be locked, the stirring rod can be conveniently driven to rotate by the motor, the adjusting rod is placed through the adjusting slot, the adjusting rod is inserted from the adjusting ring by the locking bolt, the adjusting ring and the adjusting rod can be connected by the locking bolt, the mounting and dismounting are convenient, the maintenance and repair of the reaction vessel are convenient, and the later operation is convenient.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is an enlarged view of FIG. 1 at A;
FIG. 3 is an enlarged view of FIG. 1 at B;
FIG. 4 is a front view of the present invention;
FIG. 5 is a schematic view of the interior of a reactor shell according to the present invention;
FIG. 6 is a schematic view of the piston cylinder and piston head of the present invention.
Wherein, 1, a track; 2. a slider; 3. a support frame; 4. a hydraulic cylinder; 5. fixing the disc; 6. a reactor shell; 7. an adjusting ring; 8. a manhole cover; 9. a reactor cover; 10. locking the bolt; 11. an adjustment groove; 12. a piston cylinder; 13. adjusting a rod; 14. a stirring rod; 15. inserting a block; 16. an output rod; 17. a locking pin; 18. a motor; 19. a slot; 20. stirring blades; 21. disturbing the movable blade; 22. a crankshaft; 23. a shaft pin; 24. a disturbance rod; 25. a piston head; 26. a connecting rod.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example (b):
as shown in fig. 1 to 6, an embodiment of the present invention provides a solid solution reaction vessel for processing rare earth element yttrium, including a reactor shell 6, a reactor cover 9 is disposed on a top of the reactor shell 6, a stirring rod 14 is rotatably connected to a middle portion of the reactor cover 9, stirring blades 20 are disposed on an outer side of the stirring rod 14, a power mechanism is disposed on a top end of the stirring rod 14, a plurality of piston cylinders 12 are fixedly connected to an edge of the reactor cover 9, a piston head 25 is slidably connected to an inside of the piston cylinder 12, a shaft pin 23 is fixedly connected to a bottom of the piston head 25, a connecting rod 26 is rotatably connected to a middle portion of the shaft pin 23, a crankshaft 22 is rotatably connected to a bottom end of the connecting rod 26, one end of the crankshaft 22 is rotatably connected to an inner side of the reactor shell 6, a disturbance rod 24 is fixedly connected to another end of the crankshaft 22, a disturbance blade 21 is disposed on an outer side of the disturbance rod 24, and an adjusting rod 13 is fixedly connected to a top of the piston head 25, the top of adjusting pole 13 is provided with adjustable ring 7, and the last fixed surface of adjustable ring 7 is connected with pneumatic cylinder 4, and the top fixedly connected with support frame 3 of pneumatic cylinder 4.
The stirring rod 14 is driven to rotate by the power mechanism to enable the stirring blade 20 to stir and mix the rare earth element yttrium and the acid-base mixture, the adjusting ring 7 is lifted by the hydraulic cylinder 4, the adjusting rod 13 can be lifted, the piston head 25 can further slide up and down in the piston cylinder 12, the bottom of the piston head 25 is rotatably connected with the connecting rod 26 through the shaft pin 23, the connecting rod 26 is used for driving the crankshaft 22 to rotate on the inner side of the reactor shell 6, the disturbance rod 24 and the disturbance blade 21 can be rotated, solid solution can be vigorously stirred, the molecules can be fully fused, the collision and contact probability among the molecules is increased, the reaction is more sufficient, and the quality of a product is improved.
Power unit includes fixed disk 5 and motor 18, and the top fixed connection of fixed disk 5 is in the middle part of support frame 3, and the bottom fixed connection of fixed disk 5 is in the outside of motor 18, and the output fixedly connected with output pole 16 of motor 18, the bottom of output pole 16 is connected in the top middle part of puddler 14.
The motor 18 is used for driving the output rod 16 to drive the stirring rod 14 to rotate, and the power mechanism is used for conveniently driving the stirring rod 14 to rotate.
The bottom end of the output rod 16 is fixedly connected with an insert block 15, the middle part of the top end of the stirring rod 14 is provided with a slot 19, the bottom of the insert block 15 is connected in the slot 19, and the stirring rod 14 and the insert block 15 are in through connection through a locking pin 17. Place inserted block 15 through slot 19, utilize fitting pin 17 to pass the slot 19 of puddler 14 and the inserted block 15 of output lever 16, can lock output lever 16 and puddler 14, be convenient for utilize motor 18 drive puddler 14 to rotate, easy to assemble dismantlement simultaneously, the convenience is maintained and is repaired reaction vessel.
The number of the piston cylinders 12 is three to six, the length of the connecting rods 26 located at the bottom of the piston cylinders 12 is sequentially increased, and the disturbance blades 21 and the stirring blades 20 are staggered from each other.
The plurality of piston cylinders 12 are distributed in the reactor cover 9, and the connecting rods 26 with different heights are connected with the crankshafts 22, so that the crankshafts 22 can be distributed at different heights of the reaction vessel, the stirring effect is further increased, the stirring blades 20 are prevented from being interfered by the stirring blades 21, solid solutions are disturbed at different heights, and molecules are fully fused.
Be provided with adjustment tank 11 in the middle part of adjustable ring 7, adjust the top of pole 13 and run through adjustment tank 11, one side of adjustable ring 7 is provided with locking bolt 10, and the outside through connection adjustable ring 7 of locking bolt 10 and regulation pole 13.
Place through adjustment tank 11 and adjust pole 13, recycle locking bolt 10 and insert from adjustable ring 7 and adjust pole 13, locking bolt 10 can be connected adjustable ring 7 and regulation pole 13, and convenient dismantlement adjustable ring 7 and regulation pole 13 more, and convenient installation is dismantled, and the convenience is maintained the repair, the later maintenance of being convenient for to reaction vessel.
The equal fixedly connected with slider 2 in bottom both ends of support frame 3, the equal sliding connection in bottom of two sliders 2 has track 1. Utilize support frame 3 fixed pneumatic cylinder 4 and fixed disk 5, utilize track 1 to be convenient for remove pneumatic cylinder 4 and fixed disk 5, be convenient for remove the installation and dismantle labour saving and time saving.
A manhole cover 8 is provided in one side of the reactor cover 9, and a connection pipe is provided in the other side of the reactor cover 9. The manhole cover 8 is used for cleaning, overhauling and maintaining the reaction vessel, and the connecting pipe is used for adding materials or introducing protective gas and the like.
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (7)

1. A solid solution reaction vessel for processing rare earth element yttrium, comprising a reactor shell (6), characterized in that: the reactor comprises a reactor shell (6), wherein a reactor cover (9) is arranged at the top of the reactor shell (6), a stirring rod (14) is rotatably connected to the middle of the reactor cover (9), stirring blades (20) are arranged on the outer side of the stirring rod (14), a power mechanism is arranged at the top end of the stirring rod (14), a plurality of piston cylinders (12) are fixedly connected to the edge of the reactor cover (9), a piston head (25) is slidably connected to the inner part of each piston cylinder (12), a shaft pin (23) is fixedly connected to the bottom of each piston head (25), a connecting rod (26) is rotatably connected to the middle of each shaft pin (23), a crankshaft (22) is rotatably connected to the bottom end of each connecting rod (26), one end of the crankshaft (22) is rotatably connected to the inner side of the reactor shell (6), a moving rod (24) is fixedly connected to the other end of the crankshaft (22), and a stirring blade (21) is arranged on the outer side of the stirring rod (24), the top fixedly connected with of piston head (25) adjusts pole (13), the top of adjusting pole (13) is provided with adjustable ring (7), the last fixed surface of adjustable ring (7) is connected with pneumatic cylinder (4), the top fixedly connected with support frame (3) of pneumatic cylinder (4).
2. A solid solution reaction vessel for processing rare earth element yttrium according to claim 1, wherein: the power mechanism comprises a fixed disc (5) and a motor (18), the top end of the fixed disc (5) is fixedly connected to the middle of the support frame (3), the bottom end of the fixed disc (5) is fixedly connected to the outside of the motor (18), an output end of the motor (18) is fixedly connected with an output rod (16), and the bottom end of the output rod (16) is connected to the middle of the top end of the stirring rod (14).
3. A solid solution reaction vessel for processing rare earth element yttrium according to claim 2, wherein: the bottom fixedly connected with inserted block (15) of output lever (16), the top middle part of puddler (14) is provided with slot (19), the bottom of inserted block (15) is connected in slot (19), puddler (14) and inserted block (15) are through-going connection through fitting pin (17).
4. A solid solution reaction vessel for processing rare earth element yttrium according to claim 1, wherein: the number of the piston cylinders (12) is three to six, the length of connecting rods (26) positioned at the bottom of the piston cylinders (12) is sequentially increased, and the disturbing blades (21) and the stirring blades (20) are staggered.
5. A solid solution reaction vessel for processing rare earth element yttrium according to claim 1, wherein: be provided with adjustment tank (11) in the middle part of adjustable ring (7), adjustment tank (11) are run through on the top of adjusting pole (13), one side of adjustable ring (7) is provided with locking bolt (10), the outside through connection adjustable ring (7) and the regulation pole (13) of locking bolt (10).
6. A solid solution reaction vessel for processing rare earth element yttrium according to claim 1, wherein: the equal fixedly connected with slider (2) in bottom both ends of support frame (3), two the equal sliding connection in bottom of slider (2) has track (1).
7. A solid solution reaction vessel for processing rare earth element yttrium according to claim 1, wherein: a manhole cover (8) is arranged in one side of the reactor cover (9), and a connecting pipe is arranged in the other side of the reactor cover (9).
CN202210165671.8A 2022-02-10 2022-02-10 Solid solution reaction vessel for processing rare earth element yttrium Pending CN114588858A (en)

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CN215655126U (en) * 2021-06-02 2022-01-28 李翼亨 Separation reaction kettle for application chemistry
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CN215655126U (en) * 2021-06-02 2022-01-28 李翼亨 Separation reaction kettle for application chemistry
CN215743446U (en) * 2021-09-17 2022-02-08 南京三叶搅拌设备制造有限公司 High-efficient reation kettle is used in chemical industry with reciprocal stirring function

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