CN114504834B - Calcium gluconate solution purification equipment and process thereof - Google Patents
Calcium gluconate solution purification equipment and process thereof Download PDFInfo
- Publication number
- CN114504834B CN114504834B CN202210177323.2A CN202210177323A CN114504834B CN 114504834 B CN114504834 B CN 114504834B CN 202210177323 A CN202210177323 A CN 202210177323A CN 114504834 B CN114504834 B CN 114504834B
- Authority
- CN
- China
- Prior art keywords
- calcium gluconate
- gluconate solution
- drying tower
- blade
- disc
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/16—Evaporating by spraying
- B01D1/18—Evaporating by spraying to obtain dry solids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/0082—Regulation; Control
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/16—Evaporating by spraying
- B01D1/20—Sprayers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D1/00—Evaporating
- B01D1/30—Accessories for evaporators ; Constructional details thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/087—Cleaning containers, e.g. tanks by methods involving the use of tools, e.g. brushes, scrapers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B08—CLEANING
- B08B—CLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
- B08B9/00—Cleaning hollow articles by methods or apparatus specially adapted thereto
- B08B9/08—Cleaning containers, e.g. tanks
- B08B9/093—Cleaning containers, e.g. tanks by the force of jets or sprays
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/10—Process efficiency
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The invention belongs to the technical field of purification of calcium gluconate solution, and particularly relates to calcium gluconate solution purification equipment and a calcium gluconate solution purification process, which comprise the following steps: a drying tower; an atomizer, the atomizer comprising: the automatic discharging device comprises a support, a main shaft, a motor, a discharging disc and a rotary disc, wherein the rotary disc is rotatably arranged inside the discharging disc, the rotary disc is fixedly connected with the main shaft, blades are fixedly connected to the edge of the rotary disc, and the edge of each blade is in contact with the inner wall of the discharging disc; a feeding pipe; a controller; the problem of wall sticking caused by the fact that the calcium gluconate solution cannot be dried quickly in the drying tower is solved; according to the invention, the blade is arranged, so that the calcium gluconate solution rapidly passes through the discharge chute and is not easy to remain in the discharge chute to cause blockage, and on the other hand, the blade is in contact with the inner wall of the discharge tray and can scrape substances adhered to the discharge tray, so that the calcium gluconate solution is not easy to adhere to the wall in the drying tower, and the purification quality of the calcium gluconate is ensured.
Description
Technical Field
The invention belongs to the technical field of purification of calcium gluconate solutions, and particularly relates to calcium gluconate solution purification equipment and a calcium gluconate solution purification process.
Background
The calcium gluconate solution is purified and needs to be dehydrated, the solution is directly pumped into a centrifugal spray dryer by a pump after being decolored and filtered, steam, electricity or fuel gas is used as a heat source to heat air and is introduced into the spray dryer for spray drying, the calcium gluconate solution is directly atomized into powder or granular powder, and then the powder or the granular powder is packaged to prepare a finished product of the calcium gluconate. Compared with the traditional process, the process does not need the working procedures of evaporation, crystallization, recrystallization and centrifugal separation; no mother liquor is generated, and the one-time extraction yield can reach more than 99 percent.
Spray drying is a drying technique in which a feed liquid is dispersed into fine droplets by an atomizer and a solvent is rapidly evaporated in a hot drying medium to form a dry powder product. Spray drying has the advantages of large evaporation area, short drying time (several seconds to tens of seconds), less damage to active ingredients, and the like, and is increasingly applied to drying of heat-sensitive materials.
During the spray drying process, the material to be dried sticks to the inner wall of the drying tower, which is called wall-sticking. The material stuck on the wall may be burnt or deteriorated due to staying on the hot inner wall for a long time, which affects the quality of the product. The wall-sticking material can not be brought out of the drying tower by induced air in time, so that the product yield is reduced, and when the wall-sticking phenomenon is serious, spray drying has to be stopped midway in order to remove the wall-sticking material, so that the operation period is prolonged, and the production capacity is reduced. One important reason for the occurrence of the wall-sticking phenomenon is that: the calcium gluconate solution is sent into the atomizer through the plunger pump, the atomizer nozzle is blocked to cause that the feed liquid can not be atomized or the atomization effect is poor, and the calcium gluconate solution can not be dried in the drying tower quickly to cause wall adhesion.
In view of the above, the invention provides a calcium gluconate solution purification device and a calcium gluconate solution purification process, which solve the technical problems.
Disclosure of Invention
In order to solve the defects of the prior art, the invention provides calcium gluconate solution purification equipment and a calcium gluconate solution purification process; the problem of calcium gluconate solution send into the atomizer through the plunger pump, the atomizer shower nozzle blocks and causes the feed liquid can not atomize or the atomization effect is poor, and calcium gluconate solution can not dry very fast in the drying tower, causes the wall adhesion is solved.
The technical scheme adopted by the invention for solving the technical problem is as follows: the invention relates to calcium gluconate solution purification equipment, which comprises:
a drying tower;
an atomizer, the atomizer comprising:
the support is fixedly arranged at the top of the inner side of the drying tower;
the main shaft is rotatably arranged inside the bracket;
the motor is fixedly connected to the top of the support and used for driving the spindle;
the discharging disc is fixedly installed at the bottom of the support, a discharging groove is formed in the circumference of the discharging disc, an end cover is fixedly connected to the bottom of the discharging disc, and the main shaft is rotatably connected with the end cover;
the rotary table is rotatably arranged inside the discharging disc, the rotary table is fixedly connected with the main shaft, the edge of the rotary table is fixedly connected with a blade, the blade is an elastic steel sheet, and the edge of the blade is in contact with the inner wall of the discharging disc;
the feeding pipe is fixedly arranged on one side of the support, and one end of the feeding pipe is communicated with the rotary disc;
and the controller is used for controlling the operation of the calcium gluconate solution purification equipment.
Preferably, the edge of the blade contacting with the discharging disc is provided with a cutting edge.
Preferably, the blade is helical.
Preferably, a scraper is arranged on the outer side of the discharging disc, the scraper is fixedly connected with the main shaft, and the scraper is in contact with the outer circumference of the discharging disc.
Preferably, the scraper is in line contact with the discharge disc.
Preferably, the blades and the scraper are arranged in a staggered mode in the circumferential direction.
Preferably, the turntable is fixedly connected with nozzles between the blades, the nozzles face the inner wall of the discharge tray, the nozzles are communicated with an air pump on the outer side of the drying tower through a pipeline arranged in the main shaft 22, and the nozzles are provided with electromagnetic valves.
Preferably, the lateral wall of ejection of compact dish has linked firmly the blow gun, the blow gun is towards the blade, the blow gun passes through the air pump intercommunication in pipeline and the drying tower outside, also be provided with the solenoid valve on the blow gun.
Preferably, the discharge disc is provided with two layers.
The process is suitable for the calcium gluconate solution purification equipment, and comprises the following process flows:
s1, filtering air through a filter, heating the air through a heater, feeding the air into an air distributor at the top of a drying tower, and uniformly feeding the air into a drying chamber in a spiral shape;
s2, after the hot air in the S1 reaches a proper temperature, pumping the calcium gluconate solution into an atomizer of a drying tower from a feed liquid tank through a filter, controlling a motor to rotate by a controller, spraying the calcium gluconate solution into extremely small fog-like liquid drops, enabling the calcium gluconate solution to be in parallel flow contact with the hot air, quickly evaporating water, and cleaning a discharge disc by blades and a scraper during drying and purification;
s3, after the moisture of the calcium gluconate solution in the S2 is evaporated, drying the calcium gluconate solution into a finished product, discharging the finished product from material collecting bottles at the bottom of the drying tower and the bottom of the cyclone separator, and discharging waste gas from a fan;
and S4, after the calcium gluconate solution is dried in the S3, the controller controls the air pump to supply air to the nozzle and the blowing nozzle, and meanwhile, the driving motor enables the blades and the scraper to scrape the discharging disc for cleaning, so that the inside of the atomizer is cleaned.
The invention has the following beneficial effects:
1. according to the calcium gluconate solution purification equipment and the calcium gluconate solution purification process, the blades are arranged, so that the calcium gluconate solution has higher pressure when being pressed into the discharge chute, the calcium gluconate solution can rapidly pass through the discharge chute and is not easy to remain in the discharge chute to cause blockage, on the other hand, the blades are in contact with the inner wall of the discharge tray, and the blades can scrape substances adhered to the discharge tray, so that the blockage is not easy to form in the atomizer, the atomized liquid is kept smooth, the calcium gluconate solution is not easy to stick to the wall in the drying tower, and the purification quality of the calcium gluconate is ensured.
2. According to the calcium gluconate solution purification equipment and the calcium gluconate solution purification process, the cutting edge is arranged at the edge of the blade, when the calcium gluconate solution is atomized and dried, the blade rotates in the discharge disc, when the cutting edge scratches the discharge groove, the cutting edge and the groove wall of the discharge groove form shearing, larger particles in the calcium gluconate solution can be crushed, the possibility of blockage of an atomizer is reduced, the cutting edge at the edge of the blade enables the blade to be in line contact with the inner wall of the discharge disc, the scraping effect of the blade on the inner wall of the discharge disc is improved, adhesion is formed on the inner wall of the discharge disc, and the possibility of blockage is reduced.
3. According to the calcium gluconate solution purification equipment and the calcium gluconate solution purification process, the scraper is arranged on the outer side of the discharge disc, when the calcium gluconate solution is dried and purified, the main shaft rotates to drive the scraper to rotate, the scraper is in contact with the outer circumference of the discharge disc, the scraper rotates to scrape bonded substances on the outer side of the discharge disc, the bonding on the outer side of the discharge disc is avoided, and the discharge chute is prevented from being blocked.
4. According to the calcium gluconate solution purification equipment and the calcium gluconate solution purification process, the nozzle is arranged, when the calcium gluconate solution is dried and purified, the controller controls the air pump to supply air to the nozzle, the electromagnetic valve on the nozzle is opened, the air flow is sprayed out of the nozzle and blown to the inner wall of the discharge tray and the discharge chute, the inner wall of the discharge tray and the discharge chute are further blown and cleaned, and blockage caused by adhesion of the calcium gluconate solution is reduced.
Drawings
The invention will be further described with reference to the accompanying drawings.
FIG. 1 is a perspective view of the present invention;
FIG. 2 is a schematic perspective view of the atomizer of the present invention;
FIG. 3 is a schematic view of the internal structure of the atomizer of the present invention;
FIG. 4 is a diagram of the process steps in the present invention;
in the figure: 1. a drying tower; 2. an atomizer; 21. a support; 22. a main shaft; 23. a motor; 3. a discharging tray; 31. a discharge chute; 4. a turntable; 41. a blade; 5. a feed pipe; 6. a scraper; 7. a nozzle; 8. a blowing nozzle.
Detailed Description
The present invention will be further described with reference to the following detailed description so that the technical means, the creation features, the achievement purposes and the effects of the present invention can be easily understood.
The embodiment of the invention provides calcium gluconate solution purification equipment and a process thereof, and solves the technical problems that the calcium gluconate solution is fed into an atomizer 2 through a plunger pump, a spray head of the atomizer 2 is blocked, so that feed liquid cannot be atomized or the atomization effect is poor, and the calcium gluconate solution cannot be dried quickly in a drying tower 1, so that wall adhesion is caused;
in order to solve the technical problems, the technical scheme in the embodiment of the invention has the following general idea: through setting up blade 41, calcium gluconate solution receives blade 41's stirring and produces centrifugal force, make calcium gluconate solution have bigger pressure when impressing blown down tank 31, make calcium gluconate solution pass through rapidly in blown down tank 31, be difficult for remaining in blown down tank 31 and cause the jam, on the other hand blade 41 and the inner wall contact of blown down disk 3, make calcium gluconate solution be difficult for bonding at 3 inner walls of blown down disk, and blade 41 can strike off the material that bonds on blown down disk 3, thereby be difficult for forming the jam in atomizer 2, it is unobstructed to keep the atomizing play liquid, thereby make calcium gluconate solution be difficult for gluing the wall in drying tower 1, guarantee calcium gluconate's purification quality.
As shown in fig. 1 to 4, the calcium gluconate solution purification apparatus according to the present invention includes:
a drying tower 1;
an atomizer 2, said atomizer 2 comprising:
the bracket 21 is fixedly arranged at the top of the inner side of the drying tower 1;
a main shaft 22, wherein the main shaft 22 is rotatably arranged inside the bracket 21;
the motor 23, the motor 23 is fixedly connected to the top of the bracket 21, and the motor 23 is used for driving the spindle 22;
the discharging disc 3 is fixedly arranged at the bottom of the support 21, a discharging groove 31 is formed in the circumference of the discharging disc 3, an end cover is fixedly connected to the bottom of the discharging disc 3, and the main shaft 22 is rotatably connected with the end cover;
the rotary table 4 is rotatably installed inside the discharging disc 3, the rotary table 4 is fixedly connected with the main shaft 22, the edge of the rotary table 4 is fixedly connected with a blade 41, the blade 41 is an elastic steel sheet, and the edge of the blade 41 is in contact with the inner wall of the discharging disc 3;
the feeding pipe 5 is fixedly arranged on one side of the support 21, and one end of the feeding pipe 5 is communicated with the rotary table 4;
the controller is used for controlling the operation of the calcium gluconate solution purification equipment;
the calcium gluconate solution is fed into the atomizer 2 through a plunger pump, the feed liquid cannot be atomized or the atomization effect is poor due to the blockage of a spray head of the atomizer 2, and the calcium gluconate solution cannot be dried quickly in the drying tower 1, so that the wall is adhered;
in the invention, by arranging the blades 41, when purifying the calcium gluconate solution, the calcium gluconate solution is pumped into the atomizer 2 of the drying tower 1 from the feed liquid tank through the filter, the controller controls the motor 23 to rotate, the motor 23 rotates to drive the main shaft 22 to rotate on the bracket 21, the main shaft 22 drives the turntable 4 to rotate, the blades 41 rotate synchronously with the turntable 4, the calcium gluconate solution reaches the discharge disc 3 through the feed pipe 5, the end cover prevents the calcium gluconate solution from leaking from the bottom of the discharge disc 3, the blades 41 rotate to press the calcium gluconate solution into the discharge groove 31, and then the calcium gluconate solution is discharged into the drying tower 1 through the discharge groove 31 to spray the calcium gluconate solution into extremely small mist-shaped liquid drops, the top of the drying tower 1 is fixedly provided with a filter, a heater and an air distributor, air is filtered through the filter, the air is heated through the heater, enters the air distributor at the top of the drying tower 1 and then uniformly enters the drying chamber in a spiral shape, a calcium gluconate solution is in parallel flow contact with hot air, moisture is rapidly evaporated, the calcium gluconate solution is dried into a finished product in a very short time, one side of the drying tower 1 close to the bottom is communicated with a cyclone separator through a pipeline, the bottoms of the drying tower 1 and the cyclone separator are connected with material collecting bottles, the top of the cyclone separator is provided with a fan, the finished product is discharged from the bottom of the drying tower 1 and the material collecting bottles at the bottom of the cyclone separator, and waste gas is discharged from the fan;
according to the invention, by arranging the blades 41, the calcium gluconate solution is stirred by the blades 41 to generate centrifugal force, so that the calcium gluconate solution has higher pressure when being pressed into the discharge chute 31, the calcium gluconate solution rapidly passes through the discharge chute 31 and is not easy to remain in the discharge chute 31 to cause blockage, on the other hand, the blades 41 are elastic steel sheets and can be kept in contact with the inner wall of the discharge tray 3, so that the calcium gluconate solution is not easy to adhere to the inner wall of the discharge tray 3, the blades 41 can scrape substances adhered to the discharge tray 3, and the blades 41 can generate certain vibration in the scraping process, so that some substances adhered to the blades 41 are vibrated and dropped, the cleanness of the blades 41 is kept, the scraping effect of the blades 41 is ensured, the calcium gluconate solution is not easy to form blockage in the atomizer 2, atomized liquid is kept, the calcium gluconate solution is not easy to stick to the wall in the drying tower 1, and the purification quality of the calcium gluconate is ensured.
In one embodiment of the present invention, as shown in fig. 2, the edge of the blade 41 contacting the discharge tray 3 is provided with a cutting edge.
In one embodiment of the present invention, as shown in fig. 2, the blade 41 has a spiral shape.
During operation, through setting up the cutting sword at the edge of blade 41, when carrying out the spray drying to calcium gluconate solution, blade 41 is rotatory in discharge tray 3, when the cutting sword was drawn from discharge chute 31, the cutting sword forms the shearing with the cell wall of discharge chute 31, can break great granule in the calcium gluconate solution, reduce the possibility that atomizer 2 blockked up, and the cutting sword at blade 41 edge makes blade 41 and discharge tray 3's inner wall be line contact, improve the effect of scraping of blade 41 to discharge tray 3 inner wall, thereby form the bonding at discharge tray 3 inner wall, reduce the possibility of jam, through setting up blade 41 into the spiral, calcium gluconate solution is after contacting with blade 41, spiral blade 41 rotates and forms the auger, transport calcium gluconate solution downwards, make the calcium gluconate solution pressure that is close to the bottom in discharge tray 3 increase, thereby make to pass through discharge chute 31 fast, be difficult for forming the jam in discharge chute 31, make calcium gluconate solution be difficult for glue the wall in drying tower 1, guarantee the purification quality of calcium gluconate.
As an embodiment of the present invention, as shown in fig. 2, a scraper 6 is disposed on an outer side of the discharging tray 3, the scraper 6 is fixedly connected to the main shaft 22, and the scraper 6 contacts with an outer circumference of the discharging tray 3.
In one embodiment of the present invention, as shown in fig. 2, the scraper 6 is in line contact with the discharge pan 3.
As an embodiment of the present invention, as shown in fig. 2, the blade 41 and the doctor blade 6 are arranged to be shifted in the circumferential direction.
During operation, through set up scraper 6 in the play charging tray 3 outside, when carrying out dry purification to calcium gluconate solution, main shaft 22 rotates and drives scraper 6 and rotate, scraper 6 with the outer circumference contact of play charging tray 3, scraper 6 rotates and strikes off the material of the bonding in the play charging tray 3 outside, avoid appearing bonding in the play charging tray 3 outside, prevent consequently to lead to blown down tank 31 to block up, and scraper 6 and play charging tray 3 are line contact, reduce the area of contact of scraper 6 and play charging tray 3, thereby improve the effect of striking off of scraper 6 to the play charging tray 3 outside, and reduce the hindrance of scraper 6 to the ejection of compact of play charging tray 3, guarantee the unobstructed ejection of compact of play charging tray 3, through setting scraper 6 and blade 41 stagger in the circumferencial direction, when making blade 41 extrude calcium gluconate solution from blown down tank 31 again, scraper 6 can not block up play charging tank 31, further guarantee the ejection of compact smoothly, reduce the jam, thereby make calcium gluconate solution be difficult for the bonding in drying tower 1 inner wall, and then guarantee the calcium gluconate quality after dry purification.
As an embodiment of the present invention, as shown in fig. 2 and 3, the rotating disc 4 is fixedly connected with a nozzle 7 between the blades 41, the nozzle 7 faces the inner wall of the discharging disc 3, the nozzle 7 is communicated with an air pump outside the drying tower 1 through a pipeline arranged in the main shaft 22, and an electromagnetic valve is arranged on the nozzle 7.
As an embodiment of the invention, as shown in fig. 2 and fig. 3, a blowing nozzle 8 is fixedly connected to a side wall of the discharging tray 3, the blowing nozzle 8 faces to the blades 41, the blowing nozzle 8 is communicated with an air pump outside the drying tower 1 through a pipeline, and an electromagnetic valve is also arranged on the blowing nozzle 8.
During operation, through setting up nozzle 7, when carrying out dry purification to calcium gluconate solution, controller control air pump air feed to in nozzle 7, the intercommunication pipeline sets up at main shaft 22 inside center, from main shaft 22 bottom and air pump intercommunication, thereby do not interfere the main shaft 22 and rotate, and carousel 4 and main shaft 22 rotate in step, the two is static relatively, thereby be convenient for to the air feed to nozzle 7, the solenoid valve on the nozzle 7 is opened, the air current is spout from nozzle 7, the air current blows to the inner wall and the blown down tank 31 of blown down disk 3, further blow clean the inner wall and the blown down tank 31 of blown down disk 3, reduce calcium gluconate solution bonding and cause the jam, through setting up blow gun 8, controller control air pump air feed to blow gun 8, the solenoid valve on blow gun 8 is opened, thereby make the air current in the blow gun 8 blow to the carousel 4 outside and blade 41, blow the material that bonds on the carousel 4 outside and the blade 41 off, thereby further reduce the possibility of jam, after calcium gluconate solution dry purification is accomplished, controller control air feed to nozzle 7 and blow gun 8, be convenient for inside the atomizer 2 to clean, it is convenient to use once more.
As an embodiment of the present invention, as shown in fig. 2 and 3, the discharging tray 3 is provided with a double layer; during operation, through setting up double-deck charging tray 3, through bolt fixed connection between the double-deck charging tray 3, when carrying out dry purification to calcium gluconate solution, double-deck charging tray 3 has increased the quantity of blown down tank 31, and blown down tank 31 on the double-deck charging tray 3 is the dislocation distribution on the circumference, the play liquid measure of atomizer 1 has been improved, thereby improve dry purification's efficiency, and receive spiral blade 41 to influence when going out the liquid, transport calcium gluconate solution downwards, make calcium gluconate solution preferentially discharge from the charging tray 3 of lower floor, when lower floor's charging tray 3 blocks up, can follow upper strata's charging tray 3 and continue atomizing dry purification, guarantee continuous production.
The process for purifying the calcium gluconate solution is suitable for the calcium gluconate solution purification equipment, and comprises the following process flows of:
s1, filtering air through a filter, heating the air through a heater, feeding the air into an air distributor at the top of a drying tower 1, and uniformly feeding the air into a drying chamber in a spiral shape;
s2, when the hot air in the S1 reaches a proper temperature, the calcium gluconate solution is pumped into the atomizer 2 of the drying tower 1 from the feed liquid tank through a filter, the controller controls the motor 23 to rotate, so that the calcium gluconate solution is sprayed into tiny fog-like liquid drops, the calcium gluconate solution is in parallel flow contact with the hot air, the moisture is rapidly evaporated, and the blade 41 and the scraper 6 clean the discharge disc 3 during drying and purification;
s3, after the moisture of the calcium gluconate solution in the step S2 is evaporated, drying the calcium gluconate solution into a finished product, discharging the finished product from material collecting bottles at the bottom of the drying tower 1 and the bottom of the cyclone separator, and discharging waste gas from a fan;
and S4, after the calcium gluconate solution is dried in the S3, the controller controls the air pump to supply air to the nozzle 7 and the blowing nozzle 8, and simultaneously the motor 23 is driven to enable the blades 41 and the scraper 6 to scrape and clean the discharge disc 3, so that the inside of the atomizer 2 is cleaned.
The specific working process is as follows:
when the device works, by arranging the blades 41, when purifying a calcium gluconate solution, the calcium gluconate solution is pumped into the atomizer 2 of the drying tower 1 from the feed liquid tank through the filter, the controller controls the motor 23 to rotate, the motor 23 rotates to drive the main shaft 22 to rotate on the bracket 21, the main shaft 22 drives the turntable 4 to rotate, the blades 41 rotate synchronously with the turntable 4, the calcium gluconate solution reaches the discharge tray 3 through the feed pipe 5, the blades 41 rotate to press the calcium gluconate solution into the discharge chute 31, and then the calcium gluconate solution is discharged into the drying tower 1 through the discharge chute 31 to be sprayed into extremely small fog-like liquid drops, the top of the drying tower 1 is fixedly provided with the filter, the heater and the air distributor, the air is filtered through the filter, the air is heated through the heater, enters the air distributor at the top of the drying tower 1 and then uniformly enters the drying chamber in a spiral shape, the calcium gluconate solution and the hot air are in parallel flow contact, moisture is evaporated rapidly, the calcium gluconate solution is dried to be a finished product in a very short time, one side, close to the bottom, of the drying tower 1 is communicated with a cyclone separator through a pipeline, the bottoms of the drying tower 1 and the cyclone separator are connected with material collecting bottles, a fan is arranged at the top of the cyclone separator, the finished product is discharged from the material collecting bottles at the bottoms of the drying tower 1 and the cyclone separator, waste gas is discharged by the fan, through the arrangement of the blades 41, the calcium gluconate solution is stirred by the blades 41 to generate centrifugal force, so that the calcium gluconate solution has larger pressure when being pressed into the discharge chute 31, the calcium gluconate solution rapidly passes through the discharge chute 31, the blockage caused by residue in the discharge chute 31 is not easy, on the other hand, the blades 41 are in contact with the inner wall of the discharge tray 3, and the calcium gluconate solution is not easy to adhere to the inner wall of the discharge tray 3, and the blade 41 can scrape off the substances adhered on the discharging disc 3; through set up scraper 6 in the play charging tray 3 outside, when carrying out dry purification to the calcium gluconate solution, main shaft 22 rotates and drives scraper 6 and rotate, scraper 6 with the outer circumference contact of play charging tray 3, scraper 6 rotates and strikes off the material of the bonding in the play charging tray 3 outside, avoid appearing bonding in the play charging tray 3 outside, prevent consequently to lead to blown down tank 31 to block up, and scraper 6 and play charging tray 3 are line contact, reduce the area of contact of scraper 6 and play charging tray 3, thereby improve the effect of striking off of scraper 6 to the play charging tray 3 outside, and reduce the hindrance of scraper 6 to the ejection of compact of play charging tray 3, guarantee that the ejection of compact of play charging tray 3 is unobstructed, through the setting of staggering scraper 6 and blade 41 in the circumferencial direction, when making blade 41 extrude the calcium gluconate solution from blown down tank 31 again, scraper 6 can not block blown down tank 31, further guarantee that the ejection of compact is smooth and easy.
The front, the back, the left, the right, the upper and the lower are based on the observation angle of the person, the side of the device facing the observer is defined as the front, the left side of the observer is defined as the left, and so on.
In the description of the present invention, it is to be understood that the terms "central," "longitudinal," "lateral," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," and the like are used in the orientation or positional relationship indicated in fig. 1 to facilitate the description of the invention and to simplify the description, but do not indicate or imply that the referenced device or element must have a particular orientation, be constructed and operated in a particular orientation, and are not to be construed as limiting the scope of the invention.
The foregoing shows and describes the general principles, principal features and advantages of the invention. It will be understood by those skilled in the art that the present invention is not limited to the embodiments described above, which are described in the specification and illustrated only to illustrate the principle of the present invention, but that various changes and modifications may be made therein without departing from the spirit and scope of the present invention, which fall within the scope of the invention as claimed. The scope of the invention is defined by the appended claims and equivalents thereof.
Claims (5)
1. The utility model provides a calcium gluconate solution purification equipment which characterized in that includes:
a drying tower (1);
-an atomizer (2), the atomizer (2) comprising:
the support (21), the support (21) is fixedly installed at the top of the inner side of the drying tower (1);
a main shaft (22), wherein the main shaft (22) is rotatably arranged inside the bracket (21);
the motor (23), the motor (23) is fixedly connected to the top of the bracket (21), and the motor (23) is used for driving the spindle (22);
the discharging disc (3) is fixedly mounted at the bottom of the support (21), a discharging groove (31) is formed in the circumference of the discharging disc (3), an end cover is fixedly connected to the bottom of the discharging disc (3), and the main shaft (22) is rotatably connected with the end cover;
the rotary table (4) is rotatably mounted inside the discharging disc (3), the rotary table (4) is fixedly connected with the main shaft (22), blades (41) are fixedly connected to the edge of the rotary table (4), the blades (41) are elastic steel sheets, and the edge of each blade (41) is in contact with the inner wall of the discharging disc (3);
the feeding pipe (5) is fixedly installed on one side of the support (21), and one end of the feeding pipe (5) is communicated with the rotary disc (4);
the controller is used for controlling the operation of the calcium gluconate solution purification equipment;
the edge of the blade (41) contacting with the discharging disc (3) is provided with a cutting edge;
the blade (41) is spiral;
a scraper (6) is arranged on the outer side of the discharging disc (3), the scraper (6) is fixedly connected with the main shaft (22), and the scraper (6) is in contact with the outer circumference of the discharging disc (3);
the scraper (6) is in line contact with the discharging disc (3);
the blades (41) and the scraper (6) are arranged in a staggered mode in the circumferential direction.
2. The purification equipment of calcium gluconate solution according to claim 1, wherein: carousel (4) are in nozzle (7) have been linked firmly between blade (41), nozzle (7) are towards the inner wall of play charging tray (3), nozzle (7) are through setting up the air pump intercommunication in the pipeline in main shaft (22) and drying tower (1) outside, set up the solenoid valve on nozzle (7).
3. The apparatus of claim 2, wherein the apparatus comprises: the lateral wall of ejection of compact dish (3) has linked firmly blow gun (8), blow gun (8) are towards blade (41), blow gun (8) are through the air pump intercommunication in pipeline and drying tower (1) outside, also be provided with the solenoid valve on blow gun (8).
4. The apparatus of claim 3, wherein the apparatus comprises: the discharging disc (3) is provided with a double layer.
5. A purification process of a calcium gluconate solution is characterized by comprising the following steps: the process is suitable for the calcium gluconate solution purification equipment as defined in any one of claims 1 to 4, and comprises the following process flows:
s1, filtering air through a filter, heating the air through a heater, feeding the air into an air distributor at the top of a drying tower (1), and uniformly feeding the air into a drying chamber in a spiral shape;
s2, after the hot air in the S1 reaches a proper temperature, pumping the calcium gluconate solution into the atomizer (2) of the drying tower (1) from the feed liquid tank through a filter, controlling the motor (23) to rotate by the controller, spraying the calcium gluconate solution into extremely small fog-like liquid drops, enabling the calcium gluconate solution to be in parallel flow contact with the hot air, quickly evaporating moisture, and cleaning the discharge disc (3) by the blades (41) and the scraper (6) during drying and purification;
s3, after the moisture of the calcium gluconate solution in the S2 is evaporated, drying the calcium gluconate solution into a finished product, discharging the finished product from material collecting bottles at the bottoms of the drying tower (1) and the cyclone separator, and discharging waste gas from a fan;
and S4, after the calcium gluconate solution is dried in the S3, the controller controls the air pump to supply air to the nozzle (7) and the blowing nozzle (8), and meanwhile the motor (23) is driven to enable the blades (41) and the scraper (6) to scrape the discharging disc (3) for cleaning, so that the inside of the atomizer (2) is cleaned.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210177323.2A CN114504834B (en) | 2022-02-24 | 2022-02-24 | Calcium gluconate solution purification equipment and process thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210177323.2A CN114504834B (en) | 2022-02-24 | 2022-02-24 | Calcium gluconate solution purification equipment and process thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN114504834A CN114504834A (en) | 2022-05-17 |
| CN114504834B true CN114504834B (en) | 2023-03-07 |
Family
ID=81553977
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202210177323.2A Active CN114504834B (en) | 2022-02-24 | 2022-02-24 | Calcium gluconate solution purification equipment and process thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN114504834B (en) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117450766B (en) * | 2023-12-20 | 2024-03-15 | 福建铭麟科技有限公司 | Potassium persulfate evaporative crystallization process and evaporative crystallization device |
Citations (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB964367A (en) * | 1961-02-06 | 1964-07-22 | Birs Brit Ag | Drying method and device for carrying the said method into effect |
| AU2008201720A1 (en) * | 2002-12-17 | 2008-05-08 | Medimmune, Llc | High pressure spray-dry of bioactive materials |
| CN203329386U (en) * | 2013-06-19 | 2013-12-11 | 常州市宇通干燥设备有限公司 | Hot air distributor for spray tower |
| WO2014017511A1 (en) * | 2012-07-27 | 2014-01-30 | 株式会社パウダリングジャパン | Liquid-atomizing device and liquid-atomizing method |
| CN105363231A (en) * | 2015-11-28 | 2016-03-02 | 南京威安新材料科技有限公司 | Centrifugal spray drying apparatus capable of preventing catalyst from adhering to walls |
| CN106039746A (en) * | 2016-08-01 | 2016-10-26 | 扬州日发干燥工程有限公司 | Wall-sticking-proof spraying dryer |
| CN205683848U (en) * | 2016-06-03 | 2016-11-16 | 华夏生生药业(北京)有限公司 | Medicinal liquid is dilute joins circulated filter system |
| EP3124110A1 (en) * | 2015-07-30 | 2017-02-01 | Sanovo Technologies A/S | A process and spray drying apparatus for spray drying products |
| CN106565460A (en) * | 2016-10-28 | 2017-04-19 | 山东凯翔生物化工股份有限公司 | Method for producing calcium gluconate and production device of method |
| CN206391590U (en) * | 2017-01-11 | 2017-08-11 | 哈尔滨剑桥学院 | A kind of long stroke easy to clean spray dryer |
| CN109276900A (en) * | 2017-07-20 | 2019-01-29 | 鲁娟 | A kind of anti-sticking wall efficient spray drier special nozzle |
| CN210057410U (en) * | 2019-05-29 | 2020-02-14 | 淄博锦源生物科技有限公司 | Device that peptone is dry not caking |
| CN111298464A (en) * | 2020-03-24 | 2020-06-19 | 江苏双林海洋生物药业有限公司 | Drying device is used in preparation of glucosamine sulfate double salt |
| AU2020100855A4 (en) * | 2019-11-12 | 2020-07-09 | Recom (Qingdao) Biotechnology Co. Ltd | Low-temperature drying and spraying equipment |
| CN211328190U (en) * | 2019-10-22 | 2020-08-25 | 北京宝德润生医药科技发展有限公司 | Spray drier |
| CN111707068A (en) * | 2020-07-02 | 2020-09-25 | 浙江汇翔化学工业有限公司 | Drying equipment for production of polycarboxylate water reducing agent |
| CN211721623U (en) * | 2020-01-14 | 2020-10-23 | 刘伯明 | Agricultural machine spouts medicine machine and spouts medicine liquid reserve tank |
| CN214344475U (en) * | 2021-01-11 | 2021-10-08 | 南京泛成生物科技有限公司 | Spray drying system |
| CN214714407U (en) * | 2021-04-13 | 2021-11-16 | 秸都科技(南京)有限公司 | High-speed centrifugal spray dryer with uniform spraying |
| CN113750554A (en) * | 2021-10-20 | 2021-12-07 | 福建好家景日化有限公司 | Atomizing, granulating and drying device for daily chemical production |
| CN113856226A (en) * | 2021-10-27 | 2021-12-31 | 山东省绿士农药有限公司 | Dry suspending agent type pesticide production line |
| CN215462061U (en) * | 2020-11-26 | 2022-01-11 | 徐州霍斯科技有限公司 | Spray drier |
| CN113967441A (en) * | 2021-11-17 | 2022-01-25 | 连云港瑞邦药业有限公司 | Purification and filling device and method for calcium gluconate production |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FI78453C (en) * | 1986-07-18 | 1989-08-10 | Suomen Sokeri Oy | Crystal anhydrous calcium gluconate with uniform crystal structure and process for its preparation |
| JP2868145B2 (en) * | 1994-06-09 | 1999-03-10 | 株式会社石垣 | Scraper device in screw press |
| US20050069820A1 (en) * | 2003-09-25 | 2005-03-31 | Fuji Photo Film Co., Ltd. | Thin film evaporating concentrator, method of evaporating and solidifying photographic waste solution, and reuse method of photographic waste solution |
| EP1915987A1 (en) * | 2006-10-27 | 2008-04-30 | MediGene AG | Spray-freeze-drying process for the preparation of pellets comprising percolation drying |
| DK2158029T3 (en) * | 2007-04-10 | 2019-08-19 | Gea Process Eng Inc | Process gas filter and method of cleaning this |
| US8226735B2 (en) * | 2009-06-02 | 2012-07-24 | Dennis Hudgens | Subterranean well production saltwater evaporation station |
| US9561184B2 (en) * | 2014-09-19 | 2017-02-07 | Velico Medical, Inc. | Methods and systems for multi-stage drying of plasma |
| US9861945B1 (en) * | 2017-08-04 | 2018-01-09 | ZoomEssence, Inc. | Ultrahigh efficiency spray drying apparatus and process |
| CN208066309U (en) * | 2018-01-19 | 2018-11-09 | 南京彼奥电子科技有限公司 | A kind of piezoelectric ceramics centrifugal granulating spray dryer |
| EP3753906A1 (en) * | 2019-06-19 | 2020-12-23 | Vapromax d.o.o. | A system and a method for purifying waste water in mobile homes |
-
2022
- 2022-02-24 CN CN202210177323.2A patent/CN114504834B/en active Active
Patent Citations (23)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB964367A (en) * | 1961-02-06 | 1964-07-22 | Birs Brit Ag | Drying method and device for carrying the said method into effect |
| AU2008201720A1 (en) * | 2002-12-17 | 2008-05-08 | Medimmune, Llc | High pressure spray-dry of bioactive materials |
| WO2014017511A1 (en) * | 2012-07-27 | 2014-01-30 | 株式会社パウダリングジャパン | Liquid-atomizing device and liquid-atomizing method |
| CN203329386U (en) * | 2013-06-19 | 2013-12-11 | 常州市宇通干燥设备有限公司 | Hot air distributor for spray tower |
| EP3124110A1 (en) * | 2015-07-30 | 2017-02-01 | Sanovo Technologies A/S | A process and spray drying apparatus for spray drying products |
| CN105363231A (en) * | 2015-11-28 | 2016-03-02 | 南京威安新材料科技有限公司 | Centrifugal spray drying apparatus capable of preventing catalyst from adhering to walls |
| CN205683848U (en) * | 2016-06-03 | 2016-11-16 | 华夏生生药业(北京)有限公司 | Medicinal liquid is dilute joins circulated filter system |
| CN106039746A (en) * | 2016-08-01 | 2016-10-26 | 扬州日发干燥工程有限公司 | Wall-sticking-proof spraying dryer |
| CN106565460A (en) * | 2016-10-28 | 2017-04-19 | 山东凯翔生物化工股份有限公司 | Method for producing calcium gluconate and production device of method |
| CN206391590U (en) * | 2017-01-11 | 2017-08-11 | 哈尔滨剑桥学院 | A kind of long stroke easy to clean spray dryer |
| CN109276900A (en) * | 2017-07-20 | 2019-01-29 | 鲁娟 | A kind of anti-sticking wall efficient spray drier special nozzle |
| CN210057410U (en) * | 2019-05-29 | 2020-02-14 | 淄博锦源生物科技有限公司 | Device that peptone is dry not caking |
| CN211328190U (en) * | 2019-10-22 | 2020-08-25 | 北京宝德润生医药科技发展有限公司 | Spray drier |
| AU2020100855A4 (en) * | 2019-11-12 | 2020-07-09 | Recom (Qingdao) Biotechnology Co. Ltd | Low-temperature drying and spraying equipment |
| CN211721623U (en) * | 2020-01-14 | 2020-10-23 | 刘伯明 | Agricultural machine spouts medicine machine and spouts medicine liquid reserve tank |
| CN111298464A (en) * | 2020-03-24 | 2020-06-19 | 江苏双林海洋生物药业有限公司 | Drying device is used in preparation of glucosamine sulfate double salt |
| CN111707068A (en) * | 2020-07-02 | 2020-09-25 | 浙江汇翔化学工业有限公司 | Drying equipment for production of polycarboxylate water reducing agent |
| CN215462061U (en) * | 2020-11-26 | 2022-01-11 | 徐州霍斯科技有限公司 | Spray drier |
| CN214344475U (en) * | 2021-01-11 | 2021-10-08 | 南京泛成生物科技有限公司 | Spray drying system |
| CN214714407U (en) * | 2021-04-13 | 2021-11-16 | 秸都科技(南京)有限公司 | High-speed centrifugal spray dryer with uniform spraying |
| CN113750554A (en) * | 2021-10-20 | 2021-12-07 | 福建好家景日化有限公司 | Atomizing, granulating and drying device for daily chemical production |
| CN113856226A (en) * | 2021-10-27 | 2021-12-31 | 山东省绿士农药有限公司 | Dry suspending agent type pesticide production line |
| CN113967441A (en) * | 2021-11-17 | 2022-01-25 | 连云港瑞邦药业有限公司 | Purification and filling device and method for calcium gluconate production |
Non-Patent Citations (1)
| Title |
|---|
| 中药喷雾干燥粘壁原因与解决途径;王瑞等;《临床医药文献杂志》;第5卷(第62期);第193-194页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN114504834A (en) | 2022-05-17 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN114504834B (en) | Calcium gluconate solution purification equipment and process thereof | |
| CN105363231B (en) | It can prevent catalyst from gluing the centrifugal spray drying device of wall | |
| CN117462973A (en) | Spray drying device | |
| CN112352903A (en) | A defatted protein powder processing system for albumen powder production | |
| CN113443913A (en) | Preparation method and production line of alumina ceramic lining plate for jet mill | |
| CN115574567A (en) | Spray drying equipment for protein powder production | |
| CN218793909U (en) | Spray drying device is used in production | |
| CN117463244A (en) | Vacuum atomization pharmaceutical device | |
| CN211358486U (en) | Three-stage centrifugal spray drying device for protein powder | |
| CN100333707C (en) | Spraying and drying process and apparatus for Chinese medicine concentrate | |
| CN214415615U (en) | Spray drying device | |
| CN112619190B (en) | Spray drying equipment for fertilizer production and fertilizer production method | |
| CN114590858A (en) | Novel vertical three-phase evaporative separator for desulfurization waste liquid | |
| CN105363230B (en) | Spray-drying installation for dry catalyst | |
| CN207187141U (en) | A kind of red date powder production spray drying tower | |
| CN209287225U (en) | A kind of spray-dried instrument | |
| CN208003471U (en) | The centrifugal spray drying tower of anti-sticking wall | |
| CN220558550U (en) | Glucosyl stevioside spray drying tower | |
| CN220780952U (en) | Tablet coating liquid spraying device | |
| CN207899004U (en) | The spray-drying installation of Hedysarum polybotrys | |
| CN217119784U (en) | Yeast concentrated solution drying tower | |
| CN221733241U (en) | Energy-saving environment-friendly tower-free granulating system | |
| CN217051694U (en) | Novel vertical three-phase evaporative separator of desulfurization waste liquid | |
| CN216800111U (en) | Intelligent cleaning device | |
| CN218443136U (en) | Drying device is used in production of yeast extract |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |