CN114486609B - Method for detecting segregation degree of asphalt mixture - Google Patents
Method for detecting segregation degree of asphalt mixture Download PDFInfo
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- CN114486609B CN114486609B CN202111576309.1A CN202111576309A CN114486609B CN 114486609 B CN114486609 B CN 114486609B CN 202111576309 A CN202111576309 A CN 202111576309A CN 114486609 B CN114486609 B CN 114486609B
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- asphalt mixture
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- 239000010426 asphalt Substances 0.000 title claims abstract description 93
- 239000000203 mixture Substances 0.000 title claims abstract description 90
- 238000005204 segregation Methods 0.000 title claims abstract description 54
- 238000000034 method Methods 0.000 title claims abstract description 29
- 239000002245 particle Substances 0.000 claims abstract description 50
- 238000005303 weighing Methods 0.000 claims abstract description 12
- 238000001035 drying Methods 0.000 claims abstract description 11
- 238000002791 soaking Methods 0.000 claims abstract description 7
- 238000003756 stirring Methods 0.000 claims abstract description 6
- 239000003960 organic solvent Substances 0.000 claims abstract description 5
- 238000012216 screening Methods 0.000 claims abstract description 4
- 239000000945 filler Substances 0.000 claims description 10
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 8
- 239000011707 mineral Substances 0.000 claims description 8
- 239000000843 powder Substances 0.000 claims description 8
- XSTXAVWGXDQKEL-UHFFFAOYSA-N Trichloroethylene Chemical group ClC=C(Cl)Cl XSTXAVWGXDQKEL-UHFFFAOYSA-N 0.000 claims description 4
- 238000002156 mixing Methods 0.000 claims description 4
- 238000005070 sampling Methods 0.000 claims description 4
- UBOXGVDOUJQMTN-UHFFFAOYSA-N trichloroethylene Natural products ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 claims description 4
- 238000001816 cooling Methods 0.000 claims description 3
- 239000003350 kerosene Substances 0.000 claims description 3
- 238000012360 testing method Methods 0.000 abstract description 10
- 239000011384 asphalt concrete Substances 0.000 abstract description 8
- 238000011002 quantification Methods 0.000 abstract description 3
- 239000004575 stone Substances 0.000 description 11
- 238000001514 detection method Methods 0.000 description 6
- 238000004364 calculation method Methods 0.000 description 3
- 238000010276 construction Methods 0.000 description 3
- 239000011521 glass Substances 0.000 description 3
- 239000000463 material Substances 0.000 description 3
- 239000004568 cement Substances 0.000 description 2
- 238000013461 design Methods 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- 208000024780 Urticaria Diseases 0.000 description 1
- 239000012615 aggregate Substances 0.000 description 1
- 239000000470 constituent Substances 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 238000012113 quantitative test Methods 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N5/00—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
- G01N5/04—Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by removing a component, e.g. by evaporation, and weighing the remainder
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B07—SEPARATING SOLIDS FROM SOLIDS; SORTING
- B07B—SEPARATING SOLIDS FROM SOLIDS BY SIEVING, SCREENING, SIFTING OR BY USING GAS CURRENTS; SEPARATING BY OTHER DRY METHODS APPLICABLE TO BULK MATERIAL, e.g. LOOSE ARTICLES FIT TO BE HANDLED LIKE BULK MATERIAL
- B07B1/00—Sieving, screening, sifting, or sorting solid materials using networks, gratings, grids, or the like
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/02—Devices for withdrawing samples
- G01N1/04—Devices for withdrawing samples in the solid state, e.g. by cutting
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/40—Concentrating samples
- G01N1/4055—Concentrating samples by solubility techniques
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/44—Sample treatment involving radiation, e.g. heat
Landscapes
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Road Paving Structures (AREA)
- Analysing Materials By The Use Of Radiation (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Abstract
The invention provides a method for detecting segregation degree of asphalt mixture, which comprises the following steps: sorting aggregate particles with the particle size of more than or equal to 4.75mm from the sample; soaking the aggregate particles by adopting an organic solvent, and stirring until asphalt in the aggregate particles is completely dissolved; then extracting, drying and weighing, and marking as mass m1; screening, drying and weighing the aggregate particles to obtain aggregate particles with the particle size of more than 2.36mm, weighing and marking the aggregate particles as mass m2; the resolution L, l= ((m 1-m 2)/m 1) 100 is calculated. According to the invention, from the angle of testing the segregation degree quantification of the asphalt mixture, a testing method is provided, and a testing basis is provided for controlling the segregation of the asphalt mixture, so that the working performance of the asphalt mixture is improved, and the quality of an asphalt concrete finished product is further ensured.
Description
Technical Field
The invention relates to the technical field of highway engineering materials, in particular to a method for detecting segregation degree of asphalt mixture.
Background
Asphalt mixture is a widely applied material for pavement, road performance of asphalt concrete is closely related to working performance (construction workability) of asphalt mixture, the asphalt mixture is composed of coarse and fine aggregates, filler, asphalt cement and the like, before asphalt concrete is formed, hot-mix asphalt mixture is in a loose and certain cohesiveness state after being mixed, and due to the characteristics of asphalt mixture composition, problems of coarse and fine segregation, temperature segregation and the like of the asphalt mixture can occur if the mixing proportion is improperly designed or construction is improperly controlled in the construction process, the segregation can cause larger deviation of uniformity of a formed asphalt concrete pavement structure, deformation resistance, rutting resistance, water damage resistance and fatigue performance of asphalt concrete are influenced, and damage to the performance of the asphalt concrete pavement structure can be aggravated along with the increase of asphalt mixture segregation degree.
The control of the working performance of asphalt mixtures in a good state is a common problem faced by the majority of asphalt pavement technicians, but for testing the working performance-segregation degree of asphalt mixtures, a quantitative test method is lacking.
Disclosure of Invention
In order to solve the problems, the main purpose of the invention is to provide a detection method for the segregation degree of asphalt mixture, which provides a test basis for controlling the segregation of asphalt mixture, thereby improving the working performance of asphalt mixture and further ensuring the quality of asphalt concrete finished products.
In order to achieve the above purpose, the invention provides a method for detecting segregation degree of asphalt mixture.
The method for detecting the segregation degree of the asphalt mixture comprises the following steps:
sorting aggregate particles with the particle size of more than or equal to 4.75mm from the sample;
soaking the aggregate particles by adopting an organic solvent, and stirring until asphalt in the aggregate particles is completely dissolved; then extracting, drying and weighing, and marking as mass m1;
screening, drying and weighing the aggregate particles to obtain aggregate particles with the particle size of more than 2.36mm, weighing and marking the aggregate particles as mass m2;
the resolution L, l= ((m 1-m 2)/m 1) 100 is calculated.
Further, sampling the asphalt mixture according to a quartering method to obtain a sample; wherein the asphalt mixture is a fine-grain type, medium-grain type or coarse-grain type mixture.
Further, the asphalt mixture is a fine-grain mixture, and is prepared by mixing coarse aggregate, fine aggregate, mineral powder filler and asphalt at 130-170 ℃ and cooling to room temperature.
Further, the coarse aggregate is formed by combining a first-grain-size coarse aggregate, a second-grain-size coarse aggregate and a third-grain-size coarse aggregate;
wherein the particle sizes of the first particle size coarse aggregate, the second particle size coarse aggregate and the third particle size coarse aggregate are 10-15 mm, 6-10 mm and 3-6 mm in sequence.
Further, in the asphalt mixture, the mass percentage of the first particle size coarse aggregate, the second particle size coarse aggregate and the third particle size coarse aggregate is 15-25%, 17-30% and 13-25% in sequence.
Further, the grain diameter of the fine aggregate is below 2.36mm, and the mass percentage of the fine aggregate in the asphalt mixture is 26-36%.
Further, the mass percentage of the mineral powder filler in the asphalt mixture is 2-6%, and the mass percentage of the asphalt is 3.84-5.66%.
Further, the mass of the sample is 1000-1500 g.
Furthermore, the organic solvent is trichloroethylene solution or kerosene, and the soaking time is more than or equal to 30min.
Further, the drying temperature is 105+/-5 ℃ and the drying time is 3-5 hours.
According to the invention, from the angle of testing the segregation degree quantification of the asphalt mixture, a testing method is provided, and a testing basis is provided for controlling the segregation of the asphalt mixture, so that the working performance of the asphalt mixture is improved, and the quality of an asphalt concrete finished product is further ensured.
The detection method is simple and quick, and can indirectly judge whether the oil-stone ratio of the asphalt mixture is in the optimal value range by detecting the segregation degree, thereby providing guidance for the practical application of the asphalt mixture.
Drawings
Various other advantages and benefits will become apparent to those of ordinary skill in the art upon reading the following detailed description of the preferred embodiments. The drawings are only for purposes of illustrating the preferred embodiments and are not to be construed as limiting the invention. Also, like reference numerals are used to designate like parts throughout the figures. In the drawings:
fig. 1 is a schematic flow chart of a method for detecting segregation degree of asphalt mixture according to an embodiment of the invention.
Detailed Description
Exemplary embodiments of the present disclosure will be described in more detail below with reference to the accompanying drawings. While exemplary embodiments of the present disclosure are shown in the drawings, it should be understood that the present disclosure may be embodied in various forms and should not be limited to the embodiments set forth herein. Rather, these embodiments are provided so that this disclosure will be thorough and complete, and will fully convey the scope of the disclosure to those skilled in the art.
The invention designs a quantification method for testing the segregation degree of asphalt mixture by utilizing the adhesiveness of asphalt cement at high temperature (130-170 ℃), the thickness of oil film coated on the surfaces of crushed stone and filler in the mixture, and the like.
As shown in fig. 1, the method for detecting the segregation degree of the asphalt mixture comprises the following steps:
sampling the asphalt mixture according to a quartering method to obtain a sample; wherein the mass of the sample is in the range of 1000-1500 g.
The asphalt mixture can be a fine-grain type, medium-grain type or coarse-grain type mixture, and the fine-grain type mixture can be AC-10 or AC-13 asphalt mixture; the medium particle type mixture can be, for example, an AC-16 and AC-20 asphalt mixture; the coarse-grained mixture may be, for example, an AC-25, AC-30 asphalt mixture. When a fine-grained mix is used, the mass of the sample may be 1000g; when a medium particle type mixture is used, the mass of the sample may be 1200g; when a coarse-grain mix is used, the mass of the sample may be 1500g.
In the embodiment of the invention, the AC-13 fine-grain mixture is adopted, and specifically, coarse aggregate, fine aggregate, mineral powder filler and asphalt are mixed at 130-170 ℃ and cooled to room temperature to prepare the asphalt.
Wherein the coarse aggregate is formed by combining a first-grain-size coarse aggregate, a second-grain-size coarse aggregate and a third-grain-size coarse aggregate.
The grain sizes of the first grain size coarse aggregate, the second grain size coarse aggregate and the third grain size coarse aggregate are 10-15 mm, 6-10 mm and 3-6 mm in sequence.
The mass percentage of the first grain size coarse aggregate, the second grain size coarse aggregate and the third grain size coarse aggregate is 15-25%, 17-30% and 13-25% in sequence.
The grain diameter of the fine aggregate is below 2.36mm, and the mass percentage of the fine aggregate is 26-36%.
The mass percentage of the mineral powder filler is 2-6%.
The mass percentage of the asphalt is 3.84-5.66%.
Sorting aggregate particles with the particle size of more than or equal to 4.75mm from the sample; note that during sorting, the action is gentle, avoiding the falling off of fine aggregates adhering to the aggregate particles.
Soaking coarse aggregate particles in trichloroethylene solution or kerosene for more than or equal to 30min, and properly stirring with a glass rod until asphalt is completely dissolved, wherein no asphalt is on the surface of the aggregate.
The aggregate is extracted and dried for 3 to 5 hours at the temperature of 105+/-5 ℃ and weighed and recorded as the mass m1.
And screening, drying and weighing the aggregate particles to obtain aggregate particles with the particle size of more than 2.36mm, and weighing the aggregate particles and marking the aggregate particles as mass m2.
The resolution L, l= ((m 1-m 2)/m 1) 100 is calculated.
Generally, the larger the segregation L value, the better the segregation resistance of the asphalt mixture.
However, the segregation degree L has an upper limit value, the maximum asphalt dosage of the mixture is measured according to the maximum asphalt dosage test method of the asphalt mixture, then the asphalt mixture is obtained by stirring the maximum asphalt dosage, and finally the segregation degree L obtained by the measurement method is the upper limit value.
The optimal oil-stone ratio of the asphalt mixture corresponds to the optimal segregation degree, and whether the oil-stone ratio of the asphalt mixture is within the optimal range value can be indirectly judged by detecting the segregation degree of the asphalt mixture. And for a certain asphalt mixture, the optimal oil-stone ratio of the asphalt mixture needs to be determined according to a mix proportion design method, and the corresponding segregation degree L is the optimal range value of the asphalt mixture within the fluctuation range (plus or minus 0.3%) of the optimal oil-stone ratio.
Hereinafter, a method for detecting the segregation degree of asphalt mixture according to the present invention will be described in detail by way of specific examples.
Example 1:
1. taking a stirred fine-grained asphalt mixture meeting the requirement of mixing temperature (130-170 ℃), dividing samples by a quarter method, diagonally taking two samples, and sampling 1000g of mass.
2. Placing the sample into a clean stainless steel square plate, spreading the mixture by a shovel to form a thin layer with separated aggregate and no overlapping, and cooling to room temperature.
3. Aggregate particles having a particle size above 4.75mm were sorted from the cooled samples.
4. Placing the sorted aggregate particles into a glass beaker, soaking for 30min with trichloroethylene, stirring with a glass rod to dissolve asphalt, and separating fine aggregate from the surface of the aggregate; then extracting, drying at 105 ℃ for 3 hours, weighing and marking the mass as m1.
5. The dried and weighed mixture is sieved by a square sieve with 2.36mm, and the broken stone remained on the sieve is weighed, and the mass is recorded as m2.
6. To ensure accuracy, the above test was performed in parallel twice, the degree of resolution was calculated, the degree of resolution was noted as L, the calculation formula l= ((m 1-m 2)/m 1) 100, and the result of the two calculations could not exceed 3% of the average.
In the invention, the segregation degree L represents asphalt adhered to coarse aggregates, fine aggregates below 2.36mm and mineral powder filler, and the segregation degree L accounts for the mass proportion of the total asphalt mixture.
Examples 2 to 3 used the same test method as example 1, except that the mass percentages of coarse aggregate, fine aggregate, mineral powder filler and asphalt in the asphalt mixture, the oil-stone ratio and the process parameters in each step were different. The parameters of each step in the detection methods of examples 1 to 3 are summarized in tables 1 to 2.
Table 1 summary of the respective constituent materials of the asphalt mixtures in examples 1 to 3
Table 2 summary of process parameters in the detection methods of examples 1 to 3
Meanwhile, the segregation degree L is calculated according to the detection method in the embodiments 1-3, the oilstone ratio in the embodiments 1-3 is calculated by adopting the conventional calculation method in industry, and the result is shown in Table 3 in detail.
TABLE 3 summary of results for the oil-to-stone ratios and segregation degree in examples 1 to 3
Group of | Wheal ratio (%) | Degree of segregation L |
Example 1 | 4.0 | 15.8 |
Example 2 | 5.3 | 32.3 |
Example 3 | 5.6 | 34 |
As can be seen from table 3, the segregation degree L is obtained by the detection method in the present invention, and whether the asphalt mixture has an oil-stone ratio within the optimum value range is indirectly judged by the segregation degree L. If the whetstone ratio of 5.3% in example 2 was found to be the optimum value, the corresponding degree of segregation L32.3 was the optimum degree of segregation, and the range value (27-34) of the corresponding degree of segregation L in the range of 5.0-5.6% of whetstone ratio was further obtained as the preferred degree of segregation (the preferred range value of 32.4, corresponding to the whetstone ratio of 5.0-5.6%).
It is also apparent from the combination of example 1 and example 3 that the whetstone ratio in example 1 is 4.0%, and the segregation degree L15.2 is detected to be lower than the value of the preferable segregation degree range, which means that the segregation degree L is lower and the asphalt content is lower; the oil-stone ratio in example 3 was 5.6%, and the segregation degree L34, which is the upper limit value of the segregation degree range value and above which the asphalt content in the mixture was higher, was detected.
The present invention is not limited to the above-mentioned embodiments, and any changes or substitutions that can be easily understood by those skilled in the art within the technical scope of the present invention are intended to be included in the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the claims.
Claims (10)
1. The method for detecting the segregation degree of the asphalt mixture is characterized by comprising the following steps of:
sorting aggregate particles with the particle size of more than or equal to 4.75mm from the sample;
soaking the aggregate particles by adopting an organic solvent, and stirring until asphalt in the aggregate particles is completely dissolved; then extracting, drying and weighing, and marking as mass m1;
screening, drying and weighing the aggregate particles to obtain aggregate particles with the particle size of more than 2.36mm, weighing and marking the aggregate particles as mass m2;
the resolution L, l= ((m 1-m 2)/m 1) 100 is calculated.
2. The method for detecting segregation degree of asphalt mixture according to claim 1, wherein the sample is obtained by sampling asphalt mixture by a quarter method; wherein the asphalt mixture is a fine-grain type, medium-grain type or coarse-grain type mixture.
3. The method for detecting the segregation degree of the asphalt mixture according to claim 1 or 2, wherein the asphalt mixture is a fine-grained mixture, and is prepared by mixing coarse aggregate, fine aggregate, mineral powder filler and asphalt at 130-170 ℃ and cooling to room temperature.
4. The method for detecting segregation degree of asphalt mixture according to claim 3, wherein the coarse aggregate is formed by combining a first-particle-size coarse aggregate, a second-particle-size coarse aggregate and a third-particle-size coarse aggregate;
wherein the particle sizes of the first particle size coarse aggregate, the second particle size coarse aggregate and the third particle size coarse aggregate are 10-15 mm, 6-10 mm and 3-6 mm in sequence.
5. The method according to claim 4, wherein the mass percentages of the first, second, and third coarse aggregates in the asphalt mixture are 15 to 25%, 17 to 30%, and 13 to 25% in this order.
6. The method for detecting the segregation degree of asphalt mixture according to claim 3, wherein the particle diameter of the fine aggregate is 2.36mm or less, and the mass percentage of the fine aggregate in the asphalt mixture is 26 to 36%.
7. The method for detecting segregation degree of asphalt mixture according to claim 3, wherein the mass percentage of the mineral powder filler in the asphalt mixture is 2-6%, and the mass percentage of the asphalt is 3.84-5.66%.
8. The method for detecting the segregation degree of asphalt mixture according to claim 1, wherein the mass of the sample is 1000 to 1500g.
9. The method for detecting the segregation degree of asphalt mixture according to claim 1, wherein the organic solvent is trichloroethylene solution or kerosene, and the soaking time is not less than 30min.
10. The method for detecting segregation degree of asphalt mixture according to claim 1, wherein the drying temperature is 105±5 ℃ for 3 to 5 hours.
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CN202111576309.1A CN114486609B (en) | 2021-12-21 | 2021-12-21 | Method for detecting segregation degree of asphalt mixture |
PCT/CN2022/096258 WO2023115827A1 (en) | 2021-12-21 | 2022-05-31 | Method for detecting segregation degree of asphalt mixture |
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CN114486609B (en) * | 2021-12-21 | 2024-02-09 | 中交一公局集团有限公司 | Method for detecting segregation degree of asphalt mixture |
CN114563339B (en) * | 2022-03-29 | 2024-07-23 | 武汉理工大学 | Rapid detection method for coal gangue aggregate weathering in service state and application thereof |
CN117218126B (en) * | 2023-11-09 | 2024-02-13 | 安徽省交通规划设计研究总院股份有限公司 | Asphalt mixture uniformity calculation method in image processing vision field |
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