CN114456020B - Transition layer material, application and process for improving internal stress of warhead charge - Google Patents

Transition layer material, application and process for improving internal stress of warhead charge Download PDF

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CN114456020B
CN114456020B CN202111613733.9A CN202111613733A CN114456020B CN 114456020 B CN114456020 B CN 114456020B CN 202111613733 A CN202111613733 A CN 202111613733A CN 114456020 B CN114456020 B CN 114456020B
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transition layer
warhead
layer material
shaped structure
explosive
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CN114456020A (en
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刁小强
陶俊
王晓峰
徐洪涛
方学谦
戴致鑫
邢晓玲
韩仲熙
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Xian Modern Chemistry Research Institute
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    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B27/00—Compositions containing a metal, boron, silicon, selenium or tellurium or mixtures, intercompounds or hydrides thereof, and hydrocarbons or halogenated hydrocarbons
    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B23/00—Compositions characterised by non-explosive or non-thermic constituents
    • C—CHEMISTRY; METALLURGY
    • C06—EXPLOSIVES; MATCHES
    • C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
    • C06B25/00—Compositions containing a nitrated organic compound
    • C06B25/34—Compositions containing a nitrated organic compound the compound being a nitrated acyclic, alicyclic or heterocyclic amine
    • F—MECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F42—AMMUNITION; BLASTING
    • F42B—EXPLOSIVE CHARGES, e.g. FOR BLASTING, FIREWORKS, AMMUNITION
    • F42B33/00—Manufacture of ammunition; Dismantling of ammunition; Apparatus therefor
    • F42B33/02—Filling cartridges, missiles, or fuzes; Inserting propellant or explosive charges
    • F42B33/025—Filling cartridges, missiles, or fuzes; Inserting propellant or explosive charges by compacting

Abstract

The invention discloses a transition layer material, application and a process for improving internal stress of warhead charge, which comprises the following raw material components: 10-30% of composite modified material and 70-90% of metal powder in percentage by mass; the composite modified material consists of butadiene rubber and ethylene-vinyl acetate copolymer in the mass ratio of (1-5) to 1; the metal powder is ball-milled aluminum powder with the particle size of 40-60 mu m. The transition layer material is a composite modified material consisting of butadiene rubber and ethylene-vinyl acetate copolymer, and ball-milled aluminum powder, which are common materials for mixed explosives, have wide sources and good compatibility with explosives and shells; the transition layer material has the characteristics of small modulus and easy compression deformation, and can effectively reduce the internal stress of the explosive charge generated in the temperature test process of the warhead part with the special-shaped structure; thereby achieving the purpose of reducing or eliminating the defects of charging. The explosive is suitable for high-quality explosive charging of mixed explosives in the body of the special-shaped structure bullet.

Description

Transition layer material, application and process for improving internal stress of warhead charge
Technical Field
The invention relates to a transition layer material which can be used for filling the bottom of a warhead with a special-shaped structure and can effectively improve the internal stress of the warhead when compared with the warhead powder charge without the transition layer.
Background
For the warhead with the special-shaped structure, particularly the warhead with the small mouth and big belly type explosive-killing ammunition is taken as a typical example, after the warhead is charged through a high-temperature test, the warhead often has charging defects such as bottom clearance or cracks. The reason for this is that: in the heating process of the projectile body, the explosive charge is subjected to thermal expansion, the internal expansion stress of the explosive charge reaches more than dozens of MPa, the cushion layer is subjected to compression deformation under the action of the cushion layer on the top of the projectile body, and meanwhile, the explosive charge moves upwards relative to the shell inside the projectile body. When the ambient temperature drops, the explosive charge shrinks from a thermal expansion state, the explosive charge cannot be recovered due to the fact that the expanded explosive charge is clamped at the top of the bomb body, and the shrinkage stress inside the explosive charge is transmitted layer by layer from top to bottom, so that the explosive charge defects are generated finally, if bottom gaps occur at the bottom or cracks occur locally. The charging defects can cause the bore explosion in the blasting process, and bring serious potential safety hazards to the firing safety of the ammunition. Therefore, the reduction of the internal stress generated in the temperature test process of the elastomer charge is an important means for improving the defect generation of the charge.
Disclosure of Invention
Aiming at the technical problems, the invention provides a transition layer material for improving the internal stress of the warhead charge with the special-shaped structure.
In order to achieve the purpose, the invention discloses the following technical scheme:
a transition layer material comprises the following raw material components: the composite modified material comprises 10-30% of composite modified material and 70-90% of metal powder in percentage by mass;
the composite modified material consists of butadiene rubber and ethylene-vinyl acetate copolymer in the mass ratio of (1-5) to 1;
the metal powder is ball-milled aluminum powder with the particle size of 40-60 mu m.
Further, the feed comprises the following raw material components: the composite modified material comprises 20% of composite modified material and 80% of metal powder in percentage by mass;
the composite modified material consists of butadiene rubber and ethylene-vinyl acetate copolymer in a mass ratio of 3:1.
The invention also discloses application of the transition layer material in improving the internal stress of the warhead charge with the special-shaped structure.
Furthermore, the diameter phi 1 of the mouth part of the warhead part with the special-shaped structure is 40-80 mm, the diameter phi 2 of the bottom part of the warhead part is 80-120 mm, and the height of the warhead part is 150-300 mm.
The invention relates to a process for improving the internal stress of a warhead charge with a special-shaped structure by adopting a transition layer material, which comprises the following steps:
selecting a special-shaped structure warhead simulating bomb with the mouth diameter phi 1 of 40-80 mm, the bottom diameter phi 2 of 80-120 mm and the height of 150-300 mm, and assembling a pressure sensor at the mouth of the body of the special-shaped structure warhead simulating bomb and the bottom of the special-shaped structure warhead simulating bomb; and then putting 40-200 g of the transition layer material at the bottom of the specially-shaped structure warhead simulated bomb, and carrying out RL-F explosive charging by adopting a fractional pressing process, wherein the pressing process parameters are as follows: pressing at 150MPa for five times, and controlling the final average charge density to be 1.65-1.75 g/cm 3 。
Further, the transition layer material comprises the following raw material components: by mass percentage, 20% of composite modified material and 80% of metal powder;
the composite modified material is composed of butadiene rubber and ethylene-vinyl acetate copolymer according to a mass ratio of 3:1, and the metal powder is FLQ A aluminum powder.
Specifically, the RL-F explosive comprises 78.5% of passivated hexogen, 20% of aluminum powder and 1.5% of ethylene-vinyl acetate copolymer in percentage by mass.
Compared with the prior art, the invention has the following technical effects:
the transition layer material is a composite modified material consisting of the selected butadiene rubber and the ethylene-vinyl acetate copolymer (EVA resin), and ball-milled aluminum powder, which are common mixed explosive materials, have wide sources and good compatibility with explosives and shells;
the transition layer material has the characteristics of small modulus and easy compression deformation, and can effectively reduce the internal stress of the explosive charge generated in the temperature test process of the warhead part with the special-shaped structure; thereby achieving the purpose of reducing or eliminating the defects of charging;
the content of the spherical grinding aluminum powder in the transition layer material is adjusted to enable the spherical grinding aluminum powder to reach or approach the actual charging density, and the misjudgment of the result during flaw detection due to too low and too high density is avoided.
The present invention will be described in further detail with reference to specific embodiments.
Drawings
FIG. 1 shows a simulated bomb with a special-shaped structure of a small mouth and big belly for test;
FIG. 2 shows the stress real-time measurement results of the temperature test process without adding a transition layer in example 1;
FIG. 3 shows the stress real-time measurement results of the temperature test process of example 1 with the addition of the transition layer;
FIG. 4 shows the stress real-time measurement results of the temperature test process without the addition of the transition layer in example 2;
FIG. 5 shows the stress real-time measurement results of the temperature test process of example 2 with the addition of the transition layer.
Detailed Description
Any modification of the structure, change of the ratio or adjustment of the size of the structure should still fall within the scope of the present disclosure without affecting the function and the purpose of the present disclosure.
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is described in further detail below with reference to the accompanying drawings and embodiments. It should be understood that the embodiments described herein are only for illustrating the present invention and are not to be considered as limiting the present invention, and all equivalent modifications made on the basis of the technical solutions of the present application are included in the scope of the present invention.
According to the invention, the transition material which is compatible with the explosive and the shell material, has a charge density close to that of the explosive, has a small modulus and is easy to compress and deform is added at the bottom of the inner part of the bomb body, so that the internal stress generated by the bomb body in the temperature test process is reduced, and the purpose of improving the charge defect is achieved. In the embodiment, RL-F explosive is adopted, the simulation bomb with the special-shaped structure of small belly is used for carrying out fractional compression charging forming, sensors are arranged at the top and the bottom of the simulation bomb, the stress generated by charging in the temperature experiment process is measured in real time, and the stress generated after a transition layer material is not filled and the stress generated after the transition layer material is filled are compared.
The experimental reagents used in the present invention are commercially available.
The invention discloses a transition layer material which comprises the following raw material components: by mass percentage, 10-30% of composite modified material and 70-90% of metal powder;
wherein the composite modified material consists of butadiene rubber and ethylene-vinyl acetate copolymer in a mass ratio of (1-5) to 1;
the metal powder is ball-milled aluminum powder with the particle size of 40-60 mu m.
The composite material is adopted to improve the strength of the material, pure butadiene rubber is soft, and ethylene-vinyl acetate copolymer is hard; the metal powder is ball-milled aluminum powder, the specification of the aluminum powder adopted in the embodiment is FLQ A, the granularity D50 of the aluminum powder is about 50 micrometers, the aluminum powder is selected according to the principle that the specification of the aluminum powder is consistent with that of the explosive (RL-F explosive in the embodiment) used for charging, different explosives are selected for charging, and the specification of the aluminum powder adopted in the transition layer is changed accordingly. The aim of adding the aluminum powder is to adjust the density of the transition layer material to be consistent with the actual charging density (the density of the composite modified material is lower), and to adjust the strength of the whole material;
the preparation method of the transition layer material comprises the following steps: adding butadiene rubber and ethylene-vinyl acetate copolymer into a beaker, adding a proper amount of petroleum ether solvent, heating, stirring and dissolving, adding aluminum powder after complete dissolution, uniformly stirring and mixing, pouring out from the beaker, and sieving by a sieve of 8-12 meshes or a granulator to prepare granular materials for later use after the solvent volatile materials are in a mud cluster or thick mud shape.
With reference to the attached drawing 1, the process for improving the internal stress of the shaped warhead charge by using the transition layer material comprises the following steps:
selecting a special-shaped structure warhead simulated bomb with the mouth diameter phi 1 of 40-80 mm, the bottom diameter phi 2 of 80-120 mm and the height of 150-300 mm, and putting the simulated bomb in the warhead simulated bombPressure sensors are assembled at the mouth part of the warhead simulating bomb with the special-shaped structure and the bottom part of the warhead simulating bomb with the special-shaped structure; and then putting 40-200 g (not more than 5% of the whole charge mass) of the transition layer material at the bottom of the specially-shaped structure warhead simulated bomb, and carrying out RL-F explosive charge by adopting a fractional pressing process, wherein the pressing process parameters are as follows: pressing at 150MPa for five times, and controlling the final average charge density to be 1.65-1.75 g/cm 3 And is generally 1.7g/cm 3 。
The amount of transition layer material is selected as follows: the influence on the explosive power is not reduced as much as possible, and the mass of the transition layer as an inert material is not more than 5% of the whole elastic loading. The whole-bullet explosive loading refers to the total explosive loading comprising a transition layer material and an explosive.
Example 1:
the embodiment discloses a transition layer material, which comprises the following raw material components: by mass percentage, 20% of composite modified material and 80% of metal powder; the composite modified material is composed of butadiene rubber and ethylene-vinyl acetate copolymer in a mass ratio of 3:1.
The embodiment discloses application of a transition layer material for improving internal stress of a shaped structure warhead charge.
Further, the process for improving the internal stress of the warhead charge with the special-shaped structure by adopting the transition layer material comprises the following steps:
with reference to the attached drawing 1, a specially-shaped structure warhead simulating bomb with the mouth diameter phi 1 of 40mm, the bottom diameter phi 2 of 80mm and the height of 150mm is selected, and a pressure sensor is assembled at the mouth of a body of the specially-shaped structure warhead simulating bomb and at the bottom of the specially-shaped structure warhead simulating bomb; and then, putting 40g of the transition layer material at the bottom of the specially-shaped structure warhead simulated bomb, and carrying out RL-F explosive charging by adopting a fractional pressing process, wherein the pressing process parameters are as follows: pressing under 150Mpa for five times, wherein the explosive amount of the explosive pressed for the first three times is 250g, the explosive amount of the explosive pressed for the second two times is 125g, and the final average charge density is controlled to be 1.7g/cm 3 . The total drug loading in the examples is 1000g.
The transition layer material selected in this embodiment includes the following raw material components: by mass percentage, 20% of composite modified material and 80% of metal powder; the composite modified material is composed of butadiene rubber and ethylene-vinyl acetate copolymer according to a mass ratio of 3:1, and the metal powder is FLQ A aluminum powder.
The RL-F explosive comprises 78.5 percent of passivated hexogen, 20 percent of aluminum powder and 1.5 percent of ethylene-vinyl acetate copolymer by mass percent.
In this example, the bottom of the sample is not filled with a transition layer material as a control group, and then RL-F explosive charging is directly performed by a fractional pressing process, wherein the process parameters are as follows: pressing at 150Mpa for five times, and controlling final average charge density to 1.70g/cm 3 ；
And (3) carrying out high-temperature test on the two loaded simulated bombs at the same time: raising the temperature to 65 ℃ for heat preservation, naturally cooling to room temperature, measuring the pressure of the medicine loading internal stress fed back to the top and the bottom in real time in the temperature test process, and comparing the maximum values of the top pressure and the bottom pressure, wherein the results are shown in table 1:
TABLE 1 comparison of internal stresses before and after addition of transition layer
Figure BDA0003435861350000071
It can be seen that after the transition layer material is adopted to fill a simulated bomb, in the temperature experiment process, the charging of the transition layer is added, and the maximum top stress and the maximum bottom stress fed back by the generated internal stress are both obviously smaller than the charging without the transition layer.
It can be seen from the graphs of fig. 2 and 3 that the slope of the curve is significantly relaxed after the addition of the transition layer, indicating that the pressure rise process is slowed down. The peak value reduction and slope slowing are beneficial to reducing the internal stress of the warhead with the special-shaped structure and improving the charging defects.
Example 2
In the embodiment, the abnormal-shaped structure warhead simulating bomb with the diameter phi 1 of 80mm, the diameter phi 2 of the bottom of 120mm and the height of 300mm is selected, and the pressure sensor is assembled at the mouth of the body of the abnormal-shaped structure warhead simulating bomb and the bottom of the abnormal-shaped structure warhead simulating bomb; then is different in200g of the transition layer material is placed at the bottom of the simulated warhead with the shaped structure, RL-F explosive charging is carried out by adopting a fractional pressing process, and the pressing process parameters are as follows: pressing under 150Mpa for five times, wherein the explosive amount of the explosive pressed for the first three times is 1200g, the explosive pressed for the second two times is 700g, and the final average charge density is controlled to be 1.7g/cm 3 . The total drug loading in the examples was 5000g.
The transition layer material selected in this embodiment includes the following raw material components: 15% of composite modified material and 85% of metal powder in percentage by mass; the composite modified material is composed of butadiene rubber and ethylene-vinyl acetate copolymer according to a mass ratio of 4:1, and the metal powder is FLQ A aluminum powder.
In this example, the bottom of the sample is not filled with a transition layer material as a control group, and then RL-F explosive charging is directly performed by a fractional pressing process, wherein the process parameters are as follows: pressing at 150Mpa for five times, and controlling final average charge density to 1.70g/cm 3 ；
And (3) carrying out high-temperature test on the two loaded simulated bombs at the same time: raising the temperature to 65 ℃, preserving the heat, naturally cooling to room temperature, measuring the pressure of medicine loading internal stress fed back to the top and the bottom in real time in the temperature test process, and comparing the maximum values of the top and the bottom pressure, wherein the results are shown in table 2:
TABLE 2 comparison of internal stress before and after addition of transition layer
Figure BDA0003435861350000081
It can be seen that after the transition layer material is adopted to fill a simulated bomb, in the temperature experiment process, the charging of the transition layer is added, and the maximum top stress and the maximum bottom stress fed back by the generated internal stress are both obviously smaller than the charging without the transition layer.
It can also be seen from the graphs of fig. 4 and 5 that the slope of the curve is significantly more gradual after the addition of the transition layer, indicating a slower pressure rise at the top and bottom of the warhead. The peak value reduction and slope slowing are beneficial to reducing the internal stress of the warhead with the special-shaped structure and improving the integral charging defect.
The objects, technical solutions and advantages of the present invention are further described in the above embodiments, it should be noted that the above embodiments are merely preferred embodiments of the present invention, and are not intended to limit the present invention, and any modifications, equivalent substitutions and improvements made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
The preferred embodiments of the present disclosure are described in detail with reference to the accompanying drawings, however, the present disclosure is not limited to the specific details of the above embodiments, and various simple modifications may be made to the technical solution of the present disclosure within the technical idea of the present disclosure, and these simple modifications all belong to the protection scope of the present disclosure.
It should be noted that, in the foregoing embodiments, various features described in the above embodiments may be combined in any suitable manner, and in order to avoid unnecessary repetition, various combinations that are possible in the present disclosure are not described again.
In addition, any combination of the various embodiments of the present disclosure can be made, and the same should be considered as the inventive content of the present disclosure, as long as the idea of the present disclosure is not violated.

Claims (3)

1. The utility model provides an adopt transition layer material to improve heterotypic structure warhead powder charge internal stress's technology which characterized in that includes:
selecting a special-shaped structure warhead simulated bomb with the diameter phi 1 of 40-80mm, the diameter phi 2 of the bottom of 80-120mm and the height of 150-300mm, and assembling a pressure sensor at the mouth of the body of the special-shaped structure warhead simulated bomb and the bottom of the special-shaped structure warhead simulated bomb; and then putting 40 to 200g of the transition layer material at the bottom of the warhead simulated bomb with the special-shaped structure, and filling RL-F explosive by adopting a fractional pressing process, wherein the pressing process parameters are as follows: pressing for five times under the pressure of 150Mpa, and controlling the final average charge density to be 1.65 to 1.75g/cm 3 ;
The transition layer material comprises 10-30% of composite modified material and 70-90% of metal powder in percentage by mass, the composite modified material consists of butadiene rubber and ethylene-vinyl acetate copolymer in a mass ratio of (1~5): 1, and the metal powder is ball-milled aluminum powder with the particle size of 40-60 mu m.
2. The process of claim 1, wherein the transition layer material comprises the following raw material components: by mass percentage, 20% of composite modified material and 80% of metal powder;
the composite modified material is composed of butadiene rubber and ethylene-vinyl acetate copolymer according to a mass ratio of 3:1, and the metal powder is FLQ A aluminum powder.
3. The process of claim 1, wherein the RL-F explosive comprises 78.5% by mass of passivated hexogen, 20% by mass of aluminum powder and 1.5% by mass of ethylene-vinyl acetate copolymer.
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US6737158B1 (en) * 2002-10-30 2004-05-18 Gore Enterprise Holdings, Inc. Porous polymeric membrane toughened composites
US8894783B2 (en) * 2003-03-07 2014-11-25 The United States Of America As Represented By The Secretary Of The Navy Metal augmented charge
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