CN114276017A - Flocking-imitating glazed ceramic and preparation method thereof - Google Patents
Flocking-imitating glazed ceramic and preparation method thereof Download PDFInfo
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- CN114276017A CN114276017A CN202210040361.3A CN202210040361A CN114276017A CN 114276017 A CN114276017 A CN 114276017A CN 202210040361 A CN202210040361 A CN 202210040361A CN 114276017 A CN114276017 A CN 114276017A
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- 239000000919 ceramic Substances 0.000 title claims abstract description 22
- 238000002360 preparation method Methods 0.000 title claims abstract description 15
- 239000002689 soil Substances 0.000 claims abstract description 45
- 239000013078 crystal Substances 0.000 claims abstract description 30
- 239000010453 quartz Substances 0.000 claims abstract description 28
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 28
- 239000002994 raw material Substances 0.000 claims abstract description 27
- 229910052661 anorthite Inorganic materials 0.000 claims abstract description 15
- GWWPLLOVYSCJIO-UHFFFAOYSA-N dialuminum;calcium;disilicate Chemical compound [Al+3].[Al+3].[Ca+2].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-] GWWPLLOVYSCJIO-UHFFFAOYSA-N 0.000 claims abstract description 15
- QORWJWZARLRLPR-UHFFFAOYSA-H tricalcium bis(phosphate) Chemical compound [Ca+2].[Ca+2].[Ca+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O QORWJWZARLRLPR-UHFFFAOYSA-H 0.000 claims abstract description 15
- 239000010433 feldspar Substances 0.000 claims abstract description 13
- 229910052611 pyroxene Inorganic materials 0.000 claims abstract description 13
- 239000000126 substance Substances 0.000 claims abstract description 13
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 10
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical group [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000011019 hematite Substances 0.000 claims abstract description 10
- 229910052595 hematite Inorganic materials 0.000 claims abstract description 10
- LIKBJVNGSGBSGK-UHFFFAOYSA-N iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Fe+3].[Fe+3] LIKBJVNGSGBSGK-UHFFFAOYSA-N 0.000 claims abstract description 10
- 238000001816 cooling Methods 0.000 claims abstract description 8
- 238000000034 method Methods 0.000 claims abstract description 8
- 230000000694 effects Effects 0.000 claims abstract description 7
- 238000000354 decomposition reaction Methods 0.000 claims abstract description 5
- 229910052742 iron Inorganic materials 0.000 claims abstract description 5
- 241000196324 Embryophyta Species 0.000 claims description 17
- 239000005995 Aluminium silicate Substances 0.000 claims description 15
- 235000012211 aluminium silicate Nutrition 0.000 claims description 15
- DLHONNLASJQAHX-UHFFFAOYSA-N aluminum;potassium;oxygen(2-);silicon(4+) Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[O-2].[Al+3].[Si+4].[Si+4].[Si+4].[K+] DLHONNLASJQAHX-UHFFFAOYSA-N 0.000 claims description 15
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 15
- 238000010304 firing Methods 0.000 claims description 11
- 238000010438 heat treatment Methods 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 5
- 235000010086 Setaria viridis var. viridis Nutrition 0.000 claims description 3
- 229910002114 biscuit porcelain Inorganic materials 0.000 claims description 3
- 235000015895 biscuits Nutrition 0.000 claims description 3
- 238000007598 dipping method Methods 0.000 claims description 3
- 238000002156 mixing Methods 0.000 claims description 3
- 238000005245 sintering Methods 0.000 claims description 3
- 238000005507 spraying Methods 0.000 claims description 3
- 244000050591 Veronicastrum sibiricum Species 0.000 claims description 2
- 235000000756 Veronicastrum sibiricum Nutrition 0.000 claims description 2
- 244000230342 green foxtail Species 0.000 claims 1
- 239000011521 glass Substances 0.000 description 5
- 229910052500 inorganic mineral Inorganic materials 0.000 description 3
- 239000011707 mineral Substances 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 2
- 244000304962 green bristle grass Species 0.000 description 2
- 241000446281 Eschenbachia blinii Species 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 238000009991 scouring Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P40/00—Technologies relating to the processing of minerals
- Y02P40/60—Production of ceramic materials or ceramic elements, e.g. substitution of clay or shale by alternative raw materials, e.g. ashes
Landscapes
- Compositions Of Oxide Ceramics (AREA)
- Cultivation Receptacles Or Flower-Pots, Or Pots For Seedlings (AREA)
Abstract
The invention relates to the field of ceramic preparation, in particular to an imitated flocking glaze ceramic and a preparation method thereof, wherein the glaze comprises the following raw materials in parts by weight: 3-4 parts of old stove soil, 2-3 parts of ox bone ash, 4-5 parts of plant ash, 6-8 parts of green pyroxene, 5-8 parts of quartz, 10-12 parts of feldspar and 8-10 parts of loess. The glaze is green as a whole, organic substances in the bottom layer of the glaze are combusted and vaporized to generate bubbles, unburned C in the organic substances is adsorbed to form black dot-shaped spots, and the whole glaze is similar to the natural form of moss; air bubbles generated by decomposition of iron oxide at high temperature bring partial anorthite crystals and hematite crystals to the glaze surface, an iron-rich area is formed in the part of the glaze surface, and the hematite crystals are separated out at the edge of anorthite crystal flowers and among anorthite crystal grains in the cooling process, so that brown blocky stripes are formed, the shapes of the blocky stripes are similar to brown stripes on moss, and the crystals are stacked from the surface to the inner layer to present a three-dimensional effect.
Description
Technical Field
The invention relates to the field of ceramic preparation, in particular to a flocking glaze imitating ceramic and a preparation method thereof.
Background
Ceramic raw materials belong to minerals, are mined from the earth's crust, and can be classified into oxygen, silicon, and various metal minerals. The mineral substance is formed by chemically combining various elements in viscosity, the rock is continuously subjected to scouring and attack of wind and rain for a long time, gradually digested into powder and continuously deposited and reconstructed, the glaze is a glassy thin layer covering a ceramic body, but the glaze is more complex than glass in composition, and the property and microstructure of the glaze are also greatly different from the glass, for example, the high-temperature viscosity of the glaze is far greater than that of the glass; the composition and preparation process of the glass are similar to those of a blank and different from those of glass. If the glaze surface is required to be shaped like flocking or moss imitation, the traditional process can adopt a colored drawing form, and the pattern can be realized only on a plane, so that the three-dimensional effect is lacked and the expression is unreal.
Disclosure of Invention
An object of the present invention is to solve at least the above problems by a faux-flocked glazed ceramic and a method for preparing the same.
In order to solve the technical problems, the technical scheme adopted by the invention is as follows: imitative flocking glaze pottery, its characterized in that: the glaze comprises a blank body and a glaze surface, wherein the blank body comprises the following components in parts by weight: 5-8 parts of white dry soil, 2-3 parts of yellow dry soil, 5-6 parts of kaolin, 3-4 parts of quartz and 4-6 parts of potassium feldspar, wherein the glaze comprises the following raw materials in parts by weight: 3-4 parts of old stove soil, 2-3 parts of ox bone ash, 4-5 parts of plant ash, 6-8 parts of green pyroxene, 5-8 parts of quartz, 10-12 parts of feldspar and 8-10 parts of loess.
Preferably, the blank comprises the following raw materials in parts by weight: the glaze comprises, by weight, 5 parts of white dry soil, 2 parts of yellow dry soil, 5 parts of kaolin, 3 parts of quartz and 4 parts of potassium feldspar, and comprises the following raw materials: 3 parts of old stove soil, 2 parts of ox bone ash, 4 parts of plant ash, 6 parts of green pyroxene, 5 parts of quartz, 10 parts of feldspar and 8 parts of loess
Preferably, the blank comprises the following raw materials in parts by weight: 8 parts of white dry soil, 3 parts of yellow dry soil, 6 parts of kaolin, 4 parts of quartz and 6 parts of potassium feldspar, wherein the glaze comprises the following raw materials in parts by weight: 4 parts of old stove soil, 3 parts of ox bone ash, 5 parts of plant ash, 8 parts of green pyroxene, 8 parts of quartz, 12 parts of feldspar and 10 parts of loess
Preferably, the blank comprises the following raw materials in parts by weight: 6 parts of white dry soil, 2.5 parts of yellow dry soil, 5.5 parts of kaolin, 3.4 parts of quartz and 5 parts of potassium feldspar, wherein the glaze comprises the following raw materials in parts by weight: 3.5 parts of old kitchen soil, 2.5 parts of ox bone ash, 4.5 parts of plant ash, 7 parts of green pyroxene, 6 parts of quartz, 11 parts of feldspar and 9 parts of loess
The preparation method of the imitated flocking glaze ceramic is characterized by comprising the following steps:
step a, preparing a blank body, and biscuit firing and forming;
step b, preparing a blank: the blank comprises the following raw materials in parts by weight: 5-8 parts of white dry soil, 2-3 parts of yellow dry soil, 5-6 parts of kaolin, 3-4 parts of quartz and 4-6 parts of potassium feldspar;
step c, applying glaze on the surface of the blank;
d, putting the mixture into a kiln for sintering, and heating to 800 ℃ within 6-7 hours;
raising the temperature to 1200 ℃ within 1 hour, preserving the heat for 1-1.5 hours, enabling the glaze to be green integrally, enabling organic substances in the bottom layer of the glaze to be combusted and vaporized to generate bubbles, adsorbing unburned C in the organic substances to form black dot-shaped spots, and enabling the glaze to be similar to the natural form of moss integrally;
heating to 1275 ℃ within 0.5h, keeping the temperature for 20min, bringing partial anorthite crystals and hematite crystals to a glaze surface by air bubbles generated by decomposition of iron oxide at high temperature, forming an iron-rich area at the part of the glaze surface, separating out the hematite crystals at the anorthite crystal flower edges and among anorthite crystals in the cooling process, thereby forming brown blocky stripes which are similar to brown stripes on moss, and stacking the crystals from the surface to the inner layer to show a three-dimensional effect;
stopping the fire, and naturally cooling.
Preferably, the temperature of bisque firing in the step a is 800-820 ℃.
Preferably, in the step b, the plant ash is prepared by mixing and firing green bristlegrass herb and conyza blinii according to the mass ratio of 1: 1.
Preferably, in the step c, the thickness of the glaze is 2-2.2 mm.
Preferably, in the step c, the glaze is applied by spraying glaze or dipping glaze.
Preferably, in the step d, the temperature is raised to 800 ℃ and then is kept for 1 to 2 hours.
As can be seen from the above description, the artificial flocking glaze ceramic and the preparation method thereof provided by the invention have the following beneficial effects: organic substances contained in old stove soil, ox bone ash and plant ash participate in reaction under high-temperature glaze firing, and a large amount of bubbles are generated at the same time, so that the bubbles on the glaze surface are dense; the glaze is green as a whole, organic substances in the bottom layer of the glaze are combusted and vaporized to generate bubbles, unburned C in the organic substances is adsorbed to form black dot-shaped spots, and the whole glaze is similar to the natural form of moss; air bubbles generated by decomposition of iron oxide at high temperature bring partial anorthite crystals and hematite crystals to the glaze surface, an iron-rich area is formed in the part of the glaze surface, and the hematite crystals are separated out at the edge of anorthite crystal flowers and among anorthite crystal grains in the cooling process, so that brown blocky stripes are formed, the shapes of the blocky stripes are similar to brown stripes on moss, and the crystals are stacked from the surface to the inner layer to present a three-dimensional effect.
Detailed Description
The invention is further described below by means of specific embodiments.
In order to make the technical means, the creation characteristics, the achievement purposes and the effects of the invention easy to understand, the invention is further described with the specific embodiments.
The flocking-imitating glazed ceramic comprises a blank body and a glaze, wherein the blank body comprises the following raw materials in parts by weight: 5-8 parts of white dry soil, 2-3 parts of yellow dry soil, 5-6 parts of kaolin, 3-4 parts of quartz and 4-6 parts of potassium feldspar, wherein the glaze comprises the following raw materials in parts by weight: 3-4 parts of old stove soil, 2-3 parts of ox bone ash, 4-5 parts of plant ash, 6-8 parts of green pyroxene, 5-8 parts of quartz, 10-12 parts of feldspar and 8-10 parts of loess.
Detailed description of the invention
The blank comprises the following raw materials in parts by weight: the glaze comprises, by weight, 5 parts of white dry soil, 2 parts of yellow dry soil, 5 parts of kaolin, 3 parts of quartz and 4 parts of potassium feldspar, and comprises the following raw materials: 3 parts of old stove soil, 2 parts of ox bone ash, 4 parts of plant ash, 6 parts of green pyroxene, 5 parts of quartz, 10 parts of feldspar and 8 parts of loess
Detailed description of the invention
The blank comprises the following raw materials in parts by weight: 8 parts of white dry soil, 3 parts of yellow dry soil, 6 parts of kaolin, 4 parts of quartz and 6 parts of potassium feldspar, wherein the glaze comprises the following raw materials in parts by weight: 4 parts of old stove soil, 3 parts of ox bone ash, 5 parts of plant ash, 8 parts of green pyroxene, 8 parts of quartz, 12 parts of feldspar and 10 parts of loess
Detailed description of the invention
The blank comprises the following raw materials in parts by weight: 6 parts of white dry soil, 2.5 parts of yellow dry soil, 5.5 parts of kaolin, 3.4 parts of quartz and 5 parts of potassium feldspar, wherein the glaze comprises the following raw materials in parts by weight: 3.5 parts of old kitchen soil, 2.5 parts of ox bone ash, 4.5 parts of plant ash, 7 parts of green pyroxene, 6 parts of quartz, 11 parts of feldspar and 9 parts of loess
The preparation method of the imitated flocking glaze ceramic is characterized by comprising the following steps of:
step a, preparing a blank body, and biscuit firing and forming;
step b, preparing a blank: the blank comprises the following raw materials in parts by weight: 5-8 parts of white dry soil, 2-3 parts of yellow dry soil, 5-6 parts of kaolin, 3-4 parts of quartz and 4-6 parts of potassium feldspar; organic substances contained in old stove soil, ox bone ash and plant ash participate in reaction under high-temperature glaze firing, and a large amount of bubbles are generated at the same time, so that the bubbles on the glaze surface are dense.
Step c, applying glaze on the surface of the blank;
d, putting the mixture into a kiln for sintering, and heating to 800 ℃ within 6-7 hours;
raising the temperature to 1200 ℃ within 1 hour, preserving the heat for 1-1.5 hours, enabling the glaze to be green integrally, enabling organic substances in the bottom layer of the glaze to be combusted and vaporized to generate bubbles, adsorbing unburned C in the organic substances to form black dot-shaped spots, and enabling the glaze to be similar to the natural form of moss integrally;
heating to 1275 ℃ within 0.5h, keeping the temperature for 20min, bringing partial anorthite crystals and hematite crystals to a glaze surface by air bubbles generated by decomposition of iron oxide at high temperature, forming an iron-rich area at the part of the glaze surface, separating out the hematite crystals at the anorthite crystal flower edges and among anorthite crystals in the cooling process, thereby forming brown blocky stripes which are similar to brown stripes on moss, and stacking the crystals from the surface to the inner layer to show a three-dimensional effect;
stopping the fire, and naturally cooling.
The temperature of bisque firing in the step a is 800-820 ℃.
In the step b, the plant ash is prepared by mixing and firing green bristlegrass herb and veronicastrum sibiricum at a mass ratio of 1: 1.
In the step c, the thickness of the glaze is 2-2.2 mm.
In the step c, glaze is applied by adopting a glaze spraying or glaze dipping mode.
In the step d, the temperature is raised to 800 ℃ and then is kept for 1-2 hours.
The above description is only a few specific embodiments of the present invention, but the design concept of the present invention is not limited thereto, and any insubstantial modifications made by the design concept should fall within the scope of the present invention.
Claims (10)
1. Imitative flocking glaze pottery, its characterized in that: the glaze comprises a blank body and a glaze surface, wherein the blank body comprises the following components in parts by weight: 5-8 parts of white dry soil, 2-3 parts of yellow dry soil, 5-6 parts of kaolin, 3-4 parts of quartz and 4-6 parts of potassium feldspar, wherein the glaze comprises the following raw materials in parts by weight: 3-4 parts of old stove soil, 2-3 parts of ox bone ash, 4-5 parts of plant ash, 6-8 parts of green pyroxene, 5-8 parts of quartz, 10-12 parts of feldspar and 8-10 parts of loess.
2. The imitated flocking glazed ceramic of claim 1, wherein: the blank comprises the following raw materials in parts by weight: the glaze comprises, by weight, 5 parts of white dry soil, 2 parts of yellow dry soil, 5 parts of kaolin, 3 parts of quartz and 4 parts of potassium feldspar, and comprises the following raw materials: 3 parts of old stove soil, 2 parts of ox bone ash, 4 parts of plant ash, 6 parts of green pyroxene, 5 parts of quartz, 10 parts of feldspar and 8 parts of loess.
3. The imitated flocking glazed ceramic of claim 1, wherein: the blank comprises the following raw materials in parts by weight: 8 parts of white dry soil, 3 parts of yellow dry soil, 6 parts of kaolin, 4 parts of quartz and 6 parts of potassium feldspar, wherein the glaze comprises the following raw materials in parts by weight: 4 parts of old stove soil, 3 parts of ox bone ash, 5 parts of plant ash, 8 parts of green pyroxene, 8 parts of quartz, 12 parts of feldspar and 10 parts of loess.
4. The imitated flocking glazed ceramic of claim 1, wherein: the blank comprises the following raw materials in parts by weight: 6 parts of white dry soil, 2.5 parts of yellow dry soil, 5.5 parts of kaolin, 3.4 parts of quartz and 5 parts of potassium feldspar, wherein the glaze comprises the following raw materials in parts by weight: 3.5 parts of old stove soil, 2.5 parts of ox bone ash, 4.5 parts of plant ash, 7 parts of green pyroxene, 6 parts of quartz, 11 parts of feldspar and 9 parts of loess.
5. The method for preparing the imitated flocking glazed ceramic according to the claims 1 to 4, which is characterized by comprising the following steps:
step a, preparing a blank body, and biscuit firing and forming;
step b, preparing a blank: the blank comprises the following raw materials in parts by weight: 5-8 parts of white dry soil, 2-3 parts of yellow dry soil, 5-6 parts of kaolin, 3-4 parts of quartz and 4-6 parts of potassium feldspar;
step c, applying glaze on the surface of the blank;
d, putting the mixture into a kiln for sintering, and heating to 800 ℃ within 6-7 hours;
raising the temperature to 1200 ℃ within 1 hour, preserving the heat for 1-1.5 hours, enabling the glaze to be green integrally, enabling organic substances in the bottom layer of the glaze to be combusted and vaporized to generate bubbles, adsorbing unburned C in the organic substances to form black dot-shaped spots, and enabling the glaze to be similar to the natural form of moss integrally;
heating to 1275 ℃ within 0.5h, keeping the temperature for 20min, bringing partial anorthite crystals and hematite crystals to a glaze surface by air bubbles generated by decomposition of iron oxide at high temperature, forming an iron-rich area at the part of the glaze surface, separating out the hematite crystals at the anorthite crystal flower edges and among anorthite crystals in the cooling process, thereby forming brown blocky stripes which are similar to brown stripes on moss, and stacking the crystals from the surface to the inner layer to show a three-dimensional effect;
stopping the fire, and naturally cooling.
6. The preparation method of the imitated flocking glazed ceramic according to claim 1, which is characterized in that: the temperature of bisque firing in the step a is 800-820 ℃.
7. The preparation method of the imitated flocking glazed ceramic according to claim 1, which is characterized in that: in the step b, the plant ash is prepared by mixing and firing green bristlegrass herb and veronicastrum sibiricum at a mass ratio of 1: 1.
8. The preparation method of the imitated flocking glazed ceramic according to claim 1, which is characterized in that: in the step c, the thickness of the glaze is 2-2.2 mm.
9. The preparation method of the imitated flocking glazed ceramic according to claim 1, which is characterized in that: in the step c, glaze is applied by adopting a glaze spraying or glaze dipping mode.
10. The preparation method of the imitated flocking glazed ceramic according to claim 1, which is characterized in that: in the step d, the temperature is raised to 800 ℃ and then is kept for 1-2 hours.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210040361.3A CN114276017B (en) | 2022-01-14 | 2022-01-14 | Imitation flocking glazed ceramic and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202210040361.3A CN114276017B (en) | 2022-01-14 | 2022-01-14 | Imitation flocking glazed ceramic and preparation method thereof |
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| CN114276017A true CN114276017A (en) | 2022-04-05 |
| CN114276017B CN114276017B (en) | 2023-11-28 |
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| CN114276017B (en) | 2023-11-28 |
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