CN114271598A - Toothbrush with high-efficiency Bass tooth brushing method and preparation method thereof - Google Patents
Toothbrush with high-efficiency Bass tooth brushing method and preparation method thereof Download PDFInfo
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- CN114271598A CN114271598A CN202210002161.9A CN202210002161A CN114271598A CN 114271598 A CN114271598 A CN 114271598A CN 202210002161 A CN202210002161 A CN 202210002161A CN 114271598 A CN114271598 A CN 114271598A
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- 238000000034 method Methods 0.000 title claims abstract description 58
- 230000001680 brushing effect Effects 0.000 title claims abstract description 47
- 238000002360 preparation method Methods 0.000 title abstract description 14
- 239000000463 material Substances 0.000 claims abstract description 49
- 239000002114 nanocomposite Substances 0.000 claims abstract description 28
- 230000003385 bacteriostatic effect Effects 0.000 claims abstract description 26
- 230000000844 anti-bacterial effect Effects 0.000 claims abstract description 22
- 239000000284 extract Substances 0.000 claims abstract description 21
- 239000006087 Silane Coupling Agent Substances 0.000 claims abstract description 20
- 239000000022 bacteriostatic agent Substances 0.000 claims abstract description 18
- 239000003242 anti bacterial agent Substances 0.000 claims abstract description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 39
- 238000001035 drying Methods 0.000 claims description 21
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 claims description 18
- 235000012239 silicon dioxide Nutrition 0.000 claims description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical group CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 12
- 239000005543 nano-size silicon particle Substances 0.000 claims description 12
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 9
- 239000000758 substrate Substances 0.000 claims description 8
- 238000006243 chemical reaction Methods 0.000 claims description 7
- 239000002904 solvent Substances 0.000 claims description 7
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 238000001816 cooling Methods 0.000 claims description 6
- 238000004519 manufacturing process Methods 0.000 claims description 6
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 claims description 6
- 241000219061 Rheum Species 0.000 claims description 5
- 235000009411 Rheum rhabarbarum Nutrition 0.000 claims description 5
- 239000010404 Scutellaria baicalensis extract Substances 0.000 claims description 4
- 239000002131 composite material Substances 0.000 claims description 4
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- 239000004743 Polypropylene Substances 0.000 claims description 3
- 239000000706 filtrate Substances 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- 230000004927 fusion Effects 0.000 claims description 3
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- 238000002156 mixing Methods 0.000 claims description 3
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- 238000012360 testing method Methods 0.000 description 7
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Abstract
The invention relates to the technical field of cleaning supplies, in particular to a toothbrush with a Bass tooth brushing method applied efficiently and a preparation method thereof; the multifunctional electric toothbrush comprises a toothbrush body and toothbrush filaments, wherein the toothbrush filaments are arranged on the toothbrush body, the toothbrush body comprises 20-30 parts by weight of nano composite base material, 2-10 parts by weight of color master, 3-10 parts by weight of silane coupling agent and 2-10 parts by weight of antibacterial extract, and the toothbrush filaments comprise 20-40 parts by weight of main material, 4-6 parts by weight of color master, 2-6 parts by weight of silane coupling agent and 2-6 parts by weight of antibacterial agent; the invention takes the nano-composite base material, the bacteriostatic agent and the bacteriostatic extract as the materials, so that the prepared brush body has degradability and bacteriostatic action and also has the traditional Chinese medicine effect; the quality of the prepared toothbrush which efficiently applies the Bass tooth brushing method and the preparation method thereof is effectively improved.
Description
Technical Field
The invention relates to the technical field of cleaning products, in particular to a toothbrush with a Bass tooth brushing method applied efficiently and a preparation method thereof.
Background
The pasteur tooth brushing method is also called gingival sulcus cleaning method or horizontal vibration method, and comprises the following operation steps: correct grip, thumb-to-thumb gesture of "like"; aligning the toothbrush at the joint of teeth and gum, and brushing the upper teeth with the bristles upward; the bristles form an angle of 45-60 degrees with teeth, and the bristles are lightly pressed towards the teeth to be slightly arc-shaped, and the side edges of the bristles are also in considerable contact with the teeth; after the toothbrush is positioned, the toothbrush starts to do short-distance horizontal movement, and two or two teeth brush back and forth for about ten times; when brushing teeth, the mouth is enlarged, and the last tooth on the right side of the upper row is seen. Then brushing the left side starting from the right rear buccal side; then the left occlusal surface, the left lingual side, and the right lingual side are returned to the right lingual side, and then the right occlusal surface. Thus, the brush in sequence has no omission; when the occlusal surface is brushed, two teeth are brushed back and forth; the lingual side of the upper jaw posterior teeth is a place which is difficult to brush, the brush hair is still aligned with the junction of the teeth and the gum, and the brush handle is close to the incisors; in addition, the buccal side of the posterior teeth was brushed with the same hand, i.e., the right buccal side was brushed with the right hand. The left buccal side is left handed. Meanwhile, the brush handle can open the cheek to facilitate the sight; the upper teeth are brushed and the lower teeth are brushed using the same principles and methods.
When the pasteurization method is used, a toothbrush, which is a cleaning product and is a handle-type brush, is used for adding toothpaste to the brush and then repeatedly brushing all parts of teeth to keep oral hygiene.
With the rapid development of science and technology and medicine, the living standard of people is greatly improved, the prevention and health care consciousness is continuously improved, people pay more and more attention to self health care of the oral cavity, and toothbrushes which efficiently apply the Bass tooth brushing method are favored by people, for example, an antibacterial toothbrush and a manufacturing method thereof are disclosed in Chinese patent application No. CN108359236B, although the toothbrush prepared by the patent document has a certain antibacterial effect, the antibacterial effect, toughness and degradability are not good, and the function is single, so that the performance and quality of the prepared toothbrush which efficiently applies the Bass tooth brushing method are influenced.
Disclosure of Invention
Aiming at the defects in the prior art, the invention provides the toothbrush which efficiently applies the Bass tooth brushing method and the preparation method thereof, the invention takes the nano composite base material as the material, so that the prepared brush body has degradability and bacteriostasis, and also has the effects of clearing heat, drying damp, purging fire, cooling blood, removing blood stasis, detoxifying and the like, meanwhile, the main material and the nano composite base material are taken as the raw materials, the prepared brush wire has good toughness, and the bacteriostatic agent and the bacteriostatic extract are taken as the raw materials, so that the prepared brush wire not only has the bacteriostasis, but also has good effects of clearing heat, drying damp, purging fire, detoxifying and stopping bleeding, and the use of the Bass tooth brushing method is combined, so that the tooth brushing efficiency is improved; the quality of the prepared toothbrush which efficiently applies the Bass tooth brushing method and the preparation method thereof is effectively improved.
In order to achieve the purpose, the invention provides the following technical scheme:
the toothbrush with the efficient Bass tooth brushing method comprises a brush body and brush wires, wherein the brush wires are arranged on the brush body, the brush body comprises 20-30 parts by weight of a nano composite base material, 2-10 parts by weight of a color master, 3-10 parts by weight of a silane coupling agent and 2-10 parts by weight of a bacteriostatic extract, and the brush wires comprise 20-40 parts by weight of a main material, 4-6 parts by weight of the color master, 2-6 parts by weight of the silane coupling agent and 2-6 parts by weight of the bacteriostatic extract.
By adopting the technical scheme: the invention takes the nano-composite base material as the material, so that the prepared brush body has degradability, takes the bacteriostatic agent extract as the raw material, can enable the prepared brush body to have bacteriostatic action, simultaneously takes the main material as the raw material, and has good toughness.
The invention is further configured to: the main material is one of polypropylene plastic and DuPont nylon.
By adopting the technical scheme: the main material is used as the raw material, so that the prepared toothbrush has good toughness, and can better clean tartar and protect teeth when being used in combination with a Bass tooth brushing method.
A preparation method of a toothbrush for efficiently applying a Bass tooth brushing method comprises the following steps:
s1, preparing the antibacterial brush body for later use.
S2, preparing the antibacterial brush filaments for later use.
And S3, fixing the prepared brush filaments on a brush body to obtain the toothbrush.
By adopting the technical scheme: the invention uses the bacteriostatic brush body and the bacteriostatic brush filaments to prepare the toothbrush, can inhibit bacteria when used by adopting a Bass tooth brushing method, contains the cost of traditional Chinese medicines, and can protect teeth.
The invention is further configured to: in the step S1, preparing a bacteriostatic brush includes the following steps:
s101, preparing the nano composite base material.
S102, preparing the bacteriostatic extract.
S103, placing the scutellaria baicalensis extract, the nano composite material and the silane coupling agent in a forming mold to prepare the antibacterial brush body.
By adopting the technical scheme: the bending degree of the brush body prepared by the invention is enhanced, the mechanical property of the brush body is improved, meanwhile, the brush body has biocompatibility, and the harm to a human body is reduced.
The invention is further configured to: in the step S101, a method for preparing a nanocomposite substrate includes:
carrying out water bath reaction on nano silicon dioxide, a silane coupling agent and a solvent for 5h at the temperature of 80 ℃; drying and drying in a drying oven at 90 ℃ for 1h to obtain modified nano silicon dioxide; mixing glycerol and sebacic acid, placing in a reaction bottle, and heating under vacuum pressure of 2kPa until complete fusion; adding the prepared modified nano silicon dioxide, and reacting for 20min at the temperature of 130 ℃ and under the vacuum pressure of 1 kPa; then cooling to 120 ℃, adding citric acid, and reacting for 1 h; drying in a vacuum drying oven for 30min, and pulverizing to obtain nanometer composite base material.
By adopting the technical scheme: according to the invention, the silicon dioxide is modified, the residual hydroxyl on the surface of the nano silicon dioxide is combined with the unreacted strong hydrogen bond, so that the mechanical toughness of the nano composite substrate is integrally increased, the dispersion of the silicon dioxide is improved by the added citric acid, the integral toughness of the nano composite substrate is further improved, the prepared nano composite substrate has the biodegradable characteristic, and the safety in use is improved.
The invention is further configured to: the solvent is absolute ethyl alcohol.
By adopting the technical scheme: the invention takes absolute ethyl alcohol as a solvent, so that the rice silica and the silane coupling agent are subjected to water bath reaction.
The invention is further configured to: in step 102, the method for preparing the bacteriostatic extract comprises the following steps:
placing Scutellariae radix in a boiler; adding water into a digester, soaking for 30min, and steaming at 100 deg.C for 60 min; filtering, and decocting the filtrate at 120 deg.C to obtain Scutellariae radix extract.
By adopting the technical scheme: the invention takes the extracted scutellaria baicalensis extract as the raw material, so that the prepared brush wire also has good effects of clearing heat and drying dampness, purging fire and detoxifying and stopping bleeding.
The invention is further configured to: in the step S2, the method for preparing the antibacterial brush filaments includes the following steps:
s201, preparing the bacteriostatic agent.
S202, crushing the main material through a crusher, and placing the crushed particles of the main material, the silane coupling agent and the bacteriostatic agent in a forming mold to prepare the bacteriostatic brush wire.
By adopting the technical scheme: the brush wire prepared by the invention not only has the bacteriostatic action, but also has good toughness and good effects of clearing heat and drying dampness, purging fire and detoxifying and stopping bleeding.
The invention is further configured to: in step S201, the method for preparing the bacteriostatic agent is as follows:
placing the crushed rhubarb into a flask; adding 95% ethanol into the flask; performing ultrasonic extraction at room temperature of 10 deg.C for 30min to obtain antibacterial agent.
By adopting the technical scheme: the invention uses rhubarb to extract bacteriostat, and the active ingredients of traditional Chinese medicine rhubarb are blended into the brush hair, thus realizing the effects of clearing heat and drying dampness, purging intense heat and detoxifying and stopping bleeding for users.
Advantageous effects
Compared with the known public technology, the technical scheme provided by the invention has the following beneficial effects:
the invention takes the nano composite base material as the material, so that the prepared brush body has degradability, takes the bacteriostatic agent bacterium extract as the raw material, can enable the prepared brush body to have bacteriostatic action, also has the effects of clearing heat, drying dampness, purging fire, cooling blood, removing blood stasis, detoxifying and the like, simultaneously takes the main material as the raw material, the prepared brush wire has good toughness, takes the bacteriostatic agent as the raw material, enables the prepared brush wire to have bacteriostatic action, also has good effects of clearing heat, drying dampness, purging fire, detoxifying and stopping bleeding, modifies silicon dioxide, combines residual hydroxyl on the surface of the nano silicon dioxide with unreacted strong hydrogen bonds, increases mechanical toughness on the whole nano composite base material, and adds citric acid to improve the dispersion of the silicon dioxide, further improves the toughness of the whole nano composite base material, and enables the prepared nano composite base material to have biodegradable property, the safety during use is improved, and the tooth brushing efficiency is improved by combining with a Bass tooth brushing method.
Drawings
FIG. 1 is a flow chart of a toothbrush and a method of manufacturing the toothbrush for efficient use of the Bass brushing method.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention clearer, the technical solutions in the embodiments of the present invention will be clearly and completely described below. It is to be understood that the embodiments described are only a few embodiments of the present invention, and not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The present invention will be further described with reference to the following examples.
Example 1
Referring to fig. 1, the toothbrush for efficiently applying the Bass tooth brushing method comprises a brush body and brush filaments, wherein the brush filaments are arranged on the brush body, the brush body comprises 20-30 parts by weight of a nano composite base material, 2-10 parts by weight of a color master, 3-10 parts by weight of a silane coupling agent and 2-10 parts by weight of a bacteriostatic extract, and the brush filaments comprise 20-40 parts by weight of a main material, 4-6 parts by weight of a color master, 2-6 parts by weight of a silane coupling agent and 2-6 parts by weight of a bacteriostatic agent.
The invention is further configured to: the main material is one of polypropylene plastic and DuPont nylon.
A preparation method of a toothbrush for efficiently applying a Bass tooth brushing method comprises the following steps:
step one, preparing the antibacterial brush body for later use.
And step two, preparing the antibacterial brush filaments for later use.
And step three, fixing the prepared brush filaments on a brush body to obtain the toothbrush.
The antibacterial brush is prepared by the following steps:
101) and preparing the nano composite substrate.
102) And preparing the antibacterial extract.
103) And placing the scutellaria baicalensis extract, the nano composite material and the silane coupling agent in a forming die to prepare the antibacterial brush body.
The method for preparing the nano composite substrate comprises the following steps:
carrying out water bath reaction on nano silicon dioxide, a silane coupling agent and a solvent for 5h at the temperature of 80 ℃; drying and drying in a drying oven at 90 ℃ for 1h to obtain modified nano silicon dioxide; mixing glycerol and sebacic acid, placing in a reaction bottle, and heating under vacuum pressure of 2kPa until complete fusion; adding the prepared modified nano silicon dioxide, and reacting for 20min at the temperature of 130 ℃ and under the vacuum pressure of 1 kPa; then cooling to 120 ℃, adding citric acid, and reacting for 1 h; drying in a vacuum drying oven for 30min, and pulverizing to obtain nanometer composite base material.
The solvent is absolute ethyl alcohol.
The method for preparing the antibacterial extract comprises the following steps:
placing Scutellariae radix in a boiler; adding water into a digester, soaking for 30min, and steaming at 100 deg.C for 60 min; filtering, and decocting the filtrate at 120 deg.C to obtain Scutellariae radix extract.
The method for preparing the antibacterial brush filaments comprises the following steps:
201) and preparing the bacteriostatic agent.
202) And crushing the main material by a crusher, and placing the crushed particles of the main material, the silane coupling agent and the bacteriostatic agent in a forming mould to prepare the bacteriostatic brush wire.
The method for preparing the bacteriostatic agent comprises the following steps:
placing the crushed rhubarb into a flask; adding 95% ethanol into the flask; performing ultrasonic extraction at room temperature of 10 deg.C for 30min to obtain antibacterial agent.
Example 2
The toothbrush of this embodiment for applying the effective pasteur brushing method and the manufacturing method thereof are substantially the same as those of embodiment 1, and the main differences are as follows: the brush body comprises 30 parts by weight of nano composite base material, 10 parts by weight of color master, 10 parts by weight of silane coupling agent and 10 parts by weight of antibacterial extract, and the brush filaments comprise 40 parts by weight of main material, 6 parts by weight of color master, 6 parts by weight of silane coupling agent and 6 parts by weight of antibacterial agent.
Comparative example 1
The toothbrush for high-efficiency application of the Bass tooth brushing method and the preparation method thereof provided by the embodiment are substantially the same as those of the embodiment 1, and the main differences are as follows: the brush handle is not prepared by adopting a nanometer base material.
Comparative example 2
The toothbrush for high-efficiency application of the Bass tooth brushing method and the preparation method thereof provided by the embodiment are substantially the same as those of the embodiment 1, and the main differences are as follows: no bacteriostatic extract was added.
Comparative example 3
The toothbrush for high-efficiency application of the Bass tooth brushing method and the preparation method thereof provided by the embodiment are substantially the same as those of the embodiment 1, and the main differences are as follows: no bacteriostatic agent was added.
Performance testing
Taking the toothbrushes prepared in the examples 1 to 2 and the comparative examples 1 to 3 and efficiently applying the Bass tooth brushing method, and detecting the relevant performance of the prepared toothbrushes efficiently applying the Bass tooth brushing method, wherein the detection method comprises the following steps:
1. respectively detecting the antibacterial (escherichia coli and staphylococcus) performance of the toothbrushes with high-efficiency Bass tooth brushing methods according to the detection standard GB/T2591-2003, and recording the obtained test results in a table 1;
TABLE 1 bacteriostatic effect detection table for toothbrush
2. The toughness (bending strength) of each of the toothbrushes to which the Bass tooth brushing method was efficiently applied was measured according to the test standard GB/T1449-2005, and the test results are shown in Table 2;
TABLE 2 Flexible Effect detection Table for toothbrush
| Test items | Effect of toughness detection |
| Example 1 | 946 |
| Example 2 | 938 |
| Comparative example 1 | 587 |
| Comparative example 2 | 937 |
| Comparative example 3 | 939 |
3. Respectively detecting the degradation performance of the toothbrushes with the high-efficiency Bass tooth brushing method according to the detection standard GB/T19275-2003, and recording the obtained test results in a table 3;
TABLE 3 degradation Performance Effect test Table for toothbrush
By analyzing the relevant data in the table, the toothbrush with the high-efficiency Bass tooth brushing method and the preparation method thereof have good antibacterial effect, good flexibility and good biodegradable effect, so that the quality of the prepared toothbrush with the high-efficiency Bass tooth brushing method and the preparation method thereof is effectively improved.
The invention takes the nano composite base material as the material, so that the prepared brush body has degradability, takes the bacteriostatic agent bacterium extract as the raw material, can enable the prepared brush body to have bacteriostatic action, also has the effects of clearing heat, drying dampness, purging fire, cooling blood, removing blood stasis, detoxifying and the like, simultaneously takes the main material as the raw material, so that the prepared brush wire has good toughness, takes the bacteriostatic agent as the raw material, enables the prepared brush wire to have bacteriostatic action, also has good effects of clearing heat, drying dampness, purging fire, detoxifying and stopping bleeding, modifies silicon dioxide, combines residual hydroxyl on the surface of the nano silicon dioxide with unreacted strong hydrogen bonds, increases mechanical toughness on the whole nano composite base material, and adds citric acid to improve the dispersion of the silicon dioxide, further improves the toughness of the whole nano composite base material, and enables the prepared nano composite base material to have biodegradable property, the safety during use is improved, and the tooth brushing efficiency is improved by combining with a Bass tooth brushing method.
The above examples are only intended to illustrate the technical solution of the present invention, but not to limit it; although the present invention has been described in detail with reference to the foregoing embodiments, it will be understood by those of ordinary skill in the art that: the technical solutions described in the foregoing embodiments may still be modified, or some technical features may be equivalently replaced; such modifications and substitutions do not depart from the spirit and scope of the corresponding technical solutions.
Claims (9)
1. Toothbrush of high-efficient application pasteur's method of brushing teeth, including the brush body and brush silk, the brush silk is installed on the brush body, its characterized in that, contain 20-30 parts by weight of nanometer composite substrate, 2-10 parts by weight of look mother, 3-10 parts by weight of silane coupling agent, 2-10 parts by weight of antibacterial extract in the brush body, contain 20-40 parts by weight of principal material, 4-6 parts by weight of look mother, 2-6 parts by weight of silane coupling agent, 2-6 parts by weight of antibacterial agent in the brush silk.
2. The toothbrush for enabling effective pasteur brushing according to claim 1, wherein said main material is one of polypropylene plastic and DuPont nylon.
3. A method for manufacturing a toothbrush for efficiently applying the bas tooth brushing method, which comprises the steps of using the toothbrush for efficiently applying the bas tooth brushing method according to any one of claims 1 to 2:
s1, preparing an antibacterial brush body for later use;
s2, preparing antibacterial brush filaments for later use;
and S3, fixing the prepared brush filaments on a brush body to obtain the toothbrush.
4. The method for preparing a toothbrush to which a Bass brushing method is applied with high efficiency according to claim 3, wherein in the step S1, a bacteriostatic brush is prepared, comprising the steps of:
s101, preparing a nano composite base material;
s102, preparing a bacteriostatic extract;
s103, placing the scutellaria baicalensis extract, the nano composite material and the silane coupling agent in a forming mold to prepare the antibacterial brush body.
5. The method for manufacturing a toothbrush to which a Bass brushing method is effectively applied according to claim 4, wherein the method for manufacturing the nanocomposite substrate in the step S101 is:
carrying out water bath reaction on nano silicon dioxide, a silane coupling agent and a solvent for 5h at the temperature of 80 ℃; drying and drying in a drying oven at 90 ℃ for 1h to obtain modified nano silicon dioxide; mixing glycerol and sebacic acid, placing in a reaction bottle, and heating under vacuum pressure of 2kPa until complete fusion; adding the prepared modified nano silicon dioxide, and reacting for 20min at the temperature of 130 ℃ and under the vacuum pressure of 1 kPa; then cooling to 120 ℃, adding citric acid, and reacting for 1 h; drying in a vacuum drying oven for 30min, and pulverizing to obtain nanometer composite base material.
6. The method for preparing a toothbrush for high efficiency use of the Bass brushing method as claimed in claim 4, wherein the solvent is absolute ethanol.
7. The method for preparing a toothbrush using Bass brushing technique according to claim 4, wherein the bacteriostatic extract is prepared by the following steps in step 102:
placing Scutellariae radix in a boiler; adding water into a digester, soaking for 30min, and steaming at 100 deg.C for 60 min; filtering, and decocting the filtrate at 120 deg.C to obtain Scutellariae radix extract.
8. The method for preparing a toothbrush for highly effective use of Bass brushing according to claim 3, wherein the step S2 of preparing bacteriostatic brush filaments comprises the steps of:
s201, preparing a bacteriostatic agent;
s202, crushing the main material through a crusher, and placing the crushed particles of the main material, the silane coupling agent and the bacteriostatic agent in a forming mold to prepare the bacteriostatic brush wire.
9. The method of claim 8, wherein the bacteriostatic agent is prepared by the following steps in step S201:
placing the crushed rhubarb into a flask; adding 95% ethanol into the flask; performing ultrasonic extraction at room temperature of 10 deg.C for 30min to obtain antibacterial agent.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115413878A (en) * | 2022-10-19 | 2022-12-02 | 西安交通大学口腔医院 | Toothbrush bristle, preparation method thereof and toothbrush |
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| CN110731610A (en) * | 2019-10-21 | 2020-01-31 | 江苏三笑集团有限公司 | antibacterial toothbrush and preparation method thereof |
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| CN115413878A (en) * | 2022-10-19 | 2022-12-02 | 西安交通大学口腔医院 | Toothbrush bristle, preparation method thereof and toothbrush |
| CN115413878B (en) * | 2022-10-19 | 2023-09-19 | 西安交通大学口腔医院 | Toothbrush bristle, preparation method thereof and toothbrush |
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