CN114271495A - Vine tea and cyclocarya paliurus compound feed liquid, selenium-enriched beverage and preparation method thereof - Google Patents
Vine tea and cyclocarya paliurus compound feed liquid, selenium-enriched beverage and preparation method thereof Download PDFInfo
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Abstract
The invention provides a compound feed liquid of vine tea and cyclocarya paliurus, a selenium-rich beverage and a preparation method thereof. The selenium-enriched beverage is prepared by compounding vine tea and cyclocarya paliurus compound feed liquid with a momordica grosvenori concentrated solution, a wrinkled papaya concentrated solution, a pomegranate concentrated solution and selenium-enriched cardamine violifolia, can be stored for 12 months without deterioration under the condition of not adding any preservative, is good in taste, bright in color, clear and transparent, and has a health care function.
Description
Technical Field
The invention relates to the technical field of food, in particular to a vine tea and cyclocarya paliurus compound feed liquid, a selenium-rich beverage and a preparation method thereof.
Background
Ampelopsis grossedentata is a plant of Ampelopsis genus of Vitaceae family, has cool nature, has effects of clearing heat and detoxicating, dispelling pathogenic wind and removing dampness, removing nodules and breaking knots, treating pulmonary abscess, traumatic injury, scald, inflammation, chronic nephritis, urine pain, stomach heat emesis, common cold, sore throat and the like, and is recorded in record and pharmacopoeia of all generations. In recent years, a plurality of research results also show that the ampelopsis grossedentata has the effects of protecting liver, reducing blood sugar, inhibiting bacteria, resisting tumors and the like.
The vine tea contains rich total flavonoid functional substances. However, in the conventional ampelopsis grossedentata extraction process, the storage rate of flavonoids is relatively reduced with the increase of heating temperature and the increase of extraction time. Meanwhile, in the process of processing and storing the beverage, the flavonoid substances are easily oxidized and deteriorated by factors such as temperature, air, pH and the like, and the taste and the soup color are greatly changed.
Disclosure of Invention
Therefore, the vine tea and cyclocarya paliurus compound feed liquid, the selenium-enriched beverage and the preparation method thereof are needed, and the vine tea and cyclocarya paliurus compound feed liquid can protect the stability of flavonoid substances and keep good taste and soup color on the premise of not adding any additive and preservative when the vine tea is used for preparing the beverage.
The invention adopts the following technical scheme:
the preparation method of the ampelopsis grossedentata and cyclocarya paliurus composite feed liquid is characterized by comprising the following steps: adding the vine tea and the cyclocarya paliurus leaves into extraction equipment according to the weight ratio of (7-9) to (2-4), adding water according to the material-liquid ratio of 1kg to (40-60), and extracting: extracting at 70-80 ℃ for 20-60 min, and filtering to obtain the composite feed liquid.
In some embodiments, the extraction process further comprises stirring at a speed of 10 to 20 r/min.
The invention also provides a selenium-enriched beverage which is an aqueous solution mainly prepared by mixing the following raw materials, wherein the pH value is 4.4-4.6:
preferably, the weight ratio of the wrinkled pAN _ SNer papaya concentrated solution to the pomegranate concentrated solution is 1: 1.
Preferably, the selenium-enriched beverage is an aqueous solution mainly prepared by mixing the following raw materials, and the pH value is 4.4-4.6: 550-650 mL/L of the vine tea and cyclocarya paliurus composite feed liquid, 1.8-2.0 g/L of fructus momordicae concentrated solution, 0.7-0.9 g/L of wrinkled papaya concentrated solution, 0.7-0.9 g/L of pomegranate concentrated solution and 0.13-0.17 g/L of selenium-rich cardamine violifolia.
The invention also provides a preparation method of the selenium-enriched beverage, which comprises the following steps: preparing composite feed liquid of the vine tea and the cyclocarya paliurus, and placing the composite feed liquid in a liquid storage tank; respectively adding the concentrated solution of fructus Siraitiae Grosvenorii, the concentrated solution of fructus Chaenomelis, and the concentrated solution of fructus Punicae Granati into the liquid storage tank, stirring to dissolve uniformly, cooling to 20 deg.C, centrifuging, and filtering to obtain intermediate solution; transferring the intermediate solution into a blending tank, adding the selenium-rich cardamine violifolia solution, supplementing water to a constant volume, and adjusting the pH to 4.4-4.6; and (5) sterilizing and filling.
In some embodiments, the preparation process of the selenium-enriched cardamine violifolia solution comprises the following steps: putting selenium-rich cardamine violifolia into a shearing cylinder, adding a proper amount of water to dissolve, and performing operation parameters of: the linear velocity is 40-60 m/s, the pressure is 15000PSi, the output flow is 3000L/h, and the rotating speed is 10000rpm, so that the selenium-rich cardamine violifolia solution which is uniformly dissolved is obtained.
In some embodiments, the rotation speed of the centrifugation is 5000-6000 r/min.
In some of these embodiments, the filtration is performed using a 100 mesh stainless steel screen.
In some of these embodiments, the process parameters of the sterilization are: and (3) carrying out sterilization by adopting an UHT high-temperature instantaneous sterilization method at 136 +/-2 ℃ for 5-8 s.
In some embodiments, the filling is performed by hot filling at 95-100 ℃.
The invention has the beneficial effects that:
compared with the prior art, the vine tea and cyclocarya paliurus composite feed liquid is prepared by carrying out hydrothermal composite extraction on vine tea and cyclocarya paliurus leaves, has the taste of the vine tea and the cyclocarya paliurus, is good in taste, and has the optimal content of total extract, total flavone extract and tea polyphenol, protein, amino acid and carbohydrate. The beverage is prepared by compounding the ampelopsis grosvenori concentrated solution, the wrinkled papaya concentrated solution, the pomegranate concentrated solution and the selenium-rich crushed rice with the vine tea and cyclocarya paliurus compound feed liquid, has the pH value of 4.4-4.6, can be stored for more than 12 months without deterioration under the condition of not adding any preservative, and has the advantages of good taste, bright color, clearness and transparency and a health care function.
Drawings
FIG. 1 is a statistical graph of the retention rate of flavonoids at different temperatures as a function of pH.
Detailed Description
The present invention is further described in detail below with reference to specific examples so that those skilled in the art can more clearly understand the present invention.
The following examples are provided only for illustrating the present invention and are not intended to limit the scope of the present invention. All other embodiments obtained by a person skilled in the art based on the specific embodiments of the present invention without any inventive step are within the scope of the present invention.
In the examples of the present invention, all the raw material components are commercially available products well known to those skilled in the art, unless otherwise specified; in the examples of the present invention, unless otherwise specified, all technical means used are conventional means well known to those skilled in the art.
Vine tea: the image of Enshi Tujia is provided by selenium-enriched agricultural development Co.
Cyclocarya paliurus leaves: the image of Enshi Tujia is provided by selenium-enriched agricultural development Co.
Concentrated solution of Chaenomeles speciosa nakai: sheng shi bio-technology ltd, zhejiang, pH: 2.15.
pomegranate concentrated solution: yue Peng tai (shanghai) food ltd, pH: 1.96.
concentrated solution of fructus momordicae: provided by Guilin Jifusi Grosvenor Momordica grosvenori, pH: 4.01.
selenium-rich cardamine violifolia: the selenium content is 3500mg/kg provided by Schen biological medicine development Limited.
Example 1
The embodiment provides a preparation method of a vine tea and cyclocarya paliurus compound feed liquid, which comprises the following steps: putting selected vine tea and cyclocarya paliurus leaves which are normal in color and luster, strong in fragrance, free of mildew and damage of diseases and insects into extraction equipment according to the weight ratio of 8:3, adding water according to the material-liquid ratio of 1kg to 50kg, and extracting: the extraction temperature is 75 ℃, the extraction time is 25min, and the stirring speed is 10-20 r/min, so that an extracting solution or an extracting solution is obtained. Filtering the extractive solution with 80 mesh screen, filtering with 150 mesh filter cloth to obtain composite liquid, and transferring into a liquid storage tank for storage.
The preparation process of this example is a preferential extraction process, and the preparation process is obtained by taking liquor color, taste, aroma and taste as evaluation indexes, taking total extract, total flavone extraction rate, tea polyphenol, protein, amino acid and carbohydrate as indexes, and taking shelf life as a final judgment basis.
Example 2
In this example, the influence of different pH values of the composite feed liquid of the vine tea and cyclocarya paliurus, the concentrated solution of the wrinkled papaya and the concentrated solution of the pomegranate on the content of flavone and the color and quality change of tea beverage is studied.
The specific idea is as follows: filtering the compound feed liquid of the vine tea and cyclocarya paliurus prepared in the example 1 by a 80-mesh sieve, taking a certain amount of the supernatant extracted from the leaves of the vine tea and cyclocarya paliurus, adding the wrinkle pawpaw concentrated solution and the pomegranate concentrated solution (in a weight ratio of 1: 1) with different weights into the blending liquid, regulating the pH value to 3.0, 3.5, 4.0, 4.5, 5.0, 6.0 and 6.7 by constant volume, carrying out hot canning, carrying out high-pressure sterilization at 136 ℃ for 6S, cooling, respectively placing at the conditions of high temperature of 38 ℃, room temperature of 25 ℃ and cold storage at 4 ℃ for 1 month, measuring the flavone content and the color quality change, and observing the change of the precipitate in the storage process.
The change of flavone content is shown in figure 1. As is evident from FIG. 1, the preservation rate of flavone is reduced with the increase of pH under the conditions of high temperature and room temperature, and the preservation effect is better between pH3.0 and 5.0. Analysis results show that under three storage conditions, pH has extremely obvious influence on flavone, and the flavone is most favorably stored at pH 3.0. This is probably because flavones are a kind of substances containing polyhydroxy groups, which are weakly acidic, and under appropriate conditions, the hydroxyl groups are protected, thereby avoiding oxidative deterioration. Under the condition of refrigeration, the preservation rate is obviously lower than that of the other two conditions, and the dihydromyricetin in the ampelopsis grossedentata is easy to crystallize and precipitate under the condition of low temperature.
However, in the aspect of pursuing a certain tea taste, the acidity is too high when the pH value is 3.0-4.0, and the strong acid stimulation is generated. In order to overcome the defect, the usage amount of the wrinkled pawpaw concentrated solution and the pomegranate concentrated solution is reduced, the pH value of the wrinkled pawpaw concentrated solution and the pomegranate concentrated solution is adjusted to 4.4-4.5, the soup color can be protected to different degrees, the browning is prevented, the special faint scent and special flavor of the vine tea and the cyclocarya paliurus tea are kept, and the wrinkled pawpaw concentrated solution and the pomegranate concentrated solution are cool and tasty and have a good health care function.
Example 3
The present example provides a selenium enriched beverage having the composition as shown in the following table:
| raw materials | Content (wt.) |
| Composite feed liquid of vine tea and cyclocarya paliurus prepared in example 1 | 400ml/L |
| Concentrated solution of wrinkled papaya | 0.6g/L |
| Pomegranate concentrate | 0.6g/L |
| Momordica grosvenori concentrated solution | 1.3g/L |
| Selenium-rich cardamine violifolia | 0.13g/L |
The preparation method of the selenium-enriched beverage comprises the following steps:
s1, mixing the vine tea and cyclocarya paliurus compound feed liquid, the momordica grosvenori concentrated solution, the wrinkled papaya concentrated solution and the pomegranate concentrated solution prepared in the embodiment 1 at a speed of 150r/min for 10min until the materials are uniformly dissolved, cooling the mixture to 20 ℃ with ice water, centrifuging the mixture at a high speed of 5000-6000 r/min, and filtering the mixture with a 100-mesh screen to obtain an intermediate solution. The intermediate solution was transferred to a blending tank.
Putting selenium-enriched cardamine violifolia into a shearing cylinder according to the formula amount, adding 500L of water for dissolving, and operating the following parameters: the linear velocity is 40-60 m/s, the pressure is 15000PSi, the output flow is 3000L/h, the rotating speed is 10000rpm, and the selenium-rich cardamine violifolia liquid which is uniformly dissolved is obtained. Adding the selenium-rich cardamine violifolia liquid into a blending tank, and continuously stirring and mixing for 10 min.
And (3) supplementing water and fixing the volume, sampling while adding water, detecting the pH value, and adjusting to 4.4-4.6 to obtain the product.
And S2, sterilizing by UHT high-temperature instant sterilization at 136 +/-2 ℃ for 6S.
S3, passing through an ice water cooling pipe to 95-100 ℃, and hot filling.
S4, secondary sterilization: filling, arranging, sterilizing in a sterilizing kettle for the second time, and spray sterilizing for 25 min.
And S5, carrying out conveyor belt bottle body cold drying, bottle shoulder blow drying, code spraying, arraying, boxing and date printing to obtain a finished product.
Example 4
The present example provides a selenium enriched beverage having the composition as shown in the following table:
| raw materials | Content (wt.) |
| Composite feed liquid of vine tea and cyclocarya paliurus prepared in example 1 | 500ml/L |
| Concentrated solution of wrinkled papaya | 0.8g/L |
| Pomegranate concentrate | 0.8g/L |
| Momordica grosvenori concentrated solution | 1.5g/L |
| Selenium-rich cardamine violifolia | 0.14g/L |
The preparation method of the selenium-enriched beverage is the same as that of the embodiment 3.
Example 5
The present example provides a selenium enriched beverage having the composition as shown in the following table:
the preparation method of the selenium-enriched beverage is the same as that of the embodiment 3.
Example 6
The present example provides a selenium enriched beverage having the composition as shown in the following table:
| raw materials | Content (wt.) |
| Compound vine tea and cyclocarya paliurus prepared in example 1Feed liquid | 700ml/L |
| Concentrated solution of wrinkled papaya | 1.2g/L |
| Pomegranate concentrate | 1.2g/L |
| Momordica grosvenori concentrated solution | 1.9g/L |
| Selenium-rich cardamine violifolia | 0.16g/L |
The preparation method of the selenium-enriched beverage is the same as that of the embodiment 3.
Example 7
The present example provides a selenium enriched beverage having the composition as shown in the following table:
| raw materials | Content (wt.) |
| Composite feed liquid of vine tea and cyclocarya paliurus prepared in example 1 | 800ml/L |
| Concentrated solution of wrinkled papaya | 1.4g/L |
| Pomegranate concentrate | 1.4g/L |
| Momordica grosvenori concentrated solution | 2.1g/L |
| Selenium-rich cardamine violifolia | 0.17g/L |
The preparation method of the selenium-enriched beverage is the same as that of the embodiment 3.
The selenium-enriched beverages prepared in examples 3 to 7 were subjected to sensory evaluation, and the evaluation results are shown in the following table:
as can be seen from the above table, the selenium-enriched beverages prepared in examples 3 to 7 meet the requirements specified by the general standards, have stable color and sensory properties, can be stored for more than 12 months without deterioration even without adding any preservative, are bright in color, clear and transparent, and maintain the original flavor of the ampelopsis grossedentata and cyclocarya paliurus leaf composite beverage.
In addition, it is worth explaining that the inventor team also carries out research on the dosage proportion of the wrinkled pAN _ SNer papaya concentrated solution and the pomegranate concentrated solution in the selenium-rich beverage, and the statistical results are shown in the following table:
the composite selenium-rich beverage of the vine tea and the cyclocarya paliurus restores the unique tea drink flavor of the vine tea through a plant extraction process, and retains the sweet taste of the cyclocarya paliurus leaf tea. The selenium-rich compound plant beverage contains total flavonoids up to 50mg/100mL and polysaccharides up to 400mg/100mL, contains various active ingredients such as flavonoids, triterpenes, steroids and lactones, and has obvious effects of protecting liver, reducing blood sugar and diminishing inflammation. Especially, one or two bottles of selenium-rich beverage are drunk before drinking, and the selenium-rich beverage does not make people feel tired of drinking, so that the selenium-rich beverage can help the human body to decompose alcohol and protect the liver in time. The selenium-rich beverage does not contain metabolizable sugar of human body, and the blood sugar lowering effect of the vine tea and the cyclocarya paliurus is cooperated with multiple components, multiple sites and multiple links, so that the selenium-rich beverage can be drunk by diabetic patients.
It should be noted that the above examples are only for further illustration and description of the technical solution of the present invention, and are not intended to further limit the technical solution of the present invention, and the method of the present invention is only a preferred embodiment, and is not intended to limit the protection scope of the present invention. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.
Claims (10)
1. The preparation method of the ampelopsis grossedentata and cyclocarya paliurus composite feed liquid is characterized by comprising the following steps:
putting the vine tea and the cyclocarya paliurus leaves into extraction equipment according to the weight ratio of (7-9) to (2-4), and extracting according to the material-liquid ratio of 1kg to (40-60): extracting at 70-80 ℃ for 20-60 min, and filtering to obtain the composite feed liquid.
2. The composite feed liquid of the ampelopsis grossedentata and cyclocarya paliurus as claimed in claim 1, wherein the extraction process further comprises stirring, and the stirring speed is 10-20 r/min.
3. The selenium-enriched beverage is characterized by being an aqueous solution mainly prepared by mixing the following raw materials, wherein the pH value is 4.4-4.6:
4. the selenium-enriched beverage of claim 3, wherein the weight ratio of the Chaenomeles speciosa nakai concentrate to the pomegranate concentrate is 1: 1.
5. The selenium-enriched beverage as claimed in claim 3 or 4, which is an aqueous solution mainly prepared by mixing the following raw materials, and has a pH of 4.4-4.6:
6. the method for preparing the selenium-enriched beverage as claimed in any one of claims 3 to 5, which is characterized by comprising the following steps:
preparing composite feed liquid of the vine tea and the cyclocarya paliurus, and placing the composite feed liquid in a liquid storage tank;
respectively adding the momordica grosvenori concentrated solution, the wrinkled papaya concentrated solution and the pomegranate concentrated solution into the liquid storage tank, stirring until the momordica grosvenori concentrated solution, the wrinkled papaya concentrated solution and the pomegranate concentrated solution are uniformly dissolved, cooling, centrifuging and filtering to obtain an intermediate solution;
transferring the intermediate solution into a blending tank, adding the selenium-rich cardamine violifolia solution, supplementing water to a constant volume, and adjusting the pH to 4.4-4.6;
and (5) sterilizing and filling.
7. The preparation method of the selenium-enriched beverage according to claim 6, wherein the preparation process of the selenium-enriched cardamine violifolia solution comprises the following steps: putting selenium-rich cardamine violifolia into a shearing cylinder, adding a proper amount of water to dissolve, and performing operation parameters of: and (3) obtaining the uniformly dissolved selenium-rich cardamine violifolia solution under the pressure of 15000PSi, the linear speed of 40-60 m/s, the output flow of 3000L/h and the rotation speed of 10000 rpm.
8. The method for preparing the selenium-enriched beverage according to claim 6, wherein the rotation speed of the centrifugation is 5000-6000 r/min; and/or
The filtration is performed by using a 100-mesh stainless steel screen.
9. The method for preparing the selenium-enriched beverage as claimed in any one of claims 6 to 8, wherein the sterilization process parameters are as follows: and (3) carrying out sterilization by adopting an UHT high-temperature instantaneous sterilization method at 136 +/-2 ℃ for 5-8 s.
10. The preparation method of the selenium-enriched beverage as claimed in claim 9, wherein the filling is performed by hot filling at 95-100 ℃.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115381091A (en) * | 2022-08-24 | 2022-11-25 | 湖南宝硒生物科技有限公司 | Method and device for preparing selenium-rich ferment peptide effervescent tablets |
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| CN106616132A (en) * | 2016-12-01 | 2017-05-10 | 恩施硒多宝饮品有限公司 | Selenium-enriched original plant beverage and preparation method thereof |
| CN108552533A (en) * | 2018-03-20 | 2018-09-21 | 硒多宝饮品集团股份有限公司 | A kind of composite plant original drink and preparation method thereof |
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Patent Citations (5)
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| CN105941735A (en) * | 2016-04-29 | 2016-09-21 | 湖北国技硒产品研发有限公司 | Selenium-enriched ampelopsis grossedentata tea beverage and preparation method thereof |
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| CN115381091A (en) * | 2022-08-24 | 2022-11-25 | 湖南宝硒生物科技有限公司 | Method and device for preparing selenium-rich ferment peptide effervescent tablets |
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