CN114209605A - Preparation method of air cushion loose powder - Google Patents
Preparation method of air cushion loose powder Download PDFInfo
- Publication number
- CN114209605A CN114209605A CN202210070348.2A CN202210070348A CN114209605A CN 114209605 A CN114209605 A CN 114209605A CN 202210070348 A CN202210070348 A CN 202210070348A CN 114209605 A CN114209605 A CN 114209605A
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- China
- Prior art keywords
- loose powder
- finished product
- powder
- uniformly mixing
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 239000000843 powder Substances 0.000 title claims abstract description 44
- 238000002360 preparation method Methods 0.000 title claims abstract description 12
- 239000000463 material Substances 0.000 claims abstract description 50
- 238000002156 mixing Methods 0.000 claims abstract description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000011265 semifinished product Substances 0.000 claims abstract description 24
- 239000006185 dispersion Substances 0.000 claims abstract description 21
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 16
- 239000005017 polysaccharide Substances 0.000 claims abstract description 16
- 239000003974 emollient agent Substances 0.000 claims abstract description 14
- 239000003995 emulsifying agent Substances 0.000 claims abstract description 14
- 238000011049 filling Methods 0.000 claims abstract description 13
- 238000004108 freeze drying Methods 0.000 claims abstract description 13
- 239000003755 preservative agent Substances 0.000 claims abstract description 13
- 230000002335 preservative effect Effects 0.000 claims abstract description 13
- 239000000047 product Substances 0.000 claims abstract description 13
- 239000003906 humectant Substances 0.000 claims abstract description 12
- 238000012856 packing Methods 0.000 claims abstract description 10
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 238000001035 drying Methods 0.000 claims description 18
- 239000000945 filler Substances 0.000 claims description 16
- 150000004804 polysaccharides Chemical class 0.000 claims description 15
- 238000003795 desorption Methods 0.000 claims description 12
- 239000000203 mixture Substances 0.000 claims description 12
- 238000000859 sublimation Methods 0.000 claims description 12
- 230000008022 sublimation Effects 0.000 claims description 12
- 239000000049 pigment Substances 0.000 claims description 11
- -1 hydroxymethyl lactone Chemical class 0.000 claims description 10
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 6
- 239000013078 crystal Substances 0.000 claims description 6
- 230000005496 eutectics Effects 0.000 claims description 6
- 239000001023 inorganic pigment Substances 0.000 claims description 6
- 239000003921 oil Substances 0.000 claims description 6
- 235000019198 oils Nutrition 0.000 claims description 6
- 239000012860 organic pigment Substances 0.000 claims description 6
- 239000010445 mica Substances 0.000 claims description 5
- 229910052618 mica group Inorganic materials 0.000 claims description 5
- 229920005862 polyol Polymers 0.000 claims description 5
- 150000003077 polyols Chemical class 0.000 claims description 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 4
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 claims description 4
- SHZIWNPUGXLXDT-UHFFFAOYSA-N ethyl hexanoate Chemical compound CCCCCC(=O)OCC SHZIWNPUGXLXDT-UHFFFAOYSA-N 0.000 claims description 4
- 235000014593 oils and fats Nutrition 0.000 claims description 4
- PRAKJMSDJKAYCZ-UHFFFAOYSA-N squalane Chemical compound CC(C)CCCC(C)CCCC(C)CCCCC(C)CCCC(C)CCCC(C)C PRAKJMSDJKAYCZ-UHFFFAOYSA-N 0.000 claims description 4
- 229920003229 poly(methyl methacrylate) Polymers 0.000 claims description 3
- 239000004926 polymethyl methacrylate Substances 0.000 claims description 3
- 239000000377 silicon dioxide Substances 0.000 claims description 3
- 239000004408 titanium dioxide Substances 0.000 claims description 3
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 claims description 2
- GYDYJUYZBRGMCC-INIZCTEOSA-N (2s)-2-amino-6-(dodecanoylamino)hexanoic acid Chemical compound CCCCCCCCCCCC(=O)NCCCC[C@H](N)C(O)=O GYDYJUYZBRGMCC-INIZCTEOSA-N 0.000 claims description 2
- MXOAEAUPQDYUQM-QMMMGPOBSA-N (S)-chlorphenesin Chemical compound OC[C@H](O)COC1=CC=C(Cl)C=C1 MXOAEAUPQDYUQM-QMMMGPOBSA-N 0.000 claims description 2
- PIKLCICIOVIUJV-UHFFFAOYSA-N 2-[2-(2,3-dihydroxypropoxy)-2-oxoethyl]-2-hydroxybutanedioic acid;octadecanoic acid Chemical compound OCC(O)COC(=O)CC(O)(C(O)=O)CC(O)=O.CCCCCCCCCCCCCCCCCC(O)=O PIKLCICIOVIUJV-UHFFFAOYSA-N 0.000 claims description 2
- OJRQBZGHEZSVFW-UHFFFAOYSA-N 2-octadecanoyloxyoctadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC(C(O)=O)CCCCCCCCCCCCCCCC OJRQBZGHEZSVFW-UHFFFAOYSA-N 0.000 claims description 2
- LEACJMVNYZDSKR-UHFFFAOYSA-N 2-octyldodecan-1-ol Chemical compound CCCCCCCCCCC(CO)CCCCCCCC LEACJMVNYZDSKR-UHFFFAOYSA-N 0.000 claims description 2
- QCDWFXQBSFUVSP-UHFFFAOYSA-N 2-phenoxyethanol Chemical compound OCCOC1=CC=CC=C1 QCDWFXQBSFUVSP-UHFFFAOYSA-N 0.000 claims description 2
- NCZPCONIKBICGS-UHFFFAOYSA-N 3-(2-ethylhexoxy)propane-1,2-diol Chemical compound CCCCC(CC)COCC(O)CO NCZPCONIKBICGS-UHFFFAOYSA-N 0.000 claims description 2
- KGKQNDQDVZQTAG-UHFFFAOYSA-N 8-methylnonyl 2,2-dimethylpropanoate Chemical compound CC(C)CCCCCCCOC(=O)C(C)(C)C KGKQNDQDVZQTAG-UHFFFAOYSA-N 0.000 claims description 2
- 244000215068 Acacia senegal Species 0.000 claims description 2
- 229920001817 Agar Polymers 0.000 claims description 2
- 239000005995 Aluminium silicate Substances 0.000 claims description 2
- 229910052582 BN Inorganic materials 0.000 claims description 2
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 2
- 241000206575 Chondrus crispus Species 0.000 claims description 2
- 229920002558 Curdlan Polymers 0.000 claims description 2
- 239000001879 Curdlan Substances 0.000 claims description 2
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 claims description 2
- 108010010803 Gelatin Proteins 0.000 claims description 2
- 229920002148 Gellan gum Polymers 0.000 claims description 2
- 229920000084 Gum arabic Polymers 0.000 claims description 2
- 241001072282 Limnanthes Species 0.000 claims description 2
- 229930195725 Mannitol Natural products 0.000 claims description 2
- 239000004909 Moisturizer Substances 0.000 claims description 2
- 229910019142 PO4 Inorganic materials 0.000 claims description 2
- 229920006197 POE laurate Polymers 0.000 claims description 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 2
- 229920001213 Polysorbate 20 Polymers 0.000 claims description 2
- 229920001214 Polysorbate 60 Polymers 0.000 claims description 2
- 229920002472 Starch Polymers 0.000 claims description 2
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 claims description 2
- 235000018936 Vitellaria paradoxa Nutrition 0.000 claims description 2
- 241001135917 Vitellaria paradoxa Species 0.000 claims description 2
- 239000000205 acacia gum Substances 0.000 claims description 2
- 235000010489 acacia gum Nutrition 0.000 claims description 2
- 239000008272 agar Substances 0.000 claims description 2
- 235000010419 agar Nutrition 0.000 claims description 2
- 235000012211 aluminium silicate Nutrition 0.000 claims description 2
- FKIQSOGFDBALHA-UHFFFAOYSA-L aluminum trimagnesium potassium dioxido(oxo)silane oxygen(2-) difluoride Chemical compound [O--].[F-].[F-].[Mg++].[Mg++].[Mg++].[Al+3].[K+].[O-][Si]([O-])=O.[O-][Si]([O-])=O.[O-][Si]([O-])=O FKIQSOGFDBALHA-UHFFFAOYSA-L 0.000 claims description 2
- 230000002421 anti-septic effect Effects 0.000 claims description 2
- BTFJIXJJCSYFAL-UHFFFAOYSA-N arachidyl alcohol Natural products CCCCCCCCCCCCCCCCCCCCO BTFJIXJJCSYFAL-UHFFFAOYSA-N 0.000 claims description 2
- 239000008163 avocado oil Substances 0.000 claims description 2
- 235000021302 avocado oil Nutrition 0.000 claims description 2
- UHHXUPJJDHEMGX-UHFFFAOYSA-K azanium;manganese(3+);phosphonato phosphate Chemical compound [NH4+].[Mn+3].[O-]P([O-])(=O)OP([O-])([O-])=O UHHXUPJJDHEMGX-UHFFFAOYSA-K 0.000 claims description 2
- IRERQBUNZFJFGC-UHFFFAOYSA-L azure blue Chemical compound [Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Na+].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[S-]S[S-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-].[O-][Si]([O-])([O-])[O-] IRERQBUNZFJFGC-UHFFFAOYSA-L 0.000 claims description 2
- 235000013871 bee wax Nutrition 0.000 claims description 2
- 239000012166 beeswax Substances 0.000 claims description 2
- 229940092738 beeswax Drugs 0.000 claims description 2
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 2
- 235000012745 brilliant blue FCF Nutrition 0.000 claims description 2
- 235000012730 carminic acid Nutrition 0.000 claims description 2
- 239000004106 carminic acid Substances 0.000 claims description 2
- 239000001913 cellulose Substances 0.000 claims description 2
- 229920002678 cellulose Polymers 0.000 claims description 2
- PZTQVMXMKVTIRC-UHFFFAOYSA-L chembl2028348 Chemical compound [Ca+2].[O-]S(=O)(=O)C1=CC(C)=CC=C1N=NC1=C(O)C(C([O-])=O)=CC2=CC=CC=C12 PZTQVMXMKVTIRC-UHFFFAOYSA-L 0.000 claims description 2
- 229960003993 chlorphenesin Drugs 0.000 claims description 2
- 229910000423 chromium oxide Inorganic materials 0.000 claims description 2
- 229940080423 cochineal Drugs 0.000 claims description 2
- 229920006037 cross link polymer Polymers 0.000 claims description 2
- 235000019316 curdlan Nutrition 0.000 claims description 2
- 229940078035 curdlan Drugs 0.000 claims description 2
- 229940008099 dimethicone Drugs 0.000 claims description 2
- 239000004205 dimethyl polysiloxane Substances 0.000 claims description 2
- 235000013870 dimethyl polysiloxane Nutrition 0.000 claims description 2
- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 claims description 2
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 claims description 2
- VPWFPZBFBFHIIL-UHFFFAOYSA-L disodium 4-[(4-methyl-2-sulfophenyl)diazenyl]-3-oxidonaphthalene-2-carboxylate Chemical compound [Na+].[Na+].[O-]S(=O)(=O)C1=CC(C)=CC=C1N=NC1=C(O)C(C([O-])=O)=CC2=CC=CC=C12 VPWFPZBFBFHIIL-UHFFFAOYSA-L 0.000 claims description 2
- 229940100524 ethylhexylglycerin Drugs 0.000 claims description 2
- 239000008273 gelatin Substances 0.000 claims description 2
- 229920000159 gelatin Polymers 0.000 claims description 2
- 235000019322 gelatine Nutrition 0.000 claims description 2
- 235000011852 gelatine desserts Nutrition 0.000 claims description 2
- 239000000216 gellan gum Substances 0.000 claims description 2
- 235000010492 gellan gum Nutrition 0.000 claims description 2
- 239000011521 glass Substances 0.000 claims description 2
- 235000011187 glycerol Nutrition 0.000 claims description 2
- 229930182470 glycoside Natural products 0.000 claims description 2
- 239000008169 grapeseed oil Substances 0.000 claims description 2
- 239000008172 hydrogenated vegetable oil Substances 0.000 claims description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 2
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 claims description 2
- 229940025902 konjac mannan Drugs 0.000 claims description 2
- 239000000594 mannitol Substances 0.000 claims description 2
- 235000010355 mannitol Nutrition 0.000 claims description 2
- 229910044991 metal oxide Inorganic materials 0.000 claims description 2
- 150000004706 metal oxides Chemical class 0.000 claims description 2
- LXCFILQKKLGQFO-UHFFFAOYSA-N methylparaben Chemical compound COC(=O)C1=CC=C(O)C=C1 LXCFILQKKLGQFO-UHFFFAOYSA-N 0.000 claims description 2
- 239000011707 mineral Substances 0.000 claims description 2
- 230000001333 moisturizer Effects 0.000 claims description 2
- JXTPJDDICSTXJX-UHFFFAOYSA-N n-Triacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 claims description 2
- 229940049964 oleate Drugs 0.000 claims description 2
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 claims description 2
- 229960005323 phenoxyethanol Drugs 0.000 claims description 2
- GVKCHTBDSMQENH-UHFFFAOYSA-L phloxine B Chemical compound [Na+].[Na+].[O-]C(=O)C1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1C1=C2C=C(Br)C(=O)C(Br)=C2OC2=C(Br)C([O-])=C(Br)C=C21 GVKCHTBDSMQENH-UHFFFAOYSA-L 0.000 claims description 2
- 239000010452 phosphate Substances 0.000 claims description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims description 2
- 229920000435 poly(dimethylsiloxane) Polymers 0.000 claims description 2
- 239000000256 polyoxyethylene sorbitan monolaurate Substances 0.000 claims description 2
- 235000010486 polyoxyethylene sorbitan monolaurate Nutrition 0.000 claims description 2
- 235000010482 polyoxyethylene sorbitan monooleate Nutrition 0.000 claims description 2
- 229920000053 polysorbate 80 Polymers 0.000 claims description 2
- 229920002635 polyurethane Polymers 0.000 claims description 2
- 239000004814 polyurethane Substances 0.000 claims description 2
- RUOJZAUFBMNUDX-UHFFFAOYSA-N propylene carbonate Chemical compound CC1COC(=O)O1 RUOJZAUFBMNUDX-UHFFFAOYSA-N 0.000 claims description 2
- 229940057910 shea butter Drugs 0.000 claims description 2
- 229940032094 squalane Drugs 0.000 claims description 2
- 239000008107 starch Substances 0.000 claims description 2
- 235000019698 starch Nutrition 0.000 claims description 2
- UJMBCXLDXJUMFB-UHFFFAOYSA-K trisodium;5-oxo-1-(4-sulfonatophenyl)-4-[(4-sulfonatophenyl)diazenyl]-4h-pyrazole-3-carboxylate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1N=NC1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-UHFFFAOYSA-K 0.000 claims description 2
- 235000013799 ultramarine blue Nutrition 0.000 claims description 2
- 235000013311 vegetables Nutrition 0.000 claims description 2
- 239000001993 wax Substances 0.000 claims description 2
- 229940045860 white wax Drugs 0.000 claims description 2
- 229920001285 xanthan gum Polymers 0.000 claims description 2
- 239000000230 xanthan gum Substances 0.000 claims description 2
- 235000010493 xanthan gum Nutrition 0.000 claims description 2
- 229940082509 xanthan gum Drugs 0.000 claims description 2
- 229920001221 xylan Polymers 0.000 claims description 2
- 150000004823 xylans Chemical class 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 8
- JHWNWJKBPDFINM-UHFFFAOYSA-N Laurolactam Chemical compound O=C1CCCCCCCCCCCN1 JHWNWJKBPDFINM-UHFFFAOYSA-N 0.000 claims 1
- 229920000299 Nylon 12 Polymers 0.000 claims 1
- 239000000428 dust Substances 0.000 abstract description 3
- 230000000694 effects Effects 0.000 abstract description 2
- 238000009700 powder processing Methods 0.000 abstract description 2
- 150000004676 glycans Chemical class 0.000 abstract 1
- 239000004677 Nylon Substances 0.000 description 1
- 239000007983 Tris buffer Substances 0.000 description 1
- 239000004519 grease Substances 0.000 description 1
- 125000004029 hydroxymethyl group Chemical group [H]OC([H])([H])* 0.000 description 1
- 150000002596 lactones Chemical class 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229920001778 nylon Polymers 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/26—Aluminium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/25—Silicon; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/29—Titanium; Compounds thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8152—Homopolymers or copolymers of esters, e.g. (meth)acrylic acid esters; Compositions of derivatives of such polymers
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/88—Polyamides
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/12—Face or body powders for grooming, adorning or absorbing
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/42—Colour properties
- A61K2800/43—Pigments; Dyes
- A61K2800/436—Interference pigments, e.g. Iridescent, Pearlescent
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/87—Application Devices; Containers; Packaging
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
Abstract
The invention discloses a preparation method of air cushion loose powder, belonging to the technical field of air cushion loose powder processing, comprising the following steps: (1) uniformly mixing the powder phases to obtain a material body A, uniformly mixing the natural polysaccharide and water, adding the emollient humectant and the emulsifier, and uniformly mixing to obtain a material body B; (2) uniformly mixing the material body A and the material body B obtained in the step (1), and then adding a preservative to obtain a dispersion; (3) heating the dispersion to a preset temperature, and then filling the dispersion into a packing material to obtain a semi-finished product; (4) and (5) freeze-drying the semi-finished product to obtain a finished product. The application has solved the common loose powder in existing market and has mainly used direct filling package material as main, interior material singleness, the filling dust is serious, and package material utilization is low, and the colour variety is single, and package material is with high costs, can't realize the secondary or then technical problem of the value of repetitious utilization, has reached what colour or then skin sense needs, directly changes the technical effect that the inner core can.
Description
Technical Field
The invention belongs to the technical field of air cushion loose powder processing, and particularly relates to a preparation method of air cushion loose powder.
Background
The common loose powder in the market at present mainly takes a direct filling packing material as a main material, the inner material is single, the filling dust is serious, the utilization rate of the packing material is low, the color and variety are single, and the packing material cost is high. The value of secondary or multiple utilization cannot be realized.
Disclosure of Invention
The invention aims to provide a preparation method of air cushion loose powder aiming at the existing problems.
The invention is realized by the following technical scheme:
a preparation method of air cushion loose powder comprises the following steps:
(1) uniformly mixing the powder phases to obtain a material body A, uniformly mixing the natural polysaccharide and water, adding the emollient humectant and the emulsifier, and uniformly mixing to obtain a material body B;
(2) uniformly mixing the material body A and the material body B obtained in the step (1), and then adding a preservative to obtain a dispersion;
(3) heating the dispersion to a preset temperature, and then filling the dispersion into a packing material to obtain a semi-finished product;
(4) and (5) freeze-drying the semi-finished product to obtain a finished product.
Further, the powder phase in the step (1) comprises a flaky filler, a spherical filler and a pigment.
Further, the flaky filler in the step (1) is talc powder, mica powder, kaolin, lauroyl lysine, boron nitride or a mixture of any combination thereof, the spherical filler is PMMA, chinlon-12, polyurethane, HDI/tris (hydroxymethyl) lactone crosslinked polymer, silica or a mixture of any combination thereof, and the pigment is an inorganic pigment, an organic pigment, pearlescence or a mixture of any combination thereof; the inorganic pigments include titanium dioxide, iron oxide, red, yellow, black, manganese violet, ultramarine blue, chromium oxide optionally in hydrated combination, ferric blue; the organic pigment comprises cochineal, red 6, red 7, blue 1, yellow 5 and red 28 lake pigment; the pearlescence includes white pearlescence, colored and dyed pearlescence, organic or inorganic pigment-containing mica, glass, synthetic fluorophlogopite material dyed pearlescence and metal oxide pearlescence.
Further, the natural polysaccharide and the water in the step (1) are mixed at the temperature of 0-50 ℃.
Further, the natural polysaccharide in step (1) is cellulose, xanthan gum, Chondrus crispus, agar, gum arabic, starch, curdlan, gelatin, gellan gum, konjac mannan, mannitol, xylan or a mixture of any combination thereof; emollient moisturizers are oils and fats, polyols, or combinations thereof, wherein the oils and fats comprise oils or waxes of vegetable, mineral, animal, or synthetic origin, grapeseed oil, meadowfoam oil, hydrogenated vegetable oil, avocado oil, shea butter, white oil, cetostearyl ethyl hexanoate, squalane, octyldodecanol stearoyloxystearate, propylene carbonate, isodecyl pivalate, dimethicone, beeswax, white wax, the polyols comprise glycerin, butylene glycol, propylene glycol, dipropylene glycol; the emulsifier is PEG26-PPG-30 phosphate, tween-20, tween-60, tween-80, alkyl glycoside, polyoxyethylene oleate, polyoxyethylene laurate, glyceryl citrate stearate or their mixture; the antiseptic is chlorphenesin, methyl hydroxybenzoate, phenoxyethanol, ethylhexylglycerin, octylglycol, or their mixture.
Further, the weight parts of the powder phase are 30-60 parts, the weight parts of the emollient humectant are 0.2-20 parts, the weight parts of the emulsifier are 0-5 parts, and the weight parts of the preservative are 0.05-3 parts.
Further, the preset temperature in the step (3) is 30-55 ℃.
Further, the weight percentage of water in the finished product in the step (4) is less than or equal to 5 percent.
Further, during the freeze drying in the step (4), the semi-finished product is firstly put into a freeze dryer and frozen at a low temperature, the temperature of the freeze dryer is lower than the eutectic point, then the freeze dryer is vacuumized, the temperature is raised to carry out sublimation drying after the vacuum degree reaches a preset vacuum value, the ice crystals are removed, and finally, the desorption drying is carried out after the sublimation is finished, and the bound water is removed.
Further, the temperature of the freeze dryer is-30 to-10 ℃, the preset vacuum is 10 to 40Pa, the desorption drying temperature is 5 to 60 ℃, and the pressure is 10 to 50 Pa.
Compared with the prior art, the invention has the following advantages:
the application has solved the common loose powder in existing market and has mainly used direct filling package material as main, interior material singleness, the filling dust is serious, and package material utilization is low, and the colour variety is single, and package material is with high costs, can't realize the secondary or then technical problem of the value of repetitious utilization, has reached what colour or then skin sense needs, directly changes the technical effect that the inner core can.
Detailed Description
Example 1:
a preparation method of air cushion loose powder comprises the following steps:
(1) uniformly mixing the powder phases to obtain a material body A, uniformly mixing the natural polysaccharide and water, adding the emollient humectant and the emulsifier, and uniformly mixing to obtain a material body B;
(2) uniformly mixing the material body A and the material body B obtained in the step (1), and then adding a preservative to obtain a dispersion;
(3) heating the dispersion to a preset temperature, and then filling the dispersion into a packing material to obtain a semi-finished product;
(4) and (5) freeze-drying the semi-finished product to obtain a finished product.
The powder phase in the step (1) comprises flaky fillers, spherical fillers and pigments.
Mixing the natural polysaccharide and the water in the step (1) at the temperature of 0 ℃.
30 parts of powder phase, 0.2 part of emollient humectant, 0 part of emulsifier and 0.05 part of preservative.
The preset temperature in step (3) is 30 ℃.
The weight percentage of water in the finished product in the step (4) is less than or equal to 5 percent.
During freeze drying in the step (4), firstly, the semi-finished product is put into a freeze dryer to be frozen at a low temperature, the temperature of the freeze dryer is lower than the eutectic point, then the freeze dryer is vacuumized, the temperature is raised to carry out sublimation drying after the vacuum degree reaches a preset vacuum numerical value, ice crystals are removed, and finally, the semi-finished product is subjected to desorption drying after sublimation is finished, and bound water is removed.
The temperature of the freeze dryer is-30 ℃, the preset vacuum is 10Pa, the desorption drying temperature is 5 ℃, and the pressure is 10 Pa.
Example 2:
a preparation method of air cushion loose powder comprises the following steps:
(1) uniformly mixing the powder phases to obtain a material body A, uniformly mixing the natural polysaccharide and water, adding the emollient humectant and the emulsifier, and uniformly mixing to obtain a material body B;
(2) uniformly mixing the material body A and the material body B obtained in the step (1), and then adding a preservative to obtain a dispersion;
(3) heating the dispersion to a preset temperature, and then filling the dispersion into a packing material to obtain a semi-finished product;
(4) and (5) freeze-drying the semi-finished product to obtain a finished product.
The powder phase in the step (1) comprises flaky fillers, spherical fillers and pigments.
Mixing the natural polysaccharide and the water in the step (1) at the temperature of 25 ℃.
45 parts of powder phase, 10.9 parts of emollient humectant, 2.5 parts of emulsifier and 1.55 parts of preservative.
The preset temperature in step (3) is 42.5 ℃.
The weight percentage of water in the finished product in the step (4) is less than or equal to 5 percent.
During freeze drying in the step (4), firstly, the semi-finished product is put into a freeze dryer to be frozen at a low temperature, the temperature of the freeze dryer is lower than the eutectic point, then the freeze dryer is vacuumized, the temperature is raised to carry out sublimation drying after the vacuum degree reaches a preset vacuum numerical value, ice crystals are removed, and finally, the semi-finished product is subjected to desorption drying after sublimation is finished, and bound water is removed.
The temperature of the freeze dryer is-20 ℃, the preset vacuum is 25Pa, the desorption drying temperature is 32.5 ℃, and the pressure is 30 Pa.
Example 3:
a preparation method of air cushion loose powder comprises the following steps:
(1) uniformly mixing the powder phases to obtain a material body A, uniformly mixing the natural polysaccharide and water, adding the emollient humectant and the emulsifier, and uniformly mixing to obtain a material body B;
(2) uniformly mixing the material body A and the material body B obtained in the step (1), and then adding a preservative to obtain a dispersion;
(3) heating the dispersion to a preset temperature, and then filling the dispersion into a packing material to obtain a semi-finished product;
(4) and (5) freeze-drying the semi-finished product to obtain a finished product.
The powder phase in the step (1) comprises flaky fillers, spherical fillers and pigments.
And (2) mixing the natural polysaccharide and water in the step (1) at the temperature of 0-50 ℃.
60 parts of powder phase, 20 parts of emollient humectant, 5 parts of emulsifier and 3 parts of preservative.
The preset temperature in step (3) is 55 ℃.
The weight percentage of water in the finished product in the step (4) is less than or equal to 5 percent.
During freeze drying in the step (4), firstly, the semi-finished product is put into a freeze dryer to be frozen at a low temperature, the temperature of the freeze dryer is lower than the eutectic point, then the freeze dryer is vacuumized, the temperature is raised to carry out sublimation drying after the vacuum degree reaches a preset vacuum numerical value, ice crystals are removed, and finally, the semi-finished product is subjected to desorption drying after sublimation is finished, and bound water is removed.
The temperature of the freeze dryer is-10 ℃, the preset vacuum is 40Pa, the desorption drying temperature is 60 ℃, and the pressure is 50 Pa.
Example 4:
a preparation method of air cushion loose powder comprises the following steps:
(1) uniformly mixing the powder phases to obtain a material body A, uniformly mixing the natural polysaccharide and water, adding the emollient humectant and the emulsifier, and uniformly mixing to obtain a material body B;
(2) uniformly mixing the material body A and the material body B obtained in the step (1), and then adding a preservative to obtain a dispersion;
(3) heating the dispersion to a preset temperature, and then filling the dispersion into a packing material to obtain a semi-finished product;
(4) and (5) freeze-drying the semi-finished product to obtain a finished product.
The powder phase in the step (1) comprises flaky fillers, spherical fillers and pigments.
Mixing the natural polysaccharide and the water in the step (1) at the temperature of 25 ℃.
The weight parts of the raw materials are as follows: 20 parts of mica, 40 parts of silica, 10 parts of PMMA, 1210 parts of nylon, 5 parts of titanium dioxide, 1 part of polysaccharide, 2 parts of polyol, 1 part of grease and 1 part of preservative.
The preset temperature in step (3) is 42.5 ℃.
The weight percentage of water in the finished product in the step (4) is less than or equal to 5 percent.
During freeze drying in the step (4), firstly, the semi-finished product is put into a freeze dryer to be frozen at a low temperature, the temperature of the freeze dryer is lower than the eutectic point, then the freeze dryer is vacuumized, the temperature is raised to carry out sublimation drying after the vacuum degree reaches a preset vacuum numerical value, ice crystals are removed, and finally, the semi-finished product is subjected to desorption drying after sublimation is finished, and bound water is removed.
The temperature of the freeze dryer is-20 ℃, the preset vacuum is 25Pa, the desorption drying temperature is 32.5 ℃, and the pressure is 30 Pa.
Having thus described in detail preferred embodiments of the present invention, it will be appreciated that modifications and variations can be resorted to without departing from the spirit and scope of the invention as defined by the appended claims.
Claims (10)
1. The preparation method of the air cushion loose powder is characterized by comprising the following steps:
(1) uniformly mixing the powder phases to obtain a material body A, uniformly mixing the natural polysaccharide and water, adding the emollient humectant and the emulsifier, and uniformly mixing to obtain a material body B;
(2) uniformly mixing the material body A and the material body B obtained in the step (1), and then adding a preservative to obtain a dispersion;
(3) heating the dispersion to a preset temperature, and then filling the dispersion into a packing material to obtain a semi-finished product;
(4) and (5) freeze-drying the semi-finished product to obtain a finished product.
2. The method for preparing air-cushion loose powder as claimed in claim 1, wherein the powder phase in step (1) comprises plate-like filler, spherical filler and pigment.
3. The method for preparing air-cushion loose powder according to claim 2, characterized in that the flake filler in step (1) is selected from talcum powder, mica powder, kaolin, lauroyl lysine, boron nitride, or a mixture of any combination thereof, the spherical filler is selected from PMMA, nylon-12, polyurethane, HDI/hydroxymethyl lactone crosslinked polymer, silica, or a mixture of any combination thereof, and the pigment is selected from inorganic pigment, organic pigment, pearlescent pigment, or a mixture of any combination thereof; the inorganic pigments include titanium dioxide, iron oxide, red, yellow, black, manganese violet, ultramarine blue, chromium oxide optionally in hydrated combination, ferric blue; the organic pigment comprises cochineal, red 6, red 7, blue 1, yellow 5 and red 28 lake pigment; the pearlescence includes white pearlescence, colored and dyed pearlescence, organic or inorganic pigment-containing mica, glass, synthetic fluorophlogopite material dyed pearlescence and metal oxide pearlescence.
4. The method for preparing air cushion loose powder as claimed in claim 1, wherein the natural polysaccharide and water in step (1) are mixed at 0-50 ℃.
5. The method for preparing air cushion loose powder as claimed in claim 1, wherein the natural polysaccharide in step (1) is selected from cellulose, xanthan gum, Chondrus crispus, agar, gum arabic, starch, curdlan, gelatin, gellan gum, konjac mannan, mannitol, xylan, and any mixture thereof; emollient moisturizers are oils and fats, polyols, or combinations thereof, wherein the oils and fats comprise oils or waxes of vegetable, mineral, animal, or synthetic origin, grapeseed oil, meadowfoam oil, hydrogenated vegetable oil, avocado oil, shea butter, white oil, cetostearyl ethyl hexanoate, squalane, octyldodecanol stearoyloxystearate, propylene carbonate, isodecyl pivalate, dimethicone, beeswax, white wax, the polyols comprise glycerin, butylene glycol, propylene glycol, dipropylene glycol; the emulsifier is PEG26-PPG-30 phosphate, tween-20, tween-60, tween-80, alkyl glycoside, polyoxyethylene oleate, polyoxyethylene laurate, glyceryl citrate stearate or their mixture; the antiseptic is chlorphenesin, methyl hydroxybenzoate, phenoxyethanol, ethylhexylglycerin, octylglycol, or their mixture.
6. The preparation method of the air cushion loose powder as claimed in claim 1, wherein the powder phase comprises 30-60 parts by weight, the emollient humectant comprises 0.2-20 parts by weight, the emulsifier comprises 0-5 parts by weight, and the preservative comprises 0.05-3 parts by weight.
7. The method for preparing air-cushion loose powder as claimed in claim 1, wherein the predetermined temperature in the step (3) is 30-55 ℃.
8. The method for preparing air-cushion loose powder as claimed in claim 1, wherein the weight percentage of water in the finished product in the step (4) is less than or equal to 5%.
9. The method for preparing air cushion loose powder as claimed in claim 1, wherein in the step (4), during the freeze drying, the semi-finished product is first put into a freeze dryer to be frozen at a low temperature, the temperature of the freeze dryer is lower than the eutectic point, then the freeze dryer is vacuumized, after the vacuum degree reaches a preset vacuum value, the temperature is raised to carry out sublimation drying to remove ice crystals, and finally, after the sublimation is finished, the air cushion loose powder is subjected to desorption drying to remove bound water.
10. The method for preparing air-cushion loose powder according to claim 9, wherein the temperature of the freeze dryer is-30 to-10 ℃, the preset vacuum is 10 to 40Pa, the desorption drying temperature is 5 to 60 ℃, and the pressure is 10 to 50 Pa.
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN116139023A (en) * | 2023-02-14 | 2023-05-23 | 上海臻臣化妆品有限公司 | Preparation method of powder product, powder product and powder product |
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| CN105708758A (en) * | 2016-02-18 | 2016-06-29 | 上海创馨化妆品有限公司 | Eyeshadow and preparing method thereof |
| CN111904871A (en) * | 2019-04-22 | 2020-11-10 | 上海震春生物科技有限公司 | Method for preparing powder |
| CN113520910A (en) * | 2020-04-21 | 2021-10-22 | 上海瀛彩生物科技有限公司 | High-gloss gel powder and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN105708758A (en) * | 2016-02-18 | 2016-06-29 | 上海创馨化妆品有限公司 | Eyeshadow and preparing method thereof |
| CN111904871A (en) * | 2019-04-22 | 2020-11-10 | 上海震春生物科技有限公司 | Method for preparing powder |
| CN113520910A (en) * | 2020-04-21 | 2021-10-22 | 上海瀛彩生物科技有限公司 | High-gloss gel powder and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN116139023A (en) * | 2023-02-14 | 2023-05-23 | 上海臻臣化妆品有限公司 | Preparation method of powder product, powder product and powder product |
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