CN114146451B - Extraction separation device for manufacturing dihydroxydicyclohexyl propane - Google Patents
Extraction separation device for manufacturing dihydroxydicyclohexyl propane Download PDFInfo
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- CN114146451B CN114146451B CN202111483155.1A CN202111483155A CN114146451B CN 114146451 B CN114146451 B CN 114146451B CN 202111483155 A CN202111483155 A CN 202111483155A CN 114146451 B CN114146451 B CN 114146451B
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- fixedly arranged
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- connecting pipe
- sealing
- mixing chamber
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- 238000000605 extraction Methods 0.000 title claims abstract description 31
- VWCBKYRRGAWQGH-UHFFFAOYSA-N 2,2-dicyclohexylpropane-1,1-diol Chemical compound C1CCCCC1C(C(O)O)(C)C1CCCCC1 VWCBKYRRGAWQGH-UHFFFAOYSA-N 0.000 title claims abstract description 16
- 238000000926 separation method Methods 0.000 title abstract description 27
- 238000004519 manufacturing process Methods 0.000 title abstract description 11
- 238000002156 mixing Methods 0.000 claims abstract description 44
- 238000007789 sealing Methods 0.000 claims abstract description 40
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims abstract description 28
- 238000003860 storage Methods 0.000 claims abstract description 22
- 230000007246 mechanism Effects 0.000 claims abstract description 21
- 229910052742 iron Inorganic materials 0.000 claims abstract description 14
- 238000002955 isolation Methods 0.000 claims description 8
- 239000002904 solvent Substances 0.000 abstract description 28
- 238000000034 method Methods 0.000 abstract description 16
- 230000008569 process Effects 0.000 abstract description 14
- 238000003756 stirring Methods 0.000 abstract description 7
- 230000003116 impacting effect Effects 0.000 abstract description 4
- 239000007788 liquid Substances 0.000 description 28
- 230000003068 static effect Effects 0.000 description 10
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 9
- 235000017491 Bambusa tulda Nutrition 0.000 description 9
- 241001330002 Bambuseae Species 0.000 description 9
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 9
- 239000011425 bamboo Substances 0.000 description 9
- 239000003795 chemical substances by application Substances 0.000 description 6
- 239000002699 waste material Substances 0.000 description 6
- 230000009471 action Effects 0.000 description 5
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical class C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 2
- 239000002928 artificial marble Substances 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000003822 epoxy resin Substances 0.000 description 1
- 239000011152 fibreglass Substances 0.000 description 1
- 239000012046 mixed solvent Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229920000647 polyepoxide Polymers 0.000 description 1
- 230000001105 regulatory effect Effects 0.000 description 1
- 230000002194 synthesizing effect Effects 0.000 description 1
- 229920006337 unsaturated polyester resin Polymers 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0426—Counter-current multistage extraction towers in a vertical or sloping position
- B01D11/043—Counter-current multistage extraction towers in a vertical or sloping position with stationary contacting elements, sieve plates or loose contacting elements
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/04—Solvent extraction of solutions which are liquid
- B01D11/0419—Solvent extraction of solutions which are liquid in combination with an electric or magnetic field or with vibrations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/0208—Separation of non-miscible liquids by sedimentation
- B01D17/0214—Separation of non-miscible liquids by sedimentation with removal of one of the phases
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/12—Auxiliary equipment particularly adapted for use with liquid-separating apparatus, e.g. control circuits
Abstract
The invention discloses an extraction separation device for manufacturing dihydroxydicyclohexyl propane, and particularly relates to the technical field of extraction separation devices. According to the invention, the mixing mechanism is arranged, the electromagnet is electrified to generate magnetic force and adsorb the iron blocks, the extension pipe is driven to move downwards, the sealing gasket and the pushing plate are pushed to move through the extension pipe, the solvent in the storage box is extruded, so that the solvent flows and generates pressure, the solvent enters the mixing chamber through the connecting pipe, then the impact ball is impacted in the flowing out process, and the two solvents are scattered and splashed and are mixed with each other in the impacting process, so that the additional stirring and mixing are replaced, and the device is more convenient.
Description
Technical Field
The invention relates to the technical field of extraction separation devices, in particular to an extraction separation device for manufacturing dihydroxydicyclohexyl propane.
Background
Dihydroxydicyclohexyl propane is also called hydrogenated bisphenol A, is a raw material for synthesizing unsaturated polyester resin and epoxy resin, is also a medical intermediate, and is used as a raw material in the production of products such as artificial marble and glass fiber reinforced plastic because of high water resistance and thermal stability.
During the preparation process, bisphenol A is used as raw material, and the dihydroxydicyclohexyl propane is prepared under the action of a catalyst.
In the preparation process, dihydroxydicyclohexyl propane is required to be extracted and then separated, in the process, two solvents are required to be fully mixed so that solutes can fully enter an extracting agent, the process is required to be stirred and mixed, the two solvents are complicated, and in addition, when the two solvents are separated after layering, the two solvents cannot be thoroughly separated, so that a part of extracting agent is inevitably remained at the joint of the two solvents, and waste is caused.
Disclosure of Invention
In order to overcome the above-mentioned drawbacks of the prior art, the present invention provides an extraction separation apparatus for dihydroxydicyclohexylpropane production, which solves the above-mentioned problems occurring in the prior art.
In order to achieve the above purpose, the present invention provides the following technical solutions: the extraction and separation device for manufacturing the dihydroxydicyclohexyl propane comprises a base, wherein two storage boxes are fixedly arranged at the top end of the base, and a mixing mechanism and an isolation mechanism are arranged at the top of the base.
Further, mixing mechanism includes the mixing chamber, the mixing chamber is established at the base top, the fixed connecting rod that is equipped with in mixing chamber inside top, connecting rod one end is fixed to be equipped with to dash the ball, the inside push pedal that is equipped with of bin, push pedal bottom mounting is equipped with sealed pad, push pedal and sealed pad outer end are contacted with the bin inner wall, push pedal top is fixed to be equipped with two extension pipes, extension pipe one end runs through push pedal and sealed pad, the fixed valve that is equipped with on the extension pipe, the extension pipe other end extends to the bin top, the fixed electro-magnet that is equipped with in bin top, the electro-magnet top is equipped with the iron plate, the fixed plate that is equipped with in iron plate top, electro-magnet, fixed plate, iron plate are all established between two extension pipes, fixed plate both ends respectively with two extension pipe outer fixed connection, bin one side is fixed to be equipped with the connecting pipe, connecting pipe one end and mixing chamber one side fixed connection and extend to the mixing chamber inside, two connecting pipe one end is located respectively and strikes the ball both sides.
Further, isolation mechanism is including keeping static a section of thick bamboo, it establishes between two bin to keep static a section of thick bamboo, it is equipped with the closing plate all to keep static a section of thick bamboo top and bottom, it is equipped with the removal cabin to keep static a section of thick bamboo inside, it is fixed to remove the cabin outer end and be equipped with the rubber circle, the rubber circle outer end contacts with a section of thick bamboo inner wall that keeps static, it is fixed to be equipped with the interior connecting pipe to remove cabin inside top, interior connecting pipe top extends to remove cabin top, it is equipped with outer communicating pipe to remove cabin bottom mounting, all fixed be equipped with the solenoid valve on communicating pipe and the interior connecting pipe outward, it is equipped with the nut seat to remove the cabin inside, the nut seat is established in outer communicating pipe and interior connecting pipe one side, nut seat both ends extend to the top and the bottom of removing the cabin respectively, it is equipped with the lead screw to keep static a section of thick bamboo inside, the lead screw both ends respectively with two closing plates through sealed bearing swing joint, the nut seat is established at the lead screw outer end.
Further, the bottom end of the mixing chamber is fixedly provided with a feeding pipe, and one end of the feeding pipe is fixedly connected with a sealing plate at the top.
Further, the motor is fixedly arranged at the top end of the sealing plate at the top, the motor is arranged on one side of the feeding pipe, and one end of the screw rod extends to the top end of the sealing plate at the top and is fixedly connected with an output shaft of the motor.
Further, sealing rings are fixedly arranged at two ends of the nut seat, and the inner sides of the sealing rings are contacted with the outer ends of the screw rods.
Further, the bottom sealing plate bottom end fixing is equipped with the blow off pipe, the fixed valve that is equipped with on the blow off pipe, the fixed two bracing pieces that are equipped with in base top, bracing piece one end and the sealing plate bottom end fixed connection of bottom, two the bracing piece is established respectively in the blow off pipe both sides.
The invention has the technical effects and advantages that:
1. according to the invention, the mixing mechanism is arranged, the electromagnet is electrified to generate magnetic force and adsorb the iron blocks, the extension pipe is driven to move downwards, the sealing gasket and the pushing plate are pushed to move through the extension pipe, the solvent in the storage box is extruded, so that the solvent flows and generates pressure, the solvent enters the mixing chamber through the connecting pipe, then the impact ball is impacted in the flowing out process, and the two solvents are scattered and splashed and are mixed with each other in the impacting process, so that the additional stirring and mixing are replaced, and the device is more convenient.
2. According to the invention, the motor is started after the layering of the liquid in the standing barrel is finished, the motor is used for driving the screw rod to rotate, so that the movable cabin moves, the layering is placed in the movable cabin, the layering liquid in the movable cabin is additionally stored after extraction and separation, then the extraction and separation operation is repeated, the layering liquid obtained by each operation is collected and then is subjected to one-time separation operation uniformly, and compared with the way that a certain extraction agent residue is generated after each extraction and separation operation, the method can greatly reduce the extraction agent residue, thereby reducing waste.
3. Besides being applied to the manufacturing process of the dihydroxydicyclohexyl propane, the extraction and separation device can be used for extracting and separating other products, a mixing mechanism can be used for replacing traditional stirring and mixing, the purpose of more convenient operation is achieved, the purpose of reducing extractant residues and further reducing waste can be achieved by using an isolation mechanism, and the application range is wide.
Drawings
Fig. 1 is a perspective view of the present invention.
Fig. 2 is a perspective view of the present invention.
Fig. 3 is a perspective semi-sectional view of the storage box of the present invention.
Fig. 4 is a perspective semi-cutaway view of the mixing chamber of the present invention.
FIG. 5 is a perspective semi-sectional view of a stationary barrel of the present invention.
FIG. 6 is a perspective semi-sectional view of a stationary barrel of the present invention.
Fig. 7 is a perspective semi-sectional view of the mobile pod of the present invention.
The reference numerals are: 1. a base; 2. a storage tank; 3. an electromagnet; 4. an extension tube; 5. a fixing plate; 6. a rubber ring; 7. an outer communicating tube; 8. a moving cabin; 9. standing the cylinder; 10. a sealing plate; 11. a mixing chamber; 12. iron blocks; 13. a seal ring; 14. a screw rod; 15. a connecting pipe; 16. a nut seat; 17. an electromagnetic valve; 18. a motor; 19. an inner connecting pipe; 20. a discharge pipe; 21. a feeding pipe; 22. a sealing gasket; 23. a push plate; 24. a connecting rod; 25. and (5) striking the ball.
Detailed Description
The following description of the embodiments of the present invention will be made clearly and completely with reference to the accompanying drawings, in which it is apparent that the embodiments described are only some embodiments of the present invention, but not all embodiments. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
Referring to fig. 1-7 of the specification, an extraction and separation device for manufacturing dihydroxydicyclohexyl propane of this embodiment includes a base 1, two storage tanks 2 are fixedly arranged at the top end of the base 1, an extracting agent and a solvent containing dihydroxydicyclohexyl propane are respectively stored in the two storage tanks 2, and a mixing mechanism and an isolating mechanism are arranged at the top end of the base 1.
The mixing mechanism comprises a mixing chamber 11, the mixing chamber 11 is arranged at the top of a base 1, a connecting rod 24 is fixedly arranged at the top of the inside of the mixing chamber 11, a striking ball 25 is fixedly arranged at one end of the connecting rod 24, solvents enter the mixing chamber 11 through a connecting pipe 15, then strike the striking ball 25 in the outflow process, the two solvents are scattered and splashed and mixed with each other in the striking process, the extra stirring and mixing are replaced, a push plate 23 is arranged in the storage box 2, a sealing pad 22 is fixedly arranged at the bottom of the push plate 23, the outer ends of the push plate 23 and the sealing pad 22 are contacted with the inner wall of the storage box 2, two extension pipes 4 are fixedly arranged at the top of the push plate 23, one end of each extension pipe 4 penetrates through the push plate 23 and the sealing pad 22, the liquid enters the storage box 2 through the extension pipe 4, a valve is fixedly arranged on the extension pipe 4, the other end of each extension pipe 4 extends to the top of the storage box 2, an electromagnet 3 is fixedly arranged at the top of the storage box 2, an iron block 12 is arranged at the top of each electromagnet 3, an iron block 12 is fixedly arranged at the top of each iron block 12, the two electromagnet blocks 5 are fixedly arranged at the top of each electromagnet block 12, the two electromagnet blocks are fixedly arranged at one sides of the two extension pipes 15, the two electromagnet blocks are fixedly arranged at one sides of the two sides of the extension pipes 15, and are fixedly connected with one end of each of the two electromagnet blocks, and the two electromagnet blocks are fixedly arranged at one side of the two electromagnet blocks are fixedly arranged at one end of the two connection pipe 15, and are respectively, and are fixedly connected with one end of the two connection pipe 15, and are respectively, and are connected with one end of the two connection pipe 11, and are respectively, and are fixedly connected with one end 15.
The implementation scene is specifically as follows: before extraction, two solvents are respectively placed in two storage tanks 2, liquid is positioned at the bottoms of a sealing gasket 22 and a pushing plate 23 in the storage tanks 2, dihydroxydicyclohexylpropane is contained in one solvent, after extraction is started, an electromagnet 3 is electrified, the electrified electromagnet 3 generates magnetic force to adsorb an iron block 12 on the top of the electromagnet, the iron block 12 starts to move downwards under the action of the magnetic force so as to drive a fixing plate 5 and an extension pipe 4 to move downwards, a valve on the extension pipe 4 is in a closed state, the extension pipe 4 pushes the sealing gasket 22 and the pushing plate 23 to move downwards in the downward moving process, under the action of the sealing gasket 22 and the pushing plate 23, the solvents in the two storage tanks 2 are extruded, the extruded solvents flow upwards through a connecting pipe 15 and finally enter a mixing chamber 11, the solvent has certain pressure when entering the mixing chamber 11 and flowing out from one end of the connecting pipe 15, the sprayed liquid column impacts on the impact ball 25 under the action of the pressure, so that the liquid is dispersed and splashed, the two liquids are dispersed and splashed simultaneously, the two liquids are mixed in the splashing process, the mixed liquids fall down and flow into the standing cylinder 9 through the feeding pipe 21, therefore, the two liquids impact the impact ball 25 simultaneously, the two liquids are dispersed and splashed and are mixed mutually in the impacting process, thereby replacing the additional stirring and mixing, the mixing mechanism is more convenient, the electromagnet 3 is electrified to generate magnetic force and adsorb the iron block 12, the extension pipe 4 is driven to move downwards, the sealing gasket 22 and the push plate 23 are pushed to move through the extension pipe 4, the solvent in the storage tank 2 is extruded, the solvent flows and generates pressure, the solvent enters the mixing chamber 11 through the connecting pipe 15, and then the impact ball 25 is impacted in the flowing-out process, and the two solvents are dispersed and splashed and mixed with each other in the impacting process, so that the additional stirring and mixing are replaced, and the method is more convenient.
Referring to fig. 1-7 of the specification, an extraction and separation device for manufacturing dihydroxydicyclohexylpropane of this embodiment further comprises an isolation mechanism, the isolation mechanism comprises a standing barrel 9, the standing barrel 9 is arranged between two storage tanks 2, sealing plates 10 are fixedly arranged at the top end and the bottom end of the standing barrel 9, liquid formed by mixing two solvents is placed in the standing barrel 9, a movable cabin 8 is arranged in the standing barrel 9, a rubber ring 6 is fixedly arranged at the outer end of the movable cabin 8, the outer end of the rubber ring 6 is in contact with the inner wall of the standing barrel 9, the tightness between the movable cabin 8 and the inner wall of the standing barrel 9 is improved, an inner connecting pipe 19 is fixedly arranged at the top end of the movable cabin 8, the top end of the inner connecting pipe 19 extends to the top end of the movable cabin 8, an outer communicating pipe 7 is fixedly arranged at the bottom end of the movable cabin 8, electromagnetic valves 17 are fixedly arranged on the outer communicating pipe 7 and the inner connecting pipe 19, the outside liquid is introduced into the movable cabin 8, a nut seat 16 is arranged in the movable cabin 8, the nut seat 16 is arranged at one side of the outer communicating pipe 7 and the inner connecting pipe 19, two ends of the nut seat 16 respectively extend to the top and the bottom of the movable cabin 8, a screw rod 14 is arranged in the static cylinder 9, two ends of the screw rod 14 are respectively and movably connected with two sealing plates 10 through sealing bearings, the nut seat 16 is arranged at the outer end of the screw rod 14, so that the position of the movable cabin 8 is regulated by utilizing the rotation of the screw rod 14, layering is arranged in the movable cabin 8, the layering liquid in the movable cabin 8 is additionally stored after extraction and separation, then the extraction and separation operation is repeatedly performed, the layering liquid obtained by each operation is concentrated and then is uniformly separated once, compared with the situation that a certain extraction agent residue is generated after each extraction and separation, in this way, the residual extractant can be greatly reduced, thereby reducing waste.
The bottom end of the mixing chamber 11 is fixedly provided with a feeding pipe 21, one end of the feeding pipe 21 is fixedly connected with the sealing plate 10 at the top, and liquid in the mixing chamber 11 enters the standing barrel 9 through the feeding pipe 21 for standing.
The top the fixed motor 18 that is equipped with in closing plate 10 top, motor 18 establishes in pan feeding pipe 21 one side, lead screw 14 one end extends to the closing plate 10 top at top and with the output shaft fixed connection of motor 18, provide power drive lead screw 14 rotation through motor 18.
The two ends of the nut seat 16 are fixedly provided with the sealing rings 13, and the inner sides of the sealing rings 13 are contacted with the outer ends of the screw rods 14, so that the tightness of the nut seat 16 is improved.
The bottom sealing plate 10 bottom mounting is equipped with the discharge tube 20, the fixed valve that is equipped with on the discharge tube 20 to this will rest in the section of thick bamboo 9 liquid discharge, base 1 top is fixed to be equipped with two bracing pieces for fixed stay is stood section of thick bamboo 9 and sealing plate 10, bracing piece one end and the sealing plate 10 bottom fixed connection of bottom, two the bracing piece is established respectively in the discharge tube 20 both sides.
The implementation scene is specifically as follows: the mixed solvent flows into the static cylinder 9 through the feeding pipe 21, after a period of static placement, the two solvents are layered due to mutual incompatibility, in the process, the electromagnetic valves 17 on the outer communicating pipe 7 and the inner communicating pipe 19 are both in an open state, so that the movable cabin 8 is filled with liquid, when layering occurs, the motor 18 is started, the screw rod 14 is driven to rotate by the motor 18, the nut seat 16 is sleeved at the outer end of the screw rod 14, so that the nut seat 16 slides along the outer end of the screw rod 14 after the screw rod 14 rotates, the nut seat 16 is fixed with the movable cabin 8, the movable cabin 8 is driven by the nut seat 16 to move up and down, the moving speed is not too fast, the layered liquid is prevented from being stirred again, the movable cabin 8 is utilized to move up and down in the static cylinder 9, the layered position of the solution is adjusted to be positioned inside the movable cabin 8, then closing the two electromagnetic valves 17, so that the two solvents are respectively positioned at the top and the bottom of the movable cabin 8 and are completely separated under the action of the movable cabin 8, at the moment, opening a valve on the discharge pipe 20 to completely discharge the liquid at the bottom of the movable cabin 8, then opening the electromagnetic valve 17 on the outer communicating pipe 7, discharging the liquid at the layering position in the movable cabin 8 through the discharge pipe 20 and additionally storing the liquid, thus completing one extraction and separation work, then repeatedly performing the extraction and separation work in the same way, uniformly storing the liquid at the layering position obtained by each operation until the accumulated liquid at the layering position reaches a certain degree, uniformly performing one extraction and separation operation again, generating a certain residual extractant compared with the extraction and separation operation, greatly reducing the residual extractant in the way, reducing the waste, through setting up isolation mechanism, after the layering of liquid finishes in a section of thick bamboo 9 of standing still, open motor 18, utilize motor 18 drive lead screw 14 to rotate for remove cabin 8 and remove, will laminate and handle in removing cabin 8, the layering department liquid in removing cabin 8 after the extraction separation stores in addition, then repeatedly carry out the extraction separation operation, concentrate the layering department liquid that gets every time operation back and unify and carry out a separation operation, compare and will produce certain extractant residue with this extraction separation with every, the residue of extractant that like this mode can be great reduces, with this reduces extravagant.
Besides being applied to the manufacturing process of the dihydroxydicyclohexyl propane, the extraction and separation device can be used for extracting and separating other products, a mixing mechanism can be used for replacing traditional stirring and mixing, the purpose of more convenient operation is achieved, the purpose of reducing extractant residues and further reducing waste can be achieved by using an isolation mechanism, and the application range is wide.
The last points to be described are: first, in the description of the present application, it should be noted that, unless otherwise specified and defined, the terms "mounted," "connected," and "connected" are to be construed broadly, and may be mechanical or electrical, or may be a direct connection between two elements, and "upper," "lower," "left," "right," etc. are merely used to indicate relative positional relationships, which may be changed when the absolute position of the object being described is changed;
secondly: in the drawings of the disclosed embodiments, only the structures related to the embodiments of the present disclosure are referred to, and other structures can refer to the common design, so that the same embodiment and different embodiments of the present disclosure can be combined with each other under the condition of no conflict;
finally: the foregoing description of the preferred embodiments of the invention is not intended to limit the invention to the precise form disclosed, and any such modifications, equivalents, and alternatives falling within the spirit and principles of the invention are intended to be included within the scope of the invention.
Claims (1)
1. The utility model provides an extraction separator for making of dihydroxydicyclohexyl propane, includes base (1), base (1) top is fixed to be equipped with two bin (2), its characterized in that: the top of the base (1) is provided with a mixing mechanism and an isolating mechanism;
the mixing mechanism comprises a mixing chamber (11), the mixing chamber (11) is arranged at the top of a base (1), a connecting rod (24) is fixedly arranged at the top end of the inside of the mixing chamber (11), a striking ball (25) is fixedly arranged at one end of the connecting rod (24), a push plate (23) is arranged inside the storage box (2), a sealing gasket (22) is fixedly arranged at the bottom end of the push plate (23), the outer end of the push plate (23) and the outer end of the sealing gasket (22) are contacted with the inner wall of the storage box (2), two extension pipes (4) are fixedly arranged at the top end of the push plate (23), one end of each extension pipe (4) penetrates through the push plate (23) and the sealing gasket (22), a valve is fixedly arranged on each extension pipe (4), the other end of each extension pipe (4) extends to the top of the storage box (2), an electromagnet (3) is fixedly arranged at the top end of the storage box (2), an iron block (12) is arranged at the top of each electromagnet, a fixing plate (5) is fixedly arranged at the top end of each iron block (12), two extension pipes (4) are fixedly arranged between the two extension pipes (4) and one side (15), one end of the connecting pipe (15) is fixedly connected with one side of the mixing chamber (11) and extends into the mixing chamber (11), and one ends of the two connecting pipes (15) are respectively positioned at two sides of the impact ball (25);
the isolation mechanism comprises a standing cylinder (9), the standing cylinder (9) is arranged between two storage boxes (2), sealing plates (10) are fixedly arranged at the top end and the bottom end of the standing cylinder (9), a movable cabin (8) is arranged in the standing cylinder (9), a rubber ring (6) is fixedly arranged at the outer end of the movable cabin (8), the outer end of the rubber ring (6) is contacted with the inner wall of the standing cylinder (9), an inner connecting pipe (19) is fixedly arranged at the top end of the inner part of the movable cabin (8), the top end of the inner connecting pipe (19) extends to the top end of the movable cabin (8), an outer connecting pipe (7) is fixedly arranged at the bottom end of the movable cabin (8), electromagnetic valves (17) are fixedly arranged at the top end of the outer connecting pipe (7) and the inner connecting pipe (19), nut seats (16) are arranged in the movable cabin (8), the nut seats (16) are arranged on one side of the outer connecting pipe (7) and the inner connecting pipe (19), the two ends of each nut seat (16) extend to the top and the bottom of the movable cabin (8), the inner connecting pipe (9) is fixedly provided with an inner connecting pipe (19), and two screw rods (14) are respectively connected with two screw rods (14) through two sealing ends of the sealing plates (14);
a feeding pipe (21) is fixedly arranged at the bottom end of the mixing chamber (11), and one end of the feeding pipe (21) is fixedly connected with a sealing plate (10) at the top;
the top end of the sealing plate (10) at the top is fixedly provided with a motor (18), the motor (18) is arranged on one side of a feeding pipe (21), and one end of the screw rod (14) extends to the top end of the sealing plate (10) at the top and is fixedly connected with an output shaft of the motor (18);
sealing rings (13) are fixedly arranged at two ends of the nut seat (16), and the inner sides of the sealing rings (13) are contacted with the outer ends of the screw rods (14);
the bottom sealing plate (10) bottom fixed be equipped with blow off pipe (20), the fixed valve that is equipped with on blow off pipe (20), base (1) top is fixed to be equipped with two bracing pieces, bracing piece one end and sealing plate (10) bottom fixed connection of bottom, two the bracing piece is established respectively in blow off pipe (20) both sides.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111483155.1A CN114146451B (en) | 2021-12-07 | 2021-12-07 | Extraction separation device for manufacturing dihydroxydicyclohexyl propane |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111483155.1A CN114146451B (en) | 2021-12-07 | 2021-12-07 | Extraction separation device for manufacturing dihydroxydicyclohexyl propane |
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| Publication Number | Publication Date |
|---|---|
| CN114146451A CN114146451A (en) | 2022-03-08 |
| CN114146451B true CN114146451B (en) | 2024-01-09 |
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| CN202111483155.1A Active CN114146451B (en) | 2021-12-07 | 2021-12-07 | Extraction separation device for manufacturing dihydroxydicyclohexyl propane |
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| CN115212609B (en) * | 2022-08-18 | 2023-09-26 | 江苏优普生物化学科技股份有限公司 | Separation filter equipment is used in preparation of trifluoromethyl aniline synthetic solution production |
| CN117085366B (en) * | 2023-10-20 | 2024-04-02 | 广东美宝化妆品有限公司 | Solvent bidirectional turbulence extraction device and application thereof in extraction of effective components of tricholoma matsutake |
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| CN113318477A (en) * | 2021-05-27 | 2021-08-31 | 盐城师范学院 | Solvent extraction method and solvent extraction equipment |
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| JP2005147114A (en) * | 2003-11-13 | 2005-06-09 | Yoshio Niioka | Mechanism for composite exhaust gas cleaner |
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