CN114129463A - Cleansing oil of polyglycerol emulsifier and preparation method thereof - Google Patents
Cleansing oil of polyglycerol emulsifier and preparation method thereof Download PDFInfo
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- CN114129463A CN114129463A CN202111528231.6A CN202111528231A CN114129463A CN 114129463 A CN114129463 A CN 114129463A CN 202111528231 A CN202111528231 A CN 202111528231A CN 114129463 A CN114129463 A CN 114129463A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/39—Derivatives containing from 2 to 10 oxyalkylene groups
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/31—Hydrocarbons
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
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- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
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- A61K8/731—Cellulose; Quaternized cellulose derivatives
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K8/00—Cosmetics or similar toiletry preparations
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- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/14—Preparations for removing make-up
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
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Abstract
The invention discloses a cleansing oil of a polyglycerol emulsifier, which comprises the following components: ethylhexyl palmitate, polyglycerol-6-didecanoate, glycerol triethylhexanoate, polyglycerol-10-dioleate, caprylic/capric triglyceride, vaccinium myrtillus seed oil, meadowfoam seed oil, orange peel oil, squalane, pentaerythritol tetraester and nanocellulose, wherein the polyglycerol emulsifier makeup remover oil comprises the following components in parts by weight: 35-55 parts of ethylhexyl palmitate, 5-10 parts of polyglycerol-6-dicaprate, 4-6 parts of glycerol triethyl hexanoate, 15-21 parts of polyglycerol-10-dioleate, 6-8 parts of caprylic/capric triglyceride, 4-6 parts of vaccinium myrtillus seed oil, 8-10 parts of meadowfoam seed oil, 4-6 parts of sweet orange peel oil, 5-25 parts of squalane, 7-9 parts of pentaerythritol tetraester and 15-25 parts of nanocellulose.
Description
Technical Field
The invention relates to the technical field of makeup removing oil preparation, and particularly relates to makeup removing oil of a polyglycerol emulsifier and a preparation method thereof.
Background
The makeup remover oil is an oily preparation which is used for the purpose of makeup removal, is specially used for cleaning, removes oily residues and porosebum secretion of the makeup cosmetics and mainly comprises transparent liquid oily components. Sometimes a small amount of nonionic surfactant is also contained, the makeup removing oil is special for cleaning and has excellent affinity with the makeup cosmetics and strong cleaning capability compared with other makeup removing formulations, and the makeup removing oil is also most used in the makeup removing formulations.
The makeup remover mainly comprises alkane compounds, natural oil, synthetic oil or silicon oil and other oil components with good affinity with makeup cosmetics, and sometimes a small amount of nonionic surfactant is added to improve wetting capacity and cleaning capacity.
At present, makeup remover is mostly adopted for makeup removal, although the makeup remover has a certain makeup removal effect, compared with makeup remover oil, the makeup remover with poor quality has a certain irritation on skin, has poor affinity, is easy to remain on the face of people and is not easy to clean, and therefore the makeup remover oil with the polyglycerol emulsifier and the preparation method are provided.
Disclosure of Invention
The invention aims to provide makeup removing oil of a polyglycerol emulsifier and a preparation method thereof, wherein the makeup removing oil of the polyglycerol emulsifier has a good makeup removing effect, is mild, does not irritate eyes and skin, has good affinity and is easy to clean, so as to solve the problems in the background technology.
In order to achieve the purpose, the invention provides the following technical scheme:
a cleansing oil for a polyglycerol emulsifier comprising: ethylhexyl palmitate, polyglycerol-6-didecanoate, glycerol triethylhexanoate, polyglycerol-10-dioleate, caprylic/capric triglyceride, vaccinium myrtillus seed oil, meadowfoam seed oil, orange peel oil, squalane, pentaerythritol tetraester and nanocellulose, wherein the polyglycerol emulsifier makeup remover oil comprises the following components in parts by weight: 35-55 parts of ethylhexyl palmitate, 5-10 parts of polyglycerol-6-dicaprate, 4-6 parts of glycerol triethyl hexanoate, 15-21 parts of polyglycerol-10-dioleate, 6-8 parts of caprylic/capric triglyceride, 4-6 parts of vaccinium myrtillus seed oil, 8-10 parts of meadowfoam seed oil, 4-6 parts of sweet orange peel oil, 5-25 parts of squalane, 7-9 parts of pentaerythritol tetraester and 15-25 parts of nanocellulose.
Preferably, the polyglycerol-6-dicaprate and the first active group are subjected to graft copolymerization to generate a new polyglycerol-6-dicaprate polymer, so that the emulsifying property of the polyglycerol-6-dicaprate polymer is superior to that of the polyglycerol-6-dicaprate, and the polyglycerol-10-dioleate and the second active group are subjected to graft copolymerization to generate a new polyglycerol-10-dioleate polymer, so that the emulsifying property of the polyglycerol-10-dioleate polymer is superior to that of the polyglycerol-10-dioleate.
Preferably, the graft copolymerization is performed by chemically treating the polymer of the backbone, some units with reactivity can be introduced into the polymer chain, the first reactive group can be configured as styrene, and the polyglycerol-6-didecanoate and styrene are subjected to graft copolymerization to generate a new polyglycerol-6-didecanoate polymer.
Preferably, the first active group may be acrylonitrile, and the polyglycerol-10-dioleate and acrylonitrile may undergo graft copolymerization to form a new polyglycerol-10-dioleate polymer.
Preferably, the reaction temperature of the graft copolymerization reaction is set to 40-80 ℃, the reaction time of the graft copolymerization reaction is set to 20-40min, and the polyglycerol-6-dicaprate and the polyglycerol-10-dioleate are set as waste gas treatment equipment during the graft copolymerization reaction, so as to purify waste gas generated by the graft copolymerization reaction.
Preferably, the exhaust gas treatment device is used for collecting the exhaust gas generated by the graft copolymerization reaction and purifying the collected exhaust gas, and the exhaust gas treatment device further has a gas detection function of detecting the purified gas by the exhaust gas treatment device and removing the exhaust gas after the exhaust gas reaches the emission standard.
Preferably, the nano-cellulose is configured as nano-plant cellulose, the nano-plant cellulose can increase the cleaning effect, and the particle size of the nano-cellulose is set to be 20-100 nm.
The cleansing oil of the polyglycerol emulsifier and the preparation method thereof comprise the following steps:
weighing the components according to a ratio, heating ethylhexyl palmitate, triethylhexanoin, caprylic/capric triglyceride, squalane and pentaerythritol tetraester to 50-70 ℃, and fully and uniformly mixing by using stirring equipment to form a mixed solution;
step two, respectively carrying out graft copolymerization on polyglycerol-6-didecanoate and polyglycerol-10-dioleate to generate a new polyglycerol-6-didecanoate polymer and a new polyglycerol-10-dioleate polymer, and then adding the polyglycerol-6-didecanoate polymer and the polyglycerol-10-dioleate polymer into the mixed solution obtained in the step one to be fully and uniformly mixed;
step three, adding the vaccinium myrtillus seed oil, the meadowfoam seed oil and the sweet orange peel oil into the mixed solution obtained in the step one, and fully and uniformly mixing;
step four, crushing the nano-cellulose to enable particles of the nano-cellulose to be crushed to 35-55nm, then adding the crushed particles of the nano-cellulose into the mixed solution in the step one, and fully and uniformly mixing;
and step five, reducing the temperature of the mixture obtained in the step to be below 40 ℃, and fully stirring until uniform liquid is formed to prepare the polyglycerol emulsifier cleansing oil.
As a preferred scheme, the stirring equipment in the first step comprises a stirring barrel and a stirring rod, the stirring barrel and the stirring rod can rotate simultaneously, and the rotation directions are opposite, so that the mixed materials can be quickly and uniformly mixed, and a water bath tank is arranged outside the stirring barrel, so that the materials can be mixed at a proper temperature.
Preferably, the polyglycerol emulsifier cleansing oil prepared in the fifth step is quantitatively canned in a packaging mode of a packaging can, and plastic packaging is adopted at an opening of the packaging can after packaging is completed, so that the sealing property of the packaging can is ensured.
In summary, due to the adoption of the technology, the invention has the beneficial effects that:
according to the invention, the polyglycerol-6-dicaprate and the polyglycerol-10-dioleate in the polyglycerol emulsifier are subjected to graft copolymerization, so that the emulsifying property of the polyglycerol emulsifier is enhanced, the affinity of the makeup removing oil is better, certain stimulation of the traditional makeup removing water to skin is avoided, and the makeup removing water is easy to clean and convenient to use;
according to the invention, the nano-cellulose is added into the polyglycerol emulsifier and is set as the nano-plant cellulose, the cleaning effect can be firstly improved by utilizing the nano-plant cellulose, and the nano-plant cellulose can interact with the polyglycerol-6-dicaprate and the polyglycerol-10-dioleate which are subjected to graft copolymerization reaction, so that the makeup remover oil can be quickly paved on the face, the sagging performance is good, and the makeup remover oil cannot drip everywhere due to gravity, thereby reducing the waste in the using process to the maximum extent.
Drawings
FIG. 1 is a schematic flow diagram of a cleansing oil of a polyglycerol emulsifier and a preparation method thereof according to the present invention;
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present invention more apparent, the technical solutions of the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings of the embodiments of the present invention, and it is obvious that the described embodiments are some, but not all embodiments of the present invention. All other embodiments, which can be obtained by a person skilled in the art without any inventive step based on the embodiments of the present invention, are within the scope of the present invention. Thus, the following detailed description of the embodiments of the present invention, presented in the figures, is not intended to limit the scope of the invention, as claimed, but is merely representative of selected embodiments of the invention. All other embodiments, which can be obtained by a person skilled in the art without any inventive step based on the embodiments of the present invention, are within the scope of the present invention.
Example 1
A cleansing oil for a polyglycerol emulsifier comprising: ethylhexyl palmitate, polyglycerol-6-didecanoate, glycerol triethylhexanoate, polyglycerol-10-dioleate, caprylic/capric triglyceride, vaccinium myrtillus seed oil, meadowfoam seed oil, orange peel oil, squalane, pentaerythritol tetraester and nanocellulose, wherein the polyglycerol emulsifier makeup remover oil comprises the following components in parts by weight: 35-55 parts of ethylhexyl palmitate, 5-10 parts of polyglycerol-6-dicaprate, 4-6 parts of glycerol triethyl hexanoate, 15-21 parts of polyglycerol-10-dioleate, 6-8 parts of caprylic/capric triglyceride, 4-6 parts of vaccinium myrtillus seed oil, 8-10 parts of meadowfoam seed oil, 4-6 parts of sweet orange peel oil, 5-25 parts of squalane, 7-9 parts of pentaerythritol tetraester and 15-25 parts of nanocellulose.
The polyglycerol-6-dicaprate and the first active group are subjected to graft copolymerization to generate a new polyglycerol-6-dicaprate polymer, so that the emulsifying property of the polyglycerol-6-dicaprate polymer is superior to that of polyglycerol-6-dicaprate, and the polyglycerol-10-dioleate and the second active group are subjected to graft copolymerization to generate a new polyglycerol-10-dioleate polymer, so that the emulsifying property of the polyglycerol-10-dioleate polymer is superior to that of polyglycerol-10-dioleate;
the graft copolymerization reaction is to chemically treat the polymer of the skeleton main chain, some units with reaction activity can be introduced into a polymer chain, the first active group can be set as styrene, and the polyglycerol-6-didecanoate and the styrene are subjected to graft copolymerization reaction to generate a new polyglycerol-6-didecanoate polymer;
the first active group can be acrylonitrile, and the polyglycerol-10-dioleate and the acrylonitrile are subjected to graft copolymerization to generate a new polyglycerol-10-dioleate polymer;
setting the reaction temperature of the graft copolymerization reaction to be 40-80 ℃, setting the reaction time of the graft copolymerization reaction to be 20-40min, setting the polyglycerol-6-dicaprate and the polyglycerol-10-dioleate as waste gas treatment equipment during the graft copolymerization reaction, and purifying waste gas generated by the graft copolymerization reaction;
the waste gas treatment equipment is used for collecting waste gas generated by the graft copolymerization reaction and purifying the collected waste gas, and has a gas detection function, the purified gas is detected by the waste gas treatment equipment, and the waste gas is discharged after the waste gas reaches the discharge standard;
the nano-cellulose is nano-plant cellulose, the nano-plant cellulose can increase the cleaning effect, and the particle size of the nano-cellulose is set to be 20-100 nm;
further, the coating comprises the following components in parts by mass: 35 parts of ethylhexyl palmitate, 5 parts of polyglycerol-6-didecanoate, 4 parts of glycerol triethylhexanoate, 15 parts of polyglycerol-10-dioleate, 6 parts of caprylic/capric triglyceride, 4 parts of vaccinium myrtillus seed oil, 8 parts of meadowfoam seed oil, 4 parts of sweet orange peel oil, 5 parts of squalane, 7 parts of pentaerythritol tetraester and 15 parts of nanocellulose;
further, the coating comprises the following components in parts by mass: 45 parts of ethylhexyl palmitate, 8 parts of polyglycerol-6-didecanoate, 5 parts of glycerol triethylhexanoate, 18 parts of polyglycerol-10-dioleate, 7 parts of caprylic/capric triglyceride, 5 parts of vaccinium myrtillus seed oil, 9 parts of meadowfoam seed oil, 5 parts of sweet orange peel oil, 15 parts of squalane, 8 parts of pentaerythritol tetraester and 20 parts of nanocellulose;
further, the coating comprises the following components in parts by mass: 55 parts of ethylhexyl palmitate, 10 parts of polyglycerol-6-didecanoate, 6 parts of glycerol triethylhexanoate, 21 parts of polyglycerol-10-dioleate, 8 parts of caprylic/capric triglyceride, 6 parts of vaccinium myrtillus seed oil, 10 parts of meadowfoam seed oil, 6 parts of sweet orange peel oil, 25 parts of squalane, 9 parts of pentaerythritol tetraester and 25 parts of nanocellulose;
the three sets of formulation data are specifically as follows:
| formulation 1 | Formulation 2 | Formulation 3 | |
| Ethyl hexyl palmitate | 35 portions of | 45 portions of | 55 portions of |
| Polyglycerol-6-dicaprate | 5 portions of | 8 portions of | 10 portions of |
| Glycerol triethyl hexanoate | 4 portions of | 5 portions of | 6 portions of |
| Polyglycerol-10-dioleate | 15 portions of | 18 portions of | 21 portions of |
| Caprylic/capric triglyceride | 6 portions of | 7 portions of | 8 portions of |
| Vaccinium myrtillus seed oil | 4 portions of | 5 portions of | 6 portions of |
| Potentilla chinensis seed oil | 8 portions of | 9 portions of | 10 portions of |
| Sweet orange peel oil | 4 portions of | 5 portions of | 6 portions of |
| Squalane | 5 portions of | 15 portions of | 25 portions of |
| Pentaerythritol tetraesters | 7 portions of | 8 portions of | 9 portions of |
| Nano cellulose | 15 portions of | 20 portions of | 25 portions of |
By adopting the formula, the cleansing oil has good affinity, avoids the skin from being stimulated by the traditional cleansing water to a certain extent, is easy to clean and convenient to use, can increase the cleaning effect by adding the nano plant cellulose, can interact with the polyglycerol-6-dicaprate and the polyglycerol-10-dioleate which are subjected to graft copolymerization reaction by utilizing the nano plant cellulose, can be quickly paved on the face, has good sagging performance, and cannot drip everywhere due to gravity, thereby reducing the waste in the using process to the maximum extent.
Example 2
Based on the makeup remover oil of the polyglycerol emulsifier provided in example 1, as shown in fig. 1, the makeup remover oil of the polyglycerol emulsifier and the preparation method thereof comprise the following steps:
weighing the components according to a ratio, heating ethylhexyl palmitate, triethylhexanoin, caprylic/capric triglyceride, squalane and pentaerythritol tetraester to 50-70 ℃, and fully and uniformly mixing by using stirring equipment to form a mixed solution;
step two, respectively carrying out graft copolymerization on polyglycerol-6-didecanoate and polyglycerol-10-dioleate to generate a new polyglycerol-6-didecanoate polymer and a new polyglycerol-10-dioleate polymer, and then adding the polyglycerol-6-didecanoate polymer and the polyglycerol-10-dioleate polymer into the mixed solution obtained in the step one to be fully and uniformly mixed;
step three, adding the vaccinium myrtillus seed oil, the meadowfoam seed oil and the sweet orange peel oil into the mixed solution obtained in the step one, and fully and uniformly mixing;
step four, crushing the nano-cellulose to enable particles of the nano-cellulose to be crushed to 35-55nm, then adding the crushed particles of the nano-cellulose into the mixed solution in the step one, and fully and uniformly mixing;
and step five, reducing the temperature of the mixture obtained in the step to be below 40 ℃, and fully stirring until uniform liquid is formed to prepare the polyglycerol emulsifier cleansing oil.
Before the polyglycerol-6-dicaprate and the polyglycerol-10-dioleate are added, the first active group and the second active group are respectively subjected to graft copolymerization with the polyglycerol-6-dicaprate and the polyglycerol-10-dioleate to enhance the emulsifying property and the affinity of the emulsifier and achieve the effect of easy cleaning, and the grafted two emulsifiers can further react or react with other components to enhance the emulsifying property and the affinity.
Example 3
On the basis of the cleansing oil for the polyglycerol emulsifier and the preparation method provided by the embodiment 2, the stirring device in the first step comprises a stirring barrel and a stirring rod, wherein the stirring barrel and the stirring rod can rotate simultaneously, and the rotation directions are opposite, so that the mixed materials can be quickly and uniformly mixed, and a water bath box is arranged outside the stirring barrel, so that the materials can be mixed at a proper temperature;
and D, quantitatively canning the polyglycerol emulsifier cleansing oil prepared in the fifth step in a packaging mode of a packaging tank, and plastically packaging the polyglycerol emulsifier cleansing oil at an opening of the packaging tank after packaging is finished to ensure the sealing property of the packaging tank.
By adopting the scheme, materials can be quickly and uniformly stirred, the working efficiency is improved to a certain extent, and the opening of the packaging can is sealed in a plastic way, so that the makeup remover oil in the packaging can is prevented from being oxidized by contacting with the outside air, and the quality of the makeup remover oil is ensured.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus.
Claims (10)
1. The cleansing oil of the polyglycerol emulsifier is characterized in that: the method comprises the following steps: ethylhexyl palmitate, polyglycerol-6-didecanoate, glycerol triethylhexanoate, polyglycerol-10-dioleate, caprylic/capric triglyceride, vaccinium myrtillus seed oil, meadowfoam seed oil, orange peel oil, squalane, pentaerythritol tetraester and nanocellulose, wherein the polyglycerol emulsifier makeup remover oil comprises the following components in parts by weight: 35-55 parts of ethylhexyl palmitate, 5-10 parts of polyglycerol-6-dicaprate, 4-6 parts of glycerol triethyl hexanoate, 15-21 parts of polyglycerol-10-dioleate, 6-8 parts of caprylic/capric triglyceride, 4-6 parts of vaccinium myrtillus seed oil, 8-10 parts of meadowfoam seed oil, 4-6 parts of sweet orange peel oil, 5-25 parts of squalane, 7-9 parts of pentaerythritol tetraester and 15-25 parts of nanocellulose.
2. The cleansing oil of a polyglycerol emulsifier according to claim 1, characterized in that: the polyglycerol-6-dicaprate and the first active group are subjected to graft copolymerization to generate a new polyglycerol-6-dicaprate polymer, so that the emulsifying property of the polyglycerol-6-dicaprate polymer is superior to that of polyglycerol-6-dicaprate, and the polyglycerol-10-dioleate and the second active group are subjected to graft copolymerization to generate a new polyglycerol-10-dioleate polymer, so that the emulsifying property of the polyglycerol-10-dioleate polymer is superior to that of polyglycerol-10-dioleate.
3. The makeup remover oil of polyglycerol emulsifier according to claim 2, characterized in that: the graft copolymerization reaction can introduce some units with reactivity into a polymer chain by chemically treating a polymer of a skeleton main chain, the first active group can be set as styrene, and the polyglycerol-6-didecanoate and the styrene are subjected to graft copolymerization reaction to generate a new polyglycerol-6-didecanoate polymer.
4. The cleansing oil of a polyglycerol emulsifier according to claim 3, characterized in that: the first active group can be acrylonitrile, and the polyglycerol-10-dioleate and the acrylonitrile are subjected to graft copolymerization to generate a new polyglycerol-10-dioleate polymer.
5. The cleansing oil of polyglycerol emulsifier according to claim 4, characterized in that: the reaction temperature of the graft copolymerization reaction is set to be 40-80 ℃, the reaction time of the graft copolymerization reaction is set to be 20-40min, and the polyglycerol-6-dicaprate and the polyglycerol-10-dioleate are set to be waste gas treatment equipment during the graft copolymerization reaction, so that waste gas generated by the graft copolymerization reaction is purified.
6. The cleansing oil of polyglycerol emulsifier according to claim 5, characterized in that: the waste gas treatment equipment is used for collecting waste gas generated by the graft copolymerization reaction and purifying the collected waste gas, and has a gas detection function, the purified gas is detected by the waste gas treatment equipment, and the waste gas is discharged after the waste gas reaches the discharge standard.
7. The cleansing oil of a polyglycerol emulsifier according to claim 1, characterized in that: the nano-cellulose is set to be nano-plant cellulose, the nano-plant cellulose can increase the cleaning effect, and the particle size of the nano-cellulose is set to be 20-100 nm.
8. The method for preparing a polyglycerol emulsifier cleansing oil according to any one of claims 1 to 7, characterized in that: the method comprises the following steps:
weighing the components according to a ratio, heating ethylhexyl palmitate, triethylhexanoin, caprylic/capric triglyceride, squalane and pentaerythritol tetraester to 50-70 ℃, and fully and uniformly mixing by using stirring equipment to form a mixed solution;
step two, respectively carrying out graft copolymerization on polyglycerol-6-didecanoate and polyglycerol-10-dioleate to generate a new polyglycerol-6-didecanoate polymer and a new polyglycerol-10-dioleate polymer, and then adding the polyglycerol-6-didecanoate polymer and the polyglycerol-10-dioleate polymer into the mixed solution obtained in the step one to be fully and uniformly mixed;
step three, adding the vaccinium myrtillus seed oil, the meadowfoam seed oil and the sweet orange peel oil into the mixed solution obtained in the step one, and fully and uniformly mixing;
step four, crushing the nano-cellulose to enable particles of the nano-cellulose to be crushed to 35-55nm, then adding the crushed particles of the nano-cellulose into the mixed solution in the step one, and fully and uniformly mixing;
and step five, reducing the temperature of the mixture obtained in the step to be below 40 ℃, and fully stirring until uniform liquid is formed to prepare the polyglycerol emulsifier cleansing oil.
9. The makeup remover oil of polyglycerol emulsifier and the preparation method thereof according to claim 8, wherein the makeup remover oil comprises the following components: the stirring equipment in the first step comprises a stirring barrel and a stirring rod, wherein the stirring barrel and the stirring rod can rotate simultaneously, and the rotating directions are opposite, so that the mixed materials can be quickly and uniformly mixed, and a water bath box is arranged outside the stirring barrel, so that the materials can be mixed at a proper temperature.
10. The makeup remover oil of polyglycerol emulsifier and the preparation method thereof according to claim 8, wherein the makeup remover oil comprises the following components: and D, quantitatively canning the polyglycerol emulsifier cleansing oil prepared in the fifth step in a packaging mode of a packaging tank, and plastically packaging the polyglycerol emulsifier cleansing oil at an opening of the packaging tank after packaging is finished to ensure the sealing property of the packaging tank.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202111528231.6A CN114129463A (en) | 2021-12-14 | 2021-12-14 | Cleansing oil of polyglycerol emulsifier and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
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Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2016088883A (en) * | 2014-11-04 | 2016-05-23 | ピアス株式会社 | Cosmetic |
| CN108014031A (en) * | 2017-12-27 | 2018-05-11 | 花安堂生物科技集团有限公司 | A kind of makeup remover and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2016088883A (en) * | 2014-11-04 | 2016-05-23 | ピアス株式会社 | Cosmetic |
| CN108014031A (en) * | 2017-12-27 | 2018-05-11 | 花安堂生物科技集团有限公司 | A kind of makeup remover and preparation method thereof |
Non-Patent Citations (1)
| Title |
|---|
| 王建新等, 中国纺织出版社 * |
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