CN114047082A - Method for testing shearing strength of non-uniform ground stress well cementation cement sheath and stratum interface - Google Patents

Method for testing shearing strength of non-uniform ground stress well cementation cement sheath and stratum interface Download PDF

Info

Publication number
CN114047082A
CN114047082A CN202111291046.XA CN202111291046A CN114047082A CN 114047082 A CN114047082 A CN 114047082A CN 202111291046 A CN202111291046 A CN 202111291046A CN 114047082 A CN114047082 A CN 114047082A
Authority
CN
China
Prior art keywords
cement
test piece
rock core
cylindrical
cubic
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202111291046.XA
Other languages
Chinese (zh)
Inventor
梁卫国
李静
邱宇超
张胜利
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Taiyuan University of Technology
Original Assignee
Taiyuan University of Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Taiyuan University of Technology filed Critical Taiyuan University of Technology
Priority to CN202111291046.XA priority Critical patent/CN114047082A/en
Publication of CN114047082A publication Critical patent/CN114047082A/en
Pending legal-status Critical Current

Links

Images

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N3/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N3/24Investigating strength properties of solid materials by application of mechanical stress by applying steady shearing forces
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/286Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q involving mechanical work, e.g. chopping, disintegrating, compacting, homogenising
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/36Embedding or analogous mounting of samples
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/36Embedding or analogous mounting of samples
    • G01N2001/366Moulds; Demoulding
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/0014Type of force applied
    • G01N2203/0025Shearing
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2203/00Investigating strength properties of solid materials by application of mechanical stress
    • G01N2203/02Details not specific for a particular testing method
    • G01N2203/025Geometry of the test
    • G01N2203/0252Monoaxial, i.e. the forces being applied along a single axis of the specimen

Abstract

The invention provides a method for testing the shearing strength of a non-uniform stress well cementation cement sheath-stratum interface, which comprises the following steps: (1) manufacturing a cement-rock core combined test piece; (2) placing the combined body test piece in a cubic mold, and pouring epoxy resin in the annular area to prepare a cubic test piece; (3) placing a pressure head at the top of a cylindrical cement sheath of a cubic test piece, placing the bottom of the cylindrical cement sheath on a hollow support base, and integrally placing the cylindrical cement sheath on a true triaxial rock pressure testing machine; starting the confining pressure loading system of the press to make unequal loads sigma in the horizontal direction2And σ3Respectively loaded to preset values, then a shaft pressure loading system is started, and the axial load sigma is slowly and uniformly loaded1Immediately stopping loading when the cement sheath and the rock are damaged to obtain a maximum load value FmaxAccording to cement and rockThe contact area of the stone, i.e. the lateral area of the cylindrical cement, calculates the cement-core bond shear strength. The invention has simple principle and simple and convenient operation.

Description

Method for testing shearing strength of non-uniform ground stress well cementation cement sheath and stratum interface
Technical Field
The invention belongs to the technical field of petroleum and natural gas exploitation and storage engineering, and particularly relates to a method for testing shearing strength of a cement sheath-stratum interface of non-uniform stress well cementation.
Background
The well cementation cement sheath not only can hang and protect the casing, but also has the function of interlayer isolation. In the process of oil and natural gas exploitation and storage, the interlayer packing characteristic of the well cementation cement sheath becomes a key index for evaluating the sealing integrity of a shaft. The well bore penetrates through stratums with different lithological properties from the earth surface to reach a reservoir, fluid is injected and extracted from the casing, the casing is easy to shrink, and the cement sheath is subjected to plastic deformation, so that a cement sheath cementing interface forms a micro-sheath, gas leaks from the micro-sheath, and the interlayer packing effect of the cement sheath fails.
In the prior art, a method for testing the shearing strength of the interface of a non-uniformly stressed cement sheath-stratum is not considered, so that the requirement of testing the shearing strength of a cementing two-interface under the condition of non-uniformly stress formed by structural stress is met.
Disclosure of Invention
The invention aims to provide a method for testing the shearing strength of a cement sheath-stratum interface of non-uniform ground stress well cementation, which solves the technical problem that the shearing strength of the cement sheath-stratum interface of an oil-gas well is difficult to test under the non-uniform ground stress while fully utilizing the existing test instrument under the condition that a rock core test piece is difficult to obtain.
In order to achieve the purpose, the invention adopts the following technical scheme: the method for testing the shearing strength of the interface between the non-uniform stress well cementation cement sheath and the stratum comprises the following steps:
(1) preparing a cement-rock core combined test piece:
selecting rock, preparing a rock core test piece, drilling a through hole in the middle of the rock core test piece, vertically placing the rock core test piece with the through hole on a glass plate, coating high-temperature butter on the contact surface of the glass plate and the rock core, injecting prepared cement paste into the through hole of the rock core test piece, then putting the whole body into a curing kettle for curing for seven days, and completing the preparation of the cement-rock core combined test piece.
(2) Selecting epoxy resin:
preparing epoxy resin, pouring the epoxy resin into a cylindrical mold, preparing a cylindrical test piece, performing uniaxial compression and Brazilian splitting tests after the epoxy resin is solidified, measuring the elastic modulus, Poisson's ratio and tensile strength of the cylindrical test piece, and selecting the epoxy resin proportion with small difference with the mechanical parameters of the core test piece.
(3) Preparing a cubic test piece:
and (2) placing the cement-rock core combined piece into a cubic die, wherein the height of the cubic die is the same as that of the combined piece, injecting the epoxy resin selected in the step (2) between the cubic die and the combined piece, pouring in a segmented and layered manner, pouring for 5cm each time, pouring again after solidification, and separating the epoxy resin from the cubic die after the epoxy resin is solidified.
(4) Placing the prepared cubic test piece between a pressure head and a support base, integrally placing the cubic test piece on a true triaxial rock pressure tester, and slowly applying sigma2And σ3To a preset value, then applying an axial stress sigma to the cylindrical cement by means of a ram1Observing the axial force-displacement curve, stopping the test immediately when the interface of the cement and the rock core slides relatively or the cement and the rock core break, and recording the peak load value Fmax
(5) The area of the contact surface between the cement and the rock core of the cement-rock core combined body test piece is the side area of the cylindrical cement, the diameter of the cylindrical cement is D, the length of the cylindrical cement is L, and the formula is defined by
Figure BDA0003333314040000031
And calculating the shear strength of the cement-rock core interface.
Further, the preparation of the cube test piece in the step (3) can prepare various epoxy resin poured cement-core composite test pieces with different sizes according to the core size drilled by the oil and gas well, and explore the shearing strength of the cementing two interfaces under different packing lengths of the cement sheath.
Further, σ is slowly applied in step (4)2And σ3To a predetermined value, σ2And σ3Representing two different horizontal ground stresses, and can simulate the cementing shear strength of a cementing interface under the nonuniform ground stress caused by the formation stress of rock formations with different depths.
The invention has the beneficial effects that:
(1) the method provided by the invention can be used for preparing standard cubic test pieces according to the rock core test pieces with different sizes in consideration of the actual rock core obtaining condition and the laboratory measurement condition, testing the bonding shear strength of the non-uniform ground stress cement-stratum interface under different scales, filling the blank of the existing equipment and technology, providing a theoretical basis for on-site evaluation of the interlayer packing capacity of the well cementation two-interface cement sheath and the damage condition of the cement sheath, and further evaluating the integrity failure risk of the well cementation two-interface cement sheath of the oil and gas well.
(2) The invention has simple principle and simple and convenient operation, can carry out interface shear strength test under non-uniform ground stress on cement-core combined body test pieces with different scales before and after a seepage test, is beneficial to simulating interlayer packing capacity of cement ring cementing two interfaces under real stress, better optimizes a cement slurry formula system, makes up the defects of the existing instrument and equipment, and has wide application prospect.
Drawings
FIG. 1 is a schematic diagram of a core test piece structure of a manufacturing process of a cement-core combined test piece.
Fig. 2 is a schematic structural diagram of a core test piece with a through hole after the core test piece drills the through hole in the manufacturing process of the cement-core combined test piece.
Fig. 3 is a schematic structural diagram of a core test piece with a through hole injected with cement slurry in a manufacturing process of a cement-core combination test piece.
Fig. 4 is a schematic structural diagram of the preparation of a cubic test piece.
Fig. 5 is a schematic view of an indenter, a cubic specimen, and a support base with a hollow circular hole.
Reference numbers in the figures: 1, a rock core; 2-hollow round hole; 3-cement and core cementing interface; 4-cement slurry; 5-high temperature butter; 6-glass plate; 7-epoxy resin; 8-cubic mold; 9-a pressure head; 10-a supporting base with a hollow round hole.
Detailed Description
The invention provides a method for testing the shearing strength of a non-uniform ground stress cement sheath-stratum interface by placing a cubic test piece (a cement-rock core combined test piece poured with epoxy resin) on a true triaxial rock press, which mainly comprises the following steps: epoxy resin, a cement-rock core combination test piece, a pressure head and a support base with a hollow round hole. The cement-rock core combined test piece is prepared by pouring cement slurry in the center of a cylindrical test piece with a prefabricated through hole and curing the cement slurry; the epoxy resin is used for pouring a cement-rock core combination test piece and the annular space of the cubic die to prepare a cubic test piece; the pressure head is used for applying axial load to the upper cylindrical cement; the support base with the hollow round hole is used for fixing the cubic test piece in the shearing test process, so that the cylindrical cement can be pushed out.
The method for testing the shearing strength of the cement sheath-stratum interface of the non-uniform stress well cementation sequentially comprises the following steps of:
(1) preparing a cement-rock core combination cylindrical test piece:
selecting a rock with a larger size, preparing a cylindrical rock core test piece (the size of the cylindrical rock core can be designed to be phi 50 multiplied by 100mm, phi 50 multiplied by 200mm and phi 50 multiplied by 300mm) by utilizing a linear cutting or rock core drilling machine, punching a through hole in the center of the rock core test piece, and preparing the rock core test piece with the through hole; and placing the prepared core test piece on a glass plate, and coating high-temperature grease on the contact part of the core test piece and the glass plate to play a certain sealing role. Then pouring cement slurry in the center of the core test piece with the through hole to simulate well cementation; and after the core test piece and the glass plate which are injected with the cement paste are integrally maintained for seven days in an environment with certain temperature and pressure (the maintenance temperature and pressure are determined according to the actual underground working condition), taking out the cement-core combined test piece, polishing the end surface of the test piece, cutting the test piece smoothly, and simultaneously ensuring that the axial length of the cylindrical cement is equal to that of the cylindrical core.
(2) Preparing a cubic test piece (a cement-core combined test piece poured with epoxy resin):
preparing epoxy resin according to different proportions, pouring the epoxy resin into a cylindrical mold, preparing a standard cylindrical test piece (the size is phi 50 multiplied by 100mm), placing the standard cylindrical test piece prepared from the epoxy resin on a uniaxial rock press after the standard cylindrical test piece is solidified at room temperature, testing the basic mechanical properties such as elastic modulus, Poisson ratio, tensile strength and the like, and selecting the proportion of the epoxy resin which is similar to the mechanical properties of the rock core test piece; and (2) placing the cement-core combined test piece prepared in the step (1) in the middle of a cube mould (the size of the cube mould can be designed to be 100mm multiplied by 100mm, 200mm multiplied by 200mm and 300mm multiplied by 300mm), injecting epoxy resin into an annular area of the cement-core combined test piece and the cube mould to enable the height of the epoxy resin to be consistent with the axial height of the cement-core combined test piece, placing the cement-core combined test piece at room temperature to be in a solidification state, separating the epoxy resin from the cube mould, and completing preparation of the cube test piece.
(3) Placing the cubic test piece on a true triaxial rock press machine for a shear test, and obtaining the cement-core interface shear strength through data processing, wherein the process is as follows:
a. placing a pressure head on the top of the cylindrical cement of the cubic test piece, placing a support base with a hollow round hole on the bottom of the cubic test piece, and enabling the hollow round hole to be over against the bottom of the cylindrical cement;
b. placing the whole of the step a on a base of a true triaxial rock press, and slowly applying sigma to a cubic test piece (a cement-rock core combined test piece poured with epoxy resin) at a certain speed by the press2And σ3When the preset value is reached, the press slowly applies axial load sigma to the cubic test piece through the press head1And simultaneously recording the peak load F of debonding of the interface between the cylindrical cement and the rock core of the cubic test piece until the cylindrical cement and the rock core slide relatively or the cement or rock in the cubic test piece cracksmax
The diameter of the cylindrical cement of the cement-core combined test piece is D, the height of the cylindrical cement is L, and the shear strength P of the cement-core interface is calculated according to the following formula:
Figure BDA0003333314040000061
the present invention will be described in detail below with reference to the accompanying drawings.
See the drawings. The invention provides a method for testing shearing strength of a non-uniform ground stress well cementation cement sheath-stratum interface, which mainly comprises the following steps:
the method comprises the following steps: a cylindrical rock core test piece 1 is prepared by utilizing a linear cutting or rock core drilling machine, a through hole 2 is punched in the center of the rock core test piece 1, and rock core test pieces with through holes of different sizes are prepared (figure 2). Step two: placing the prepared core test piece (figure 2) on a glass plate 6, coating high-temperature butter 5 on a place contacted with the glass plate, pouring cement paste 4 in the center of the core test piece (figure 2), wherein the cement paste 4 and the core test piece 1 form a contact surface 3, then placing the core test piece (figure 3) in an environment with certain temperature and pressure (determined according to the formation temperature and the ground stress of the actual embedded depth of a shaft) for curing for seven days, and completing the preparation of the cement-core combined test piece.
Step three: and taking out the cement-core combined test piece from the maintenance kettle, polishing the end face of the cement-core combined test piece, cutting the test piece smoothly, and simultaneously ensuring that the axial length of the cylindrical cement is equal to that of the cylindrical core.
Step four: the central cylindrical cement 4 was measured to have a diameter D and a height L, i.e. the lateral area a of the cylindrical cement ═ pi DL.
Step five: preparing epoxy resin 7 according to the weight ratio of the AB glue to the glue B of 3:1, placing a cement-rock core combined test piece into a cubic die 8, pouring the epoxy resin 7 in a layered manner in an annular area of the cement-rock core combined test piece and the cubic die until the axial length of the epoxy resin is the same as that of the cylindrical cement and the cylindrical rock core, stopping pouring, and after the epoxy resin is solidified, finishing the preparation of the cubic test piece.
Step six: the cubic test piece is taken out of the cubic mold 8 and placed between the indenter 9 and the support base 10 with the hollow circular hole.
Step seven: a cubic test piece, a pressure head 9 and a supporting base 10 with hollow round holes are integrally placed on a base of the true triaxial rock press, and sigma is slowly applied to the cubic test piece at the speed of 0.02Mpa/s by the press2And σ3After the preset value is reached, slowly applying an axial load sigma to the cubic test piece through the pressure head 91And simultaneously recording the peak load F of debonding of the interface between the cylindrical cement and the rock core of the cubic test piece until the cylindrical cement 4 and the rock core 1 slide relatively or the cement 4 and the rock core 1 in the cubic test piece crackmax
Step eight: calculating the bond shear strength P acting on the bonding interface 3 of the cubic test piece cement and the rock, namely
Figure BDA0003333314040000071
Examples
A method for testing the shearing strength of a cement sheath-stratum interface of non-uniform stress well cementation, taking the core size phi 50 multiplied by 100mm as an example, comprises the following steps:
the method comprises the following steps: a cylindrical rock core test piece 1 is prepared by utilizing a linear cutting or rock core drilling machine, a through hole 2 is punched in the center of the rock core test piece 1, and a rock core test piece with the outer diameter of 50mm, the inner diameter of 18mm and the height of 100mm is prepared (figure 2).
Step two: placing the prepared core test piece (figure 2) on a glass plate 6, coating high-temperature butter 5 at the position contacted with the glass plate, pouring cement paste 4 in the center of the hollow rock test piece, wherein the cement paste 4 and the core test piece 1 form a contact surface 3, then placing the core test piece (figure 3) into a curing kettle with the temperature of 25 ℃ and the pressure of 8MPa for curing for seven days, and completing the preparation of the cement-core combined test piece. Step three: and taking out the cement-core combined test piece from the maintenance kettle, polishing the end face of the cement-core combined test piece, cutting the test piece smoothly, and simultaneously ensuring that the axial length of the cylindrical cement is equal to that of the cylindrical core.
Step four: the central cylindrical cement 4 was measured to have a diameter of 18mm and a height of 100mm, i.e. the lateral area a of the cylindrical cement pi x 18 x 100 i 5654.87mm2=56.5487cm2
Step five: preparing epoxy resin 7 according to the weight ratio of the AB glue to the glue of 3:1, placing a cement-core combination test piece into a cubic mold 8 with the thickness of 100mm multiplied by 100mm, pouring the epoxy resin 7 in a layered mode in the annular area of the cement-core combination test piece and the cubic mold until the axial length of the epoxy resin is the same as that of the cylindrical cement and the cylindrical core, stopping pouring, waiting for the epoxy resin to solidify, and completing the preparation of the cubic test piece.
Step six: the cubic test piece is taken out of the cubic mold 8 and placed between the indenter 9 and the support base 10 with the hollow circular hole.
Step seven: a cubic test piece, a pressure head 9 and a supporting base 10 with hollow round holes are integrally placed on a base of the true triaxial rock press, and a pressure machine is used for simultaneously applying sigma to the cubic test piece at the speed of 0.02Mpa/s2And σ3When the pressure respectively reaches 6MPa and 8MPa, slowly applying axial load to a cement-rock core combined body test piece poured with epoxy resin at the speed of 0.5mm/min through a pressure head 9 until the cylindrical cement 4 and the rock core (figure 2) slide relatively or the cement 4 and the rock core (figure 2) in the cubic test piece crack, and simultaneously recording the peak load F of debonding of the interface between the cylindrical cement and the rock core of the cubic test piecemaxAnd 9.56 kN.
Step eight: calculating the bond shear strength P acting on the cement-rock bond interface 3 in a cubic test piece, i.e.
Figure BDA0003333314040000091
Finally, it is noted that the above embodiments illustrate rather than limit the invention, and that while the invention has been described with reference to the embodiments thereof, it will be understood by those skilled in the art that various changes in form and details may be made therein without departing from the spirit and scope of the invention as defined by the appended claims.

Claims (3)

1. The method for testing the shearing strength of the interface between the non-uniform ground stress well cementation cement sheath and the stratum is characterized by comprising the following steps: the method comprises the following steps:
(1) preparing a cement-rock core combined test piece:
selecting rock, preparing a rock core test piece, drilling a through hole in the middle of the rock core test piece, vertically placing the rock core test piece with the through hole on a glass plate, coating high-temperature butter on the contact surface of the glass plate and the rock core, injecting prepared cement paste into the through hole of the rock core test piece, then putting the whole body into a curing kettle for curing for seven days, and completing the preparation of the cement-rock core combined test piece;
(2) selecting epoxy resin:
preparing epoxy resin, pouring the epoxy resin into a cylindrical mold, preparing a cylindrical test piece, performing uniaxial compression and Brazilian splitting tests after the epoxy resin is solidified, measuring the elastic modulus, Poisson's ratio and tensile strength of the cylindrical test piece, and selecting the proportion of the epoxy resin with small difference with the mechanical parameters of the core test piece;
(3) preparing a cubic test piece:
placing a cement-rock core combined test piece into a cubic mold, wherein the height of the cubic mold is the same as that of the combined test piece, injecting the epoxy resin selected in the step (2) between the cubic mold and the combined test piece, pouring in a segmented and layered mode, pouring for 5cm each time, pouring again after solidification, and separating the epoxy resin from the cubic mold until the pouring is finished and the epoxy resin is solidified;
(4) placing the prepared cubic test piece between a pressure head and a support base, integrally placing the cubic test piece on a true triaxial rock pressure tester, and slowly applying sigma2And σ3To a preset value, then applying an axial stress sigma to the cylindrical cement by means of a ram1Observing the axial force-displacement curve, stopping the test immediately when the interface of the cement and the rock core slides relatively or the cement and the rock core break, and recording the peak load value Fmax
(5) The area of the contact surface between the cement and the rock core of the cement-rock core combined body test piece is the side area of the cylindrical cement, the diameter of the cylindrical cement is D, the length of the cylindrical cement is L, and the formula is defined by
Figure FDA0003333314030000021
And calculating the shear strength of the cement-rock core interface.
2. The method for testing the shear strength of the interface between the non-uniformly stressed well-cementing cement sheath and the stratum according to claim 1, wherein: and (3) preparing the cube test piece in the step (3), preparing various epoxy resin poured cement-core assembly test pieces with different sizes according to the core size drilled by the oil and gas well, and exploring the shearing strength of the two well cementation interfaces of the cement sheath under different packing lengths.
3. The method for testing the shear strength of the interface between the non-uniformly stressed well-cementing cement sheath and the stratum according to claim 1, wherein: slowly applying sigma in step (4)2And σ3To a predetermined value, σ2And σ3Representing two different horizontal ground stresses, and can simulate the cementing shear strength of a cementing interface under the nonuniform ground stress caused by the formation stress of rock formations with different depths.
CN202111291046.XA 2021-11-02 2021-11-02 Method for testing shearing strength of non-uniform ground stress well cementation cement sheath and stratum interface Pending CN114047082A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202111291046.XA CN114047082A (en) 2021-11-02 2021-11-02 Method for testing shearing strength of non-uniform ground stress well cementation cement sheath and stratum interface

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202111291046.XA CN114047082A (en) 2021-11-02 2021-11-02 Method for testing shearing strength of non-uniform ground stress well cementation cement sheath and stratum interface

Publications (1)

Publication Number Publication Date
CN114047082A true CN114047082A (en) 2022-02-15

Family

ID=80206839

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202111291046.XA Pending CN114047082A (en) 2021-11-02 2021-11-02 Method for testing shearing strength of non-uniform ground stress well cementation cement sheath and stratum interface

Country Status (1)

Country Link
CN (1) CN114047082A (en)

Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201627577U (en) * 2010-01-27 2010-11-10 中国石油大学(北京) True triaxial drilling-plugging simulation and evaluation device
CN102169061A (en) * 2011-01-07 2011-08-31 河海大学 Manufacture method for rock samples
CN102768174A (en) * 2011-05-06 2012-11-07 中国石油大学(北京) Experimental apparatus for determining permeability of raw coal and method thereof
CN103048178A (en) * 2013-01-22 2013-04-17 中国石油大学(华东) Method for preparing artificial rock core of simulated carbonate rock for acoustics experiment
CN204188439U (en) * 2014-11-17 2015-03-04 中国石油大学(北京) Irregular shale samples and ultrasonic inspection system
CN105259034A (en) * 2015-10-22 2016-01-20 东南大学 Method for measuring and representing microcosmic interface phases of asphalt concrete
CN106908292A (en) * 2017-02-28 2017-06-30 中国石油化工股份有限公司 A kind of mud shale artificial core preparation method and application
CN109724867A (en) * 2019-03-13 2019-05-07 合肥工业大学 Rock fracture response visual Simulation experimental system and method under hydraulic pressure are moved in pulse
CN109946147A (en) * 2019-04-03 2019-06-28 中国矿业大学 A kind of coal measures composite reservoir pressure break physical analogy test material preparation method
CN110333124A (en) * 2019-06-12 2019-10-15 华北水利水电大学 The reparation of rock dimensional defects and standard specimen preparation method
CN210660065U (en) * 2019-04-23 2020-06-02 成都理工大学 High-simulation well cementation bonding strength joint test auxiliary device
CN113504132A (en) * 2021-07-20 2021-10-15 山东科技大学 Critical trigger simulation method suitable for rock mass shear fracture in deep coupling state

Patent Citations (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN201627577U (en) * 2010-01-27 2010-11-10 中国石油大学(北京) True triaxial drilling-plugging simulation and evaluation device
CN102169061A (en) * 2011-01-07 2011-08-31 河海大学 Manufacture method for rock samples
CN102768174A (en) * 2011-05-06 2012-11-07 中国石油大学(北京) Experimental apparatus for determining permeability of raw coal and method thereof
CN103048178A (en) * 2013-01-22 2013-04-17 中国石油大学(华东) Method for preparing artificial rock core of simulated carbonate rock for acoustics experiment
CN204188439U (en) * 2014-11-17 2015-03-04 中国石油大学(北京) Irregular shale samples and ultrasonic inspection system
CN105259034A (en) * 2015-10-22 2016-01-20 东南大学 Method for measuring and representing microcosmic interface phases of asphalt concrete
CN106908292A (en) * 2017-02-28 2017-06-30 中国石油化工股份有限公司 A kind of mud shale artificial core preparation method and application
CN109724867A (en) * 2019-03-13 2019-05-07 合肥工业大学 Rock fracture response visual Simulation experimental system and method under hydraulic pressure are moved in pulse
CN109946147A (en) * 2019-04-03 2019-06-28 中国矿业大学 A kind of coal measures composite reservoir pressure break physical analogy test material preparation method
CN210660065U (en) * 2019-04-23 2020-06-02 成都理工大学 High-simulation well cementation bonding strength joint test auxiliary device
CN110333124A (en) * 2019-06-12 2019-10-15 华北水利水电大学 The reparation of rock dimensional defects and standard specimen preparation method
CN113504132A (en) * 2021-07-20 2021-10-15 山东科技大学 Critical trigger simulation method suitable for rock mass shear fracture in deep coupling state

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
刘海龙 等: "非均匀地应力下水泥环完整性规律研究", 科学技术与工程, vol. 14, no. 23, pages 34 - 41 *
曾德智 等: "非均匀地应力下水泥环界面应力分布规律研究", 石油钻探技术, vol. 35, no. 1, pages 32 - 34 *
闫相祯 等: "泥岩蠕变导致套管变形损坏机理分析", 钻采工艺, vol. 26, no. 3, pages 65 - 68 *

Similar Documents

Publication Publication Date Title
CN109030137B (en) Experimental device and method for simulating frozen soil stratum cement sheath consolidation
CN108590601B (en) Experimental method for optimizing water injection expansion construction parameters
CN104458445A (en) Shear test device and shear test method in in-situ soil body pore
CN112268768B (en) Similar simulation test system and method for unloading of vertical shaft slit type grouting curtain excavation
Yu et al. Triaxial test research on mechanical properties and permeability of sandstone with a single joint filled with gypsum
CN109342195B (en) Method for testing bonding strength of first bonding surface of oil well cement
CN111366472B (en) True triaxial hydraulic fracturing physical simulation equipment and method for variable core size
CN115639083B (en) True triaxial hydraulic fracturing simulation experiment method and device for mine field level
CN107589020B (en) A kind of hydraulic fracturing test method based on stress path
Chiu et al. Appropriate techniques for triaxial testing of saturated soft rock
CN105952445B (en) A kind of boring test method under large ground pressure based on mathematical model
CN113281182A (en) Multi-means integrated fracture quantitative evaluation method
CN107063791B (en) Test method and test sample for bonding characteristics of disintegrated soft rock and concrete
CN114414326A (en) Rock sample making and experiment method for interference of natural fracture network on hydraulic fracture
CN109241651B (en) Universal stratum fracture pressure prediction method
CN104374650A (en) Testing device and method for testing static force shear property between tubular pile and grouting soil body
CN204461905U (en) A kind of test unit testing static(al) shear property between pile tube and the slip casting soil body
CN113914851B (en) Experimental method for simulating seepage and suction of fracturing fluid in complex fracture system
CN114047082A (en) Method for testing shearing strength of non-uniform ground stress well cementation cement sheath and stratum interface
Zou et al. Experimental evaluation of the mechanical properties of cement sheath under high-temperature conditions
Guo et al. An experimental investigation into hydraulic fracture propagation—Part 1. Experimental facilities
CN112504938B (en) Seepage simulation device, real triaxial rock permeability real-time measuring system and method
CN113945467A (en) Multifunctional shear test device suitable for multi-material combined interface
CN113063664A (en) Device and method for testing tensile bond strength of first interface of well cementation cement sheath of oil-gas well
CN107059956B (en) Simple test method for measuring long-term shear strength of pile-soil contact surface

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination