CN113943614A - 一种羊奶手工皂及其制备工艺 - Google Patents

一种羊奶手工皂及其制备工艺 Download PDF

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CN113943614A
CN113943614A CN202111279011.4A CN202111279011A CN113943614A CN 113943614 A CN113943614 A CN 113943614A CN 202111279011 A CN202111279011 A CN 202111279011A CN 113943614 A CN113943614 A CN 113943614A
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goat milk
parts
handmade soap
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于广清
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Yangzhou Dongyuan Daily Chemical Tourist Products Factory
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Abstract

本发明涉及日用品制备技术领域，尤其涉及一种羊奶手工皂及其制备工艺。所述羊奶手工皂由石油菜提取物、椰子油、强碱、羊奶提取物、表面活性剂、稳定剂、润肤剂、无水乙醇、甘油、10％蔗糖溶液、去离子水组成。本发明通过添加石油菜提取物，与羊奶提取物共同配伍，能协同起到驱螨、抑螨的效果；其次，本发明中含有椰子油和肉豆蔻酸豆酯，润肤效果更佳，能有效抵消表面活性剂对皮肤的伤害。

Description

一种羊奶手工皂及其制备工艺
技术领域
本发明涉及日用品制备技术领域，尤其涉及一种羊奶手工皂及其制备工艺。
背景技术
皮肤是覆盖于人体表面的天然外衣，也是人体最大的器官，健康的皮肤能够完成复杂的生理功能，还能体现人体的美感，使人容光焕发富有健康活力。但是由于螨虫和细菌的侵袭，皮肤会因为代谢废物堵塞毛孔，而变得肤色暗黄，皮肤红肿长痘痘。
面部清洁对于预防螨虫脸非常重要，但是刺激性过强的化学产品会破坏皮肤的天然屏障，甚至会导致皮肤被清洁的越彻底，油脂分泌越亢进的矛盾循环。不少西药成分的杀菌除螨类药物有水杨酸、三氯生等，但是刷酸是通过削薄皮肤角质层来达到祛痘除螨效果，对皮肤伤害比较大。
瑶药石油菜为荨麻科植物波缘冷水花Pilea cavaleriei H.Lév.的全草，别名石花菜、肥奴奴草,小石芥、冷冻草、疳积草，石苋菜、肥猪菜、打不死、石凉菜、青蛙腿，分布在广西、广东、贵州、湖南等地。生于石山阴处，多见于海拔300-1500米的山坡林下石上。全年均可采收，洗净，鲜用或晒干。微苦，性凉；归肺、脾经。清肺止咳，利水消肿，解毒止痛。主治肺热咳嗽，肺结核，肾炎水肿，烧烫伤，跌打损伤，疮疖肿毒。从瑶医理论的角度上讲，石油菜既具风类药的功能，又具打类药的特性，是风打相兼类的瑶药。
基于上述情况，本发明提出了一种羊奶手工皂及其制备工艺，可有效解决以上问题。
发明内容
本发明的目的在于提供一种羊奶手工皂及其制备工艺。
为实现上述目的，本发明提供了一种羊奶手工皂，所述羊奶手工皂由石油菜提取物、椰子油、强碱、羊奶提取物、表面活性剂、稳定剂、润肤剂、无水乙醇、甘油、10％蔗糖溶液、去离子水组成。
优选地，所述羊奶手工皂由以下重量份的原料组成：椰子油20～40份、羊奶提取物25～45份、强碱30～40份、石油菜提取物20～40份、表面活性剂15～30份、稳定剂10～16份、润肤剂8～16份、无水乙醇10～30份、甘油6～10份、10％蔗糖溶液15～35份、去离子水120～140份。
在其中一个实施例中，所述石油菜提取物通过以下方法制备：
取石油菜药材备用，加入药材重量8～10倍的水，浸泡30～35min后，加热煮沸50～60min，200目滤布过滤，浓缩，即得。
优选地，所述强碱为氢氧化钠、氢氧化钾的其中一种。
优选地，所述表面活性剂为月桂醇聚醚硫酸酯钠、椰油酰胺丙基甜菜碱、月桂基羟基磺基甜菜碱中的一种或两种以上的组合。
优选地，所述表面活性剂为椰油酰胺丙基甜菜碱。
优选地，所述稳定剂包含氯化钠、椰子油二乙醇酰胺、PEG-150二硬脂酸酯、PPG-2羟乙基椰油酰胺中的一种或两种以上的混合。
有限地，所述稳定剂为椰子油二乙醇酰胺。
优选地，所述的润肤剂为肉豆蔻酸豆酯、辛酸辛酯、油醇油酸酯中的一种或两种以上的组合。
优选地，所述润肤剂为肉豆蔻酸豆酯。
本发明还提供一种羊奶手工皂的制备方法，所述方法包括以下步骤：
(1)取椰子油和羊奶提取物，加热溶解混合均匀后恒温至60～65℃，得到奶脂溶液；
(2)取氢氧化钠溶解于去离子水中，搅拌放热，冷却至指定的60～65℃，得到碱液，随后加入到步骤(1)的奶脂溶液中，以200～300r/min搅拌反应90～100min；
(3)向步骤(2)加入石油菜提取物、表面活性剂、稳定剂、润肤剂、无水乙醇，以200～300r/min搅拌反应120～140min；
(4)向步骤(3)加入甘油和10％蔗糖溶液，搅拌均匀，倒入模具中，室温放凉，24～48h后脱模即得。
与现有技术相比，本发明具有如下有益效果：
1.本发明通过添加石油菜提取物，与羊奶提取物共同配伍，能协同起到驱螨、抑螨的效果；其次，本发明中含有椰子油和肉豆蔻酸豆酯，润肤效果更佳，能有效抵消表面活性剂对皮肤的伤害。
2.本发明原材料在国内充足，价格适宜，使其规模化生产没有太高的成本限制；同时，制备方法简单，总体生产成本不高，有利于工业的大规模生产。
具体实施方式
实施例1
按表1称量具体原料，其余步骤制备步骤如下：
(1)取椰子油和羊奶提取物，加热溶解混合均匀后恒温至60℃，得到奶脂溶液；
(2)取氢氧化钠溶解于去离子水中，搅拌放热，冷却至指定的60℃，得到碱液，随后加入到步骤(1)的奶脂溶液中，以300r/min搅拌反应100min；
(3)向步骤(2)加入石油菜提取物、表面活性剂、稳定剂、润肤剂、无水乙醇，以300r/min搅拌反应140min；
(4)向步骤(3)加入甘油和10％蔗糖溶液，搅拌均匀，倒入模具中，室温放凉，48h后脱模即得。
实施例2
按表1称量具体原料，其余步骤制备步骤如下：
(1)取椰子油和羊奶提取物，加热溶解混合均匀后恒温至65℃，得到奶脂溶液；
(2)取氢氧化钠溶解于去离子水中，搅拌放热，冷却至指定的65℃，得到碱液，随后加入到步骤(1)的奶脂溶液中，以200r/min搅拌反应90min；
(3)向步骤(2)加入石油菜提取物、表面活性剂、稳定剂、润肤剂、无水乙醇，以200r/min搅拌反应120min；
(4)向步骤(3)加入甘油和10％蔗糖溶液，搅拌均匀，倒入模具中，室温放凉，24h后脱模即得。
实施例3
按表1称量具体原料，其余步骤制备步骤如下：
(1)取椰子油和羊奶提取物，加热溶解混合均匀后恒温至65℃，得到奶脂溶液；
(2)取氢氧化钠溶解于去离子水中，搅拌放热，冷却至指定的65℃，得到碱液，随后加入到步骤(1)的奶脂溶液中，以300r/min搅拌反应100min；
(3)向步骤(2)加入石油菜提取物、表面活性剂、稳定剂、润肤剂、无水乙醇，以300r/min搅拌反应140min；
(4)向步骤(3)加入甘油和10％蔗糖溶液，搅拌均匀，倒入模具中，室温放凉，48h后脱模即得。
对比例1
按表1称量具体原料，步骤制备步骤如下：
(1)取椰子油和羊奶提取物，加热溶解混合均匀后恒温至65℃，得到奶脂溶液；
(2)取氢氧化钠溶解于去离子水中，搅拌放热，冷却至指定的65℃，得到碱液，随后加入到步骤(1)的奶脂溶液中，以300r/min搅拌反应100min；
(3)向步骤(2)加入石油菜提取物、表面活性剂、稳定剂、润肤剂、无水乙醇，以300r/min搅拌反应140min；
(4)向步骤(3)加入甘油和10％蔗糖溶液，搅拌均匀，倒入模具中，室温放凉，48h后脱模即得。
表1
物料种类 实施例1 实施例2 实施例3 对比例1
椰子油 20 30 40 40
羊奶提取物 25 35 45 45
氢氧化钠 30 35 40 40
石油菜提取物 20 30 40 /
椰油酰胺丙基甜菜碱 15 25 30 30
椰子油二乙醇酰胺 10 12 16 16
肉豆蔻酸豆酯 8 12 16 16
无水乙醇 10 20 30 30
甘油 6 8 10 10
10％蔗糖溶液 15 25 35 35
去离子水 120 130 140 140
实施例4除螨效果测试
除螨效果测试：取实施例1～3以及对比例1制备羊奶手工皂，参照GB/T 242532009进行螨虫抑制率试验。测试结果见表2。
表2除螨性能结果
60min抑制率％ 120min抑制率％
实施例1 85 95
实施例2 82 94
实施例3 86 95
对比例1 42 50
前述对本发明的具体示例性实施方案的描述是为了说明和例证的目的。这些描述并非想将本发明限定为所公开的精确形式，并且很显然，根据上述教导，可以进行很多改变和变化。对示例性实施例进行选择和描述的目的在于解释本发明的特定原理及其实际应用，从而使得本领域的技术人员能够实现并利用本发明的各种不同的示例性实施方案以及各种不同的选择和改变。本发明的范围意在由权利要求书及其等同形式所限定。

Claims (9)

1.一种羊奶手工皂，其特征在于，所述羊奶手工皂由以下重量份的原料组成：椰子油20～40份、羊奶提取物25～45份、强碱30～40份、石油菜提取物20～40份、表面活性剂15～30份、稳定剂10～16份、润肤剂8～16份、无水乙醇10～30份、甘油6～10份、10％蔗糖溶液15～35份、去离子水120～140份。
2.根据权利要求1所述的羊奶手工皂，其特征在于，所述石油菜提取物通过以下方法制备：取石油菜药材备用，加入药材重量8～10倍的水，浸泡30～35min后，加热煮沸50～60min，200目滤布过滤，浓缩，即得。
3.根据权利要求1所述的羊奶手工皂，其特征在于，所述强碱为氢氧化钠、氢氧化钾的其中一种。
4.根据权利要求1所述的羊奶手工皂，其特征在于，所述表面活性剂为月桂醇聚醚硫酸酯钠、椰油酰胺丙基甜菜碱、月桂基羟基磺基甜菜碱中的一种或两种以上的组合。
5.根据权利要求4所述的羊奶手工皂，其特征在于，所述表面活性剂为椰油酰胺丙基甜菜碱。
6.根据权利要求1所述的羊奶手工皂，其特征在于，所述稳定剂包含氯化钠、椰子油二乙醇酰胺、PEG-150二硬脂酸酯、PPG-2羟乙基椰油酰胺中的一种或两种以上的混合。
7.根据权利要求1所述的羊奶手工皂，其特征在于，所述的润肤剂为肉豆蔻酸豆酯、辛酸辛酯、油醇油酸酯中的一种或两种以上的组合。
8.根据权利要求7所述的羊奶手工皂，其特征在于，所述的润肤剂为肉豆蔻酸豆酯。
9.一种制备权利要求1～8任一所述的羊奶手工皂的工艺，其特征在于，所述工艺包括以下步骤组成：
(1)取椰子油和羊奶提取物，加热溶解混合均匀后恒温至60～65℃，得到奶脂溶液；
(2)取氢氧化钠溶解于去离子水中，搅拌放热，冷却至指定的60～65℃，得到碱液，随后加入到步骤(1)的奶脂溶液中，以200～300r/min搅拌反应90～100min；
(3)向步骤(2)加入石油菜提取物、表面活性剂、稳定剂、润肤剂、无水乙醇，以200～300r/min搅拌反应120～140min。
(4)向步骤(3)加入甘油和10％蔗糖溶液，搅拌均匀，倒入模具中，室温放凉，24～48h后脱模即得。
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Publication number Priority date Publication date Assignee Title
WO2006064974A1 (ja) * 2004-12-17 2006-06-22 Shiseido Company, Ltd. 美白用皮膚外用剤、美白剤、美白方法および美白用皮膚外用剤の製造方法
CN101530087A (zh) * 2008-03-14 2009-09-16 北京绿色农华植保科技有限责任公司 一种含有唑螨酯和炔螨特的杀螨剂混合物
WO2017153943A1 (en) * 2016-03-09 2017-09-14 Biopharm Nz Limited Topical composition
CN113208992A (zh) * 2021-05-11 2021-08-06 广州杨森药业有限公司 一种温和祛痘除螨羊奶皂及其制备方法

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2006064974A1 (ja) * 2004-12-17 2006-06-22 Shiseido Company, Ltd. 美白用皮膚外用剤、美白剤、美白方法および美白用皮膚外用剤の製造方法
CN101530087A (zh) * 2008-03-14 2009-09-16 北京绿色农华植保科技有限责任公司 一种含有唑螨酯和炔螨特的杀螨剂混合物
WO2017153943A1 (en) * 2016-03-09 2017-09-14 Biopharm Nz Limited Topical composition
CN113208992A (zh) * 2021-05-11 2021-08-06 广州杨森药业有限公司 一种温和祛痘除螨羊奶皂及其制备方法

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