CN113893804A - High-boiling silicon oil hydrolysis production line - Google Patents

High-boiling silicon oil hydrolysis production line Download PDF

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Publication number
CN113893804A
CN113893804A CN202111143019.8A CN202111143019A CN113893804A CN 113893804 A CN113893804 A CN 113893804A CN 202111143019 A CN202111143019 A CN 202111143019A CN 113893804 A CN113893804 A CN 113893804A
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wall
boiling
reaction kettle
transmission mechanism
connecting rod
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舍布有沙
陈维
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She Buyousha
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She Buyousha
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/1456—Removing acid components
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/18—Absorbing units; Liquid distributors therefor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/14—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by absorption
    • B01D53/18—Absorbing units; Liquid distributors therefor
    • B01D53/185—Liquid distributors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0053—Details of the reactor
    • B01J19/0066—Stirrers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J4/00—Feed or outlet devices; Feed or outlet control devices
    • B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G77/00—Macromolecular compounds obtained by reactions forming a linkage containing silicon with or without sulfur, nitrogen, oxygen or carbon in the main chain of the macromolecule
    • C08G77/04—Polysiloxanes
    • C08G77/06—Preparatory processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00092—Tubes

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The invention relates to the field of chemical production, in particular to a high-boiling-point silicon oil hydrolysis production line which comprises a reaction kettle, wherein two motors are symmetrically arranged on the outer side of the reaction kettle, the axes of output shafts of the two motors are on the same straight line, the output shafts penetrate through the inner wall of the reaction kettle, one end, far away from the motors, of each output shaft is fixedly provided with a first transmission mechanism, a stirring mechanism is arranged between the first transmission mechanisms, a second transmission mechanism is symmetrically arranged on the inner wall of the reaction kettle and close to the upper end of a liquid level, an installation plate is movably arranged between the first transmission mechanism and the second transmission mechanism, the top end of the installation plate is fixedly provided with an atomizing system, a feeding system is arranged on the installation plate in a sliding manner, and a cooling system is fixedly arranged on the outer wall of the reaction kettle The production process has the problem of hydrochloric acid overflow and poor field environment.

Description

High-boiling silicon oil hydrolysis production line
Technical Field
The invention relates to the field of chemical production, in particular to a high-boiling-point silicon oil hydrolysis production line.
Background
The high-boiling silicone oil is an important chemical product, and the existing production method is that trimethylchlorosilane and organosilicon chlorosilane high-boiling components (hereinafter referred to as high-boiling components) are uniformly mixed in a storage tank of a raw material tank area according to a certain proportion and transferred into a workshop high-boiling head tank by a transfer pump. Adding a certain amount of clear water into the hydrolysis reaction kettle in the elevated tank, starting a reaction kettle stirrer, slowly dropwise adding the high-boiling substances in the elevated tank into the reaction kettle, and then performing hydrolysis reaction on the high-boiling substances and water to generate hydrolyzed silicone oil and byproduct hydrochloric acid. And after the dropwise addition is finished, stopping stirring, standing for 30-60 minutes, discharging the hydrochloric acid on the lower layer in the kettle into a collecting tank, containing the silicone oil on the upper layer in a ton barrel, and then transferring to a neutralization kettle to add soda for neutralization. And (4) filling the neutralized salt-oil mixture again in a turnover ton barrel, standing for 24-48 hours, packaging the upper layer of silicon oil, and separately treating the lower layer of oil-salt mixture.
The current production method has the following problems: the manpower consumption is large; the removal capability of reaction heat is poor, and the production cannot be carried out at high temperature; the production process has hydrochloric acid overflow and poor field environment.
Disclosure of Invention
The invention aims to provide a high-boiling-point silicon oil hydrolysis production line, which solves the problems that the labor consumption is high, the reaction heat removal capacity is poor, the production cannot be carried out when the temperature is high, and the production process has the problem that the site environment is poor due to hydrochloric acid overflow.
In order to achieve the purpose, the invention adopts the following technical scheme:
the invention provides a high-boiling-point silicon oil hydrolysis production line which comprises a reaction kettle, wherein two motors are symmetrically arranged on the outer side of the reaction kettle, the axes of the output shafts of the two motors are on the same straight line, the output shafts penetrate through the inner wall of the reaction kettle, a first transmission mechanism is fixedly installed at one end, far away from the motors, of each output shaft, a stirring mechanism is arranged between the first transmission mechanisms, a second transmission mechanism is symmetrically arranged on the inner wall of the reaction kettle and close to the upper end of a liquid level, an installation plate is movably arranged between the first transmission mechanism and the second transmission mechanism, an atomization system is fixedly installed at the top end of the installation plate, a feeding system is arranged on the installation plate in a sliding mode, and a cooling system is fixedly installed on the outer wall of the reaction kettle.
Preferably, the first transmission mechanism comprises a first transmission rod and a first connecting rod, one end of the first transmission rod is fixedly connected with the output shaft, the other end of the first transmission rod is rotatably connected with the first connecting rod, and one end, far away from the first transmission rod, of the second connecting rod is rotatably connected with the bottom end of the mounting plate.
Preferably, rabbling mechanism includes first pivot, the both ends of first pivot with one side bottom fixed connection of motor is kept away from to the mounting panel, rotate on the first pivot and install a plurality of rotation seats, fixed mounting has a plurality of flabellums on the rotation seat lateral wall.
Preferably, second drive mechanism includes second pivot, second transfer line and second connecting rod, the second pivot is rotated and is installed on reation kettle's the inner wall and be located liquid level upper end position, the one end that the inner wall was kept away from in the second pivot with the middle part fixed connection of second transfer line, the one end of second transfer line with the middle part of mounting panel is rotated and is connected, the other end of second transfer line with the second connecting rod rotates and is connected, the one end that the second transfer line was kept away from to the second connecting rod with charging system rotates and connects.
Preferably, atomizing system includes the atomizing groove, atomizing groove fixed mounting be in the top of mounting panel, one side in atomizing groove is equipped with the flexonics pipe, the flexonics pipe with cooling system intercommunication.
Preferably, charging system includes elevated tank and slider, slider slidable mounting be in on the mounting panel, the slider is close to one side of reation kettle inner wall with the second connecting rod rotates to be connected, the both ends of elevated tank respectively with two slider fixed connection, the elevated tank upper end is equipped with the conveying pipeline, the conveying pipeline is flexible material.
Preferably, the cooling system comprises a supporting plate, the supporting plate is fixedly connected with the outer wall of the reaction kettle, the cross section of the supporting plate is L-shaped, a cooling water pipe is spirally arranged between the supporting plate and the outer wall of the reaction kettle, and the upper end of the cooling water pipe is communicated with the flexible connecting pipe.
Preferably, the inner wall, the output shaft, the first transmission mechanism, the stirring mechanism, the second transmission mechanism, the mounting plate, the atomizing system, the feeding system and the cooling system of the reaction kettle are made of acid corrosion resistant materials.
The invention has the beneficial effects that:
1. by arranging the feeding mechanism, the reaction raw materials can be directly mixed in the reaction kettle and added into water in the reaction kettle dropwise for reaction, and the raw materials do not need to be completely mixed in one step and then added into water dropwise for reaction, so that the working procedure is optimized, and the labor for mixing high-boiling-point substances is saved;
2. by arranging the cooling system and the atomization system communicated with the cooling system, the reaction heat can be removed in time, and the influence of the external environment temperature on the hydrolysis reaction can be reduced; the water mist sprayed by the atomization system can absorb HCl gas overflowing during reaction, the quality of the production environment is improved, and water which is one of reaction raw materials in the reaction kettle can be supplemented.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings required to be used in the embodiments of the present invention will be briefly described below. It is obvious that the drawings described below are only some embodiments of the invention, and that for a person skilled in the art, other drawings can be derived from them without inventive effort.
FIG. 1 is a schematic structural view of the present invention;
fig. 2 is a schematic diagram of the overall structure of the first transmission mechanism, the stirring mechanism, the second transmission mechanism and the atomization system in the invention.
In the figure: the device comprises a reaction kettle 1, a motor 2, an output shaft 21, a first transmission mechanism 3, a first transmission rod 31, a first connecting rod 32, a stirring mechanism 4, a first rotating shaft 41, a rotating seat 42, fan blades 43, a second transmission mechanism 5, a second rotating shaft 51, a second transmission rod 52, a second connecting rod 53, a mounting plate 6, an atomization system 7, an atomization groove 71, a flexible connecting pipe 72, a feeding system 8, a high-level groove 81, a material conveying pipe 82, a sliding block 83, a cooling system 9, a supporting plate 91 and a cooling water pipe 92.
Detailed Description
The technical scheme of the invention is further explained by the specific implementation mode in combination with the attached drawings. Wherein the showings are for the purpose of illustration only and are shown by way of illustration only and not in actual form, and are not to be construed as limiting the present patent; to better illustrate the embodiments of the present invention, some parts of the drawings may be omitted, enlarged or reduced, and do not represent the size of an actual product; it will be understood by those skilled in the art that certain well-known structures in the drawings and descriptions thereof may be omitted.
The same or similar reference numerals in the drawings of the embodiments of the present invention correspond to the same or similar components; in the description of the present invention, it should be understood that if the terms "upper", "lower", "left", "right", "inner", "outer", etc. are used for indicating the orientation or positional relationship based on the orientation or positional relationship shown in the drawings, it is only for convenience of description and simplification of description, but it is not indicated or implied that the referred device or element must have a specific orientation, be constructed in a specific orientation and be operated, and therefore, the terms describing the positional relationship in the drawings are only used for illustrative purposes and are not to be construed as limitations of the present patent, and the specific meanings of the terms may be understood by those skilled in the art according to specific situations.
In the description of the present invention, unless otherwise explicitly specified or limited, the term "connected" or the like, if appearing to indicate a connection relationship between the components, is to be understood broadly, for example, as being fixed or detachable or integral; can be mechanically or electrically connected; they may be directly connected or indirectly connected through intervening media, or may be connected through one or more other components or may be in an interactive relationship with one another. The specific meanings of the above terms in the present invention can be understood in specific cases to those skilled in the art.
Referring to fig. 1-2, a high boiling silicon oil hydrolysis production line, including reation kettle 1, reation kettle 1 outside symmetry is provided with two motors 2, the axis of the output shaft 21 of two motors 2 is on the collinear, output shaft 21 runs through reation kettle 1's inner wall, the one end fixed mounting that output shaft 21 kept away from motor 2 has first drive mechanism 3, be equipped with rabbling mechanism 4 between the first drive mechanism 3, on reation kettle 1's the inner wall and be close to the upper end position symmetry of liquid level and be equipped with second drive mechanism 5, the activity is provided with mounting panel 6 between first drive mechanism 3 and the second drive mechanism 5, 6 top fixed mounting in mounting panel has atomizing system 7, it is provided with charging system 8 to slide on mounting panel 6, fixed mounting has cooling system 9 on reation kettle 1's the outer wall.
Specifically, first drive mechanism 3 includes first transfer line 31 and first connecting rod 32, the one end and the output shaft 21 fixed connection of first transfer line 31, the other end and the first connecting rod 32 of first transfer line 31 rotate to be connected, the one end that first transfer line 31 was kept away from to second connecting rod 32 rotates with the bottom of mounting panel 6 to be connected, starter motor 2, output shaft 21 drives two first transfer lines 31 mirror image synchronous rotations, and then drives the motion of mounting panel 6 through the transmission of first connecting rod 32.
Concretely, rabbling mechanism 4 includes first pivot 41, motor 2's one side bottom fixed connection is kept away from with mounting panel 6 at the both ends of first pivot 41, rotate on the first pivot 41 and install a plurality of rotation seats 42, rotate on the seat 42 lateral wall fixed mounting have a plurality of flabellums 43, drive rabbling mechanism 4 during the motion of mounting panel 6 and move in liquid, flabellum 43 receives the influence of liquid resistance during the motion, self produces independent rotation, stir reaction liquid, reaction rate is improved.
Specifically, the second transmission mechanism 5 includes a second rotating shaft 51, a second transmission rod 52 and a second connecting rod 53, the second rotating shaft 51 is rotatably installed on the inner wall of the reaction kettle 1 and located at the upper end of the liquid level, one end of the second rotating shaft 51, which is far away from the inner wall, is fixedly connected with the middle part of the second transmission rod 52, one end of the second transmission rod 52 is rotatably connected with the middle part of the mounting plate 6, the other end of the second transmission rod 52 is rotatably connected with the second connecting rod 53, one end of the second connecting rod 53, which is far away from the second transmission rod 52, is rotatably connected with the feeding system 8, the mounting plate 6 drives the second transmission rod 52 to rotate by taking the second rotating shaft 51 as an axis during movement, and further drives the feeding mechanism 8 to slide on the mounting plate 6 through the second connecting rod 53.
Specifically, atomizing system 7 includes atomizing groove 71, atomizing groove 71 fixed mounting is on the top of mounting panel 6, one side of atomizing groove 71 is equipped with flexible connection pipe 72, flexible connection pipe 72 and cooling system 9 intercommunication, cooling water gets into atomizing groove 71 and sprays into reation kettle 1 in from cooling system 9 via flexible connection pipe 72, because atomizing groove 71 follows mounting panel 6 synchronous motion, make the scope of spraying expand, HCl gas that overflows when fully absorbing the reaction has improved the quality of production environment also can supply one of the interior reaction raw materials' of reation kettle water.
Concretely, charging system 8 includes elevated tank 81 and slider 83, slider 83 slidable mounting is on mounting panel 6, one side that slider 83 is close to reation kettle 1 inner wall rotates with second connecting rod 53 to be connected, elevated tank 81's both ends respectively with two slider 83 fixed connection, elevated tank 81 upper end is equipped with conveying pipeline 82, conveying pipeline 82 is flexible material, make the restriction that elevated tank 81 received when the motion reduce, elevated tank 81 follows slider 83 also along with mounting panel 6 swings along the gliding while of mounting panel 6, make the aquatic that reaction of hydrolysis in the direct dropwise add entering reation kettle 1 in the back of the reaction raw materials can one step of misce bene earlier, the manpower of being responsible for mixing high boiling material in advance has been saved.
Specifically, cooling system 9 includes backup pad 91, backup pad 91 and reation kettle 1's outer wall fixed connection, backup pad 91's cross-section is "L" type, the spiral is provided with condenser tube 92 between backup pad 91 and reation kettle 1's the outer wall, condenser tube 92's upper end and flexible connection pipe 72 intercommunication, condenser tube 92 spiral winding is on reation kettle 1 surface and with the laminating of reation kettle outer wall, be convenient for remove the reaction heat, make hydrolysis go on smoothly, also can reduce the influence of external environment temperature to the reaction.
Specifically, the inner wall of the reaction kettle 1, the output shaft 21, the first transmission mechanism 3, the stirring mechanism 4, the second transmission mechanism 5, the mounting plate 6, the atomizing system 7, the feeding system 8 and the cooling system 9 are all made of acid corrosion resistant materials, so that the device structure is prevented from being corroded by hydrochloric acid generated by reaction.
The working principle is as follows: when the device is used, a high-boiling-point substance of one of the reaction raw materials is conveyed into the high-level tank 81 through the conveying pipe 82, the motor 2 is started, the output shaft 21 drives the two first transmission rods 31 to synchronously rotate in a mirror image manner, the mounting plate 6 is driven to move through the transmission of the first connecting rod 32, the stirring mechanism 4 is driven to move in liquid when the mounting plate 6 moves, and the fan blades 43 are influenced by liquid resistance during movement and independently rotate to stir reaction liquid, so that the reaction speed is improved; meanwhile, the mounting plate 6 drives the second transmission rod 52 to rotate by taking the second rotating shaft 51 as an axis when moving, and then the second connecting rod 53 drives the sliding block 83 to slide along the mounting plate 6, so that the elevated tank 81 can follow the sliding block 83 to slide along the mounting plate 6 and swing along with the mounting plate 6, so that the reaction raw materials can be uniformly mixed in one step and then directly dripped into water in the reaction kettle 1 for hydrolysis reaction, and the manpower for mixing high-boiling residues in advance is saved; open external water source, condenser tube 92 flows through, condenser tube 92 spiral winding is on reation kettle 1 surface and with the laminating of reation kettle outer wall, be convenient for remove the reaction heat, make the hydrolysis go on smoothly, also can reduce the influence of external environment temperature to the reaction, the cooling water gets into atomizing groove 71 and sprays into reation kettle 1 in from condenser tube 92 via flexible connection pipe 72, because atomizing groove 71 follows mounting panel 6 synchronous motion, make the scope of spraying expand, also can supply one of the interior reaction raw materials' of reation kettle when fully absorbing the HCl gas that overflows during the reaction and having improved the quality of production environment.
It should be understood that the above-described embodiments are merely preferred embodiments of the invention and the technical principles applied thereto. It will be understood by those skilled in the art that various modifications, equivalents, changes, and the like can be made to the present invention. However, such variations are within the scope of the invention as long as they do not depart from the spirit of the invention. In addition, certain terms used in the specification and claims of the present application are not limiting, but are used merely for convenience of description.

Claims (8)

1. The utility model provides a high-boiling silica oil hydrolysis production line, includes reation kettle (1), its characterized in that: two motors (2) are symmetrically arranged on the outer side of the reaction kettle (1), the axes of output shafts (21) of the two motors (2) are on the same straight line, the output shaft (21) penetrates through the inner wall of the reaction kettle (1), one end of the output shaft (21) far away from the motor (2) is fixedly provided with a first transmission mechanism (3), a stirring mechanism (4) is arranged between the first transmission mechanisms (3), a second transmission mechanism (5) is symmetrically arranged on the inner wall of the reaction kettle (1) and close to the upper end of the liquid level, a mounting plate (6) is movably arranged between the first transmission mechanism (3) and the second transmission mechanism (5), the top end of the mounting plate (6) is fixedly provided with an atomizing system (7), the mounting plate (6) is provided with a charging system (8) in a sliding way, and a cooling system (9) is fixedly arranged on the outer wall of the reaction kettle (1).
2. The high-boiling-point silicon oil hydrolysis production line of claim 1, characterized in that: first drive mechanism (3) include first transfer line (31) and first connecting rod (32), the one end of first transfer line (31) with output shaft (21) fixed connection, the other end of first transfer line (31) with first connecting rod (32) rotate and connect, second connecting rod (32) keep away from the one end of first transfer line (31) with the bottom of mounting panel (6) rotates and connects.
3. The high-boiling-point silicon oil hydrolysis production line of claim 1, characterized in that: rabbling mechanism (4) include first pivot (41), the both ends of first pivot (41) with one side bottom fixed connection of motor (2) is kept away from in mounting panel (6), rotate on first pivot (41) and install a plurality of rotation seats (42), fixed mounting has a plurality of flabellums (43) on rotation seat (42) lateral wall.
4. The high-boiling-point silicon oil hydrolysis production line of claim 1, characterized in that: second drive mechanism (5) include second pivot (51), second transfer line (52) and second connecting rod (53), second pivot (51) rotate to be installed on the inner wall of reation kettle (1) and be located liquid level upper end position, second pivot (51) keep away from the one end of inner wall with the middle part fixed connection of second transfer line (52), the one end of second transfer line (52) with the middle part of mounting panel (6) is rotated and is connected, the other end of second transfer line (52) with second connecting rod (53) rotate and connect, second transfer line (52) are kept away from in second connecting rod (53) one end with charging system (8) rotate and connect.
5. The high-boiling-point silicon oil hydrolysis production line of claim 1, characterized in that: atomizing system (7) are including atomizing groove (71), atomizing groove (71) fixed mounting be in the top of mounting panel (6), one side of atomizing groove (71) is equipped with flexible connection pipe (72), flexible connection pipe (72) with cooling system (9) intercommunication.
6. The high boiling silicon oil hydrolysis line as set forth in claim 1 or 4, wherein: charging system (8) are including elevated tank (81) and slider (83), slider (83) slidable mounting be in on mounting panel (6), slider (83) are close to one side of reation kettle (1) inner wall with second connecting rod (53) rotate and are connected, the both ends of elevated tank (81) respectively with two slider (83) fixed connection, elevated tank (81) upper end is equipped with conveying pipeline (82), conveying pipeline (82) are flexible material.
7. The high boiling silicon oil hydrolysis line as set forth in claim 1 or 5, wherein: cooling system (9) include backup pad (91), backup pad (91) with the outer wall fixed connection of reation kettle (1), the cross-section of backup pad (91) is "L" type, backup pad (91) with spiral arrangement has cooling water pipe (92) between the outer wall of reation kettle (1), the upper end of cooling water pipe (92) with flexonics pipe (72) intercommunication.
8. The high-boiling-point silicon oil hydrolysis production line of claim 1, characterized in that: the inner wall of the reaction kettle (1), the output shaft (21), the first transmission mechanism (3), the stirring mechanism (4), the second transmission mechanism (5), the mounting plate (6), the atomizing system (7), the feeding system (8) and the cooling system (9) are all made of acid corrosion resistant materials.
CN202111143019.8A 2021-09-28 2021-09-28 High-boiling silicon oil hydrolysis production line Pending CN113893804A (en)

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KR101921870B1 (en) * 2018-07-19 2018-11-23 박병민 Device for processing hydrolysis
CN109443068A (en) * 2018-12-29 2019-03-08 南京工业大学 Spray cooling system adaptable to different gravity environments
CN209985165U (en) * 2019-05-21 2020-01-24 山东瑞兴阻燃科技有限公司 Tail gas purification and absorption device for high-concentration hydrochloric acid production
CN213160571U (en) * 2020-06-15 2021-05-11 张莉颖 Mixing arrangement is used in agricultural fertilization

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Publication number Priority date Publication date Assignee Title
CN102153752A (en) * 2010-12-03 2011-08-17 湖北新四海化工股份有限公司 Method and device for preparing high-boiling-point silicone oil
CN207581711U (en) * 2017-10-17 2018-07-06 江西元康硅业科技有限公司 A kind of hydrolysis loop system of the high containing hydrogen silicone oil of continuous production
KR101921870B1 (en) * 2018-07-19 2018-11-23 박병민 Device for processing hydrolysis
CN109443068A (en) * 2018-12-29 2019-03-08 南京工业大学 Spray cooling system adaptable to different gravity environments
CN209985165U (en) * 2019-05-21 2020-01-24 山东瑞兴阻燃科技有限公司 Tail gas purification and absorption device for high-concentration hydrochloric acid production
CN213160571U (en) * 2020-06-15 2021-05-11 张莉颖 Mixing arrangement is used in agricultural fertilization

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