CN113892647A - Preparation and addition method of white tomato colorless carotene - Google Patents

Preparation and addition method of white tomato colorless carotene Download PDF

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Publication number
CN113892647A
CN113892647A CN202111231064.9A CN202111231064A CN113892647A CN 113892647 A CN113892647 A CN 113892647A CN 202111231064 A CN202111231064 A CN 202111231064A CN 113892647 A CN113892647 A CN 113892647A
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white tomato
parts
white
tomato
carotene
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薛圣山
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/105Plant extracts, their artificial duplicates or their derivatives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L19/00Products from fruits or vegetables; Preparation or treatment thereof
    • A23L19/09Mashed or comminuted products, e.g. pulp, purée, sauce, or products made therefrom, e.g. snacks
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L33/00Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
    • A23L33/10Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
    • A23L33/115Fatty acids or derivatives thereof; Fats or oils
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23PSHAPING OR WORKING OF FOODSTUFFS, NOT FULLY COVERED BY A SINGLE OTHER SUBCLASS
    • A23P10/00Shaping or working of foodstuffs characterised by the products
    • A23P10/30Encapsulation of particles, e.g. foodstuff additives
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Chemical & Material Sciences (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Nutrition Science (AREA)
  • Health & Medical Sciences (AREA)
  • Mycology (AREA)
  • Botany (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Cosmetics (AREA)
  • Medicinal Preparation (AREA)
  • Medicines Containing Plant Substances (AREA)

Abstract

The invention provides a preparation and addition method of white tomato colorless carotene, which comprises the following steps: s1, pretreating fresh white tomatoes: selecting 8-9 mature white tomato fresh fruits, cleaning and disinfecting the white tomato fresh fruits, and then pulping the white tomato fresh fruits to obtain white tomato pulp; extracting oleoresin in the white tomato serum by using a solvent extraction method according to 5-12% of effective components to obtain white tomato oleoresin; according to the mass parts, 6-30 parts of white tomato oleoresin, 25-35 parts of refined substance oil, 1-2 parts of casein, 0.5-2 parts of dipotassium hydrogen phosphate, 0.5-1.5 parts of sodium stearoyl lactate, 1-2 parts of mono-diglycerol fatty acid ester, 2 parts of water and 50 parts of glucose syrup are fully mixed and then prepared into capsules, which belongs to the technical field of extraction and application of white tomato effective components.

Description

Preparation and addition method of white tomato colorless carotene
Technical Field
The invention relates to the technical field of extraction and application of active ingredients of white tomatoes, in particular to a preparation and addition method of colorless carotene of the white tomatoes.
Background
The content of the colorless carotene (octahydro and hexahydro lycopene) in the white tomato is not comparable with that of other plants, and the colorless carotene has the effects of inhibiting the generation of human body melanoidin, resisting the damage of UVB and UVA in ultraviolet rays to human body skin and blocking the formation of tyrosinase, thereby achieving the effects of whitening and brightening the skin.
The content of the colorless carotene of the fresh fruits in different growth periods is different, the picking time period is arranged according to market demands, effective components of the effective content in the extraction process are ensured, and the effective components are accurately submitted to clients for subdividing the effective components.
Disclosure of Invention
The invention provides a preparation method and an addition method of white tomato colorless carotene, aiming at solving the problem that the application of the colorless carotene in white tomatoes is influenced by natural environment.
In order to achieve the purpose, the invention adopts the following technical scheme: a method for adding white tomato colorless carotene comprises the following steps:
s1, pretreatment of white tomato fresh fruits
Selecting 8-9 mature white tomato fresh fruits, cleaning and disinfecting the white tomato fresh fruits, and then pulping the white tomato fresh fruits to obtain white tomato pulp;
s2, extracting white tomato oleoresin
Extracting oleoresin in the white tomato serum by using a solvent extraction method according to 5-12% of effective components to obtain white tomato oleoresin;
s3, and processing by capsule wrapping
Fully mixing 6-30 parts of white tomato oleoresin, 25-35 parts of refined substance oil, 1-2 parts of casein, 0.5-2 parts of dipotassium hydrogen phosphate, 0.5-1.5 parts of sodium stearoyl lactylate, 1-2 parts of mono-diglycerol fatty acid ester, 2 parts of water and 50 parts of glucose syrup according to the mass parts, and then preparing into capsules;
s4, mixing and adding
And (3) three-dimensionally mixing the capsules and the white tomato freeze-dried powder to obtain the white tomato whitening raw material.
As a further description of the above technical solution:
the length of the particles of the capsule is 80-100 microns, and the wall thickness of the capsule is 10-20 microns.
As a further description of the above technical solution:
also comprises the detection of the content of the colorless carotene in the capsule.
A preparation method of white tomato colorless carotene comprises the following steps:
s1, extracting the multiple lycopene in the white tomato powder;
s2, separating oily substances from the multi-element lycopene by a supercritical extraction method, and then placing the oily substances in a light-proof container;
s3, measuring the content of the colorless carotene in the separated oily substance by using a PHLC analysis and measurement method.
As a further description of the above technical solution:
the white tomato powder is white tomato freeze-dried powder or spray-dried white tomato powder.
As a further description of the above technical solution:
pre-adding the oily substances with the content of the colorless carotene determined and the white tomato freeze-dried powder or the spray-dried white tomato powder, and fully mixing on a three-dimensional mixer to obtain the white tomato powder with high content of the colorless carotene.
The invention has the beneficial effects that: pure substances rich in the colorless carotene in the white tomatoes are extracted firstly and added into the white tomato freeze-dried powder according to the requirements of customers, so that the content proportion of effective components can be ensured, and the embarrassing situation that COA is inconsistent with raw materials in the sale process can be reduced;
by carrying out capsule wrapping treatment on the white tomato oleoresin, the damage to the effective components (white tomato colorless carotene) of the white tomato oleoresin in the middle process can be effectively avoided, and particularly the damage of illumination to the effective components is avoided.
Drawings
To more clearly illustrate the preparation and addition of a white tomato leuco carotene, the following figures are shown;
FIG. 1 is a diagram showing the melanin distribution on the body surface of a zebra fish embryo before an experiment;
FIG. 2 is a diagram showing the melanin distribution of the zebra fish embryo body surface after the experiment;
FIG. 3 is the melanin distribution map of the zebra fish embryo body surface after the test.
Detailed Description
Example one
The embodiment provides a method for adding white tomato colorless carotene, which comprises the following steps:
s1, pretreatment of white tomato fresh fruits
Selecting 8-9 mature white tomato fresh fruits, cleaning and disinfecting the white tomato fresh fruits, and then pulping the white tomato fresh fruits to obtain white tomato pulp;
s2, extracting white tomato oleoresin
Extracting oleoresin in the white tomato serum according to 5% of effective components by adopting a solvent extraction method to obtain white tomato oleoresin;
s3, and processing by capsule wrapping
Fully mixing 6 parts of white tomato oleoresin, 25 parts of refined substance oil, 1 part of casein, 0.5 part of dipotassium hydrogen phosphate, 0.5 part of sodium stearoyl lactylate, 1 part of mono-diglycerol fatty acid ester, 2 parts of water and 50 parts of glucose syrup according to the mass parts, and then preparing into capsules;
s4, mixing and adding
And (3) three-dimensionally mixing the capsule and the white tomato freeze-dried powder to obtain the white tomato whitening raw material, wherein the particle length of the capsule is 80-100 microns, and the wall thickness of the capsule is 10-20 microns.
Also comprises the detection of the content of the colorless carotene in the capsule.
Example two
The embodiment provides a method for adding white tomato colorless carotene, which comprises the following steps:
s1, pretreatment of white tomato fresh fruits
Selecting 8-9 mature white tomato fresh fruits, cleaning and disinfecting the white tomato fresh fruits, and then pulping the white tomato fresh fruits to obtain white tomato pulp;
s2, extracting white tomato oleoresin
Extracting oleoresin in the white tomato serum according to 12% of effective components by adopting a solvent extraction method to obtain white tomato oleoresin;
s3, and processing by capsule wrapping
Fully mixing 30 parts of white tomato oleoresin, 35 parts of refined substance oil, 2 parts of casein, 2 parts of dipotassium hydrogen phosphate, 1.5 parts of sodium stearoyl lactylate, 2 parts of mono-diglycerol fatty acid ester, 2 parts of water and 50 parts of glucose syrup according to parts by mass, and then preparing into capsules;
s4, mixing and adding
And (3) three-dimensionally mixing the capsule and the white tomato freeze-dried powder to obtain the white tomato whitening raw material, wherein the particle length of the capsule is 80-100 microns, and the wall thickness of the capsule is 10-20 microns.
Also comprises the detection of the content of the colorless carotene in the capsule.
EXAMPLE III
The embodiment provides a preparation method of white tomato colorless carotene, which comprises the following steps:
s1, extracting the multiple lycopene in the white tomato powder;
s2, separating oily substances from the multi-element lycopene by a supercritical extraction method, and then placing the oily substances in a light-proof container;
s3, measuring the content of the colorless carotene in the separated oily substance by using a PHLC analysis and measurement method.
The white tomato powder is white tomato freeze-dried powder or spray-dried white tomato powder.
Further comprising: pre-adding the oily substances with the content of the colorless carotene determined and the white tomato freeze-dried powder or the spray-dried white tomato powder, and fully mixing on a three-dimensional mixer to obtain the white tomato powder with high content of the colorless carotene.
And (3) experimental determination: diluting the test sample according to the gradient of 1%, 0.5%, 0.25%, 0.125% and 0.0625%, and counting the deformity rate and the death rate after 48 hours;
1%, 0.5%, 0.25% of the groups died. The embryo development of 0.125% group zebra fish and 0.0625% group zebra fish is normal and has no malformation, the melanin plaque on the body surface is reduced compared with the blank group (refer to attached figures 1 and 2), the imaging result is imported by using Image J software, the area of the melanin plaque in the figure is counted, the melanin content of the positive group is reduced (365)%, the two groups have a significant difference (P <0.01), the melanin content of the tested product of 0.0625% group is reduced (1615)%, and the two groups have no significant difference (P > 0.05). The melanin content of the test article 0.125% group is reduced (325)%, and the two groups have a significant difference (P <0.05), and the statistical results are shown in fig. 3.
Other embodiments of the invention will be apparent to those skilled in the art from consideration of the specification and practice of the disclosure herein. This application is intended to cover any variations, uses, or adaptations of the invention following, in general, the principles of the invention and including such departures from the present disclosure as come within known or customary practice within the art to which the invention pertains. It is intended that the specification and examples be considered as exemplary only, with a true scope and spirit of the invention being indicated by the following claims.
It is to be understood that relational terms such as "first" and "second," and the like, may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. The invention is not limited to the precise arrangements described above and shown in the drawings, and various modifications and changes may be made without departing from the scope thereof. The scope of the invention is limited only by the appended claims.

Claims (6)

1. A method for adding white tomato colorless carotene is characterized by comprising the following steps:
s1, pretreatment of white tomato fresh fruits
Selecting 8-9 mature white tomato fresh fruits, cleaning and disinfecting the white tomato fresh fruits, and then pulping the white tomato fresh fruits to obtain white tomato pulp;
s2, extracting white tomato oleoresin
Extracting oleoresin in the white tomato serum by using a solvent extraction method according to 5-12% of effective components to obtain white tomato oleoresin;
s3, and processing by capsule wrapping
Fully mixing 6-30 parts of white tomato oleoresin, 25-35 parts of refined substance oil, 1-2 parts of casein, 0.5-2 parts of dipotassium hydrogen phosphate, 0.5-1.5 parts of sodium stearoyl lactylate, 1-2 parts of mono-diglycerol fatty acid ester, 2 parts of water and 50 parts of glucose syrup according to the mass parts, and then preparing into capsules;
s4, mixing and adding
And (3) three-dimensionally mixing the capsules and the white tomato freeze-dried powder to obtain the white tomato whitening raw material.
2. The method for adding the colorless carotene of white tomato according to claim 1, wherein: the length of the particles of the capsule is 80-100 microns, and the wall thickness of the capsule is 10-20 microns.
3. The method for preparing and adding the colorless carotene of the white tomato, as claimed in claim 1, wherein the method comprises the following steps: also comprises the detection of the content of the colorless carotene in the capsule.
4. A preparation method of white tomato colorless carotene is characterized by comprising the following steps:
s1, extracting the multiple lycopene in the white tomato powder;
s2, separating oily substances from the multi-element lycopene by a supercritical extraction method, and then placing the oily substances in a light-proof container;
s3, measuring the content of the colorless carotene in the separated oily substance by using a PHLC analysis and measurement method.
5. The method for preparing the colorless carotene of white tomato according to claim 4, characterized in that: the white tomato powder is white tomato freeze-dried powder or spray-dried white tomato powder.
6. The method for preparing the colorless carotene of white tomato as claimed in claim 4, further comprising: pre-adding the oily substances with the content of the colorless carotene determined and the white tomato freeze-dried powder or the spray-dried white tomato powder, and fully mixing on a three-dimensional mixer to obtain the white tomato powder with high content of the colorless carotene.
CN202111231064.9A 2021-10-22 2021-10-22 Preparation and addition method of white tomato colorless carotene Pending CN113892647A (en)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH07147929A (en) * 1993-11-29 1995-06-13 Kagome Co Ltd Production of lycopene oil
WO2008015490A1 (en) * 2006-08-02 2008-02-07 Pierre Srl Food supplement based on biological lycopene and process to obtain biological lycopene
CN103861537A (en) * 2014-03-20 2014-06-18 中国热带农业科学院农产品加工研究所 Preparation method of essential oil microcapsule
CN111568783A (en) * 2020-06-23 2020-08-25 昆仑技术研究(广州)有限公司 Preparation method and application of white tomato extract liposome freeze-dried powder

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH07147929A (en) * 1993-11-29 1995-06-13 Kagome Co Ltd Production of lycopene oil
WO2008015490A1 (en) * 2006-08-02 2008-02-07 Pierre Srl Food supplement based on biological lycopene and process to obtain biological lycopene
CN103861537A (en) * 2014-03-20 2014-06-18 中国热带农业科学院农产品加工研究所 Preparation method of essential oil microcapsule
CN111568783A (en) * 2020-06-23 2020-08-25 昆仑技术研究(广州)有限公司 Preparation method and application of white tomato extract liposome freeze-dried powder

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