CN113811199A

CN113811199A - Tobacco composition comprising a tobacco component and an aerosol-forming material

Info

Publication number: CN113811199A
Application number: CN202080032613.7A
Authority: CN
Inventors: 瓦莱里奥·塞博尔德
Original assignee: Nicoventures Trading Ltd
Current assignee: Nicoventures Trading Ltd
Priority date: 2019-03-11
Filing date: 2020-03-11
Publication date: 2021-12-17
Also published as: EP3937663A1; KR20210135299A; JP2022524804A; AU2020235416A1; AU2020235416B2; US20220167659A1; WO2020183175A1; MX2021010947A; CA3132103C; IL286095A; CA3132103A1; JP2023113792A; UA128146C2; GB201903287D0; BR112021018054A2

Abstract

The present disclosure relates to a tobacco composition comprising a tobacco component and an aerosol-forming material, wherein the tobacco component comprises a tobacco leaf material in an amount between about 10% and about 90% by weight of the tobacco component, and wherein the tobacco leaf material has a nicotine content of greater than 1.5% by weight of the tobacco leaf material, and to a method of making the tobacco composition. The present disclosure also relates to an article comprising a tobacco composition for use in an aerosol provision system and to a system comprising a device arranged to heat the tobacco composition and generate an aerosol from the tobacco composition.

Description

Tobacco composition comprising a tobacco component and an aerosol-forming material

Technical Field

The present invention relates to tobacco compositions comprising an aerosol forming material, methods for preparing tobacco compositions, and articles of manufacture for use with aerosol generating devices, the articles of manufacture for use with aerosol generating devices comprising tobacco compositions.

Background

Many tobacco industry products include aerosolizable materials, such as tobacco compositions. Articles such as cigarettes, cigars, and the like burn an aerosolizable material during use to produce tobacco smoke. Attempts have been made to provide alternatives to these types of articles that burn tobacco materials by creating products that release compounds without burning. Examples of such products are so-called heat-not-burn products, also known as tobacco heating products or tobacco heating devices, which release compounds by heating but not burning the aerosolizable material.

Disclosure of Invention

According to an embodiment of the present invention, in a first aspect, there is provided a tobacco composition comprising a tobacco component and an aerosol-forming material, wherein the tobacco component comprises a tobacco leaf material (leaftobacco material) in an amount between about 10% and about 90% by weight of the tobacco component, and wherein the tobacco leaf material has a nicotine content of greater than 1.5% by weight of the tobacco leaf material.

According to an embodiment of the present invention, in a second aspect, there is provided a tobacco composition comprising a tobacco component and an aerosol-forming material, wherein the tobacco component comprises a tobacco leaf material in an amount of between about 10% and about 90% by weight of the tobacco component, and wherein the tobacco leaf material comprises the aerosol-forming material in an amount of up to about 10% by weight of the tobacco leaf material, and wherein the tobacco composition comprises the aerosol-forming material in an amount of between about 10% and about 30% by weight of the tobacco composition.

According to an embodiment of the invention, in a third aspect, there is provided a tobacco composition comprising a tobacco component and an aerosol-forming material, wherein the tobacco component comprises a tobacco leaf material in an amount of between about 10% and about 90% by weight of the tobacco component, and wherein the tobacco component comprises menthol in an amount of between about 3mg and about 16 mg.

According to an embodiment of the invention, in a fourth aspect, there is provided a process for preparing the tobacco composition of the first or second aspects above, the process comprising applying the aerosol-forming material to the tobacco leaf material.

According to an embodiment of the present invention, in a fifth aspect, there is provided a tobacco composition prepared using the method of the fourth aspect above.

According to an embodiment of the present invention, in a sixth aspect, there is provided the use of a tobacco composition according to the above first, second, third or fourth aspects in an article for use within an aerosol delivery system.

According to an embodiment of the present invention, in a seventh aspect, there is provided an article for use in an aerosol provision system, the article comprising a tobacco composition as described in the first, second, third and fourth aspects above.

According to an embodiment of the invention, in an eighth aspect, there is provided a system comprising a tobacco composition as described in the first, second, third and fourth aspects above and a device arranged for heating the tobacco composition and generating an aerosol from the tobacco composition.

Drawings

Embodiments of the invention will now be described, by way of example only, with reference to the accompanying drawings, in which:

FIG. 1 shows a flow diagram of a process for the paper-making reconstituted tobacco;

FIG. 2 shows a flow diagram of a process for making extruded tobacco;

FIG. 3 shows a flow diagram of a process for making a tobacco composition;

FIG. 4 is a side cross-sectional view of an article for use with a non-combustible aerosol provision device, the article comprising a mouthpiece;

FIG. 5a is a side cross-sectional view of another article for use with a non-combustible aerosol provision device, in this embodiment the article comprises a capsule-containing mouthpiece;

figure 5b is a cross-sectional view of the capsule-containing mouthpiece shown in figure 5 a;

FIG. 6 is a perspective view of a non-combustible aerosol provision device for generating an aerosol from the aerosol generating material of the article of FIGS. 4, 5a and 5 b;

FIG. 7 shows the device of FIG. 6 with the outer cover removed and no article present;

FIG. 8 is a partial cross-sectional side view of the device of FIG. 6;

FIG. 9 is an exploded view of the device of FIG. 6 with the outer cover omitted;

FIG. 10A is a cross-sectional view of a portion of the device of FIG. 6;

FIG. 10B is a close-up illustration of a region of the device of FIG. 6; and

FIG. 11 is a flow chart illustrating a method of manufacturing an article of manufacture for use with a non-combustible aerosol provision device.

Detailed Description

As used herein, the term "delivery system" is intended to encompass a system for delivering a substance to a user, and includes:

a non-combustible aerosol provision system that releases compounds from an aerosolizable material without combusting the aerosolizable material, such as an electronic cigarette, a tobacco heating product, and a mixing system, to generate an aerosol using a combination of aerosolizable materials;

an article comprising an aerosolizable material and configured for use within one of the non-combustible aerosol supply systems; and

aerosol-free delivery systems, such as lozenges, gums, patches, articles comprising inhalable powders, and smokeless tobacco products such as snus and snuff (snuff), deliver the material to the user without forming an aerosol.

According to the present disclosure, a "non-combustible" aerosol provision system is a system in which the ingredients of the aerosol provision system (or components thereof) may be aerosolized without burning or igniting to facilitate delivery to a user. A non-combustible aerosol supply system.

In one embodiment, the delivery system is a non-combustible aerosol supply system, such as a powered non-combustible aerosol supply system.

In one embodiment, the non-combustible aerosol provision system is an electronic cigarette, also referred to as an electronic smoking device or an electronic nicotine delivery system (END).

In one embodiment, the non-combustible aerosol provision system is a tobacco heating system, also referred to as a heated non-combustion system.

In one embodiment, the non-combustible aerosol provision system is a hybrid system that generates an aerosol using a combination of aerosolizable materials, one or more of which may be heated. Each aerosolizable material can be in the form of, for example, a solid, a liquid, or a gel. In one embodiment, the mixing system includes a liquid or gel aerosolizable material and a solid aerosolizable material. The solid aerosolizable material can include, for example, a tobacco material or a non-tobacco product.

In general, the non-combustible aerosol supply system can include a non-combustible aerosol supply device (also referred to herein as an aerosol generating device) and an article of manufacture for use with the non-combustible aerosol supply system. However, it is envisaged that the article itself comprising the means for powering the aerosol generating assembly may itself form a non-combustible aerosol provision system.

In one embodiment, the non-combustible aerosol provision device may include a power source and a controller. The power source may be an electrical power source or an exothermic power source. In one embodiment, the exothermic power source comprises a carbon substrate that can be energized to distribute electricity in the form of heat to an aerosolizable material or a heat transfer material proximate the exothermic power source. In one embodiment, a power source, such as an exothermic power source, is provided in the article to form a non-flammable aerosol supply.

In one embodiment, an article for use with a non-combustible aerosol provision device may include an aerosolizable material, an aerosol generating component, an aerosol generating region, a mouthpiece, and/or a region for receiving an aerosolizable material.

In one embodiment, the aerosol generating assembly is a heater capable of interacting with the aerosolizable material to release one or more volatiles from the aerosolizable material to form an aerosol. In one embodiment, the aerosol generating assembly is capable of generating an aerosol from an aerosolizable material without heating. For example, the aerosol generating assembly may be capable of generating an aerosol from an aerosolizable material without the application of heat thereto, e.g., via one or more of vibration, mechanical, pressure, or electrostatic means.

In one embodiment, the aerosolizable material can comprise an active material, an aerosol-forming material, and optionally one or more functional materials. The active material may comprise nicotine (optionally included in tobacco or a tobacco derivative) or one or more other non-olfactory physiologically active materials. Non-olfactory physiologically active materials are materials included in an aerosolizable material to effect a physiological response other than olfactory perception.

The aerosol-forming material may comprise one or more of glycerol, propylene glycol, diethylene glycol, triethylene glycol, tetraethylene glycol, 1, 3-butanediol, erythritol, meso-erythritol, ethyl vanillate, ethyl laurate, diethyl suberate, triethyl citrate, triacetin (triacetin), diacetin mixture (diacetin mixture), benzyl benzoate, benzyl phenylacetate (benzyl phenyl acetate), glyceryl tributyrate, lauryl acetate, lauric acid, myristic acid and propylene carbonate.

The one or more functional materials may include one or more of a fragrance, a carrier, a pH adjuster, a stabilizer, and/or an antioxidant.

In one embodiment, an article for use with a non-combustible aerosol provision device may include an aerosolizable material or a region for receiving an aerosolizable material. In one embodiment, an article for use with a non-combustible aerosol provision device may comprise a mouthpiece. The area for receiving the aerosolizable material may be a storage area for storing the aerosolizable material. For example, the storage area may be a memory. In one embodiment, the area for receiving the aerosolizable material may be separate from or combined with the aerosol-generating area.

An aerosolizable material, which may also be referred to herein as an aerosol-generating material and an aerosol-generating substrate, is a material that is capable of generating an aerosol, for example, when heated, irradiated, or energized in any other manner. The aerosolizable material may, for example, be in the form of a solid, liquid, or gel, which may or may not include nicotine and/or flavoring agents. In some embodiments, the aerosolizable material can comprise an "amorphous solid," which can alternatively be referred to as a "monolithic solid" (i.e., non-fibrous). In some embodiments, the amorphous solid may be a dried gel. An amorphous solid is a solid material in which some fluid, such as a liquid, may be retained. In some embodiments, the aerosolizable material can, for example, comprise about 50, 60, or 70 wt% amorphous solids to about 90, 95, or 100 wt% amorphous solids.

The aerosolizable material can be present on a substrate. The substrate may for example be or comprise paper, card, cardboard, reconstituted aerosolizable material, plastic material, ceramic material, composite material, glass, metal or metal alloy.

An aerosol modifier is a substance that is capable of modifying an aerosol in use. The agent can be modified into aerosol to produce physiological or organoleptic effect. Examples of aerosol modifiers are flavors and sensates (sensates). Sensates produce sensory sensations that can be perceived by feeling, such as a cooling or sour sensation.

Susceptors are materials that can be heated by penetrating them with a changing magnetic field, such as an alternating magnetic field. The heating material may be an electrically conductive material such that penetration of the heating material with a varying magnetic field causes inductive heating of the heating material. The heating material may be a magnetic material such that penetration of the heating material with a varying magnetic field causes hysteresis heating of the heating material. The heating material may be electrically conductive and magnetic, such that the heating material is heatable by two heating means.

Induction heating is the process of heating an electrically conductive object by penetrating the object with a changing magnetic field. The process is described by Faraday's law of induction and Ohm's law. The induction heater may comprise an electromagnet and means for passing a varying current, such as an alternating current, through the electromagnet. When the electromagnet and the object to be heated are suitably positioned relative to each other such that the resulting varying magnetic field generated by the electromagnet penetrates the object, one or more eddy currents are generated inside the object. The object has a resistance to the flow of current. Thus, when such eddy currents are generated in the object, they cause the object to be heated against the flow of the object's electrical resistance. This process is known as joule, ohmic or resistive heating. An object capable of induction heating is called a susceptor.

In one embodiment, the susceptor is in the form of a closed loop. It has been found that when the susceptor is in the form of a closed loop, the magnetic coupling between the susceptor and the electromagnet is enhanced in use, which results in greater or improved joule heating.

Hysteresis heating is the process of heating an object made of a magnetic material by penetrating the object with a varying magnetic field. Magnetic materials can be considered to include many atomic-scale magnets or magnetic dipoles. When a magnetic field penetrates such a material, the magnetic dipole aligns with the magnetic field. Thus, when a changing magnetic field (such as an alternating magnetic field, e.g. generated by an electromagnet) penetrates a magnetic material, the orientation of these magnetic dipoles changes with the applied changing magnetic field. This magnetic dipole reorientation results in the generation of heat in the magnetic material.

When an object is both electrically conductive and magnetic, penetrating the object with a varying magnetic field can cause both joule heating and hysteresis heating in the object. Furthermore, the use of magnetic materials may enhance the magnetic field, which may enhance joule heating.

In each of the above processes, since heat is generated within the object itself, rather than by an external heat source through heat conduction, rapid temperature rise and more uniform heat distribution in the object can be achieved, particularly by selecting appropriate object materials and geometries, and appropriate varying magnetic field size (magnitude) and orientation relative to the object. Furthermore, since induction heating and hysteresis heating do not require a physical connection to be provided between the source of the varying magnetic field and the object, design freedom and control of the heating profile can be greater and costs can be lower.

Articles, such as those in the shape of rods, are often named according to product length: "regular" (typically in the range of 68-75mm, e.g. from about 68mm to about 72mm), "short" or "mini" (68mm or less), "extra-long dimension" (typically in the range of 75-91mm, e.g. from about 79mm to about 88mm), "long" or "super-long" (typically in the range of 91-105mm, e.g. from about 94mm to about 101mm) and "super-long" (typically in the range of from about 110mm to about 121 mm).

They are also named according to product perimeter: "regular" (about 23-25mm), "wide" (greater than 25mm), "slim" (about 22-23mm), "semi-slim" (about 19-22mm), "ultra-slim" (about 16-19mm), and "microfibrous" (less than about 16 mm).

Thus, for example, an article in the form of an extra long, ultra-thin sheet will have a length of about 83mm and a circumference of about 17 mm.

Each form may be produced with a different length of mouthpiece. The mouthpiece length will be about 30mm to 50 mm. The tipping paper attaches the mouthpiece to the aerosol generating material and will typically have a longer length than the mouthpiece, for example 3mm to 10mm longer, such that the tipping paper covers the mouthpiece and overlaps the aerosol generating material (for example in the form of a rod of substrate material) to attach the mouthpiece to the rod.

The articles described herein and their aerosol generating materials and mouthpieces may be made in, but are not limited to, any of the forms described above.

The terms 'upstream' and 'downstream' as used herein are relative terms defined with respect to the direction of the mainstream aerosol drawn through the article or device in use.

The filamentary tow (filamentary tow) material described herein may comprise cellulose acetate tow. Other materials for forming fibers may also be used to form the filamentary tow, such as polyvinyl alcohol (PVOH), polylactic acid (PLA), Polycaprolactone (PCL), poly (1-4-butanediol succinate) (PBS), poly (butylene adipate-co-terephthalate) (PBAT), starch based materials (starch based materials), cotton, aliphatic polyester materials, and polysaccharide polymers or combinations thereof. The filamentary tow may be plasticized with a plasticizer suitable for the tow, such as triacetin, where the material is cellulose acetate tow, or the tow may be unplasticized. The tow may be of any suitable gauge, such as fibers having a 'Y' shape or other cross-section such as an 'X' shape, with a filament denier value between 2.5 and 15 denier per filament, for example between 8.0 and 11.0 denier per filament, and a total denier value of 5,000 to 50,000, for example between 10,000 to 40,000.

As used herein, the term "tobacco material" refers to any material that includes tobacco or derivatives or substitutes thereof. The term "tobacco material" may include one or more of tobacco, tobacco derivatives, expanded tobacco, reconstituted tobacco or tobacco substitutes. The tobacco material may include one or more of ground tobacco, tobacco fiber, cut tobacco, extruded tobacco, tobacco leaf, tobacco stem, reconstituted tobacco, and/or tobacco extracts. As used herein, "tobacco leaves (leaf tobaccos, leafy tobaccos)" refers to cut lamina tobaccos (cut lamina tobaccos).

As used herein, the terms "flavoring agent" and "flavoring agent" refer to materials that can be used to produce a desired taste or aroma in products for adult consumers, as permitted by local regulations.

As used herein, the terms "flavoring agent" and "flavoring agent" refer to materials that can be used to produce a desired taste or aroma in products for adult consumers, as permitted by local regulations. They may include extracts (e.g. licorice, hydrangea, japanese white bark magnolia leaf, chamomile, fenugreek, clove, menthol, japanese mint, anise, cinnamon, herbs, wintergreen, cherry, berry, peach, apple, scotch whiskey (Drambuie), bourbon, scotch whiskey, spearmint, peppermint, lavender, cardamom, celery, gooseberry, sandalwood, bergamot, geranium, honey essence, rose oil, vanilla, lemon oil, orange oil, cinnamon, caraway, french brandy, jasmine, ylang-ylang, sage, fennel, allspice, ginger, anise, coriander, coffee, or peppermint oil from any species of the genus mentha), flavour enhancers, bitter receptor blockers, sensory receptor activators or stimulators, sugar and/or sugar substitutes (e.g. sucralose and/or sugar substitutes (e.g. peppermint oil, cinnamon, caraway, jasmine, caraway, etc.) Acesulfame potassium, aspartame, saccharin, cyclamate, lactose, sucrose, glucose, fructose, sorbitol, or mannitol) and other additives such as charcoal, chlorophyll, minerals, botanical products, or breath fresheners. They may be imitation, synthetic or natural ingredients or blends thereof. They may be in any suitable form, for example oil, liquid or powder.

Preferably, the aerosol-generating material or substrate 3 is formed from a tobacco material as described herein, which tobacco material includes a tobacco component. The tobacco component comprises tobacco leaf. In some embodiments, the tobacco component comprises a tobacco material selected from the group consisting of extruded tobacco, bandcast tobacco (bandcast tobacaco), and mixtures thereof.

The tobacco leaf that may be used in the tobacco compositions described herein may be any suitable tobacco, such as single or blend, cut rags, or whole leaves, including Virginia (Virginia) (flue-cured and/or air-dried) and/or Burley (Burley) and/or Oriental (Oriental) tobaccos. The tobacco composition may comprise a blend of any of these tobacco leaf materials.

The tobacco leaf is present in an amount between about 10% and about 90% by weight of the tobacco component. In some embodiments, the tobacco leaf can be present in an amount between about 11% and about 48%, about 12% and about 46%, about 13% and about 44%, about 14% and about 42%, about 15% and about 40%, about 16% and about 38%, about 17% and about 36%, about 18% and about 34%, or about 19% and about 32%, by weight of the tobacco component. In preferred embodiments, the tobacco component comprises tobacco leaf in an amount between about 15% and about 25%, about 35% and about 45%, or about 55% and 65%, by weight of the tobacco component. In preferred embodiments, the tobacco component may comprise tobacco leaf in an amount of about 15%, about 16%, about 17%, about 18%, about 19%, about 20%, about 21%, about 22%, about 23%, about 24%, about 25%, about 26%, about 27%, about 28%, about 29%, or about 30% by weight of the tobacco component.

In some embodiments, the tobacco component comprises tobacco leaf in an amount of about 31%, 32%, 33%, 34%, 35%, 36%, 37%, 38%, 39%, 40%, 41%, 42%, 43%, 44%, 45%, 46%, 47%, 48%, 49% or 50%, 51%, 52%, 53%, 54%, 55%, 56%, 57%, 58%, 59%, 60%, 61%, 62%, 63%, 64%, 65%, 66%, 67%, 68%, 69%, or 70%.

In the compositions described herein, where amounts are given in% by weight, for the avoidance of doubt, this is on a dry weight basis unless specifically indicated to the contrary. Thus, any water that may be present in the tobacco composition or any of its components is completely disregarded for the purpose of determining weight percent. The moisture content of the tobacco compositions described herein can vary and can be, for example, from 5 to 15% by weight. The moisture content of the tobacco compositions described herein can vary depending on, for example, the temperature, pressure, and humidity conditions under which the compositions are maintained. The water content can be determined by Karl-Fisher analysis, as described herein.

On the other hand, for the avoidance of doubt, even when the aerosol-forming material is a component in the liquid phase (such as glycerol or propylene glycol), any component other than water is included in the weight of the tobacco composition. However, when the aerosol-forming material is provided in a tobacco component of a tobacco composition, or in a filler component of a tobacco composition (if present), the aerosol-forming material is not included in the weight of the tobacco component or filler component, but is included in the weight of the "aerosol-forming material" as defined herein in weight%, instead of or in addition to being added separately to the tobacco composition. All other ingredients present in the tobacco component are included in the weight of the tobacco component, even if not of tobacco origin (e.g., non-tobacco fibers in the case of paper reconstituted tobacco).

The tobacco component described herein contains nicotine. The nicotine content is from 0.5% to 2% by weight of the tobacco component, and can be, for example, from 0.5% to 1.75% by weight of the tobacco component, from 0.8% to 1.2% by weight of the tobacco component, or from about 0.8% to about 1.75% by weight of the tobacco component. In embodiments, the nicotine content may be from 0.8% to 1.0% by weight of the tobacco component.

According to an embodiment of one aspect of the present disclosure, there is provided a tobacco composition comprising a tobacco component and an aerosol-forming material, wherein the tobacco component comprises tobacco leaf in an amount between about 10% and about 90% by weight of the tobacco component, and wherein the tobacco leaf has a nicotine content of greater than 1.5% by weight of the tobacco leaf.

It may be important to control the nicotine content of the composition. In conventional tobacco heating products, the tobacco composition comprises primarily reconstituted tobacco material. The nicotine content of reconstituted tobacco material is generally relatively low. For example, the reconstituted tobacco material can include nicotine in an amount less than about 1.5% by weight of the reconstituted tobacco material. Increasing the nicotine content of such compositions is challenging.

The inventors have discovered that the nicotine content of a tobacco composition can be carefully controlled by incorporating tobacco leaves into the composition in addition to reconstituted tobacco material. In particular, it was found to be particularly advantageous to incorporate tobacco leaves having a nicotine content of more than 1.5% (by weight of the composition) into the composition. It has been found that incorporation of tobacco leaves having a nicotine content of greater than about 1.5% by weight enhances the organoleptic properties (e.g., taste) of the tobacco composition when heated.

Without wishing to be bound by theory, it is believed that incorporating a tobacco leaf material having a nicotine content of greater than 1.5% by weight of the tobacco leaf material into the composition promotes the release of components from the tobacco composition that have a positive effect on the organoleptic properties of the tobacco composition when the tobacco composition is heated by the aerosol generating device. Advantageously, the amount of nicotine delivered to the user from the tobacco composition comprising tobacco leaf material having a nicotine content of greater than 1.5% by weight of the tobacco leaf material may be similar to the amount of nicotine delivered to the user of a conventional combustible smoking article when the tobacco composition comprising tobacco leaf material is heated in the aerosol generating device. In one embodiment, the tobacco material consists essentially of a tobacco component as defined herein and an aerosol-forming material as defined herein. In one embodiment, the tobacco material is comprised of a tobacco component as defined herein and an aerosol-forming material as defined herein.

The tobacco composition includes a tobacco component and an aerosol-forming material. The tobacco component may comprise tobacco leaf material in an amount between about 10% and about 90% by weight of the tobacco component, and the tobacco leaf material may comprise said aerosol-forming material in an amount up to about 10% by weight of the tobacco leaf material. The tobacco composition may comprise the aerosol-forming material in an amount between about 10% and about 30% by weight of the tobacco composition. Preferably, the tobacco composition comprises the aerosol-forming material in an amount between about 10% and about 20% by weight of the tobacco composition.

It was found that including the aerosol-forming material in an amount between about 10% and about 30% by weight of the tobacco composition, when heated by the aerosol generating device, further enhances the organoleptic properties of the tobacco composition. Advantageously, a loading of aerosol generating material of between about 10% and about 30% by weight of the tobacco composition can cause the sensory properties of the composition to be similar to the sensory properties of conventional combustible smoking articles.

The tobacco composition may include a tobacco component and an aerosol-forming material, wherein the tobacco component includes a tobacco leaf material in an amount between about 10% and about 90% by weight of the tobacco component, and wherein the tobacco component includes menthol in an amount of about 3mg to about 16 mg. Advantageously, loading menthol in an amount of from about 3mg to about 16mg by weight of the tobacco component can improve the organoleptic properties of the tobacco composition when the tobacco composition is heated by the aerosol-generating device.

The tobacco leaf has a nicotine content of greater than 1.5% by weight of the tobacco leaf. In some embodiments, the tobacco leaf has a nicotine content of between 1.5% and about 5% by weight of the tobacco leaf, preferably between about 1.5% and about 4% by weight of the tobacco leaf. The tobacco leaf may have a nicotine content of 1.5%, 1.6%, 1.7%, 1.8%, 1.9%, 2%, 2.1%, 2.2%, 2.3%, 2.4%, 2.5%, 2.6%, 2.7%, 2.8%, 2.9%, 3%, 3.1%, 3.2%, 3.3%, 3.4%, 3.5%, 3.6%, 3.7%, 3.8%, 3.9%, 4%, 4.1%, 4.2%, 4.3%, 4.4%, 4.5%, 4.6%, 4.7%, 4.8%, 4.9% or 5% by weight of the tobacco leaf. In some embodiments, the tobacco leaf has a nicotine content of greater than about 1.5% and up to about 4% by weight of the tobacco leaf material.

The remainder of the tobacco component may include paper reconstituted tobacco, extruded tobacco, bandcast reconstituted tobacco (bandcast reconstituted tobaccos), or a combination of bandcast reconstituted tobacco and another form of tobacco, such as tobacco particles. Preferably, the tobacco component comprises a paper-process reconstituted tobacco material.

Papermaking reconstituted tobacco refers to tobacco material formed by a process in which tobacco raw material is extracted with a solvent to provide an extract of soluble matter and a residue comprising fibrous material, and then the extract is recombined (typically after concentration, and optionally after further processing) with fibrous material from the residue (typically after refining of the fibrous material, and optionally adding a portion of non-tobacco fibers) by depositing the extract onto the fibrous material. The recombination process is similar to the papermaking process.

The paper-process reconstituted tobacco can be any type of paper-process reconstituted tobacco known in the art. In a particular embodiment, the papermaking reconstituted tobacco is made from a raw material comprising one or more of tobacco rod, tobacco stalk, and whole leaf tobacco. In a further embodiment, the paper-process reconstituted tobacco is made from a raw material consisting of tobacco rod and/or whole leaf tobacco and tobacco stems. However, in other embodiments, crumb, fines and winnings (winnowing) may alternatively or additionally be used in the feedstock.

The papermaking reconstituted tobacco for use in the tobacco materials described herein can be prepared by methods known to those skilled in the art for preparing papermaking reconstituted tobacco.

Referring to fig. 1, a tobacco ingredient (tobacco feed), such as leaves, strands, stems, scraps, fines, and/or winnings (in some embodiments, leaves, strands, and stems), is first mixed with an aqueous solvent (e.g., water, and a water-miscible solvent such as ethanol). Distilled, deionized or tap water may be used. The suspension of tobacco in the solvent is agitated by stirring or shaking, for example, to increase the rate of extraction of the soluble fraction from the tobacco fibre fraction. Stirring is usually carried out for half an hour to 6 hours. Agitation may be achieved in an agitator comprising a vessel and a blade to achieve agitation. The amount of solvent in the suspension may vary widely from about 75 to 99% by weight of the suspension, depending on the tobacco ingredients, the type of solvent and the stirring equipment (particularly the type of blades), and the temperature of the suspension. The suspension temperature typically ranges from about 10 ℃ to about 100 ℃.

The soluble portion of the tobacco furnish is separated from the insoluble fibrous portion of the tobacco, for example by pressing with a pneumatic, hydraulic or mechanical press or by filtration. After separation, the fibrous portion of the tobacco is typically subjected to mechanical refining (refining) to produce a fibrous pulp. Suitable refiners may typically be disc refiners or conical refiners. The fibrous pulp is then formed into a base web comprising tobacco fibre pulp on a paper making station, such as a Fourdrinier-type paper machine. It is usually laid onto a flat ribbon where excess water is removed by gravity drainage and suction drainage. At this stage, non-tobacco fibers (such as cellulose, wheat fiber, or wood fiber) may be included with the tobacco-derived fiber portion. The soluble portion of the tobacco material is concentrated using any known type of concentrator, such as a thin film evaporator or a vacuum evaporator. After concentration, ingredients such as aerosol-forming materials (as defined herein), shells (e.g. cocoa, licorice) and acids such as malic acid or flavourants (as defined herein) may be added and mixed with the concentrated tobacco solubles. The concentrated tobacco solubles, potentially containing aerosol-forming material and/or shell and/or flavourant, are then recombined with the dried tobacco fibre sheet to form reconstituted tobacco. The concentrated solubles can be added back to the web by various methods such as spraying, coating, saturating, sizing.

Finally, the reconstituted tobacco is dried. It may optionally be cut into strips or wound into rolls and then cut into shafts (bobbin) or chopped into cut chips. As used herein, the terms "flavoring agent" and "flavoring agent" refer to materials that can be used to produce a desired taste or aroma in products for adult consumers, as permitted by local regulations. They may include extracts (e.g. licorice, hydrangea, japanese white bark magnolia leaf, chamomile, fenugreek, clove, menthol, japanese mint, anise, cinnamon, herbs, wintergreen, cherry, berry, peach, apple, scotch whiskey (Drambuie), bourbon, scotch whiskey, spearmint, peppermint, lavender, cardamom, celery, gooseberry, sandalwood, bergamot, geranium, honey essence, rose oil, vanilla, lemon oil, orange oil, cinnamon, caraway, french brandy, jasmine, ylang-ylang, sage, fennel, allspice, ginger, anise, coriander, coffee, or peppermint oil from any species of the genus mentha), flavour enhancers, bitter receptor blockers, sensory receptor activators or stimulators, sugar and/or sugar substitutes (e.g. sucralose and/or sugar substitutes (e.g. peppermint oil, cinnamon, caraway, jasmine, caraway, etc.) Acesulfame potassium, aspartame, saccharin, cyclamate, lactose, sucrose, glucose, fructose, sorbitol, or mannitol) and other additives such as charcoal, chlorophyll, minerals, botanical products, or breath fresheners. They may be imitation, synthetic or natural ingredients or blends thereof. They may be in any suitable form, for example oil, liquid or powder. Examples of paper-making reconstituted tobaccos that can be used in the present invention are provided in the examples.

The tobacco component may comprise a blend of tobacco leaf and paper-process reconstituted tobacco material. The paper-process reconstituted tobacco material can have a nicotine content of less than one equivalent of the nicotine content of tobacco leaf. For example, the reconstituted tobacco material can have a nicotine content of less than 1.5% by weight of the reconstituted tobacco material.

It has advantageously been found that the use of tobacco leaves having a nicotine content of greater than 1.5% in combination with a lower nicotine base material, such as a paper process reconstituted tobacco, provides a tobacco material having a suitable nicotine level but better organoleptic properties than paper process reconstituted tobacco alone. The tobacco component can include a paper-process reconstituted tobacco in an amount from about 10% to about 90% by weight of the tobacco component. In embodiments, the papermaking reconstituted tobacco is present in an amount of 10% to 80% by weight of the tobacco component or 20% to 70% by weight of the tobacco component. In some embodiments, the tobacco component includes a papermaker's reconstituted tobacco material in an amount between about 50% and about 90% of the tobacco component. In some embodiments, the reconstituted tobacco may be present in an amount between about 10% and about 89%, about 20% and about 88%, about 30% and about 87%, about 40% and about 86%, about 50% and about 85%, about 60% and about 84%, about 70% and about 83% by weight of the tobacco component. In some embodiments, the tobacco component can include reconstituted tobacco in an amount between about 75% and about 85% by weight of the tobacco component.

In preferred embodiments, the tobacco component can include reconstituted tobacco in an amount of about 70%, about 71%, about 72%, about 73%, about 74%, about 75%, about 76%, about 77%, about 78%, about 79%, about 80%, about 81%, about 82%, about 83%, about 84%, or about 85% by weight of the tobacco component.

In one embodiment, the tobacco leaf is present in an amount of at least 10% by weight of the tobacco component, with the remainder of the tobacco component comprising a combination of a paper-making reconstituted tobacco, a belt cast reconstituted tobacco, or a belt cast reconstituted tobacco and another form of tobacco, such as tobacco particles.

The reconstituted tobacco material can have a density of less than about 700 milligrams per cubic centimeter (mg/cc).

Such tobacco materials have been found to be particularly effective in providing aerosol generating materials that can be heated rapidly to release an aerosol, as compared to more dense materials. For example, the inventors tested the properties of various aerosol generating materials (such as tape cast reconstituted tobacco material and paper-process reconstituted tobacco material) upon heating. It was found that for each given aerosol generating material there is a specific zero heat flow temperature below which the net heat flow is endothermic, in other words more heat enters the material than leaves the material, and above which the net heat flow is exothermic, in other words more heat leaves the material than enters the material while heat is applied to the material. Materials with densities less than 700mg/cc have lower zero heat flux temperatures. Since the majority of the heat flow out of the material is through the formation of the aerosol, having a lower zero heat flow temperature has a beneficial effect on the time taken to initially release the aerosol from the aerosol generating material. For example, an aerosol generating material having a density of less than 700mg/cc has been found to have a zero heat flux temperature of less than 164 ℃ compared to a material having a density of more than 700mg/cc and a zero heat flux temperature of greater than 164 ℃.

The density of the aerosol generating material also has an effect on the rate of heat conduction through materials having lower densities (e.g. those below 700 mg/cc), conducting heat more slowly through the material, thus enabling a more sustained release of the aerosol.

The weight ratio of tobacco leaves to the paper-making reconstituted tobacco material may be 10:90, 11:89, 12:88, 13:87, 14:86, 15:85, 16:84, 17:83, 18:82, 19:81, 20:80, 21:79, 22:78, 23:77, 24:76, 25:75, 26:74, 27:73, 28:72, 29:71, 30:70, 31:69, 32:68, 33:67, 34:66, 35:65, 36:64, 37:63, 38:62, 39:61, 40:60, 41:59, 42:58, 43:57, 44:56, 45:55, 46:54, 47:53, 48:52, 49:51, 50:50, 51:49, 52:48, 53:47, 54:46, 55:45, 56:44, 57:43, 58:42, 59:41, 60:40, 63: 62, 39: 38: 64, 35: 36:64, 33: 32: 36:64, 33: 61, 40: 60: 46: 45, 44: 43: 42, 58: 41: 61, 60: 40: 64, 38: 64, 35: 64, 36:64, 33: 64, 36: 64: 36: 60: 45: 60: 45, 36: 45: 44, 36: 60: 45, 35: 44, 35: 36: 60: 36: 60: 45, 35: 60: 45, 35: 36: 60: 36: 60, 35: 60: 36, 35: 36: 60: 45, 35: 60: 36, 35: 60: 45, 35: 36: 60: 45, 35: 36, 35: 36: 45, 35: 36, 35: 45, 35: 36, 35: 45, 35: 36, 35: 60, 35: 36: 45, 35: 36, 35: 45, 35: 36, 35: 45, 35: 36, 35: 60, 35: 36, 35: 45, 35: 36, 35: 60, 35: 45, 35:6, 35: 36, 35: 60, 35: 36, 35: 45, 35: 36, 69:31, 70:30, 71:29, 72:28, 73:27, 74:26, 75:25, 76:24, 77:23, 78:22, 79:21, 80:20, 81:19, 82:18, 83:17, 84:16, 85:15, 86:14, 87:13, 88:12, 89:11 or 90:10 (weight of tobacco leaf: weight of paper-making reconstituted tobacco).

Preferably, the aerosol generating material 3 comprises a reconstituted tobacco material, such as a paper-making reconstituted tobacco material, having a density of less than about 700 mg/cc. More preferably, the aerosol generating material 3 comprises reconstituted tobacco material having a density of less than about 600 mg/cc. Alternatively or additionally, the aerosol-generating material 3 preferably comprises reconstituted tobacco material having a density of at least 350mg/cc, which is believed to allow a sufficient amount of heat conduction through the material.

The tobacco composition includes an aerosol-forming material. As used herein, an "aerosol-forming material" is an agent that facilitates aerosol generation. The aerosol-forming material may facilitate aerosol generation by promoting initial vaporization and/or condensation of the gas into an inhalable solid and/or liquid aerosol. In some embodiments, the aerosol-forming material may improve the delivery of flavourant from the aerosol-generating material.

In general, any suitable aerosol-forming material or agent may be included in the aerosol-generating material of the invention. Suitable aerosol-forming materials include, but are not limited to: polyols such as sorbitol, glycerol and glycols such as propylene glycol or triethylene glycol; non-polyhydric alcohols such as monohydric alcohols, high boiling hydrocarbons, acids such as lactic acid, glycerol derivatives, esters such as diacetin, triacetin, triethylene glycol diacetate, triethyl citrate or myristate (including ethyl myristate and isopropyl myristate), and aliphatic carboxylic acid esters such as methyl stearate, dimethyl dodecanedioate and dimethyl tetradecanedioate.

In a preferred embodiment, the aerosol-forming material is selected from the group consisting of: glycerin, sorbitol, propylene glycol, triethylene glycol, lactic acid, diacetin, triacetin, triethylene glycol diacetate, triethyl citrate, ethyl myristate, isopropyl myristate, methyl stearate, dimethyl dodecanedioate, dimethyl tetradecanedioate, and mixtures thereof.

It has been found that aerosol-forming materials improve the sensory properties of articles comprising tobacco compositions for use with aerosol-generating devices by helping to transfer compounds (such as flavour compounds) from the tobacco material to the consumer.

The aerosol-forming material may be included in any component of the tobacco composition. Alternatively or additionally, the aerosol-forming material may be added separately to the tobacco composition. In either case, the total amount of aerosol-forming material in the tobacco material should be as defined herein.

The tobacco leaf material may comprise the aerosol-forming material in an amount up to about 10% by weight of the tobacco leaf material. In other embodiments, the tobacco leaf may comprise the aerosol-forming material in an amount up to about 20% or between about 15% and about 20% by weight of the tobacco leaf. The tobacco leaf may comprise the aerosol-forming material in an amount of about 5%, about 10% or about 15% by weight of the tobacco leaf.

In order to achieve a total level of aerosol-forming material of between 10% and 20% by weight of the tobacco material, it has advantageously been found that it can be added to another component of the tobacco material, such as reconstituted tobacco material, in higher weight percentages.

According to an embodiment of one aspect of the present disclosure, there is provided a tobacco composition comprising a tobacco component and an aerosol-forming material, wherein the tobacco component comprises a tobacco leaf material in an amount of between about 10% and about 90% by weight of the tobacco component, and wherein the tobacco leaf material comprises the aerosol-forming material in an amount of up to about 10% by weight of the tobacco leaf material, and wherein the tobacco composition comprises the aerosol-forming material in an amount of between about 10% and about 30% by weight of the tobacco composition. Preferably, the tobacco composition comprises the aerosol-forming material in an amount between about 10% and about 20% by weight of the tobacco composition.

In some embodiments, the aerosol-forming material may be glycerol, propylene glycol or a mixture of glycerol and propylene glycol. Preferably, the aerosol-forming material comprises glycerol. The glycerin may be present in an amount of 10% to 20% by weight of the tobacco material, for example 13% to 16% by weight of the composition, or about 14% or 15% by weight of the composition. Propylene glycol (if present) may be present in an amount of 0.1 to 0.3% by weight of the composition.

The aerosol-forming material may be included in a component of the tobacco composition. For example, the aerosol-forming material may be included in the reconstituted tobacco and/or filler component (if present).

Alternatively or additionally, the aerosol-forming material may be applied separately to the tobacco material. In either case, the total amount of aerosol-forming material in the tobacco material should be as defined herein.

The papermaking reconstituted tobacco material can include an aerosol-forming material. The papermaking reconstituted tobacco material can include an aerosol-forming material in an amount between about 10% and about 20% by weight of the reconstituted tobacco material. In some embodiments, the papermaking reconstituted tobacco material may include an aerosol-forming material in an amount of about 10%, about 11%, about 12%, about 13%, about 14%, about 15%, about 16%, about 17%, about 18%, about 19%, or about 20% by weight of the reconstituted tobacco material.

The tobacco material described herein can include an aerosol modifier, such as any of the flavorants described herein. In one embodiment, the tobacco material comprises menthol, forming a menthol-alcoholized article. The tobacco material may comprise 3mg to 20mg of menthol, preferably between 5mg and 18mg and more preferably between 8mg and 16mg of menthol. In this example, the tobacco material contained 16mg of menthol. The tobacco material may comprise between 2% and 8% by weight menthol, preferably between 3% and 7% by weight menthol and more preferably between 4% and 5.5% by weight menthol. In one embodiment, the tobacco material comprises 4.7% by weight menthol. Such high levels of menthol loading can be achieved using a high percentage of reconstituted tobacco material, for example greater than 50% by weight of tobacco material. Alternatively or additionally, the use of a high volume of aerosol generating material (e.g. tobacco material) may increase the level of menthol loading that can be achieved, for example where an aerosol generating material (such as tobacco material) of greater than about 500mm3 or suitably greater than about 1000mm3 is used.

The tobacco material may be provided in the form of cut shredded tobacco (rag tobaco). The cut shredded tobacco may have a cut width of at least 15 cuts per inch (about 5.9 cuts/cm, corresponding to a cut width of about 1.7 mm). Preferably, the cut shredded tobacco has a cut width of at least 18 cuts per inch (about 7.1 cuts per cm, corresponding to a cut width of about 1.4 mm), more preferably at least 20 cuts per inch (about 7.9 cuts per cm, corresponding to a cut width of about 1.27 mm). In one example, the cut shredded tobacco has a cut width of 22 cuts per inch (about 8.7 cuts/cm, corresponding to a cut width of about 1.15 mm). Preferably, the cut shredded tobacco has a cut width of 40 cuts or less than 40 cuts per inch (about 15.7 cuts/cm, corresponding to a cut width of about 0.64 mm). It was found that a cut width of between 0.5mm and 2.0mm, for example between 0.6mm and 1.5mm or between 0.6mm and 1.7mm, results in a tobacco material which is preferred in terms of surface area to volume ratio, in particular when heated, as well as overall density and pressure drop of the substrate 3. The cut shredded tobacco may be formed from a blend in the form of a tobacco material, such as a blend of tobacco leaf and one or more of paper-process reconstituted tobacco, extruded tobacco, and belt cast tobacco. Preferably, the tobacco material comprises paper-process reconstituted tobacco.

The tobacco leaf and/or papermaker's reconstituted tobacco material may include a width of between about 0.5mm and about 2mm, between about 0.6mm and about 1.75mm, between about 0.6mm and about 1.7mm, or between about 0.7 and about 1.5 mm.

In the tobacco compositions described herein, the tobacco composition can include a filler component. The filler component is typically a non-tobacco component, i.e., a component that does not contain tobacco-derived ingredients. The filler component may be a non-tobacco fibre such as wood fibre or pulp or wheat fibre. The filler component may also be an inorganic material such as chalk, perlite, vermiculite, diatomaceous earth, colloidal silica, magnesium oxide, magnesium sulphate, magnesium carbonate. The filler component may also be a non-tobacco cast material or a non-tobacco extruded material.

The filler component may be present in an amount of 0 to 20% by weight of the tobacco material, or in an amount of 1 to 10% by weight of the composition. In a preferred embodiment, the tobacco composition comprises between about 5% and about 10% by weight of the tobacco composition. In some embodiments, no filler component is present.

Extruded tobacco can optionally be included in the tobacco compositions described herein. If extruded tobacco is included, it may be present in an amount of, for example, 10 to 30% or 10 to 20% by weight of the tobacco component. Extruded tobacco that can be used in the tobacco compositions described herein can be prepared by methods known to those skilled in the art for preparing extruded tobacco. In some embodiments, the extruded tobacco can be prepared as follows. The tobacco ingredients may include virginia tobacco (flue-cured), burley tobacco and/or oriental tobacco. The tobacco material may be stems, scraps, strips, fines or winnings. Additional components may include non-tobacco fibers, such as straw fibers or wheat fibers; binders, for example cellulose or modified celluloses, such as hydroxypropyl cellulose and carboxymethyl cellulose; and a shell, for example an acid such as malic acid.

As shown in fig. 2, the tobacco ingredients and any additional components are mixed in a mixing silo (mixing silo) and conveyed by a metering screw (feeding screw) and a conveying screw to an extruder where they are mixed with water, at which stage the aerosol-forming material may also be added. After extrusion, the extruded tobacco is cooled on a cooling belt.

Materials similar to those described above in this section, but made using only non-tobacco fibers (such as wheat fibers or wood fibers) can be used in the filler component of the tobacco composition.

According to some embodiments of an aspect of the present disclosure, there is provided a method of making a tobacco composition described herein, wherein the method comprises applying an aerosol-forming material described herein to a tobacco leaf material.

The method can include combining a tobacco leaf material with a papermaking process reconstituted tobacco material, the papermaking process reconstituted tobacco material including an aerosol-forming material in an amount between 10% and 20% by weight of the papermaking process reconstituted tobacco material.

As shown in fig. 3, the tobacco composition may be manufactured by a process that includes applying an aerosol-forming material to tobacco leaves, and then combining the tobacco leaves including the aerosol-forming material with reconstituted tobacco material.

For example, the aerosol-forming material may be applied to the tobacco leaf by spraying it onto the tobacco leaf or by dipping the tobacco leaf in the aerosol-forming material. Alternatively or additionally, the tobacco composition may be manufactured by applying an aerosol-forming material to a reconstituted tobacco material.

According to an embodiment of one aspect of the present disclosure, there is provided a tobacco composition made by the method described herein.

According to an embodiment of one aspect of the present disclosure, the tobacco composition described herein is used in an article of manufacture for use with an aerosol-generating device. The tobacco composition may be used in a process for making an article for use with an aerosol generating device.

According to an embodiment of one aspect of the present disclosure, there is provided an article for use with an aerosol-generating device, the article comprising a tobacco composition as described herein. An article for use with an aerosol-generating device comprises a rod of a tobacco composition. The rod may have a total weight of between about 250mg and about 350 mg.

In one embodiment, the tobacco composition may be wrapped in a wrapper (wrapper) having a permeability (permeability) of less than 100Coresta units.

Articles for use with aerosol-generating devices may include reconstituted tobacco material having a density of less than about 700 mg/cc.

An article for use with an aerosol-generating device may have an outer circumference of at least about 19mm, preferably between about 19mm and about 23mm, or about 21 mm. This may facilitate insertion of an article for use with the aerosol-generating device into the aerosol-generating device.

According to an embodiment of one aspect of the present disclosure, there is provided a system comprising a tobacco composition as described herein and a device arranged to heat the tobacco composition and generate an aerosol from the tobacco composition.

In some embodiments, the system comprises an article for use with an aerosol-generating device described herein, the aerosol-generating device being arranged for receiving at least a portion of the article for use with the aerosol-generating device comprising the tobacco composition and heating the portion of the article for use with the aerosol-generating device comprising the tobacco composition and generating an aerosol from the tobacco composition.

Fig. 4 is a side cross-sectional view of an article 1 for use with a non-combustible aerosol provision device.

The article 1 comprises a mouthpiece 2 and a cylindrical rod of aerosol generating material 3 (in this case tobacco material) connected to the mouthpiece 2. The aerosol-generating material 3 (also referred to herein as an aerosol-generating substrate 3) comprises at least one aerosol-forming material. In this example, the aerosol-forming material is glycerol. In alternative examples, the aerosol-forming material may be another material as described herein or a combination thereof. It has been found that aerosol-forming materials improve the organoleptic properties of the article by helping to transfer compounds (such as flavour compounds) from the aerosol-generating material to the consumer. However, a problem with adding such aerosol-forming materials to aerosol-generating materials within articles for use in non-combustible aerosol provision systems may be that the aerosol-forming material may increase the quality of the aerosol delivered by the article when it is aerosolized under heating, and that such increased quality may be maintained at a higher temperature as it passes through the mouthpiece. As the aerosol passes through the mouthpiece, the aerosol transfers heat into the mouthpiece, which warms the outer surface of the mouthpiece, including the areas that come into contact with the lips of the consumer during use. The mouthpiece temperature may be significantly higher than that which a consumer may be accustomed to when smoking a cigarette (e.g. a conventional cigarette), and this may be an undesirable effect caused by the use of such aerosol-forming materials.

The portion of the mouthpiece that contacts the lips of the consumer is typically a paper tube that is hollow or cylindrical around the filter material.

As shown in figure 4, the mouthpiece 2 of the article 1 comprises an upstream end 2a adjacent the aerosol generating substrate 3 and a downstream end 2b remote from the aerosol generating substrate 3. At the downstream end 2b, the mouthpiece 2 has a hollow tubular element 4 formed from a filamentary tow. It has advantageously been found that this significantly reduces the temperature of the outer surface of the mouthpiece 2 at the downstream end 2b of the mouthpiece, which downstream end is in contact with the mouth of the consumer when the article 1 is in use. Furthermore, it has been found that the use of the tubular element 4 significantly reduces the temperature of the outer surface of the mouthpiece 2, even upstream of the tubular element 4. Without wishing to be bound by theory, it is hypothesized that this is due to the tubular element 4 guiding the aerosol closer to the centre of the mouthpiece 2 and thus reducing the heat transfer from the aerosol to the outer surface of the mouthpiece 2.

In this example, the article 1 has an outer perimeter of about 21mm (i.e., the article is in a semi-slim form). In other examples, the article may be provided in any form described herein, for example having an outer perimeter between 15mm and 25 mm. Because the article is to be heated to release the aerosol, improved heating efficiency may be achieved using articles having a smaller outer perimeter in this range (e.g., a perimeter of less than 23 mm). In order to achieve improved aerosol by heating while maintaining a suitable product length, article perimeters of greater than 19mm have also been found to be particularly effective. It was found that articles having a circumference between 19mm and 23mm, and more preferably between 20mm and 22mm, provide a good balance between providing effective aerosol delivery while allowing effective heating.

The outer circumference of the mouthpiece 2 is substantially the same as the outer circumference of the rod of aerosol-generating material 3 so that there is a smooth transition between these components. In this example, the outer circumference of the mouthpiece 2 is about 20.8 mm. The tipping wrapper 5 is wrapped around the entire length of the mouthpiece 2 and over a portion of the rod of aerosol generating material 3 and has adhesive on its inner surface to join the mouthpiece 2 and the rod 3. In the present example, the tipping paper 5 extends 5mm over the rod of aerosol generating material 3, but it may alternatively extend between 3mm and 10mm, or more preferably between 4mm and 6mm, over the rod 3 in order to provide a secure attachment between the mouthpiece 2 and the rod 3. The tipping paper 5 may have a basis weight higher than the basis weight of the plug wrap (plug wrap) used in the article 1, for example a basis weight of 40gsm to 80gsm, more preferably between 50gsm and 70gsm, and in this example 58 gsm. These basis weight ranges were found to result in a tipping paper having acceptable tensile strength while being sufficiently flexible to wrap around the article 1 and adhere to itself along the longitudinal lap seam on the paper. Once wrapped around the mouthpiece 2, the outer circumference of the tipping paper 5 is about 21 mm.

The "wall thickness" of the hollow tubular element 4 corresponds to the thickness of the wall of the tube 4 in the radial direction. This can be measured, for example, using a caliper. The wall thickness is advantageously greater than 0.9mm, and more preferably 1.0mm or greater. Preferably, the wall thickness is substantially constant around the entire wall of the hollow tubular element 4. However, in case the wall thickness is not substantially constant, the wall thickness is preferably larger than 0.9mm, more preferably 1.0mm or more at any point around the hollow tubular element 4.

Preferably, the hollow tubular element 4 has a length of less than about 20 mm. More preferably, the hollow tubular element 4 has a length of less than about 15 mm. Still more preferably, the hollow tubular element 4 has a length of less than about 10 mm. Additionally or alternatively, the length of the hollow tubular element 4 is at least about 5 mm. Preferably, the length of the hollow tubular element 4 is at least about 6 mm. In some preferred embodiments, the length of hollow tubular element 4 is from about 5mm to about 20mm, more preferably from about 6mm to about 10mm, even more preferably from about 6mm to about 8mm, most preferably about 6mm, 7mm or about 8 mm. In the present example, the length of the hollow tubular element 4 is 6 mm.

Preferably, the hollow tubular member 4 has a density of at least about 0.25 grams per cubic centimeter (g/cc), more preferably at least about 0.3 g/cc. Preferably, the hollow tubular member 4 has a density of less than about 0.75 grams per cubic centimeter (g/cc), more preferably less than 0.6 g/cc. In some embodiments, the hollow tubular element 4 has a density of between 0.25 and 0.75g/cc, more preferably between 0.3 and 0.6g/cc, and more preferably between 0.4g/cc and 0.6g/cc or about 0.5 g/cc. These densities were found to provide a good balance between the improved hardness provided by the denser material and the lower heat transfer properties of the less dense material. For the purposes of the present invention, the "density" of the hollow tubular element 4 refers to the density of the filamentary tow forming the element in combination with any plasticizer. The density may be determined by dividing the total weight of the hollow tubular element 4 by the total volume of the hollow tubular element 4, wherein the total volume may be calculated using a suitable measurement of the hollow tubular element 4, for example using a caliper. If necessary, the appropriate size can be measured using a microscope.

The filamentous tow forming hollow tubular element 4 preferably has a total denier of less than 45,000, more preferably less than 42,000. This total denier has been found to allow the formation of less dense tubular elements 4. Preferably, the total denier is at least 20,000, more preferably at least 25,000. In a preferred embodiment, the filamentous tow forming hollow tubular element 4 has a total denier of between 25,000 and 45,000, more preferably between 35,000 and 45,000. Preferably, the cross-sectional shape of the filaments in the tow is 'Y' -shaped, although in other embodiments, other shapes, such as 'X' -shaped filaments, may be used.

The filamentary tow forming hollow tubular element 4 preferably has a denier per filament (denier per filament) greater than 3. It was found that such a monofilament denier allows the formation of a less dense tubular element 4. Preferably, the filament denier is at least 4, more preferably at least 5. In a preferred embodiment, the filamentary tow forming the hollow tubular element 4 has a denier per filament between 4 and 10, more preferably between 4 and 9. In one example, the filamentary tow forming hollow tubular member 4 has an 8Y40,000 tow formed of cellulose acetate and containing 18% plasticizer (e.g., triacetin).

The hollow tubular element 4 preferably has an inner diameter greater than 3.0 mm. A smaller diameter than this may result in the velocity of the aerosol through the mouthpiece 2 to the consumer's mouth increasing more than desired so that the aerosol becomes too hot, for example reaching a temperature of greater than 40 ℃ or greater than 45 ℃. More preferably, the hollow tubular element 4 has an internal diameter greater than 3.1mm, still more preferably greater than 3.5mm or 3.6 mm. In one embodiment, the inner diameter of the hollow tubular element 4 is about 3.9 mm.

The hollow tubular element 4 preferably comprises from 15 to 22% by weight of a plasticizer. For cellulose acetate tow, the plasticizer is preferably triacetin, although other plasticizers such as polyethylene glycol (PEG) may be used. More preferably, the tubular element 4 comprises 16% to 20% by weight of plasticizer, for example about 17%, about 18% or about 19% of plasticizer.

The pressure drop or pressure differential (also referred to as the resistance to draw) across (across, through) the mouthpiece (e.g. the portion of the article 1 downstream of the aerosol-generating material 3) is preferably less than about 40mmH₂And O. It has been found that this pressure drop allows sufficient aerosol (including the desired compound such as a flavour compound) to pass through the mouthpiece 2 to the consumer. More preferably, the pressure drop across the mouthpiece 2 is less than about 32mmH₂And O. In some embodiments, the use has less than 31mmH₂O (e.g. about 29 mmH)₂O, about 28mmH₂O or about 27.5mmH₂O) achieves a particularly improved aerosol. Alternatively or additionally, the mouthpiece pressure drop may be at least 10mmH₂O, preferably at least 15mmH₂O, and more preferably at least 20mmH₂And O. In some embodiments, the mouthpiece pressure drop may be at about 15mmH₂O and 40mmH₂And O is between. These values enable the mouthpiece 2 to slow the aerosol as it passes through the mouthpiece 2 so that the temperature of the aerosol has time to decrease before reaching the downstream end 2b of the mouthpiece 2.

In this example, the mouthpiece 2 comprises a body of material 6 upstream of the hollow tubular element 4, in this example adjacent to and in abutting relationship with the hollow tubular element 4. The body of material 6 and the hollow tubular element 4 each define a substantially cylindrical overall profile and share a common longitudinal axis. The material body 6 is wrapped in a first plug wrap 7. Preferably, the first plug wrap 7 has a basis weight of less than 50gsm, more preferably between about 20gsm and 40 gsm. Preferably, the first plug wrap 7 has a thickness of between 30 μm and 60 μm, more preferably between 35 μm and 45 μm. Preferably, the first plug wrap 7 is a non-porous plug wrap, e.g. having a permeability of less than 100Coresta units, e.g. less than 50 Coresta units. However, in other embodiments, the first plug wrap 7 may be a porous plug wrap, for example, having a permeability greater than 200 Coresta units.

Preferably, the length of the body of material 6 is less than about 15 mm. More preferably, the length of the body of material 6 is less than about 10 mm. Additionally or alternatively, the length of the body of material 6 is at least about 5 mm.

Preferably, the length of the body of material 6 is at least about 6 mm. In some preferred embodiments, the length of the body of material 6 is about 5mm to about 15mm, more preferably about 6mm to about 12mm, even more preferably about 6mm to about 12mm, most preferably about 6mm, 7mm, 8mm, 9mm or 10 mm. In this example, the length of the material body 6 is 10 mm.

In the present example, the body of material 6 is formed from filamentary tows. In the present example, the tow used in the material body 6 has a denier per filament (d.p.f.) of 8.4 and a total denier of 21,000. Alternatively, the tow may, for example, have a denier per filament (d.p.f.) of 9.5 and a total denier of 12,000. In this example, the tow comprises plasticized cellulose acetate tow. The plasticizer used in the tow comprises about 7% by weight of the tow. In this example, the plasticizer is triacetin. In other examples, different materials may be used to form the material body 6. For example, instead of tow, the body 6 may be formed from paper, for example in a similar manner to paper filters known for use in cigarettes.

Alternatively, the body 6 may be formed from a tow other than cellulose acetate (e.g., polylactic acid (PLA)), other materials described herein for filamentary tows, or the like. The tow is preferably formed of cellulose acetate. The tow, whether formed of cellulose acetate or other material, preferably has a d.p.f. of at least 5, more preferably at least 6, still more preferably at least 7. These filament denier values provide a tow having relatively coarse, thick fibers with a lower surface area, which results in a lower pressure drop across the mouthpiece 2 compared to a tow having a lower d.p.f. value. Preferably, in order to obtain a sufficiently homogeneous material body 6, the tow has a denier per filament of not more than 12d.p.f., preferably not more than 11d.p.f., and still more preferably not more than 10d.p.f.

The total denier of the tow forming the body of material 6 is preferably at most 30,000, more preferably at most 28,000, still more preferably at most 25,000. These total denier values provide a tow that occupies a reduced proportion of the cross-sectional area of the mouthpiece 2, which results in a lower pressure drop across the mouthpiece 2 than a tow having a higher total denier value. For a suitable solidity of the material body 6, the tow preferably has a total denier of at least 8,000, more preferably at least 10,000. Preferably, the filament denier is between 5 and 12 and the total denier is between 10,000 and 25,000. More preferably, the denier per filament is between 6 and 10 and the total denier is between 11,000 and 22,000. Preferably, the cross-sectional shape of the filaments of the tow is 'Y' -shaped, but in other embodiments, other shapes having the same d.p.f. and total denier values provided herein, such as 'X' -shaped filaments, may be used.

In the present example, the hollow tubular element 4 is a first hollow tubular element 4, and the mouthpiece comprises a second hollow tubular element 8, also referred to as a cooling element, located upstream of the first hollow tubular element 4. In this example, the second hollow tubular element 8 is located upstream of the material body 6, adjacent to the material body 6 and in abutting relationship with the material body 6. The body of material 6 and the second hollow tubular element 8 each define a substantially cylindrical overall profile and share a common longitudinal axis. The second hollow tubular element 8 is formed from a plurality of layers of paper wound in parallel with a butt seam to form the tubular element 8. In this example, the first and second paper layers are provided in a two-layer tube, but in other examples, 3, 4, or more paper layers may be used to form a 3, 4, or more layer tube. Other configurations may be used, such as a layer of paper that is spirally wound, a paperboard tube, a tube formed using a tissue-type process, a molded or extruded plastic tube, or the like. The second hollow tubular element 8 may also be formed using a rigid plug wrap and/or tipping paper as the second plug wrap 9 and/or tipping paper 5 described herein, which means that a separate tubular element is not required. The rigid plug wrap and/or tipping paper is manufactured to have sufficient rigidity to withstand axial compression and bending moments that may occur during manufacture and when the article 1 is in use. For example, the rigid plug wrap and/or tipping paper may have a basis weight of between 70gsm and 120gsm, more preferably between 80gsm and 110 gsm. Additionally or alternatively, the rigid plug wrap and/or tipping paper may have a thickness of between 80 μm and 200 μm, more preferably between 100 μm and 160 μm, or from 120 μm to 150 μm. It may be desirable that both the second plug wrap 9 and the tipping paper 5 have values within these ranges in order to achieve an acceptable level of overall rigidity of the second hollow tubular element 8.

The second hollow tubular element 8 preferably has a wall thickness of at least about 100 μm and up to about 1.5mm, preferably between 100 μm and 1mm and more preferably between 150 μm and 500 μm, or about 300 μm, which can be measured in the same way as the first hollow tubular element 4. In the present example, the second hollow tubular element 8 has a wall thickness of about 290 μm.

Preferably, the length of the second hollow tubular element 8 is less than about 50 mm. More preferably, the length of the second hollow tubular element 8 is less than about 40 mm. Still more preferably, the length of the second hollow tubular element 8 is less than about 30 mm. In addition or as an alternative, the length of the second hollow tubular element 8 is preferably at least about 10 mm. Preferably, the length of the second hollow tubular element 8 is at least about 15 mm. In some preferred embodiments, the length of the second hollow tubular element 8 is from about 20mm to about 30mm, more preferably from about 22mm to about 28mm, even more preferably from about 24mm to about 26mm, most preferably about 25 mm. In the present example, the length of the second hollow tubular element 8 is 25 mm.

A second hollow tubular element 8 is positioned around the mouthpiece 2 and defines an air gap within the mouthpiece 2 which acts as a cooling segment. The air gap provides a chamber through which the heated volatile components produced by the aerosol generating material 3 flow. The second hollow tubular element 8 is hollow to provide a chamber for aerosol accumulation, but is sufficiently rigid to withstand axial compression and bending moments that may occur during manufacture and when the article 1 is in use. The second hollow tubular element 8 provides physical displacement between the aerosol generating material 3 and the body of material 6. The physical displacement provided by the second hollow tubular element 8 will provide a thermal gradient across the length of the second hollow tubular element 8.

Preferably, the mouthpiece 2 comprises a mouthpiece having a diameter greater than 450mm³The internal volume of (a). It has been found that providing a cavity of at least this volume enables the formation of an improved aerosol. Such cavity dimensions provide sufficient space within the mouthpiece 2 to allow the heated volatile components to cool, thus allowing the aerosol generating material 3 to be exposed to higher temperatures than would otherwise be possible, as they could cause the aerosol to overheat. In the present example, the cavity is formed by the second hollow tubular element 8, but in an alternative arrangement the cavity may be formed within a different part of the mouthpiece 2. More preferably, the mouthpiece 2 comprises a cavity, for example formed within the second hollow tubular element 8, having a diameter greater than 500mm³More preferably greater than 550mm³Thereby allowing further improvement of the aerosol. In some examples, the internal cavity is included at about 550mm³And about 750mm³A volume in between, for example, about 600mm³Or 700mm³。

The second hollow tubular element 8 may be configured to provide a temperature differential of at least 40 degrees celsius between the heated volatile components entering the first upstream end of the second hollow tubular element 8 and the heated volatile components exiting the second downstream end of the second hollow tubular element 8. The second hollow tubular element 8 is preferably configured to provide a temperature difference of at least 60 degrees celsius, preferably at least 80 degrees celsius and more preferably at least 100 degrees celsius between the heated volatile components entering the first upstream end of the second hollow tubular element 8 and the heated volatile components exiting the second downstream end of the second hollow tubular element 8. This temperature difference over the length of the second hollow tubular element 8 protects the body of temperature sensitive material 6 from the high temperature of the aerosol generating material 3 as it is heated.

In alternative articles, the second hollow tubular element 8 may be replaced by an alternative cooling element, for example an element formed by a body of material which allows the aerosol to pass longitudinally through it and which also performs the function of cooling the aerosol.

In this example, the first hollow tubular element 4, the material body 6 and the second hollow tubular element 8 are combined using a second plug wrap 9 wrapped around all three sections. Preferably, the second plug wrap 9 has a basis weight of less than 50gsm, more preferably between about 20gsm and 45 gsm. Preferably, the second plug wrap 9 has a thickness of between 30 μm and 60 μm, more preferably between 35 μm and 45 μm. The second plug wrap 9 is preferably a non-porous plug wrap having a permeability of less than 100Coresta units, for example less than 50 Coresta units. However, in alternative embodiments, the second plug wrap 9 may be a porous plug wrap, for example having a permeability greater than 200 Coresta units.

In this example, the aerosol generating material 3 is wrapped in a wrapper 10. The wrap 10 may be, for example, a paper or paper-backed foil wrap. In this example, the wrap 10 is substantially air impermeable. In an alternative embodiment, the wrap 10 preferably has a permeability of less than 100Coresta units, more preferably less than 60 Coresta units. It was found that for example a low permeability wrap having a permeability of less than 100Coresta units, more preferably less than 60 Coresta units, results in an improved aerosol formation in the aerosol-generating material 3. Without wishing to be bound by theory, it is hypothesized that this is due to the reduced loss of aerosol compound through the wrap 10. The permeability of the wrap 10 may be measured according to ISO 2965:2009, which relates to determining the air permeability of materials used as cigarette paper, filter plug wrap and filter connecting paper.

In the present embodiment, the wrapper 10 includes an aluminum foil. Aluminium foil has been found to be particularly effective in enhancing aerosol formation within the aerosol-generating material 3. In this example, the aluminum foil has a metal layer having a thickness of about 6 μm. In this example, the aluminum foil has a paper backing. However, in alternative arrangements, the aluminium foil may have other thicknesses, for example a thickness between 4 μm and 16 μm. The aluminum foil also need not have a paper backing, but may have a backing formed of other materials, for example, to help provide the foil with adequate tensile strength, or it may not have a backing material. Metal layers or foils other than aluminum may also be used. The total thickness of the wrap is preferably between 20 μm and 60 μm, more preferably between 30 μm and 50 μm, which may provide a wrap with suitable structural integrity and heat transfer characteristics. The tensile force that may be applied to the wrapper before the wrapper breaks may be greater than 3,000 grams-force, for example between 3,000 and 10,000 grams-force or between 3,000 and 4,500 grams-force.

The article has a ventilation level of about 75% of the aerosol inhaled through the article. In alternative embodiments, the article may have a ventilation level of between 50% and 80%, for example 65% and 75%, of the aerosol inhaled through the article. Ventilation at these levels helps to slow the flow of aerosol drawn through the mouthpiece 2, thereby enabling the aerosol to cool sufficiently before it reaches the downstream end 2b of the mouthpiece 2. Ventilation is provided directly into the mouthpiece 2 of the article 1. In the present example, ventilation is provided into the second hollow tubular element 8, which has been found to be particularly beneficial in assisting the aerosol generation process. Ventilation is provided via first and second parallel rows of perforations 12, formed in the present case as laser perforations, at locations 17.925mm and 18.625mm respectively from the downstream mouth end 2b of the mouthpiece 2. These perforations pass through the tipping paper 5, the second plug wrap 9 and the second hollow tubular element 8. In alternative embodiments, ventilation may be provided into the mouthpiece at other locations, for example into the material body 6 or the first tubular element 4.

In this example, the aerosol-forming material added to the aerosol-generating substrate 3 comprises 14% by weight of the aerosol-generating substrate 3. Preferably, the aerosol-forming material comprises at least 5%, more preferably at least 10% by weight of the aerosol-generating substrate. Preferably, the aerosol-forming material comprises less than 25%, more preferably less than 20%, for example between 10% and 20%, between 12% and 18% or between 13% and 16% by weight of the aerosol-generating substrate.

Preferably, the aerosol generating material 3 is provided as a cylindrical rod of aerosol generating material. Regardless of the form of the aerosol generating material, it preferably has a length of about 10mm to 100 mm. In some embodiments, the length of the aerosol generating material is preferably in the range of about 25mm to 50mm, more preferably in the range of about 30mm to 45mm, and still more preferably about 30mm to 40 mm.

The volume of aerosol generating material 3 provided may be from about 200mm³To about 4300mm³Preferably from about 500mm³To 1500mm³More preferably from about 1000mm³To about 1300mm³And (4) changing. Providing these volumes of aerosol generating material, for example from about 1000mm³To about 1300mm³It has been advantageously shown that a superior aerosol is achieved, with greater visibility and sensory properties than that obtained with a volume selected from the lower limit of the range.

The mass of aerosol-generating material 3 provided may be greater than 200mg, for example from about 200mg to 400mg, preferably from about 230mg to 360mg, more preferably from about 250mg to 360 mg. It has advantageously been found that providing an aerosol generating material of higher quality results in improved organoleptic properties compared to aerosols generated from lower quality tobacco material.

Preferably, the aerosol-generating material or substrate is formed from a tobacco material as described herein, which tobacco material comprises a tobacco component.

Figure 5a is a side cross-sectional view of another article 1 'comprising a capsule-containing mouthpiece 2'. Figure 5b is a cross-sectional view of the capsule containing mouthpiece shown in figure 5a through line a-a' thereof. The article 1 ' and capsule-containing mouthpiece 2 ' are the same as the article 1 and mouthpiece 2 shown in figure 4, except that the aerosol modifier is disposed within the material body 6 (in this example in the form of a capsule 11) and the oil resistant first plug wrap 7 ' surrounds the material body 6. In other examples, the aerosol-modifying agent may be provided in other forms, such as a material injected into the body of material 6, or on a thread (thread) (e.g., a thread carrying a flavoring or other aerosol-modifying agent) that may also be disposed within the body of material 6.

Capsule 11 may comprise a breakable capsule, such as a capsule having a solid, frangible shell surrounding a liquid payload. In the present example, a single capsule 11 is used. The capsule 11 is completely embedded within the body of material 6. In other words, the capsule 11 is completely surrounded by the material forming the body 6. In other examples, a plurality of breakable capsules may be disposed within the body of material 6, such as 2, 3, or more breakable capsules. The length of the body of material 6 may be increased to accommodate the number of capsules required. In instances where multiple capsules are used, the individual capsules may be identical to one another, or may differ from one another in size and/or capsule payload. In other examples, a plurality of bodies of material 6 may be provided, wherein each body contains one or more capsules.

The capsule 11 has a core-shell structure. In other words, the capsule 11 includes a shell that encapsulates a liquid agent (e.g., a flavoring agent or other agent), which may be any of the flavoring agents or aerosol modifiers described herein. The shell of the capsule may be ruptured by the user to release the flavouring or other agent into the body of material 6. The first plug wrap 7' may include a barrier coating such that the material of the plug wrap is substantially impermeable to the liquid payload of the capsule 11. Alternatively or in addition, the second plug wrap 9 and/or tipping paper 5 may comprise a barrier coating so as to render the material of the plug wrap and/or tipping paper substantially impermeable to the liquid payload of the capsule 11.

In the present example, the capsule 11 is spherical and has a diameter of about 3 mm. In other examples, other shapes and sizes of capsules may be used. The total weight of the capsule 11 may range from about 10mg to about 50 mg.

In this example, the capsule 11 is located at a longitudinally central position within the body of material 6. That is, the capsule 11 is positioned such that its center is 4mm from each end of the material body 6. In other examples, the capsule 11 may be located in the material body 6 at a position other than the longitudinal center position, i.e., closer to the downstream end of the material body 6 than the upstream end, or closer to the upstream end of the material body 6 than the downstream end. Preferably, the mouthpiece 2 'is configured such that the capsule 11 and the ventilation holes 12 are longitudinally offset from each other in the mouthpiece 2'.

A cross-section of the mouthpiece 2 'is shown in figure 5b, which is taken through line a-a' of figure 5 a. Figure 5b shows the capsule 11, the body of material 6, the first and second plug wraps 7', 9 and the tipping paper 5. In the present example, the capsule 11 is centered on the longitudinal axis (not shown) of the mouthpiece 2'. The first and second plug wraps 7', 9 and tipping paper 5 are arranged coaxially around the body of material 6.

The breakable capsule 11 has a core-shell structure. That is, the encapsulating or barrier material creates a shell around the core containing the aerosol modifier. The shell structure hinders the migration of the aerosol modifier during storage of the article 1', but allows for the controlled release of the aerosol modifier (also referred to as aerosol modifier) during use.

In some cases, the barrier material (also referred to herein as an encapsulant material) is frangible. The capsule is crushed or otherwise ruptured or ruptured by a user to release the encapsulated aerosol modifier. Typically, the capsule is ruptured immediately before heating begins, but the user can select when to release the aerosol modifier. The term "breakable capsule" refers to a capsule in which the shell can be broken by pressure to release the core; more specifically, when the user wants to release the core of the capsule, the shell can be ruptured under the pressure exerted by the user's finger.

In some cases, the barrier material is heat resistant. That is, in some cases, the barrier material does not rupture, melt, or otherwise fail at the temperature of reaching the capsule site during operation of the aerosol provision device. For example, the capsule located in the mouthpiece may be exposed to a temperature in the range of, for example, 30 ℃ to 100 ℃, and the barrier material may continue to retain the liquid core until at least about 50 ℃ to 120 ℃.

In other cases, the capsules release the core composition upon heating, for example by melting the barrier material or by expansion of the capsules causing rupture of the barrier material.

The total weight of the capsule may be in the range of about 1mg to about 100mg, suitably about 5mg to about 60mg, about 8mg to about 50mg, about 10mg to about 20mg, or about 12mg to about 18 mg.

The total weight of the core formulation may be in the range of about 2mg to about 90mg, suitably about 3mg to about 70mg, about 5mg to about 25mg, about 8mg to about 20mg, or about 10mg to about 15 mg.

The capsule according to the invention comprises a core and a shell as described above. The capsules may have a crush strength of from about 4.5N to about 40N, more preferably from about 5N to about 30N or to about 28N (e.g., from about 9.8N to about 24.5N). The capsule burst strength can be measured when the capsule is removed from the material body 6 and a force gauge is used to measure the force with which the capsule bursts when pressed between two flat metal plates. A suitable measuring device is the Sauter FK50 load cell with a flat head attachment which can be used to crush the capsule to a flat hard surface with a surface similar to the attachment.

The capsule may be substantially spherical and have a diameter of at least about 0.4mm, 0.6mm, 0.8mm, 1.0mm, 2.0mm, 2.5mm, 2.8mm or 3.0 mm. The capsule may have a diameter of less than about 10.0mm, 8.0mm, 7.0mm, 6.0mm, 5.5mm, 5.0mm, 4.5mm, 4.0mm, 3.5mm, or 3.2 mm. By way of example, the capsule diameter may be in the range of about 0.4mm to about 10.0mm, about 0.8mm to about 6.0mm, about 2.5mm to about 5.5mm, or about 2.8mm to about 3.2 mm. In some cases, the capsule may have a diameter of about 3.0 mm. These dimensions are particularly suitable for incorporating the capsules into an article as described herein.

In some embodiments, the cross-sectional area of the capsule 11 at its largest cross-sectional area is less than 28%, more preferably less than 27%, still more preferably less than 25% of the cross-sectional area of the portion of the mouthpiece 2' where the capsule 11 is provided. For example, for a spherical capsule with a diameter of 3.0mm, the maximum cross-sectional area of the capsule is 7.07mm². For a mouthpiece 2' as described herein having a circumference of 21mm, the body of material 6 has an outer circumference of 20.8mm and the radius of the assembly will be 3.31mm, corresponding to 34.43mm²Cross-sectional area of. In this example, the cross-sectional area of the capsule is 20.5% of the cross-sectional area of the mouthpiece 2'. As another example, if the capsule has a diameter of 3.2mm, its maximum cross-sectional area is 8.04mm². In this case, the cross-sectional area of the capsule will be 23.4% of the cross-sectional area of the material body 6. Capsules having a maximum cross-sectional area less than 28% of the cross-sectional area of the portion of the mouthpiece 2' where the capsule 11 is located have the following advantages: and capsules having a large cross-sectional areaIn contrast, the pressure drop over the mouthpiece 2 'is reduced and sufficient space is left around the capsule for the aerosol to pass through, without the body of material 6 removing a significant amount of the aerosol substance as it passes through the mouthpiece 2'.

Preferably, the pressure drop or pressure difference (also called the resistance to suction) over the article, measured as the open pressure drop (i.e. the ventilation openings open), decreases by less than 8mmH when the capsule is ruptured₂And O. More preferably, the open pressure drop is reduced by less than 6mmH₂O, more preferably less than 5mmH₂And O. These values are measured as the average of the values achieved by at least 80 articles made to the same design. This small variation in pressure drop means that other aspects of the product design, such as setting the correct ventilation level for a given product pressure drop, can be achieved whether or not the consumer chooses to rupture the capsule.

The barrier material may comprise one or more of a gelling agent, bulking agent, buffer, colorant and plasticizer.

Suitably, the gelling agent may be, for example, a polysaccharide or cellulose gelling agent, gelatin, gum, gel, wax, or a mixture thereof. Suitable polysaccharides include alginates, dextrans, maltodextrins, cyclodextrins, and pectins. Suitable alginates include, for example, alginate, esterified alginate or alginic acid glyceride. Alginates include ammonium alginate, triethanolamine alginate and group I or II metal ion alginates such as sodium alginate, potassium alginate, calcium alginate and magnesium alginate. Esterified alginates include propylene glycol alginate and glycerol alginate. In one embodiment, the barrier material is sodium alginate and/or calcium alginate. Suitable cellulosic materials include methyl cellulose, ethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, carboxymethyl cellulose, cellulose acetate, and cellulose ethers. The gelling agent may comprise one or more modified starches. The gelling agent may comprise carrageenan. Suitable gums include agar, gellan, gum arabic, pullulan, mannan, gum ghatti, gum tragacanth, karaya, locust bean, acacia, guar, fenugreek seed, and xanthan. Suitable gels include agar, agarose, carrageenan, fucoidan, and furcellaran. Suitable waxes include carnauba wax. In some cases, the gelling agent may include carrageenan and/or gellan gum; these gelling agents are particularly suitable to be included as gelling agents, since the pressure required to rupture the resulting capsules is particularly suitable.

The barrier material may comprise one or more bulking agents such as starch, modified starch (such as oxidized starch) and sugar alcohols such as maltitol.

The barrier material may contain a colorant that facilitates positioning of the capsule within the aerosol-generating device during manufacture of the aerosol-generating device. The colorant is preferably selected from the group consisting of a coloring agent and a pigment.

The barrier material may further comprise at least one buffer, such as a citrate or phosphate compound.

The barrier material may further comprise at least one plasticizer which may be glycerol, sorbitol, maltitol, triacetin, polyethylene glycol, propylene glycol or another polyol having plasticizing properties, and optionally an acid of the mono-, di-or tri-acid type, in particular citric acid, fumaric acid, malic acid, etc. The amount of plasticizer is in the range of 1 to 30% by weight, preferably 2 to 15% by weight, even more preferably 3 to 10% by weight of the total dry weight of the shell.

The barrier material may also comprise one or more fillers. Suitable fillers include starch derivatives such as dextrin, maltodextrin, cyclodextrin (alpha, beta or gamma), or cellulose derivatives such as hydroxypropyl methylcellulose (HPMC), hydroxypropyl cellulose (HPC), Methylcellulose (MC), carboxymethyl cellulose (CMC), polyvinyl alcohol, polyols or mixtures thereof. Dextrin is a preferred filler. The amount of filler in the shell is at most 98.5%, preferably from 25 to 95%, more preferably from 40 to 80% and even more preferably from 50 to 60% by weight based on the total dry weight of the shell.

The capsule shell may additionally comprise a hydrophobic outer layer which reduces the susceptibility of the capsule to moisture-induced degradation. The hydrophobic outer layer is suitably selected from the group comprising waxes, especially carnauba wax, candelilla wax or beeswax, carbowax, shellac (in alcoholic or aqueous solution), ethyl cellulose, hydroxypropyl methyl cellulose, hydroxypropyl cellulose, latex compositions, polyvinyl alcohol or combinations thereof. More preferably, the at least one moisture barrier is ethyl cellulose or a mixture of ethyl cellulose and shellac.

The capsule core comprises an aerosol modifier. The aerosol modifier can be any volatile material that alters at least one property of the aerosol. For example, the aerosol substance may alter pH, sensory properties, moisture content, delivery characteristics, or flavor. In some cases, the aerosol modifier may be selected from an acid, a base, water, or a flavoring agent. In some embodiments, the aerosol modifier comprises one or more flavoring agents.

The flavouring agent may suitably be licorice, rose oil, vanilla, lemon oil, orange oil, mint flavour, suitably menthol and/or mint oil from any species of the genus mentha, such as peppermint and/or spearmint oil, or lavender, fennel or anise.

In some cases, the flavoring agent comprises menthol.

In some cases, a capsule may comprise at least about 25% w/w flavouring (based on the total weight of the capsule), suitably at least about 30% w/w flavouring, 35% w/w flavouring, 40% w/w flavouring, 45% w/w flavouring or 50% w/w flavouring.

In some cases, the core may comprise at least about 25% w/w flavoring (based on the total weight of the core), suitably at least about 30% w/w flavoring, 35% w/w flavoring, 40% w/w flavoring, 45% w/w flavoring, or 50% w/w flavoring. In some cases, the core may comprise less than or equal to about 75% w/w flavoring (based on the total weight of the core), suitably less than or equal to about 65% w/w flavoring, 55% w/w flavoring, or 50% w/w flavoring. By way of example, the capsule may contain flavouring in an amount in the range of 25-75% w/w (based on the total weight of the core), about 35-60% w/w or about 40-55% w/w.

The capsule may contain at least about 2mg, 3mg or 4mg of the aerosol modifier, suitably at least about 4.5mg of the aerosol modifier, 5mg of the aerosol modifier, 5.5mg of the aerosol modifier or 6mg of the aerosol modifier.

In some cases, the consumable comprises at least about 7mg of the aerosol modifier, suitably at least about 8mg of the aerosol modifier, 10mg of the aerosol modifier, 12mg of the aerosol modifier, or 15mg of the aerosol modifier. The core may also comprise a solvent that dissolves the aerosol modifier.

Any suitable solvent may be used.

When the aerosol modifier comprises a flavoring agent, the solvent may suitably comprise short or medium chain fats and oils. For example, the solvent may comprise a triglyceride of glycerol, such as a C2-C12 triglyceride, suitably a C6-C10 triglyceride or a C5-C12 triglyceride. For example, the solvent may comprise medium chain triglycerides (MCT-C8-C12), which may be derived from palm oil and/or coconut oil.

Esters may be formed with caprylic and/or capric acid. For example, the solvent may comprise a medium chain triglyceride which is caprylic acid triglyceride and/or capric acid triglyceride. For example, the solvent may comprise a compound identified by numbers 73398-61-5, 65381-09-1, 85409-09-2 in the CAS registry. Such medium chain triglycerides are odorless and tasteless.

The Hydrophilic Lipophilic Balance (HLB) of the solvent may be in the range 9 to 13, suitably 10 to 12. The process for preparing the capsules comprises co-extrusion, optionally followed by centrifugation and solidification and/or drying. The contents of WO 2007/010407a2 are incorporated by reference in their entirety.

In the example described above, the mouthpieces 2, 2' each comprise a single material body 6. In other examples, the mouthpiece of figure 4 or figures 2a and 2b may comprise a plurality of material bodies. The mouthpiece 2, 2' may comprise a cavity between the bodies of material.

In some examples, the mouthpiece 2, 2' downstream of the aerosol-generating material 3 may comprise a wrapper, for example a first plug wrapper 7 or a second plug wrapper 9 or tipping paper 5, comprising an aerosol-modifying agent as described herein. The aerosol modifier may be disposed on an inward or outward facing surface of the mouthpiece wrapper. For example, the aerosol-modifying agent may be provided on a region of the wrapper, such as the outwardly facing surface of the tipping paper 5 which comes into contact with the lips of the consumer during use. By disposing the aerosol modifier on the outwardly facing surface of the mouthpiece wrapper, the aerosol modifier may be transferred to the lips of the consumer during use. Transferring the aerosol-modifying agent to the lips of the consumer during use of the article may alter the sensory properties (e.g., taste) of the aerosol produced by the aerosol-generating substrate 3 or otherwise provide the consumer with an alternative sensory experience. For example, the aerosol-modifying agent may impart a flavour to an aerosol produced by the aerosol-generating substrate 3. The aerosol modifier may be at least partially soluble in water such that it is transferred to the user via the saliva of the consumer. The aerosol modifier may be a material that is volatilized by heat generated by the aerosol provision system. This may facilitate transfer of the aerosol-modifying agent to the aerosol generated by the aerosol-generating substrate 3.

The aerosol generating material 3 of the articles 1, 1' described herein is heated using a non-combustible aerosol provision device. The non-combustible aerosol provision device preferably comprises a coil, as this is found to enable improved heat transfer to the article 1, 1' compared to other arrangements.

In some examples, the coil is configured to cause heating of the at least one electrically conductive heating element, in use, such that thermal energy is conducted from the at least one electrically conductive heating element to the aerosol generating material, thereby causing heating of the aerosol generating material.

In some examples, the coil is configured for generating, in use, a varying magnetic field for penetrating the at least one heating element, thereby causing inductive heating and/or hysteresis heating of the at least one heating element. In such an arrangement, the or each heating element may be referred to as a "susceptor" as defined herein. A coil configured for generating, in use, a varying magnetic field for penetrating the at least one electrically conductive heating element to thereby cause inductive heating of the at least one electrically conductive heating element may be referred to as an "induction coil" or an "induction coil".

The device may comprise a heating element, for example an electrically conductive heating element, and the heating element may be suitably positioned or positionable relative to the coil to effect such heating of the heating element. The heating element may be in a fixed position relative to the coil. Alternatively, at least one heating element, e.g. at least one electrically conductive heating element, may be included in the article 1, 1 'for insertion into a heating zone of the device, wherein the article 1, 1' further comprises the aerosol generating material 3 and is removable from the heating zone after use. Alternatively, both the device and such an article 1, 1' may comprise at least one corresponding heating element, e.g. at least one electrically conductive heating element, and the coil may be used to cause heating of the respective heating elements of the device and the article when the article is in the heating zone.

In some examples, the coil is helical. In some examples, the coil-encircling device is configured to receive at least a portion of the heating zone of the aerosol generating material. In some examples, the coil is a helical coil that surrounds at least a portion of the heating zone.

In some examples, the device includes an electrically conductive heating element at least partially surrounding the heating region, and the coil is a helical coil surrounding at least a portion of the electrically conductive heating element. In some examples, the electrically conductive heating element is tubular. In some examples, the coil is an induction coil.

In some examples, the use of a coil enables the non-combustible aerosol provision device to reach operating temperatures faster than a non-coil aerosol provision device. For example, the non-combustible aerosol provision device comprising a coil as described above may reach an operating temperature such that a first suction (puff) may be provided in less than 30 seconds, more preferably in less than 25 seconds, from the start of the device heating program. In some examples, the device may reach the operating temperature within about 20 seconds from the start of the device heating program.

It has been found that the use of a coil as described herein in a device to cause heating of an aerosol generating material enhances the generated aerosol. For example, consumers have reported that aerosols produced by devices including coils as described herein are perceptually closer to aerosols produced in factory-manufactured cigarette (FMC) products than aerosols produced by other non-combustible aerosol provision systems. Without wishing to be bound by theory, it is hypothesized that this is a result of the reduced time to reach the required heating temperature when using a coil, the higher heating temperatures achievable when using a coil, and/or the fact that the coil enables such systems to heat relatively large volumes of aerosol generating material simultaneously, resulting in an aerosol temperature similar to the FMC aerosol temperature. In FMC products, the burning coal produces a hot aerosol that heats the tobacco in the tobacco rod behind the coal as the aerosol is drawn through the rod. Such a hot aerosol is understood to release the flavour compound from the tobacco in the rod behind the burning coal. It is believed that a device comprising a coil as described herein is also capable of heating an aerosol generating material, such as a tobacco material as described herein, to release a flavour compound to generate an aerosol which has been reported to more closely resemble an FMC aerosol.

Using an aerosol provision system comprising a coil as described herein, for example an induction coil that heats at least some of the aerosol generating material to at least 200 ℃, more preferably at least 220 ℃, may enable an aerosol to be generated from the aerosol generating material having particular characteristics that are believed to be more similar to those of an FMC product. For example, when an inductive heater heated to at least 250 ℃ is used to heat an aerosol generating material (including nicotine) for a period of two seconds, one or more of the following characteristics have been observed at an airflow of at least 1.50L/m during this period:

aerosolizing at least 10 μ g of nicotine from the aerosol generating material;

the weight ratio of aerosol generated to nicotine of the aerosol-forming material is at least about 2.5:1, suitably at least 8.5: 1;

an aerosol-forming material which can be aerosolized by the aerosol-generating material by at least 100 μ g;

the average particle or droplet size in the aerosol produced is less than about 1000 nm; and

the aerosol density is at least 0.1 μ g/cc.

In some cases, at least 10 μ g of nicotine, suitably at least 30 μ g or 40 μ g of nicotine, is aerosolized by the aerosol generating material under an airflow of at least 1.50L/m during the period of time. In some cases, less than about 200 μ g, suitably less than about 150 μ g, or less than about 125 μ g of nicotine is aerosolized by the aerosol generating material under an airflow of at least 1.50L/m during the period of time.

In some cases, the aerosol comprises at least 100 μ g of aerosol-forming material, suitably at least 200 μ g, 500 μ g or 1mg of aerosol-forming material is aerosolized by the aerosol-generating material under an airflow of at least 1.50L/m during the period of time. Suitably, the aerosol-forming material may comprise or consist of glycerol.

As defined herein, the term "average particle or droplet size" refers to the average size of the solid or liquid component of an aerosol (i.e., the component suspended in a gas). When an aerosol comprises suspended liquid droplets and suspended solid particles, the term refers to the average size of all components together.

In some cases, the average particle or droplet size of the generated aerosol may be less than about 900nm, 800nm, 700nm, 600nm, 500nm, 450nm, or 400 nm. In some cases, the average particle or droplet size may be greater than about 25nm, 50nm, or 100 nm.

In some cases, the aerosol produced over the period of time has a density of at least 0.1 μ g/cc. In some cases, the aerosol density is at least 0.2 μ g/cc, 0.3 μ g/cc, or 0.4 μ g/cc. In some cases, the aerosol density is less than about 2.5 μ g/cc, 2.0 μ g/cc, 1.5 μ g/cc, or 1.0 μ g/cc.

The non-combustible aerosol provision means is preferably arranged to heat the aerosol-generating material 3 of the article 1, 1' to a maximum temperature of at least 160 ℃. Preferably, the non-combustible aerosol provision device is arranged to heat the aerosol-forming material 3 of the article 1, 1' at least once to a maximum temperature of at least about 200 ℃, or at least about 220 ℃, or at least about 240 ℃, more preferably at least about 270 ℃ during a heating process prior to the non-combustible aerosol provision device.

Using an aerosol provision system comprising a coil as described herein, for example an induction coil that heats at least some of the aerosol generating material to at least 200 ℃, more preferably at least 220 ℃, may enable an aerosol to be generated from the aerosol generating material in an article 1, 1 'as described herein, which article has a higher temperature than previous devices when the aerosol leaves the mouth end of the mouthpiece 2, 2', thereby facilitating the generation of an aerosol which is believed to be closer to the FMC product. For example, the maximum aerosol temperature measured at the mouth end of the article 1, 1' may preferably be greater than 50 ℃, more preferably greater than 55 ℃ and still more preferably greater than 56 ℃ or 57 ℃. Additionally or alternatively, the maximum aerosol temperature measured at the mouth end of the article 1, 1' may be less than 62 ℃, more preferably less than 60 ℃ and more preferably less than 59 ℃. In some embodiments, the maximum aerosol temperature measured at the mouth end of the article 1, 1' may preferably be between 50 ℃ and 62 ℃, more preferably between 56 ℃ and 60 ℃.

Fig. 6 shows an example of a non-combustible aerosol provision device 100 for generating an aerosol from an aerosol generating medium/material, such as the aerosol generating material 3 of the articles 1, 1' described herein. In general terms, the device 100 may be used to heat a replaceable article 110 comprising an aerosol generating medium, such as the articles 1, 1' described herein, to generate an aerosol or other inhalable medium to be inhaled by a user of the device 100. Together, the apparatus 100 and the alternative article 110 form a system.

The device 100 includes a housing 102 (in the form of an outer cover) that surrounds and contains the various components of the device 100. The device 100 has an opening 104 at one end through which the article 110 may be inserted for heating by the heating assembly. In use, the article 110 may be fully or partially inserted into a heating assembly, where it may be heated by one or more components of the heater assembly.

The device 100 of this embodiment includes a first end member 106 that includes a cover 108, the cover 108 being movable relative to the first end member 106 to close the opening 104 when no article 110 is in place. In fig. 6, the cover 108 is shown in an open configuration, however the cover 108 may be moved into a closed configuration. For example, the user may slide the cover 108 in the direction of arrow "B".

The device 100 may also include a user-operable control element 112, such as a button or switch, which when pressed operates the device 100. For example, a user may turn on the device 100 by operating the switch 112.

The device 100 may also include electrical components such as a socket/port 114 that may receive a cable to charge the battery of the device 100. For example, the receptacle 114 may be a charging port, such as a USB charging port.

Fig. 7 depicts the device 100 of fig. 6 with the outer cover 102 removed and no article 110 present. The device 100 defines a longitudinal axis 134.

As shown in fig. 7, the first end member 106 is disposed at one end of the device 100 and the second end member 116 is disposed at an opposite end of the device 100. Together, the first end member 106 and the second end member 116 at least partially define an end surface of the device 100. For example, a bottom surface of the second end member 116 at least partially defines a bottom surface of the device 100. The edge of the outer cover 102 may also define a portion of the end surface. In this embodiment, the cover 108 also defines a portion of the top surface of the device 100.

The end of the device closest to the opening 104 may be referred to as the proximal end (or mouth end) of the device 100, since it is closest to the user's mouth in use. In use, a user inserts the article 110 into the opening 104, operates the user controls 112 to begin heating the aerosol generating material and drawing an aerosol generated in the device. This causes the aerosol to flow through the device 100 along the flow path toward the proximal end of the device 100.

The other end of the device furthest from the mouth 104 may be referred to as the distal end of the device 100, as it is the end furthest from the user's mouth in use. When a user draws on an aerosol generated in the device, the aerosol flows away from the distal end of the device 100.

The apparatus 100 also includes a power supply 118. The power source 118 may be, for example, a battery, such as a rechargeable battery or a non-rechargeable battery. Examples of suitable batteries include, for example, lithium batteries (such as lithium ion batteries), nickel batteries (such as nickel-cadmium batteries), and alkaline batteries. The battery is electrically coupled to the heating assembly to supply power to heat the aerosol generating material when needed and under the control of a controller (not shown). In this embodiment, the batteries are connected to a central support 120 that holds the batteries 118 in place.

The device further comprises at least one electronic module 122. The electronic module 122 may include, for example, a Printed Circuit Board (PCB). The PCB 122 may support at least one controller, such as a processor and memory. PCB 122 may also include one or more electrical traces for electrically connecting together the different electronic components of device 100. For example, the battery terminals may be electrically connected to the PCB 122 so that power may be distributed throughout the device 100. The receptacle 114 may also be electrically coupled to a battery via electrical traces.

In the example device 100, the heating component is an induction heating component and includes different components for heating the aerosol generating material of the article 110 via an induction heating process. Induction heating is the process of heating an electrically conductive object, such as a susceptor, by electromagnetic induction. The induction heating assembly may comprise an induction element (e.g. one or more induction coils) and means for passing a varying current (such as an alternating current) through the induction element. The varying current in the inductive element generates a varying magnetic field. The varying magnetic field penetrates a susceptor, which is suitably positioned with respect to the inductive element, and generates eddy currents inside the susceptor. The susceptor has an electrical resistance to eddy currents, so the flow of eddy currents against this resistance causes the susceptor to heat by joule heating. In case the susceptor comprises a ferromagnetic material, such as iron, nickel or cobalt, heat may also be generated by hysteresis losses in the susceptor, i.e. a varying orientation of the magnetic dipoles in the magnetic material due to the magnetic dipoles being aligned with a varying magnetic field. In induction heating, heat is generated inside the susceptor, allowing for rapid heating, as compared to heating, for example, by conduction. Furthermore, no physical contact between the induction heater and the susceptor is required, allowing for an increased degree of freedom in construction and application.

The induction heating assembly of the example apparatus 100 includes a susceptor arrangement 132 (referred to herein as a "susceptor"), a first induction coil 124, and a second induction coil 126. The first induction coil 124 and the second induction coil 126 are made of an electrically conductive material. In this embodiment, the first and second induction coils 124, 126 are made of Litz (Litz) wire/cable that is wound in a spiral fashion to provide the

spiral induction coils

124, 126. Litz wire comprises a plurality of individual wires that are individually insulated and twisted together to form a single wire. Litz wire is designed to reduce skin effect losses in the conductor. In the example apparatus 100, the first induction coil 124 and the second induction coil 126 are made of copper litz wire having a rectangular cross section. In other embodiments, the litz wire may have a cross-section of other shapes, such as circular.

The first induction coil 124 is configured to generate a first varying magnetic field for heating a first section of the susceptor 132, and the second induction coil 126 is configured to generate a second varying magnetic field for heating a second section of the susceptor 132. In the present embodiment, the first induction coil 124 is adjacent to the second induction coil 126 in a direction along the longitudinal axis 134 of the device 100 (i.e., the first induction coil 124 and the second induction coil 126 do not overlap). The susceptor arrangement 132 may comprise a single susceptor, or two or more separate susceptors. Ends 130 of the first and second induction coils 124, 126 may be connected to the PCB 122.

It will be appreciated that in some embodiments, the first and second induction coils 124, 126 may have at least one characteristic that is different from one another. For example, the first inductive coil 124 may have at least one characteristic that is different from the second inductive coil 126. More specifically, in one embodiment, the first induction coil 124 may have a different inductance value than the second induction coil 126. In fig. 2, the first induction coil 124 and the second induction coil 126 have different lengths such that the first induction coil 124 is wound on a smaller portion of the susceptor 132 than the second induction coil 126. Thus, the first inductive coil 124 may include a different number of turns than the second inductive coil 126 (assuming that the spacing between the individual turns is substantially the same). In yet another embodiment, the first inductive coil 124 may be made of a different material than the second inductive coil 126. In some embodiments, the first induction coil 124 and the second induction coil 126 may be substantially identical.

In this embodiment, the first induction coil 124 and the second induction coil 126 are wound in opposite directions. This may be useful when the induction coil is active at different times. For example, initially, the first induction coil 124 may operate to heat a first section/portion of the article 110, and at a later time, the second induction coil 126 may operate to heat a second section/portion of the article 110. Winding the coil in the opposite direction helps to reduce the current induced in the inactive coil when used in conjunction with a particular type of control circuit. In the apparatus 100 of fig. 7, the first induction coil 124 is a right-hand helix and the second induction coil 126 is a left-hand helix. However, in another embodiment, the induction coils 124, 126 may be wound in the same direction, or the first induction coil 124 may be a left helix and the second induction coil 126 may be a right helix.

The susceptor 132 of this embodiment is hollow, thus defining a receptacle for receiving aerosol generating material. For example, the article 110 may be inserted into the susceptor 132. In this embodiment, the susceptor 120 is tubular with a circular cross-section.

The susceptor 132 may be made of one or more materials. Preferably, the susceptor 132 comprises carbon steel with a nickel or cobalt coating.

In some embodiments, the susceptor 132 may comprise at least two materials that can be heated at two different frequencies for selective aerosolization of the at least two materials. For example, a first section of the susceptor 132 (heated by the first induction coil 124) may contain a first material, while a second section of the susceptor 132 (heated by the second induction coil 126) may contain a second, different material. In another embodiment, the first section may contain a first material and a second material, wherein the first material and the second material may be heated differently based on the operation of the first induction coil 124. The first and second materials may be adjacent along an axis defined by the susceptor 132, or may form different layers within the susceptor 132. Similarly, the second section may contain third and fourth materials, where the third and fourth materials may be heated differently based on the operation of the second induction coil 126. The third material and the fourth material may be adjacent along an axis defined by the susceptor 132, or may form different layers within the susceptor 132. For example, the third material may be the same as the first material, and the fourth material may be the same as the second material. Alternatively, each material may be different. The susceptor may comprise, for example, carbon steel or aluminum.

The apparatus 100 of fig. 7 further comprises an insulating element 128, which may be generally tubular and at least partially surrounds the susceptor 132. The insulating element 128 may be constructed of any insulating material, such as plastic. In this particular embodiment, the insulating element is composed of Polyetheretherketone (PEEK). The insulating element 128 may help insulate various components of the apparatus 100 from heat generated in the susceptor 132.

The insulating element 128 may also fully or partially support the first and second induction coils 124, 126. For example, as shown in fig. 7, first induction coil 124 and second induction coil 126 are positioned around insulating member 128 and in contact with a radially outward surface of insulating member 128. In some embodiments, the insulating element 128 does not abut the first inductive coil 124 and the second inductive coil 126. For example, there may be a small gap between the outer surface of the insulating element 128 and the inner surfaces of the first and second induction coils 124, 126.

In a particular embodiment, the susceptor 132, the insulating element 128, and the first and second induction coils 124, 126 are coaxial about a central longitudinal axis of the susceptor 132.

Fig. 8 shows a side view of the device 100 in partial cross-section. In this embodiment there is an outer cover 102. The rectangular cross-sectional shape of the first induction coil 124 and the second induction coil 126 is more clearly visible.

The apparatus 100 further includes a support 136 that engages an end of the susceptor 132 to hold the susceptor 132 in place. The support 136 is connected to the second end member 116.

The apparatus may also include a second printed circuit board 138 associated with the control element 112.

The device 100 further comprises a second cap 140 and a spring 142 arranged towards the distal end of the device 100. The spring 142 allows the second cover 140 to open to provide access to the susceptor 132. The user may open the second cover 140 to clean the susceptor 132 and/or the support 136.

The device 100 further includes an expansion chamber 144 extending away from the proximal end of the susceptor 132 toward the opening 104 of the device. Located at least partially within the expansion chamber 144 is a retaining clip 146 to abut and retain the article 110 when the article 110 is received within the device 100. Expansion chamber 144 is connected to end member 106.

Fig. 9 is an exploded view of the device 100 of fig. 8, with the outer cover 102 omitted.

Fig. 10A depicts a cross-section of a portion of the device 100 of fig. 8. Fig. 10B depicts a close-up view of the region of fig. 10A. Fig. 10A and 10B illustrate the article 110 received within the susceptor 132, wherein the article 110 is sized such that an outer surface of the article 110 abuts an inner surface of the susceptor 132. This ensures that heating is most efficient. The article 110 of this embodiment includes an aerosol generating material 110 a. The aerosol-generating material 110a is located within the susceptor 132. The article 110 may also include other components, such as filters, wrap materials, and/or cooling structures.

Figure 10B shows that the outer surface of the susceptor 132 is spaced from the inner surfaces of the induction coils 124, 126 by a distance 150, measured in a direction perpendicular to the longitudinal axis 158 of the susceptor 132. In a particular embodiment, the distance 150 is about 3mm to 4mm, about 3-3.5mm, or about 3.25 mm.

Figure 10B further illustrates that the outer surface of the insulating element 128 is spaced from the inner surfaces of the induction coils 124, 126 by a distance 152, measured in a direction perpendicular to the longitudinal axis 158 of the susceptor 132. In one particular embodiment, the distance 152 is about 0.05 mm. In another embodiment, the distance 152 is substantially 0mm such that the induction coils 124, 126 abut and contact the insulating element 128.

In one embodiment, the susceptor 132 has a wall thickness 154 of about 0.025mm to 1mm or about 0.05 mm.

In one embodiment, the susceptor 132 has a length of about 40mm to 60mm, about 40mm to 45mm, or about 44.5 mm.

In one embodiment, the insulating element 128 has a wall thickness 156 of about 0.25mm to 2mm, 0.25mm to 1mm, or about 0.5 mm.

In use, the article 1, 1' described herein may be inserted into a non-combustible aerosol supply device, such as the device 100 described with reference to fig. 6 to 10. At least a portion of the mouthpiece 2, 2 'of the article 1, 1' protrudes from the non-combustible aerosol provision device 100 and can be placed into the mouth of a user. The aerosol is generated by heating the aerosol generating material 3 using the apparatus 100. The aerosol generated by the aerosol generating material 3 passes through the mouthpiece 2 to the mouth of the user.

The articles 1, 1' described herein have particular advantages, for example when used with a non-flammable aerosol supply device such as the device 100 described with reference to fig. 6 to 10. In particular, it was surprisingly found that the first tubular element 4 formed by the filamentary tow has a significant effect on the temperature of the outer surface of the mouthpiece 2, 2 'of the article 1, 1'. For example, where the hollow tubular element 4 formed from filamentary tow is wrapped in an outer wrapper (e.g. tipping paper 5), it has been found that the outer surface of the outer wrapper reaches a maximum temperature of less than 42 ℃, suitably less than 40 ℃ and more suitably less than 38 ℃ or less than 36 ℃ during use.

The various embodiments described herein are intended only to aid in understanding and teaching the claimed features. These embodiments are provided merely as representative samples of embodiments and are not exhaustive and/or exclusive. It is to be understood that advantages, embodiments, examples, functions, features, structures, and/or other aspects described herein are not to be considered limitations on the scope of the invention as defined by the claims or limitations on equivalents to the claims, and that other embodiments may be utilized and modifications may be made without departing from the scope of the invention as claimed. Various embodiments of the present invention may suitably comprise, consist of, or consist essentially of, suitable combinations of the disclosed elements, components, features, components, steps, means, etc., in addition to those specifically described herein. Moreover, this disclosure may include other inventions not presently claimed, but which may be claimed in the future.

Examples

Experiment of

Determination of the content of nicotine and aerosol-forming materials

The amounts of nicotine and aerosol-forming material can be measured using the following methods.

The extraction solution can be prepared as follows. 2.5. + -. 0.01g of n-heptadecane was weighed into a weighing vessel and added to a 5L volumetric flask containing 400-500mL of methanol, and the contents of the volumetric flask were mixed well to dissolve the n-heptadecane. When dissolved, methanol was added to replenish the correct volume of the volumetric flask and form an extraction solution.

Prior to analysis, the aerosol generating material (5-10mm wide pieces) was stored in a sealed plastic bag or an air tight container. The samples were mixed in the bag before use to ensure homogeneity.

Weigh 1.0g (. + -. 0.01g) of the sample into a 150mL Erlenmeyer flask. 1.00mL of deionized water from a calibrated pipette was added and the mixture was left for 5 minutes. 50mL of extraction solution was added with a calibrated dispenser (see above). The flask was stoppered and then shaken on an orbital/horizontal shaker at 150rpm for 3 hours.

Some of the extracts were filtered through a 0.45 μm PVDF filter into 2mL GC vials using a plastic 5mL syringe.

The extracts in the GC vials can then be analyzed using GC (see parameters in the table below) against a working calibration solution that has been previously prepared.

The sample is injected into an injection port connected to an analytical column. Capillary GC columns (phenomenex ZB-WAXplus (30m x 0.53.53 mm id x 1.00 μm)) and Flame Ionization Detectors (FID) can be used for the analysis.

TABLE 1 column parameters

TABLE 2 Inlet/Syringe parameters

	pre-MNPH
		Mode(s)	Without diversion
Temperature (. degree.C.)	270
		Pressure (psi)	5.1
Split ratio	N/A

Flow diversion (mL/min)	N/A
		Total flow (mL/min)	48
Injection volume (μ L)	1
		Gas Saver (Gas Saver)	Opening device

TABLE 3 Detector parameters

	pre-MNPH
		Type (B)	FID
Temperature (. degree.C.)	270
		H₂stream/Ref	30
Air flow (mL/min)	400
		Composition of	Constant
Composition He (mL/min)	15.0
		On/off	Flame opening (Flame On)
Negative polarity	N/A

TABLE 4 oven parameters

Initial temperature	120℃
		Initial time	4min
Rate of temperature rise	20℃/min
		Final temperature	230℃
Final time	2.5min

The final results for nicotine and aerosol-forming material [ CNH (%) (dwb) ] can be expressed as a percentage of the dried sample, corrected for water content using the following equation. The water content can be determined by the Karl Fisher method.

NH: nicotine and/or humectant (propylene glycol and glycerin) analytes

CNH (mg/g): concentration of analyte in mg/g

CNH (%) (dwb): concentration of analyte expressed as% of dry sample

Dwb: dry weight basis (dry weight bases)

C water (%): concentration of water in%

ANH: area of analyte (nicotine, glycerol or propylene glycol)

AISTD: area of internal standard

INT: linear regression y-intercept

And (3) CISTD: concentration of internal standard in extraction solution (mg/mL)

V: volume of extraction solution (mL) +1.00mL deionized Water

D: slope of linear regression

m: quality (g) of total THP reconstituted tobacco (THP recon) used for extraction

The% nicotine target provided herein can be determined by analyzing the nicotine content of a series of samples (e.g., 20-40 samples) and then taking an average.

Determination of the Water content

In the compositions described herein, the% by weight are on a dry weight basis unless specifically indicated to the contrary. Thus, any water that may be present in the tobacco composition or any of its components is completely disregarded for the purpose of determining weight percent. However, other liquid components (such as aerosol-forming materials) are included in the weight%. The moisture content of the tobacco compositions described herein can vary and can be, for example, from 5% to 15% by weight. The water content can be determined by Karl-Fisher analysis.

Water content by Karl-Fisher analysis

Karl Fisher water analysis can be performed on a Mettler Toledo Karl Fisher V30 volumetric titrator. Prior to sample testing, the background water content of the extraction solvent (methanol) was determined and this value was recorded in the analytical method.

Approximately 0.5g of the material to be analyzed is weighed accurately (decimal point 4) into a 100mL Erlenmeyer flask and the weight is recorded. 50mL of dry methanol was dispensed into the Erlenmeyer flask, which was then sealed and stirred on a plate shaker (155rpm) for 30 minutes. Approximately 2mL of sample extract was placed into a syringe and injected into the titration apparatus (weight was determined by post-weighing of the syringe). Results are reported as% moisture by weight of the sample. Samples were assayed in triplicate and the mean reported along with the standard deviation.

Leaf material

Nine blends consisting of leaf material were prepared. The amount of nicotine in each blend by weight of the blend can be determined. The results are shown in tables 5 and 5 a:

TABLE 5

TABLE 5a

Comparative example

Six tobacco reconstituted tobacco materials (reconstituted tobaccos 1-6) comprising Low Nicotine Reconstituted Tobacco (LNRT) and/or Medium Nicotine Reconstituted Tobacco (MNRT) and/or High Nicotine Reconstituted Tobacco (HNRT) were prepared and then analyzed to determine their nicotine content. The results are shown in table 6 and table 6 a.

TABLE 6

It is noted that the nicotine content of the reconstituted tobacco material is less than or equal to 1.5% by weight.

TABLE 6a

Components of reconstituted tobacco material	Reconstituted tobacco 4	Reconstituted tobacco 5	Reconstituted tobacco 6
				LNRT	77.0	0.0	0.0
MNRT	0.0	77.0	0.0
				HNRT	0.0	0.0	76.5
Virginia tobacco leaf	0.0	0.0	0.0
				Burley tobacco leaf	0.0	0.0	0.0
Oriental tobaccoLeaf of Chinese character	0.0	0.0	0.0
				Total amount of tobacco	77.0	77.0	76.5
Wood pulp	8.0	8.0	8.5
				Glycerol in reconstituted tobacco	15.0	15.0	15.0
Additional Glycerol (%)	0.0	0.0	0.0
				Total of	100.0	100.0	100.0

				Target% of nicotine	1.15	1.30	1.50
Additional Glycerol (%)	0.00	0.00	0.00
				Cut Per Inch (CPI)	32	32	32
Net weight of rod (mg)	260	260	260

Rods with a net weight of 340mg were also produced

Examples 1 to 3

Three blends comprising tobacco leaves, Low Nicotine Reconstituted Tobacco (LNRT) and/or Medium Nicotine Reconstituted Tobacco (MNRT) and/or High Nicotine Reconstituted Tobacco (HNRT) were prepared and then analyzed for their nicotine content. The results are shown in Table 7.

TABLE 7

Examples 4 to 21

18 additional blends comprising tobacco leaf and reconstituted tobacco material were prepared and then analyzed for nicotine content. The results are shown in tables 8, 9a, 9b and 9 c.

TABLE 8

Reconstituted tobacco components	Blend	4	Blend 5	Blend 6	Blend 7	Blend 8
							Virginia tobacco grade/LNRC	62.7	31.2	63.5	31.7	61.4
Virginia tobacco grade/MNRC	0.0	0.0	0.0	0.0	0.0
						Virginia tobacco grade/HNRC	0.0	31.2	0.0	31.7	0.0
Virginia tobacco grade/leaf	6.1	6.1	6.2	6.2	6.0
						Burley tobacco grade/leaf	0.0	0.0	0.0	0.0	0.0
Oriental tobacco grade/leaf	10.6	10.6	6.5	6.5	6.3
						DAC levels/leaves	0.0	0.0	0.0	0.0	0.0
DFC and the likeStage/leaf	0.0	0.0	3.1	3.1	6.0
						Total amount of tobacco	79.4	79.2	79.3	79.1	79.6
Wood pulp	6.5	6.7	6.6	6.8	6.4
						Glycerol in reconstituted tobacco	12.1	12.1	12.1	12.1	12.0
Additional Glycerol (%)	2.0	2.0	2.0	2.0	2.0
						Total of	100.0	100.0	100.0	100.0	100.0
Target% of nicotine	1.00	1.25	1.05	1.30	1.15
						Cut Per Inch (CPI)	22	22	22	22	22
Net weight of rod (mg)	260	260	260	260	260

TABLE 9

TABLE 9a

Reconstituted tobacco components	Blend 14	Blend 15
			Virginia tobacco grade/LNRC (%)	0.0	0.0
Virginia tobacco grade/MNRC (%)	0.0	60.4
			Virginia tobacco grade/HNRC (%)	60.0	0.0
Virginia tobacco grade/leaf (%)	19.5	19.6
			Burley tobacco grade/leaf (%)	0.0	0.0
Oriental tobacco grade/leaf (%)	0.0	0.0
			DAC grade/leaf (%)	0.0	0.0
DFC grade/leaf (%)	0.0	0.0
			Tobacco Total (%)	79.5	80.0
Wood pulp (%)	6.2	6.3
			Glycerol in reconstituted tobacco (%)	11.7	11.8
Additional Glycerol (%)	2.0	2.0
			Additional shell (%)	0.6	0
In total (%)	100	100
			Nicotine target (%)	1.75	1.60
Cut Per Inch (CPI)	22	32
			Net weight of rod (mg)	260	260

Rods with a net weight of 340mg were also produced

TABLE 9b

Reconstituted tobacco components	Blend 16	Blend 17	Blend 18
				Virginia tobacco grade/LNRC (%)	0.0	44.1	0.0
Virginia tobacco grade/MNRC (%)	0.0	0.0	44.1
				Virginia tobacco grade/HNRC (%)	44.2	0.0	0.0
Virginia tobacco grade/leaf A (%)	36.1	36.0	36.0
				Burley tobacco grade/leaf A (%)	0.0	0.0	0.0
Oriental tobacco grade/leaf (%)	0.0	0.0	0.0
				DAC grade/leaf (%)	0.0	0.0	0.0
DFC grade/leaf (%)	0.0	0.0	0.0
				Tobacco Total (%)	80.3	80.1	80.1
Wood pulp (%)	4.9	4.9	4.9
				Glycerol in reconstituted tobacco (%)	8.7	8.6	8.6
Additional Glycerol (%)	5.6	5.6	5.6
				Additional shell (%)	0.5	0.8	0.8
In total (%)	100	100	100
				Nicotine target (%)	1.80	1.60	1.15
Cut Per Inch (CPI)	32	22	32
				Net weight of rod (mg)	260	260	260

Rods with a net weight of 340mg were also produced

TABLE 9c

Reconstituted tobacco components	Blend 19	Blend 20	Blend 21
				Virginia tobacco grade/LNRC (%)	0.0	0.0	29.2
Virginia tobacco grade/MNRC (%)	0.0	29.2	0.0
				Virginia tobacco grade/HNRC (%)	29.2	0.0	0.0
Virginia tobacco grade/leaf B (%)	53.7	53.7	53.7
				Burley tobacco grade/leaf (%)	0.0	0.0	0.0
Oriental tobacco grade/leaf (%)	0.0	0.0	0.0
				DAC grade/leaf (%)	0.0	0.0	0.0
DFC grade/leaf (%)	0.0	0.0	0.0
				Tobacco Total (%)	82.9	82.9	82.9
Wood pulp (%)	3.2	3.2	3.2
				Glycerol in reconstituted tobacco (%)	5.7	5.7	5.7
Additional Glycerol (%)	7.4	7.4	7.4
				Additional shell (%)	0.8	0.8	0.8
In total (%)	100	100	100
				Nicotine target (%)	1.95	1.85	1.75
Cut Per Inch (CPI)	32	32	32
				Net weight of rod (mg)	260	260	260

Rods with a net weight of 340mg were also produced

The results show that the nicotine content of the tobacco composition can be customized by combining reconstituted tobacco material with tobacco leaves having a nicotine content of greater than about 1.5% by weight of the tobacco leaves. Thus, a variety of tobacco compositions having a wide range of nicotine concentrations can be manufactured.

Table 10 below shows the temperature of the outer surface of the article 1 described with reference to fig. 4 herein when heated using the apparatus 100 described with reference to fig. 6 to 10B herein. First, second and third temperature measurement probes are used as respective first, second and third locations along the mouthpiece 2 of the article 1. The first position (numbered position 1 in table 10) was spaced from the downstream end 2b of the mouthpiece 2 by 4mm, the second position (numbered position 2 in table 10) was spaced from the downstream end 2b of the mouthpiece 2 by 8mm, and the third position (numbered position 3 in table 10) was spaced from the downstream end 2b of the mouthpiece 2 by 12 mm.

Thus, the first position is located on the outer surface of the portion of the mouthpiece 2 where the first tubular element 4 is provided, while the second and third positions are located on the outer surface of the portion of the mouthpiece 2 where the material body 6 is provided.

The control article was tested for comparison with the filamentary tow tubular member 4 described herein and the filamentary tow tubular member 4 was replaced with a known helically wound paper tube of the same construction as the second hollow tubular member 8 described herein, but 6mm instead of 25mm in length.

The first 5 puffs on the article were tested because by the 5 th puff temperature generally had peaked and began to drop, such that an approximate maximum temperature could be observed. Each sample was tested 5 times and the temperature provided was the average of these 5 tests. The known Health Canada Intense (Health Canada Intense) suction protocol (55 ml suction volume applied every 30 seconds for 2 seconds duration) was applied using standard test equipment.

As shown in the table below, it was surprisingly found that the use of a tubular element 4 formed from a filamentary tow reduces the outer surface temperature of the mouthpiece 2 at each puff and at each test location on the mouthpiece 2 compared to the control article. The tubular element 4 formed by the filamentary tow is particularly effective in reducing the temperature at the first probe location where the lips of the consumer will be positioned when the article 1 is used. In particular, the temperature of the outer surface of the mouthpiece 2 at the first probe position was reduced by more than 7 ℃ in the first three puffs and by more than 5 ℃ in the fourth and fifth puffs.

Watch 10

FIG. 11 illustrates a method of making an article of manufacture for a non-combustible aerosol provision system. In step S101, first and second portions of aerosol generating material (each comprising aerosol forming material) are positioned adjacent respective first and second longitudinal ends of a mouthpiece rod comprising a hollow tubular element rod formed from filamentary tow disposed between the first and second ends. In this embodiment, the hollow tubular element rod comprises a double length first hollow tubular element 4 arranged between respective first and second bodies of material 6. At the outer end of each material body 6 is located a respective second tubular element 8, and the first and second portions of aerosol generating material are located adjacent the outer ends of these second tubular elements 8. The mouthpiece rod is wrapped in a second plug wrap as described herein.

In step S102, first and second portions of aerosol generating material are attached to a mouthpiece rod. In this embodiment, this is done by wrapping tipping paper 5 as described herein around at least a portion of each of the portions of the mouthpiece rod and aerosol-generating material 3. In this embodiment, the tipping paper 5 extends longitudinally for about 5mm over the outer surface of each of the said portions of aerosol-generating material 3.

In step S103, a hollow tubular element stem is cut to form a first article and a second article, each article comprising a mouthpiece comprising a portion of the hollow tubular element stem located at a downstream end of the mouthpiece. In this embodiment, a double length first hollow tubular member 4 of the mouthpiece rod is cut at a location along about half its length to form first and second substantially identical articles.

Claims

1. A tobacco composition comprising a tobacco component and an aerosol-forming material, wherein the tobacco component comprises a tobacco leaf material in an amount between about 10% and about 90% by weight of the tobacco component, and wherein the tobacco leaf material has a nicotine content of greater than 1.5% by weight of the tobacco leaf material.

2. A tobacco composition according to claim 1, wherein the tobacco leaf material comprises the aerosol-forming material in an amount of up to about 10% by weight of the tobacco leaf material.

3. A tobacco composition comprising a tobacco component and an aerosol-forming material, wherein the tobacco component comprises a tobacco leaf material in an amount of between about 10% and about 90% by weight of the tobacco component, and wherein the tobacco leaf material comprises the aerosol-forming material in an amount of up to about 10% by weight of the tobacco leaf material, and wherein the tobacco composition comprises the aerosol-forming material in an amount of between about 10% and about 30% by weight of the tobacco composition.

4. A tobacco composition comprising a tobacco component and an aerosol-forming material, wherein the tobacco component comprises a tobacco leaf material in an amount between about 10% and about 90% by weight of the tobacco component, and wherein the tobacco component comprises menthol in an amount between about 3mg and about 16 mg.

5. A tobacco composition according to any one of claims 1 to 4, wherein the total amount of aerosol-forming material is between about 10% and about 20% by weight of the tobacco composition.

6. The tobacco composition according to any one of claims 1 to 5, wherein the tobacco component comprises tobacco leaf material in an amount between about 11% and about 48%, between about 12% and about 46%, between about 13% and about 44%, between about 14% and about 42%, between about 15% and about 40%, between about 16% and about 38%, between about 17% and about 36%, between about 18% and about 34%, or between about 19% and about 32% by weight of the tobacco component.

7. The tobacco composition according to any one of claims 1 to 6, wherein the tobacco component comprises tobacco leaf material in an amount between about 15% and about 25%, between about 35% and about 45%, or between about 55% and 65% by weight of the tobacco component.

8. The tobacco composition according to any one of claims 1 to 7, wherein the tobacco component has a nicotine content of between 0.8% and 1.75% by weight of the tobacco component.

9. A tobacco composition according to any one of claims 1 to 8, wherein the tobacco leaf material has a nicotine content of greater than about 1.5% and up to about 4% by weight of the tobacco leaf material.

10. A tobacco composition according to any one of claims 1 to 9, wherein the aerosol-forming material is selected from the group consisting of: glycerin, sorbitol, propylene glycol, triethylene glycol, lactic acid, diacetin, triacetin, triethylene glycol diacetate, triethyl citrate, ethyl myristate, isopropyl myristate, methyl stearate, dimethyl dodecanedioate, dimethyl tetradecanedioate, and mixtures thereof.

11. A tobacco composition according to claim 10, wherein the aerosol-forming material comprises glycerine.

12. The tobacco composition of any one of claims 1-11, wherein the tobacco component comprises a paper-process reconstituted tobacco material.

13. The tobacco composition of claim 12, wherein the papermaking reconstituted tobacco material comprises the aerosol-forming material in an amount between about 10% and about 20% by weight of the reconstituted tobacco material.

14. The tobacco composition of claim 12 or 13, wherein the tobacco component comprises a papermaker's reconstituted tobacco material in an amount between about 50% and about 90% by weight of the tobacco component.

15. The tobacco composition of any one of claims 1 to 14, wherein the tobacco component comprises a tobacco material selected from the group consisting of: extruded tobacco, bandcast tobacco, and mixtures thereof.

16. The tobacco composition of any one of claims 1 to 15, wherein the tobacco composition comprises a filler.

17. The tobacco composition of claim 16, wherein the tobacco composition includes between about 5% and about 10% of the filler.

18. The tobacco composition of any one of claims 1 to 17, wherein the tobacco leaf material and/or paper-process reconstituted tobacco material comprises a width of between about 0.5mm and about 2mm, or between about 0.6mm and about 1.75mm, or between about 0.7 and about 1.5 mm.

19. A process of making a tobacco composition according to any one of claims 1 to 18, the process comprising applying the aerosol-forming material to the tobacco leaf material.

20. The method of claim 19, wherein the method comprises combining the tobacco leaf material with a paper-process reconstituted tobacco material comprising an aerosol-forming material in an amount between 10% and 20% by weight of the paper-process reconstituted tobacco material.

21. A tobacco composition prepared by the method of claim 19 or 20.

22. Use of a tobacco composition according to any one of claims 1 to 18 or claim 21 in an article of manufacture for a non-combustible aerosol provision system.

23. An article of manufacture for an aerosol provision system comprising a tobacco composition according to any one of claims 1 to 18 or claim 21.

24. An article according to claim 23, wherein the article for use with an aerosol-generating device comprises a rod of the tobacco composition.

25. The article of claim 24, wherein the rod of tobacco composition has a length of between about 10mm and 100 mm.

26. The article of claim 24 or claim 25, wherein the stem has a total weight of between about 250mg and about 350 mg.

27. The article of any of claims 23 to 26, wherein the tobacco composition is wrapped in a wrapper having a permeability of less than 100Coresta units.

28. The article of any of claims 23-27, wherein the article for use with an aerosol-generating device comprises a reconstituted tobacco material having a density of less than about 700 mg/cc.

29. An article according to any one of claims 23 to 28, wherein the article for use with an aerosol-generating device has an outer perimeter of at least about 19 mm.

30. An article according to any one of claims 23 to 29, wherein the article for use with an aerosol-generating device has an outer perimeter of between about 19mm and about 23 mm.

31. A system comprising the tobacco composition according to any one of claims 1 to 18 or claim 21 and a device arranged to heat the tobacco composition and generate an aerosol from the tobacco composition.

32. A system according to claim 31, wherein the system comprises an article for use with an aerosol-generating device according to any of claims 23 to 30, and wherein the device is arranged to receive at least a portion of the article for use with an aerosol-generating device containing the tobacco composition, and is arranged to heat the portion of the article for use with an aerosol-generating device containing the tobacco composition and to generate the aerosol from the tobacco composition.