CN113802392A - Dyeing method for ecological fiber artistic dyeing and finishing vegetation - Google Patents
Dyeing method for ecological fiber artistic dyeing and finishing vegetation Download PDFInfo
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- CN113802392A CN113802392A CN202111124145.9A CN202111124145A CN113802392A CN 113802392 A CN113802392 A CN 113802392A CN 202111124145 A CN202111124145 A CN 202111124145A CN 113802392 A CN113802392 A CN 113802392A
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Images
Classifications
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/34—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using natural dyestuffs
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P1/00—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed
- D06P1/44—General processes of dyeing or printing textiles, or general processes of dyeing leather, furs, or solid macromolecular substances in any form, classified according to the dyes, pigments, or auxiliary substances employed using insoluble pigments or auxiliary substances, e.g. binders
- D06P1/653—Nitrogen-free carboxylic acids or their salts
- D06P1/6533—Aliphatic, araliphatic or cycloaliphatic
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/02—Material containing basic nitrogen
- D06P3/04—Material containing basic nitrogen containing amide groups
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P3/00—Special processes of dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form, classified according to the material treated
- D06P3/58—Material containing hydroxyl groups
- D06P3/60—Natural or regenerated cellulose
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06P—DYEING OR PRINTING TEXTILES; DYEING LEATHER, FURS OR SOLID MACROMOLECULAR SUBSTANCES IN ANY FORM
- D06P5/00—Other features in dyeing or printing textiles, or dyeing leather, furs, or solid macromolecular substances in any form
- D06P5/12—Reserving parts of the material before dyeing or printing ; Locally decreasing dye affinity by chemical means
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- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Coloring (AREA)
Abstract
The application relates to a dyeing method of ecological fiber art dyeing and finishing vegetation, which comprises the following steps: selecting a fabric and two groups of plant dyes; the method comprises the following steps of (1) abstract tie-dyeing one group of vegetable dyes on a fabric, wherein tie-dyeing comprises a plurality of tie-dyeing process flows, and each tie-dyeing process flow comprises pretreatment, tie-dyeing, soaping, softening and drying; and the other group of plant dyes is injected and dyed on the fabric, wherein the injection dyeing process flow comprises multiple injection dyeing process flows, and each injection dyeing process flow comprises pretreatment, scratching, injection dyeing, steaming, soaping, softening and drying. The method has the advantages that the fabric is subjected to the abstract tie-dyeing and injection-dyeing process steps in sequence, so that the finished fabric can generate a unique dyeing and finishing culture effect visually, the bright characteristic of mutual infiltration and symbiosis of modern dyeing and finishing skills and art creation is realized, and the unique dyeing and finishing culture of product individuation, dyeing and finishing artistry, process differentiation and natural return is realized.
Description
Technical Field
The application belongs to the technical field of dyeing, and particularly relates to a dyeing method for ecological fiber artistic dyeing and finishing of vegetation.
Background
The artistic dyeing and finishing is to inherit the traditional flower binding technique, carry out physical anti-dyeing flower binding by the traditional twisting and dyeing technique such as sewing, twisting, wrapping, clamping and the like, and show or exquisite and realistic visual effect by combining different dyeing techniques such as dipping, hanging, splashing, drawing, spraying and the like; or the grazing effect of hazy gradual change and blending; or a post-modern style of leisure, street art. The application of the method has the distinctive characteristic of mutual infiltration and symbiosis of modern dyeing and finishing skills and art creation, realizes unique dyeing and finishing culture of product individuation, dyeing and finishing artistry and process differentiation, and meets the requirement of era individuation aesthetic.
The vegetation dyeing is a manual technology combined with tie dyeing, green natural fabrics are applied, a vegetation dyeing technology is adopted, the base material is natural and renewable vegetation dye, and the vegetation dyeing is green and environment-friendly and meets the trend of ecological development of textiles. The product dyed by the grass and the wood not only has natural color, but also has strong medicinal value.
In the process of realizing the application, the applicant finds that the dyeing of the artistic dyeing and finishing vegetation solves and breaks through the dyeing method of using chemical dye as a base material in the conventional artistic dyeing and finishing, and the chemical dyeing is not environment-friendly and has harm to human bodies. The tie-dyeing process using the grass wood for dyeing is ecological, environment-friendly and individual, breaks through the traditional manual workshop type operation mode, and realizes industrial application, so that a tie-dyeing process application method of the grass wood dye is urgently needed.
Disclosure of Invention
In order to solve the technical problems in the prior art, the embodiment of the application provides a dyeing method for ecological fiber artistic dyeing and finishing of vegetation. The specific technical scheme is as follows:
in a first aspect, a dyeing method for ecological fiber art dyeing and finishing of grass and wood is provided, which comprises the following steps: selecting a fabric and two groups of plant dyes; the method comprises the following steps of (1) abstract tie-dyeing one group of vegetable dyes on a fabric, wherein tie-dyeing comprises a plurality of tie-dyeing process flows, and each tie-dyeing process flow comprises pretreatment, tie-dyeing, soaping, softening and drying; and the other group of plant dyes is injected and dyed on the fabric, wherein the injection dyeing process flow comprises multiple injection dyeing process flows, and each injection dyeing process flow comprises pretreatment, scratching, injection dyeing, steaming, soaping, softening and drying.
In a first possible implementation manner of the first aspect, the material of the fabric is cellulose fiber or protein fiber; each group of vegetable dyes comprises rose bengal, yellow brown, brilliant yellow, light brown, red brown, brown bean, autumn yellow and watermelon red.
With reference to the first possible implementation manner of the first aspect, in a second possible implementation manner of the first aspect, when the material of the fabric is cellulose fiber, the times of the tie-dyeing process flow and the injection-dyeing process flow are five times, the first and second pretreatments include soaking, modifying and removing, and the third and fifth pretreatments include soaking, pre-dyeing and removing.
With reference to the first possible implementation manner of the first aspect, in a third possible implementation manner of the first aspect, when the material of the fabric is protein fiber, the times of the tie-dyeing process flow and the injection-dyeing process flow are five times, the pretreatment in the first and second tie-dyeing process flows includes soaking and dewatering, and the pretreatment in the third and fifth tie-dyeing process flows includes soaking, priming and dewatering.
With reference to the second or third possible implementation manner of the first aspect, in a fourth possible implementation manner of the first aspect, while soaking in water, the fabric is rinsed with 2g/L of a scouring agent, 5g/L of oxalic acid, 80 ℃ x 30min, and then soaked in soft water.
With reference to the second possible implementation manner of the first aspect, in a fifth possible implementation manner of the first aspect, during modification, the modifier BS 10% and the bath ratio are 1:30, after the low-temperature heat preservation is performed for 5-10min, the temperature is raised to 80 ℃ at a rate of 1.5 ℃/min, the temperature is increased by 80 ℃ for 30min, and the residual liquid is discharged after the temperature is reduced.
With reference to the third possible implementation manner of the first aspect, in a sixth possible implementation manner of the first aspect, in the pre-medium process, 10% of mordant alum is used, the bath ratio is 1:30, after the temperature is kept at the low temperature for 5-10min, the temperature is raised to 80 ℃ at the speed of 1.5 ℃/min, the temperature is increased to 80 ℃ for 30min, and the residual liquid is discharged after the temperature is lowered.
In a seventh possible implementation manner of the first aspect, during soaping, an acidic or neutral soaping agent at 50-60 ℃ is selected and washed for 10min to remove loose color.
In an eighth possible implementation manner of the first aspect, during dyeing, 0.1-5% of dye to the weight of the fabric is configured, the bath ratio is 1:30, the pH value of the dye is adjusted, the temperature is kept at a low temperature for 5-10min, then the temperature is raised to 80-95 ℃ at the speed of 1.5 ℃/min, if the use amount of the color is more than 3, the dyeing time is prolonged to 60min, then the temperature is reduced after the color is matched, residual liquid is discharged, the washing is omitted, and water is fed.
In a ninth possible implementation manner of the first aspect, during injection dyeing, 0.1-5% of dye is prepared, the pH value of the dye is adjusted, after injection dyeing, the temperature is raised to 80-95 ℃ at a rate of 5 ℃/min, if the usage amount of the dye is more than 3, the steaming time is prolonged to 60min, and then the dye is taken out of a cylinder, washed once and fed with water.
Compared with the prior art, the application has the advantages that:
the dyeing method for the ecological fiber artistic dyeing and finishing of the grass and the wood mainly applies the technological methods of garland, rope twisting, bundle protection, injection dyeing and the like, and the dyeing process selects the additives such as a modifier, a mordant and the like according to different fabric components and different natural dye varieties. In the experiment, different fabric components, different dyeing temperatures and different dyeing times matched with natural dyes and different pH values of dye liquor are forcibly adjusted, so that the dyeing uniformity and the repeatability are improved, and the industrial application of the tie-dyeing process with the natural fabric as a carrier and the natural dyes as raw materials is completed. Meanwhile, the fabric dyed and finished by the ecological fiber artistic dyeing and finishing vegetation dyeing method generates a unique dyeing and finishing culture effect visually, has the bright characteristic of mutual infiltration and symbiosis of modern dyeing and finishing skills and artistic creation, and realizes unique dyeing and finishing culture with product individuation, dyeing and finishing artistry, process differentiation and natural return.
Drawings
In order to more clearly illustrate the technical solutions in the embodiments of the present application, the drawings needed to be used in the description of the embodiments are briefly introduced below, and it is obvious that the drawings in the following description are only some embodiments of the present application, and it is obvious for those skilled in the art to obtain other drawings based on these drawings without creative efforts.
Fig. 1 is a schematic flow chart illustrating steps of a dyeing method for ecological fiber art dyeing and finishing vegetation according to an embodiment of the present application.
Detailed Description
To make the objects, technical solutions and advantages of the present application more clear, embodiments of the present application will be described in further detail below with reference to the accompanying drawings.
Please refer to fig. 1, which shows a schematic flow chart of steps of a dyeing method for ecological fiber art dyeing and finishing vegetation according to an embodiment of the present application. The dyeing method 1 for ecological fiber artistic dyeing and finishing vegetation comprises the following steps 101 to 103. In step 101, a dyeing and finishing material is selected. Selecting a fabric and two groups of plant dyes. The fabric is made of cellulose fibers or protein fibers; each group of vegetable dyes comprises rose bengal, yellow brown, brilliant yellow, light brown, red brown, brown bean, autumn yellow and watermelon red.
Next, in step 102, the fabric is abstract banddyed. And (2) performing abstract tie-dyeing on the fabric by using one group of vegetable dyes, wherein the tie-dyeing process comprises a plurality of tie-dyeing process flows, and each tie-dyeing process flow comprises pretreatment, tie-dyeing, soaping, softening and drying. Finally, in step 103, the fabric is injection dyed. And the other group of plant dyes is injected and dyed on the fabric, wherein the injection dyeing process flow comprises multiple injection dyeing process flows, and each injection dyeing process flow comprises pretreatment, scratching, injection dyeing, steaming, soaping, softening and drying.
The ecological fiber art dyeing and finishing vegetation dyeing method 1 of the embodiment can realize that the finished fabric generates a unique dyeing and finishing culture effect visually by sequentially carrying out the abstract tie dyeing and injection dyeing process steps on the fabric, has the vivid characteristic of mutual infiltration and symbiosis of modern dyeing and finishing skills and art creation, and realizes unique dyeing and finishing culture of product individuation, dyeing and finishing artistry, process differentiation and natural return.
The following will use the application steps of the ecological fiber art dyeing and finishing vegetation dyeing and finishing method 1 in practical production in example 1 and example 2 to further illustrate the beneficial effects of the ecological fiber art dyeing and finishing vegetation dyeing and finishing method in the present application.
Example 1
1. Selecting raw materials:the fabric is cellulose fiber, and each group of vegetable dye comprises: 0001 rose red, 0002 yellow brown, 0003 bright yellow, 0005 light brown, 0006 red brown, 0007 bean paste, 0008 watermelon red, 0009 autumn yellow.
2. Abstract tie-dyeing:the method adopts the flower tying methods of disorder, spiral, twisting, tying, rope twisting, tying plus rope twisting, tying section protection, rolling and tying, clamping and the like, represents various abstract and changeable complex composition effects, is novel and unique, and comprises the following steps 2.1 to 2.5, and the concrete steps are as follows:
2.1 plant dye selection: 0001 rose, 0002 yellow brown, 0003 bright yellow and 0005 light brown.
2.1.1 technological process: soaking in water → modifying → washing → bundling flower → dyeing → soaping → softening → drying.
2.1.2 Process recipe and considerations
1. Soaking in water (2 g/L of scouring agent, 5g/L of oxalic acid, treatment at 80 ℃ for 30min, and modification after two times of elimination).
2. Modification: 10% of modifier BS (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. And (5) binding flowers.
5. Dyeing: dye (weight to fabric) 0.1-5%, bath ratio: 1:30, 1g/L acetic acid, adjusting the pH value to 5-6, keeping the temperature at low temperature for 5-10min, then heating to 95 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 95 ℃, and if the amount of the dye is more than 3, prolonging the dyeing time to 60 min. After color matching, the temperature is reduced (the temperature reduction cannot be too fast), and residual liquid is discharged, so that the washing is eliminated once, and water is fed. (when acetic acid is used to adjust the pH, the amount of acetic acid is determined according to the water quality, and 0.15g/L citric acid is recommended to replace acetic acid because citric acid is stable and is not easy to volatilize at high temperature).
6. Soaping: removing net loose color (acid or neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
7. Description of the operation: diluting modifier with 3 times of water, stirring, adding acetic acid (25-30 times of dilution) during dyeing, running for 5 min, adding dye (the dye is dissolved in a chemical material barrel with 50 times of 80 deg.C hot water, and filtering).
2.2 plant dye selection: 0006 red brown, 0007 bean paste color and 0009 autumn yellow.
2.2.1 technological process: soaking in water → modifying → washing → bundling flower → dyeing → soaping → softening → drying.
2.2.2 Process recipe and notes
1. Soaking in water.
2. Modification: 10% of modifier BS (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. And (5) binding flowers.
5. Dyeing: dye (weight to fabric) 0.1-5%, bath ratio: 1:30, 1g/L of soda ash, adjusting the pH value to 7-8, keeping the temperature at low temperature for 5-10min, then heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, and if the amount of the used soda is more than 3, prolonging the dyeing time to 60 min. After color matching, the temperature is reduced (the temperature reduction cannot be too fast), and residual liquid is discharged, so that the washing is eliminated once, and water is fed.
6. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
7. Description of the operation: diluting the modifier with 3 times of water, uniformly stirring, adding soda (dissolved and uniformly stirred with 25-30 times of water in advance) during dyeing, running for 5 minutes, adding the dye (the dye is fully dissolved in a material dissolving barrel with 50 times of hot water at 80 ℃ in advance, and filtering, when 0007 bean paste is dyed, using 0.5-1g/L of soda as the material dissolving aid of the material dissolving water, wherein the amount of the soda is specifically determined according to the amount of the dye and the material dissolving water, because the alkali resistance of the plant dye is limited, the amount of the soda cannot be high, and the amount of the plant residue liquid is more when 0007 bean paste is filtered).
2.3 plant dye selection: 0008 watermelon red.
2.3.1 technological process: soaking water → pre-medium → washing in jig → bundling flower → dyeing → soaping → softening → drying.
2.3.2 Process recipe and notes
1. Soaking in water.
2. Pre-medium: 10% of mordant alum (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. And (5) binding flowers.
5. Dyeing: acid dyeing: dye (weight to fabric) 0.1-5%, bath ratio: 1:30, 1g/L acetic acid, adjusting the PH to 5-6, keeping the temperature at low temperature for 10min, then heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, and if the amount of the dye is more than 3, prolonging the dyeing time to 60 min. After color matching, the temperature is reduced (the temperature reduction cannot be too fast), and residual liquid is discharged, so that the washing is eliminated once, and water is fed. (when acetic acid is used to adjust the pH, the amount of acetic acid is determined according to the water quality, and 0.15g/L citric acid is recommended to replace acetic acid because citric acid is stable and is not easy to volatilize at high temperature). During dyeing, the dye liquor is golden yellow under acidic conditions and obviously flocculent, which is a normal phenomenon. The hue of the dye changes greatly along with the rise of the temperature in the dyeing temperature rise process, and the dye is easy to color, so the temperature rise process is necessarily slow, especially the temperature rise is slow at 40-70 ℃.
6. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
7. Description of the operation: the mordant alum is dissolved in hot water of 25-30 times and 80 ℃, filtered and added into a jar (chemical name of alum is aluminum potassium sulfate, and the water solution is acidic). Adding auxiliary agent (dissolved and stirred uniformly by 25-30 times of water in advance) according to the process during dyeing, running for 5 minutes, adding dye (the dye is fully dissolved by 50 times of 80 ℃ hot water in a material dissolving barrel in advance and filtered, when 0008 watermelon red material is dissolved by 0.5-1g/L of soda ash of material dissolving water, the amount of soda ash is determined by the amount of the dye and the material dissolving water, because plant dye has limited alkali resistance, the amount of soda ash cannot be high, the solution of 0008 watermelon red added with soda is purple red, and more plant residue liquid is obtained during filtering).
2.4 plant dye selection: 0008 watermelon red.
2.4.1 technological process: soaking water → pre-medium → washing in jig → bundling flower → dyeing → soaping → softening → drying.
2.4.2 Process recipe and notes
1. Soaking in water.
2. Pre-medium: 10% of mordant alum (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. And (5) binding flowers.
5. Dyeing: alkaline dyeing: dye (weight to fabric) 0.1-5%, bath ratio: 1:30, 1g/L of soda ash, adjusting the pH value to 7-8, keeping the temperature at a low temperature for 10min, then heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, and if the amount of the used color is more than 3, prolonging the dyeing time to 60 min. After color matching, the temperature is reduced (the temperature reduction cannot be too fast), and residual liquid is discharged, so that the washing is eliminated once, and water is fed. (the color phase changes greatly with the rise of temperature in the dyeing temperature rise process, so that the dyeing is easy to flower, so the temperature rise process is slow, especially the temperature rise is slow at 40-70 ℃).
6. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
7. Description of the operation: the mordant alum is dissolved in hot water of 25-30 times and 80 ℃, filtered and added into a jar (chemical name of alum is aluminum potassium sulfate, and the water solution is acidic). Adding auxiliary agent (dissolved and stirred uniformly by 25-30 times of water in advance) according to the process during dyeing, running for 5 minutes, adding dye (the dye is fully dissolved by 50 times of 80 ℃ hot water in a material dissolving barrel in advance and filtered, when 0008 watermelon red material is dissolved by 0.5-1g/L of soda ash of material dissolving water, the amount of soda ash is determined by the amount of the dye and the material dissolving water, because plant dye has limited alkali resistance, the amount of soda ash cannot be high, the solution of 0008 watermelon red added with soda is purple red, and more plant residue liquid is obtained during filtering).
2.5 plant dye selection: 0008 watermelon red.
2.5.1 technological process: soaking water → pre-medium → washing in jig → bundling flower → dyeing → soaping → softening → drying.
2.5.2 Process recipe and notes
1. Soaking in water.
2. Pre-medium: 10% of mordant alum (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. And (5) binding flowers.
5. Dyeing: neutral dyeing: dye (weight to fabric) 0.1-5%, bath ratio: 1:30, keeping the temperature at the low temperature for 10min, then heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying the temperature by 80 ℃ for 30min, and if the use amount of the dye is more than 3, prolonging the dyeing time to 60 min. After color matching, the temperature is reduced (the temperature reduction cannot be too fast), and residual liquid is discharged, so that the washing is eliminated once, and water is fed. (the color phase changes greatly with the rise of temperature in the dyeing temperature rise process, so that the dyeing is easy to flower, so the temperature rise process is slow, especially the temperature rise is slow at 40-70 ℃).
6. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
7. Description of the operation: the mordant alum is dissolved in hot water of 25-30 times and 80 ℃, filtered and added into a jar (chemical name of alum is aluminum potassium sulfate, and the water solution is acidic). Adding auxiliary agent (dissolved and stirred uniformly by 25-30 times of water in advance) according to the process during dyeing, running for 5 minutes, adding dye (the dye is fully dissolved by 50 times of 80 ℃ hot water in a material dissolving barrel in advance and filtered, when 0008 watermelon red material is dissolved by 0.5-1g/L of soda ash of material dissolving water, the amount of soda ash is determined by the amount of the dye and the material dissolving water, because plant dye has limited alkali resistance, the amount of soda ash cannot be high, the solution of 0008 watermelon red added with soda is purple red, and more plant residue liquid is obtained during filtering).
3. And (3) injection dyeing:the method adopts the flower tying methods of disorder, spiral, twisting, tying, rope twisting, tying plus rope twisting, tying section protection, rolling and tying, clamping and the like, represents various abstract and changeable complex composition effects, is novel and unique, and comprises the following steps 3.1 to 3.5, and the specific steps are as follows:
3.1 plant dye selection: 0001 rose, 0002 yellow brown, 0003 bright yellow and 0005 light brown.
3.1.1 Process flow: soaking in water → modifying → washing → grabbing flower → injecting and dyeing → steaming → soaping → softening → drying.
3.1.2 Process recipe and notes
1. Soaking in water (2 g/L of scouring agent, 5g/L of oxalic acid, treatment at 80 ℃ for 30min, and modification after two times of elimination).
2. Modification: 10% of modifier BS (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. And (5) grabbing the flowers.
5. And (3) injection dyeing: 0.1-5% of dye (by weight of water) and 1g/L of acetic acid, adjusting the pH value to 5-6, after injection dyeing, raising the temperature to 95 ℃ at the speed of 5 ℃/min, multiplying 30min at 95 ℃, and if the consumption of the dye is more than 3, prolonging the steaming time to 60 min. (when the pH value is adjusted by using acetic acid, the dosage of the acetic acid is determined according to the water quality, and the citric acid is stable and is not easy to volatilize at high temperature, 0.15g/L of citric acid is recommended to be used for replacing the acetic acid) and is taken out of the cylinder, and the acetic acid is eliminated and washed once and then is fed with water.
6. Soaping: removing net loose color (acid or neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
7. Description of the operation: diluting modifier with 3 times of water, stirring, adding acetic acid (25-30 times of dilution) during dyeing, running for 5 min, adding dye (the dye is dissolved in a chemical material barrel with 50 times of 80 deg.C hot water, and filtering).
3.2 plant dye selection: 0006 red brown, 0007 bean paste color and 0009 autumn yellow.
3.2.1 Process flow: soaking in water → modifying → washing → grabbing flower → injecting and dyeing → steaming → soaping → softening → drying.
3.2.2 Process recipe and notes
1. Soaking in water (2 g/L of scouring agent, 5g/L of oxalic acid, treatment at 80 ℃ for 30min, and modification after two times of elimination).
2. Modification: 10% of modifier BS (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. And (5) grabbing the flowers.
5. And (3) injection dyeing: dye (weight to fabric) 0.1-5%, bath ratio: 1:30, 1g/L of soda, adjusting the PH to be 7-8, after injection dyeing, heating to 80 ℃ at the speed of 5 ℃/min, and multiplying 30min at 80 ℃, and if the consumption of the color is more than 3, prolonging the steaming time to 60 min. Taking out of the tank, eliminating and washing once, and feeding water.
6. Soaping: removing net floating color (acid or neutral soaping agent for soaping agent) at 50-60 deg.C for 10min
7. Description of the operation: diluting modifier with 3 times of water, stirring, adding acetic acid (25-30 times of dilution) during dyeing, running for 5 min, adding dye (the dye is dissolved in a chemical material barrel with 50 times of 80 deg.C hot water, and filtering).
3.3 plant dye selection: 0008 watermelon red.
3.3.1 Process flow: soaking water → pre-medium → washing → grabbing flower → injecting dye → steaming → soaping → softening → drying.
3.3.2 Process recipe and notes
1. Soaking in water.
2. Pre-medium: 10% of mordant alum (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. And (5) grabbing the flowers.
5. And (3) injection dyeing: acid injection dyeing: 0.1-5% of dye (for fabric weight) and 1g/L of acetic acid, adjusting the pH value to 5-6, after injection dyeing, raising the temperature to 80 ℃ at the speed of 5 ℃/min, and multiplying 30min at 80 ℃, and if the consumption of the dye is more than 3, prolonging the steaming time to 60 min. Taking out of the tank, eliminating and washing once, and feeding water. (when acetic acid is used to adjust the pH, the amount of acetic acid is determined according to the water quality, and 0.15g/L citric acid is recommended to replace acetic acid because citric acid is stable and is not easy to volatilize at high temperature). And (3) injecting a dye solution, wherein the dye solution is golden yellow under an acidic condition and is obviously flocculent, and the phenomenon is normal.
6. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
7. Description of the operation: the mordant alum is dissolved in hot water of 25-30 times and 80 ℃, filtered and added into a jar (chemical name of alum is aluminum potassium sulfate, and the water solution is acidic). (the dye is fully dissolved in a material dissolving barrel by 50 times of hot water with the temperature of 80 ℃ in advance, and is filtered, when 0008 watermelon red material is dissolved, the material is dissolved by 0.5-1g/L of material dissolving water, the amount of the calcined soda is specifically determined according to the amount of the dye and the material dissolving water, because the alkali resistance of the plant dye is limited, the amount of the calcined soda cannot be high, the solution of 0008 watermelon red after adding the alkali is purple red, and more plant slag liquid is obtained during filtering).
3.4 plant dye selection: 0008 watermelon red.
3.4.1 Process flow: soaking water → pre-medium → washing → grabbing flower → injecting dye → steaming → soaping → softening → drying.
3.4.2 formula and notes
1. Soaking in water.
2. Pre-medium: 10% of mordant alum (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. And (5) grabbing the flowers.
5. And (3) injection dyeing: alkaline dyeing: 0.1-5% of dye (for fabric weight) and 1g/L of soda, adjusting the pH value to 7-8, after injection dyeing, raising the temperature to 80 ℃ at the speed of 5 ℃/min, multiplying 30min at 80 ℃, and if the dosage of the color is more than 3, prolonging the steaming time to 60 min. Taking out of the tank, eliminating and washing once, and feeding water.
6. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10min
7. Description of the operation: the mordant alum is dissolved in hot water of 25-30 times and 80 ℃, filtered and added into a jar (chemical name of alum is aluminum potassium sulfate, and the water solution is acidic). (the dye is fully dissolved in a material dissolving barrel by 50 times of hot water with the temperature of 80 ℃ in advance, and is filtered, when 0008 watermelon red material is dissolved, the material is dissolved by 0.5-1g/L of material dissolving water, the amount of the calcined soda is specifically determined according to the amount of the dye and the material dissolving water, because the alkali resistance of the plant dye is limited, the amount of the calcined soda cannot be high, the solution of 0008 watermelon red after adding the alkali is purple red, and more plant slag liquid is obtained during filtering).
3.5 plant dye selection: 0008 watermelon red.
3.5.1 Process flow: soaking water → pre-medium → washing → grabbing flower → injecting dye → steaming → soaping → softening → drying.
3.5.2 Process recipe and notes
1. Soaking in water.
2. Pre-medium: 10% of mordant alum (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. And (5) grabbing the flowers.
5. And (3) injection dyeing: neutral dyeing: 0.1-5% dye (for fabric weight), after injection dyeing, heating to 80 deg.C at 5 deg.C/min, and 30min at 80 deg.C, if the amount of dye is greater than 3, steaming for 60 min. Taking out of the tank, eliminating and washing once, and feeding water.
6. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10min
7. Description of the operation: the mordant alum is dissolved in hot water of 25-30 times and 80 ℃, filtered and added into a jar (chemical name of alum is aluminum potassium sulfate, and the water solution is acidic). (the dye is fully dissolved in a material dissolving barrel by 50 times of hot water with the temperature of 80 ℃ in advance, and is filtered, when 0008 watermelon red material is dissolved, the material is dissolved by 0.5-1g/L of material dissolving water, the amount of the calcined soda is specifically determined according to the amount of the dye and the material dissolving water, because the alkali resistance of the plant dye is limited, the amount of the calcined soda cannot be high, the solution of 0008 watermelon red after adding the alkali is purple red, and more plant slag liquid is obtained during filtering).
Example 2
1. Selecting raw materials:the fabric is protein fiber, and each group of vegetable dye comprises: 0001 rose red, 0002 yellow brown, 0003 bright yellow, 0005 light brown, 0006 red brown, 0007 bean paste, 0008 watermelon red, 0009 autumn yellow.
2. Abstract tie-dyeing:the flower tying method of disorder, spiral, twisting, tying, rope twisting, tying plus rope twisting, tying segment protection, rolling and tying, clamping and the like is adopted. The method represents various abstract and changeable complex composition effects, and is novel and unique. The abstract tie-dyeing method comprises the following steps 2.1 to 2.5, and comprises the following specific steps:
2.1 plant dye selection: 0001 rose, 0002 yellow brown, 0003 bright yellow and 0005 light brown.
2.1.1 technological process: soaking water → dewatering → bundling → dyeing → soaping → softening → drying.
2.1.2 Process recipe and considerations
1. Soaking in water.
2. Dyeing: dye (weight to fabric) 0.1-5%, bath ratio: 1:30, 1g/L acetic acid, adjusting the pH value to 5-6, keeping the temperature at low temperature for 5-10min, then heating to 95 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 95 ℃, and if the amount of the dye is more than 3, prolonging the dyeing time to 60 min. After color matching, the temperature is reduced (the temperature reduction cannot be too fast), and residual liquid is discharged, so that the washing is eliminated once, and water is fed. (when acetic acid is used to adjust the pH, the amount of acetic acid is determined according to the water quality, and 0.15g/L citric acid is recommended to replace acetic acid because citric acid is stable and is not easy to volatilize at high temperature).
3. Soaping: removing net loose color (acid or neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
4. Description of the operation: adding acetic acid (diluted by 25-30 times) during dyeing, running for 5 min, adding dye (the dye is dissolved in 50 times of 80 deg.C hot water in a material barrel in advance, and filtering).
2.2 plant dye selection: 0006 red brown, 0007 bean paste color and 0009 autumn yellow.
2.2.1 technological process: soaking water → dewatering → bundling → dyeing → soaping → softening → drying.
1.1.2.2 formula and notes
1. Soaking water
2. Dyeing: dye (weight to fabric) 0.1-5%, bath ratio: 1:30, 1g/L acetic acid, adjusting the pH value to 5-6, keeping the temperature at low temperature for 5-10min, then heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, and if the amount of the dye is more than 3, prolonging the dyeing time to 60 min. After color matching, the temperature is reduced (the temperature reduction cannot be too fast), and residual liquid is discharged, so that the washing is eliminated once, and water is fed. (when acetic acid is used to adjust the pH, the amount of acetic acid is determined according to the water quality, and 0.15g/L citric acid is recommended to replace acetic acid because citric acid is stable and is not easy to volatilize at high temperature).
3. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
4. Description of the operation: adding acetic acid (diluted by 25-30 times) during dyeing, running for 5 min, adding dye (the dye is dissolved in 50 times of 80 deg.C hot water in a material barrel, and filtering.
2.3 plant dye selection: 0008 watermelon red
2.3.1 technological process: soaking water → premedium → dehydration → bundling flower → dyeing → soaping → softening → drying.
2.3.2 Process recipe and notes
1. Soaking in water.
2. Pre-medium: 10% of mordant alum (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. Dyeing: acid dyeing: dye (weight to fabric) 0.1-5%, bath ratio: 1:30, 1g/L acetic acid, adjusting the PH to 5-6, keeping the temperature at low temperature for 10min, then heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, and if the amount of the dye is more than 3, prolonging the dyeing time to 60 min. After color matching, the temperature is reduced (the temperature reduction cannot be too fast), and residual liquid is discharged, so that the washing is eliminated once, and water is fed. (when acetic acid is used to adjust the pH, the amount of acetic acid is determined according to the water quality, and 0.15g/L citric acid is recommended to replace acetic acid because citric acid is stable and is not easy to volatilize at high temperature). During dyeing, the dye liquor is golden yellow under acidic conditions and obviously flocculent, which is a normal phenomenon. The hue of the dye changes greatly along with the rise of the temperature in the dyeing temperature rise process, and the dye is easy to color, so the temperature rise process is necessarily slow, especially the temperature rise is slow at 40-70 ℃.
5. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
6. Description of the operation: the mordant alum is dissolved in hot water of 25-30 times and 80 ℃, filtered and added into a jar (chemical name of alum is aluminum potassium sulfate, and the water solution is acidic). Adding auxiliary agent (dissolved and stirred uniformly by 25-30 times of water in advance) according to the process during dyeing, running for 5 minutes, adding dye (the dye is fully dissolved by 50 times of 80 ℃ hot water in a material dissolving barrel in advance and filtered, when 0008 watermelon red material is dissolved by 0.5-1g/L of soda ash of material dissolving water, the amount of soda ash is determined by the amount of the dye and the material dissolving water, because plant dye has limited alkali resistance, the amount of soda ash cannot be high, the solution of 0008 watermelon red added with soda is purple red, and more plant residue liquid is obtained during filtering).
2.4 plant dye selection: 0008 watermelon red.
2.4.1 technological process: soaking water → premedium → dehydration → bundling flower → dyeing → soaping → softening → drying.
2.4.2 Process recipe and notes
1. Soaking in water.
2. Pre-medium: 10% of mordant alum (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. Dyeing: alkaline dyeing: dye (weight to fabric) 0.1-5%, bath ratio: 1:30, 1g/L of soda ash, adjusting the pH value to 7-8, keeping the temperature at a low temperature for 10min, then heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, and if the amount of the used color is more than 3, prolonging the dyeing time to 60 min. After color matching, the temperature is reduced (the temperature reduction cannot be too fast), and residual liquid is discharged, so that the washing is eliminated once, and water is fed. (in the dyeing temperature rise process, the hue changes greatly along with the rise of the temperature, so the dyeing is easy to flower, so the temperature rise process is necessarily slow, especially the temperature rise is slow at 40-70 ℃), and the dyeing is carried out under the alkaline condition as far as possible.
5. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
6. Description of the operation: the mordant alum is dissolved in hot water of 25-30 times and 80 ℃, filtered and added into a jar (chemical name of alum is aluminum potassium sulfate, and the water solution is acidic). Adding auxiliary agent (dissolved and stirred uniformly by 25-30 times of water in advance) according to the process during dyeing, running for 5 minutes, adding dye (the dye is fully dissolved by 50 times of 80 ℃ hot water in a material dissolving barrel in advance and filtered, when 0008 watermelon red material is dissolved by 0.5-1g/L of soda ash of material dissolving water, the amount of soda ash is determined by the amount of the dye and the material dissolving water, because plant dye has limited alkali resistance, the amount of soda ash cannot be high, the solution of 0008 watermelon red added with soda is purple red, and more plant residue liquid is obtained during filtering).
2.5 plant dye selection: 0008 watermelon red.
2.5.1 technological process: soaking water → premedium → dehydration → bundling flower → dyeing → soaping → softening → drying.
2.5.2 Process recipe and notes
1. Soaking in water.
2. Pre-medium: 10% of mordant alum (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. Dyeing: neutral dyeing: dye (weight to fabric) 0.1-5%, bath ratio: 1:30, keeping the temperature at the low temperature for 10min, then heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying the temperature by 80 ℃ for 30min, and if the use amount of the dye is more than 3, prolonging the dyeing time to 60 min. After color matching, the temperature is reduced (the temperature reduction cannot be too fast), and residual liquid is discharged, so that the washing is eliminated once, and water is fed. (the color phase changes greatly with the rise of temperature in the dyeing temperature rise process, so that the dyeing is easy to flower, so the temperature rise process is slow, especially the temperature rise is slow at 40-70 ℃).
5. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
6. Description of the operation: the mordant alum is dissolved in hot water of 25-30 times and 80 ℃, filtered and added into a jar (chemical name of alum is aluminum potassium sulfate, and the water solution is acidic). Adding auxiliary agent (dissolved and stirred uniformly by 25-30 times of water in advance) according to the process during dyeing, running for 5 minutes, adding dye (the dye is fully dissolved by 50 times of 80 ℃ hot water in a material dissolving barrel in advance and filtered, when 0008 watermelon red material is dissolved by 0.5-1g/L of soda ash of material dissolving water, the amount of soda ash is determined by the amount of the dye and the material dissolving water, because plant dye has limited alkali resistance, the amount of soda ash cannot be high, the solution of 0008 watermelon red added with soda is purple red, and more plant residue liquid is obtained during filtering).
3. And (3) injection dyeing:patterns with various effects are formed by manually coloring the colorful colors on the clothes according to certain effects, wherein the colors are left white or crossed. The pattern has free and running pattern form, strong rhythm sense, extremely high visual impact force and unique artistic dyeing and finishing visual aesthetic style. The injection dyeing comprises the following steps 3.1 to 3.5, and the specific steps are as follows:
3.1 plant dye selection: 0001 rose, 0002 yellow brown, 0003 bright yellow and 0005 light brown.
3.1, a process flow: soaking water → grabbing flowers → injecting and dyeing → steaming → soaping → softening → drying.
3.1.2 Process recipe and notes
1. Soaking in water (2 g/L of scouring agent, 5g/L of oxalic acid, treatment at 80 ℃ for 30min, and modification after two times of elimination).
2. And (5) grabbing the flowers.
3. And (3) injection dyeing: 0.1-5% of dye (by weight of water) and 1g/L of acetic acid, adjusting the pH value to 5-6, after injection dyeing, raising the temperature to 95 ℃ at the speed of 5 ℃/min, multiplying 30min at 95 ℃, and if the consumption of the dye is more than 3, prolonging the steaming time to 60 min. (when the pH value is adjusted by using acetic acid, the dosage of the acetic acid is determined according to the water quality, and the citric acid is stable and is not easy to volatilize at high temperature, 0.15g/L of citric acid is recommended to be used for replacing the acetic acid) and is taken out of the cylinder, and the acetic acid is eliminated and washed once and then is fed with water.
4. Soaping: removing net loose color (acid or neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
3.2 plant dye selection: 0006 red brown, 0007 bean paste color and 0009 autumn yellow.
3.2.1 Process flow: soaking water → grabbing flowers → injecting and dyeing → steaming → soaping → softening → drying.
3.2.2 Process recipe and notes
1. Soaking in water (2 g/L of scouring agent, 5g/L of oxalic acid, treatment at 80 ℃ for 30min, and modification after two times of elimination).
2. And (5) grabbing the flowers.
3. And (3) injection dyeing: 0.1-5% of dye (for fabric weight) and 1g/L of acetic acid, adjusting the pH value to 5-6, after injection dyeing, raising the temperature to 80 ℃ at the speed of 5 ℃/min, and multiplying 30min at 80 ℃, and if the consumption of the dye is more than 3, prolonging the steaming time to 60 min. Taking out of the tank, eliminating and washing once, and feeding water. (when acetic acid is used to adjust the pH, the amount of acetic acid is determined according to the water quality, and 0.15g/L citric acid is recommended to replace acetic acid because citric acid is stable and is not easy to volatilize at high temperature).
6. Soaping: removing net loose color (acid or neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
3.3 plant dye selection: 0008 watermelon red.
3.3.1 Process flow: soaking water → pre-medium → washing → grabbing flower → injecting dye → steaming → soaping → softening → drying.
3.3.2 Process recipe and notes
1. Soaking in water.
2. Pre-medium: 10% of mordant alum (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. And (5) grabbing the flowers.
5. And (3) injection dyeing: acid injection dyeing: 0.1-5% of dye (for fabric weight) and 1g/L of acetic acid, adjusting the pH value to 5-6, after injection dyeing, raising the temperature to 80 ℃ at the speed of 5 ℃/min, and multiplying 30min at 80 ℃, and if the consumption of the dye is more than 3, prolonging the steaming time to 60 min. Taking out of the tank, eliminating and washing once, and feeding water. (when acetic acid is used to adjust the pH, the amount of acetic acid is determined according to the water quality, and 0.15g/L citric acid is recommended to replace acetic acid because citric acid is stable and is not easy to volatilize at high temperature). And (3) injecting a dye solution, wherein the dye solution is golden yellow under an acidic condition and is obviously flocculent, and the phenomenon is normal.
6. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
7. Description of the operation: the mordant alum is dissolved in hot water of 25-30 times and 80 ℃, filtered and added into a jar (chemical name of alum is aluminum potassium sulfate, and the water solution is acidic). (the dye is fully dissolved in a material dissolving barrel by 50 times of hot water with the temperature of 80 ℃ in advance, and is filtered, when 0008 watermelon red material is dissolved, the material is dissolved by 0.5-1g/L of material dissolving water, the amount of the calcined soda is specifically determined according to the amount of the dye and the material dissolving water, because the alkali resistance of the plant dye is limited, the amount of the calcined soda cannot be high, the solution of 0008 watermelon red after adding the alkali is purple red, and more plant slag liquid is obtained during filtering).
3.4 plant dye selection: 0008 watermelon red.
2.2.4.1 Process flow: soaking water → pre-medium → washing → grabbing flower → injecting dye → steaming → soaping → softening → drying.
2.2.4.2 formula and notes
1. Soaking in water.
2. Pre-medium: 10% of mordant alum (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. And (5) grabbing the flowers.
5. And (3) injection dyeing: alkaline dyeing: 0.1-5% of dye (for fabric weight) and 1g/L of soda, adjusting the pH value to 7-8, after injection dyeing, raising the temperature to 80 ℃ at the speed of 5 ℃/min, multiplying 30min at 80 ℃, and if the dosage of the color is more than 3, prolonging the steaming time to 60 min. Taking out of the tank, eliminating and washing once, and feeding water.
6. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
7. Description of the operation: the mordant alum is dissolved in hot water of 25-30 times and 80 ℃, filtered and added into a jar (chemical name of alum is aluminum potassium sulfate, and the water solution is acidic). (the dye is fully dissolved in a material dissolving barrel by 50 times of hot water with the temperature of 80 ℃ in advance, and is filtered, when 0008 watermelon red material is dissolved, the material is dissolved by 0.5-1g/L of material dissolving water, the amount of the calcined soda is specifically determined according to the amount of the dye and the material dissolving water, because the alkali resistance of the plant dye is limited, the amount of the calcined soda cannot be high, the solution of 0008 watermelon red after adding the alkali is purple red, and more plant slag liquid is obtained during filtering).
3.5 plant dye selection: 0008 watermelon red.
3.5.1 Process flow: soaking water → pre-medium → washing → grabbing flower → injecting dye → steaming → soaping → softening → drying.
3.5.2 Process recipe and notes
1. Soaking in water.
2. Pre-medium: 10% of mordant alum (weight of fabric), bath ratio: 1:30, keeping the temperature at low temperature for 5-10min, heating to 80 ℃ at the speed of 1.5 ℃/min, multiplying 30min at 80 ℃, cooling and discharging residual liquid.
3. Washing with normal temperature water and feeding water.
4. And (5) grabbing the flowers.
5. And (3) injection dyeing: neutral dyeing: 0.1-5% dye (for fabric weight), after injection dyeing, heating to 80 deg.C at 5 deg.C/min, and 30min at 80 deg.C, if the amount of dye is greater than 3, steaming for 60 min. Taking out of the tank, eliminating and washing once, and feeding water.
6. Soaping: removing net loose color (neutral soaping agent for soaping agent) at 50-60 deg.C for 10 min.
7. Description of the operation: the mordant alum is dissolved in hot water of 25-30 times and 80 ℃, filtered and added into a jar (chemical name of alum is aluminum potassium sulfate, and the water solution is acidic). (the dye is fully dissolved in a material dissolving barrel by 50 times of hot water with the temperature of 80 ℃ in advance, and is filtered, when 0008 watermelon red material is dissolved, the material is dissolved by 0.5-1g/L of material dissolving water, the amount of the calcined soda is specifically determined according to the amount of the dye and the material dissolving water, because the alkali resistance of the plant dye is limited, the amount of the calcined soda cannot be high, the solution of 0008 watermelon red after adding the alkali is purple red, and more plant slag liquid is obtained during filtering).
As can be seen from the above examples 1 and 2, the dyeing method for ecological fiber artistic dyeing and finishing vegetation of the present embodiment mainly applies the process techniques of garbling, rope twisting, tie protection, injection dyeing, etc., and the dyeing process selects the additives such as the modifier, the mordant, etc. according to different fabric components and different natural dye varieties. In the experiment, different fabric components, different dyeing temperatures and different dyeing times matched with natural dyes and different pH values of dye liquor are forcibly adjusted, so that the dyeing uniformity and the repeatability are improved, and the industrial application of the tie-dyeing process with the natural fabric as a carrier and the natural dyes as raw materials is completed.
The foregoing description shows and describes several preferred embodiments of the present application, but as aforementioned, it is to be understood that the application is not limited to the forms disclosed herein, but is not to be construed as excluding other embodiments and is capable of use in various other combinations, modifications, and environments and is capable of changes within the scope of the application as described herein, commensurate with the above teachings, or the skill or knowledge of the relevant art. And that modifications and variations may be effected by those skilled in the art without departing from the spirit and scope of the application, which is to be protected by the claims appended hereto.
Claims (10)
1. The dyeing method of the ecological fiber art dyeing and finishing vegetation is characterized by comprising the following steps:
selecting a fabric and two groups of plant dyes;
the method comprises the following steps of (1) abstract tie-dyeing one group of the vegetable dyes on the fabric, wherein tie-dyeing comprises a plurality of tie-dyeing process flows, and each tie-dyeing process flow comprises pretreatment, tie-dyeing, soaping, softening and drying;
and the other group of the vegetable dyes is injected and dyed on the fabric, wherein the injection dyeing process flow comprises multiple injection dyeing process flows, and each injection dyeing process flow comprises pretreatment, flower grabbing, injection dyeing, steaming, soaping, softening and drying.
2. The ecological fiber artistic dyeing and finishing vegetation dyeing method as claimed in claim 1, wherein the material of the fabric is cellulose fiber or protein fiber; each group of said vegetable dyes comprises rose bengal, yellow brown, brilliant yellow, light brown, red brown, brown-bean, autumn yellow and watermelon red.
3. The ecological fiber artistic dyeing and finishing vegetation dyeing method as claimed in claim 2, wherein when the fabric is made of cellulose fiber, the times of the tie-dyeing process and the injection-dyeing process are five times, the first and second pretreatments include soaking, modifying and washing, and the third and fifth pretreatments include soaking, pre-dyeing and washing.
4. The ecological fiber artistic dyeing and finishing vegetation dyeing method as claimed in claim 2, wherein when the fabric is made of protein fiber, the times of the tie-dyeing process flow and the injection dyeing process flow are five times, the pre-treatments in the first and second tie-dyeing process flows comprise soaking and dewatering, and the pre-treatments in the third and fifth tie-dyeing process flows comprise soaking, pre-dyeing and dewatering.
5. The dyeing and finishing method for ecological fiber art dyeing and finishing vegetation according to claim 3 or 4, characterized in that, in the soaking, the fabric is rinsed with scouring agent 2g/L, oxalic acid 5g/L, 80 ℃ x 30min, and then soaked in soft water.
6. The dyeing method of ecological fiber art dyeing and finishing vegetation as claimed in claim 3, characterized in that, during modification, the modifier BS 10% with a bath ratio of 1:30 is kept at low temperature for 5-10min, then heated to 80 ℃ at a rate of 1.5 ℃/min, and the temperature is increased to 80 ℃ for 30min, and the residual liquid is discharged after cooling.
7. The dyeing method of ecological fiber artistic dyeing and finishing of vegetation as claimed in claim 4, wherein in the pre-medium, the mordant alum is 10%, the bath ratio is 1:30, after the low temperature is kept for 5-10min, the temperature is raised to 80 ℃ at the speed of 1.5 ℃/min, the temperature is increased to 80 ℃ for 30min, and the residual liquid is discharged after the temperature is lowered.
8. The dyeing method for ecological fiber artistic dyeing and finishing vegetation according to claim 1, wherein during soaping, an acidic or neutral soaping agent at 50-60 ℃ is selected and washed for 10min to remove loose color.
9. The dyeing method of ecological fiber art dyeing and finishing vegetation according to claim 1, characterized in that, during dyeing, 0.1-5% of dye to fabric weight is prepared, the bath ratio is 1:30, the pH value is adjusted, the temperature is kept at low temperature for 5-10min, then the temperature is raised to 80-95 ℃ at the speed of 1.5 ℃/min, if the dosage of fruit color is more than 3, the dyeing time is prolonged to 60min, then the temperature is reduced after color matching, the residual liquid is discharged, and the washing is eliminated and the water is fed.
10. The dyeing method of ecological fiber artistic dyeing and finishing vegetation according to claim 1, characterized in that in the injection dyeing, 0.1-5% of dye to water weight is prepared, the pH value is adjusted, after the injection dyeing, the temperature is raised to 80-95 ℃ at the rate of 5 ℃/min, if the amount of the color is more than 3, the steaming time is prolonged to 60min, and then the dyeing method is taken out of a cylinder, eliminated and washed once and fed with water.
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| CN1563559A (en) * | 2004-04-02 | 2005-01-12 | 江苏华艺服饰有限公司 | Artistic dyeing-collating technique for integrated dyeing and patterning process for ready-made clothes |
| CN101368341A (en) * | 2008-09-28 | 2009-02-18 | 殷大卫 | Natural vegetable dye textile dyeing and printing technique |
| CN103938468A (en) * | 2014-05-12 | 2014-07-23 | 祝一鸣 | Natural plant dyestuff dyeing and finishing processing method for loose cellulose fiber |
| CN109653006A (en) * | 2017-10-11 | 2019-04-19 | 赤峰东黎羊绒设备有限公司 | A kind of manufacturing process for hanging dye, tie dyeing for cashmere product |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1563559A (en) * | 2004-04-02 | 2005-01-12 | 江苏华艺服饰有限公司 | Artistic dyeing-collating technique for integrated dyeing and patterning process for ready-made clothes |
| CN101368341A (en) * | 2008-09-28 | 2009-02-18 | 殷大卫 | Natural vegetable dye textile dyeing and printing technique |
| CN103938468A (en) * | 2014-05-12 | 2014-07-23 | 祝一鸣 | Natural plant dyestuff dyeing and finishing processing method for loose cellulose fiber |
| CN109653006A (en) * | 2017-10-11 | 2019-04-19 | 赤峰东黎羊绒设备有限公司 | A kind of manufacturing process for hanging dye, tie dyeing for cashmere product |
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