CN113696297A - Floor board preparation process using composite material as core board and floor board - Google Patents

Floor board preparation process using composite material as core board and floor board Download PDF

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Publication number
CN113696297A
CN113696297A CN202110960412.XA CN202110960412A CN113696297A CN 113696297 A CN113696297 A CN 113696297A CN 202110960412 A CN202110960412 A CN 202110960412A CN 113696297 A CN113696297 A CN 113696297A
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China
Prior art keywords
floor
plate
wood
composite material
cooling
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Pending
Application number
CN202110960412.XA
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Chinese (zh)
Inventor
张峰
黄云峰
夏朝彦
刘家福
陈远强
陶云科
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Power Dekor Group Co ltd
Guangzhou Homebon Timber Manufacturing Co ltd
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Power Dekor Group Co ltd
Guangzhou Homebon Timber Manufacturing Co ltd
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Application filed by Power Dekor Group Co ltd, Guangzhou Homebon Timber Manufacturing Co ltd filed Critical Power Dekor Group Co ltd
Priority to CN202110960412.XA priority Critical patent/CN113696297A/en
Publication of CN113696297A publication Critical patent/CN113696297A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27NMANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
    • B27N3/00Manufacture of substantially flat articles, e.g. boards, from particles or fibres
    • B27N3/08Moulding or pressing
    • B27N3/10Moulding of mats
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27MWORKING OF WOOD NOT PROVIDED FOR IN SUBCLASSES B27B - B27L; MANUFACTURE OF SPECIFIC WOODEN ARTICLES
    • B27M3/00Manufacture or reconditioning of specific semi-finished or finished articles
    • B27M3/04Manufacture or reconditioning of specific semi-finished or finished articles of flooring elements, e.g. parqueting blocks
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B27WORKING OR PRESERVING WOOD OR SIMILAR MATERIAL; NAILING OR STAPLING MACHINES IN GENERAL
    • B27NMANUFACTURE BY DRY PROCESSES OF ARTICLES, WITH OR WITHOUT ORGANIC BINDING AGENTS, MADE FROM PARTICLES OR FIBRES CONSISTING OF WOOD OR OTHER LIGNOCELLULOSIC OR LIKE ORGANIC MATERIAL
    • B27N1/00Pretreatment of moulding material
    • EFIXED CONSTRUCTIONS
    • E04BUILDING
    • E04FFINISHING WORK ON BUILDINGS, e.g. STAIRS, FLOORS
    • E04F15/00Flooring
    • E04F15/02Flooring or floor layers composed of a number of similar elements
    • E04F15/10Flooring or floor layers composed of a number of similar elements of other materials, e.g. fibrous or chipped materials, organic plastics, magnesite tiles, hardboard, or with a top layer of other materials
    • E04F15/107Flooring or floor layers composed of a number of similar elements of other materials, e.g. fibrous or chipped materials, organic plastics, magnesite tiles, hardboard, or with a top layer of other materials composed of several layers, e.g. sandwich panels

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  • Engineering & Computer Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Wood Science & Technology (AREA)
  • Forests & Forestry (AREA)
  • Architecture (AREA)
  • Civil Engineering (AREA)
  • Structural Engineering (AREA)
  • Floor Finish (AREA)
  • Dry Formation Of Fiberboard And The Like (AREA)

Abstract

The invention belongs to the technical field of floor processing, and relates to a floor preparation process taking a composite material as a core plate, which comprises the following steps: crushing and mixing polylactic acid particles, waste paper pulp particles, wood fibers and an auxiliary agent; putting into a co-rotating double-screw extruder, and extruding the mixture; placing a bottom plate below the inside of the shaping mold, injecting the mixture into the shaping mold, arranging a decorative panel above the mixture, cooling to room temperature, and forming a plate blank to be shaped; hot pressing to obtain a plate blank, cold pressing, maintaining, sanding two sides, and processing a matched groove and a matched tenon; and coating a transparent or semitransparent coating on the surface and the back of the floor, and cooling to obtain the floor. The invention fully utilizes waste resources such as waste paper, wood product excess material and the like, and the waste resources are thermoformed into the composite material and used as the core board of the floor. The process steps are simple, and the prepared composite floor meets the national standard requirements. The invention provides a feasible industrialization path for reasonable utilization of waste wood fiber resources.

Description

Floor board preparation process using composite material as core board and floor board
Technical Field
The invention belongs to the technical field of floor processing, relates to a composite material floor, and particularly relates to a floor preparation process taking a composite material as a core plate and a floor.
Background
The waste paper is used as renewable resources, and the recovery and the utilization have important meanings for saving natural resources, slowing down carbon dioxide emission, slowing down water resource pollution, developing sustainable economy and the like. At present, the most used waste paper recycling is to produce recycled paper after deinking, but the deinking process can cause pollution to water resources, and meanwhile, the repeated recycling of waste paper and the pulping and papermaking processes can cause damage to fibers and reduce the mechanical properties of the fibers. If the waste paper resource can be efficiently utilized, the method has great economic and social benefits.
Wood products processing enterprises can produce a large amount of leftover bits and pieces, wood flour and other remainders in the process of producing wood products, and the wood fiber structure has good rigidity and toughness. However, most of the residual materials are recycled and processed into biomass fuel which is burnt once, the heat energy value is low, and the economic value is not high.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to disclose a floor preparation process taking a composite material as a core plate.
Technical scheme
A floor preparation process taking a composite material as a core plate comprises the following steps:
A. feeding polylactic acid particles, waste paper pulp particles, wood fibers and an auxiliary agent into a crusher according to a mass ratio of 30-50: 5-20: 0.5-8, and mixing at 2000-5000 r/min for 3-6 min;
B. after fully mixing, putting into a co-rotating double-screw extruder, and extruding the mixture, wherein the rotating speed of the double screws is 90-110 r/min, and the extrusion temperature is 170-190 ℃;
C. placing a bottom plate below the inside of the shaping mold, injecting the mixture into the shaping mold, arranging a decorative panel above the mixture, cooling to room temperature, and forming a plate blank to be shaped;
D. placing the plate blank into a hot press, wherein the temperature of an upper plate and a lower plate of the hot press is 190-220 ℃, the hot pressing time is 160-250 s, the surface pressure is 8-12 MPa, and cooling to room temperature after hot press forming;
E. transferring the plate blank into a cold press, cooling the upper plate and the lower plate of the cold press through water cooling circulation, setting the pressure to be 2-4 MPa, setting the plate blank cooling rate to be 10-20 ℃/min, setting the time to be 150-300 s, and moving the plate blank out of the cold press after the plate blank is cooled to the room temperature;
F. sequentially stacking cold-pressed plate blanks into a stack, covering a heavy object on the uppermost layer, curing for 1-5 d, sanding the two sides of the plate blanks after curing, and processing matched grooves and tenons to obtain the floor;
G. and coating a transparent or semitransparent coating on the surface and the back of the floor, and cooling to obtain the floor.
In the preferred embodiment of the invention, the waste paper pulp particles obtained in the step A can be subjected to humidification treatment, and the water content reaches 15-25%.
In the preferred embodiment of the invention, the wood fiber in the step A has a length of 0.1-10 mm and an average diameter of 0.01-0.4 mm, preferably a length of 0.3-4 mm and an average diameter of 0.01-0.06 mm.
Further, the wood fibers obtained in the step A are screened by a 16-18-mesh screen and then subjected to humidification treatment, and the water content reaches 15-25%.
In the preferred embodiment of the present invention, the surface of the wood fiber in step a is pretreated by using a chemical or physical method to treat the surface of the wood fiber, so as to change the structure and performance of the surface of the wood fiber, thereby achieving the purpose of improving the surface compatibility. The wood fiber surface contains a large amount of polar hydroxyl, phenolic hydroxyl and the like, and shows extremely strong chemical activity, so that the hydrophobic non-polar functional group is generated on the wood fiber mainly by performing modification treatment such as esterification, etherification, graft copolymerization and the like on the polar functional group. Treatment methods include, but are not limited to, acid treatment (DA), base treatment (DB), hydrothermal treatment (HW), organic solvent treatment (OR), sodium chlorite solution bleaching treatment (SCB), continuous Screw Extrusion Steam Explosion (SESE), and the like. As the woody material of the wood fiber to be surface-treated, there is no limitation of species. For example: small diameter wood, wood block and wood chip are boiled and softened, and then enter equipment for fiber separation.
In the preferred embodiment of the invention, the assistant in the step A is calcium carbonate or montmorillonite.
The invention also discloses a floor manufactured by the method, which is provided with a decorative panel, a core plate and a bottom plate from top to bottom, wherein the surfaces of the decorative panel and the bottom plate are coated with transparent or semitransparent coatings.
The core plate is made of the composite material prepared by the process, and the density of the core plate is 0.5-1.3 g/cm3The thickness is 3 to 18mm, preferably 5 to 8 mm.
The decoration panel is a veneer or a jointed board or a recombined veneer which is processed by natural wood, and the thickness of the decoration panel is 0.2-4 mm.
The bottom plate is a single plate or jointed plate or recombined single plate processed by natural wood, and the thickness of the bottom plate is 0.2-4 mm.
The coating is a cross-linked polymer of a mixture taking ultraviolet/electron beam cured acrylate functional resin as a main component, and has the thickness of 30-400 microns, and preferably the thickness of 50-100 microns.
Further, the coating can also be formed by naturally solidifying wood wax oil.
Advantageous effects
The invention fully utilizes waste resources such as waste paper, wood product excess material and the like, mixes and granulates the waste resources and the wood product excess material with polylactic acid, thermally forms the waste resources into composite materials, and uses the composite materials as core plates of floors. The process disclosed by the invention has the advantages of simple steps, wide raw material sources of the composite material, no much investment in pretreatment steps, and capability of meeting the national standard requirements of the prepared composite floor. The invention improves the economic value of the waste paper and wood product excess material, and provides a feasible industrialization path for the reasonable utilization of waste wood fiber resources.
Drawings
FIG. 1 is a schematic structural view of a composite flooring manufactured according to the present invention; the name of each part is 1, coating 2, bottom plate 3, core plate 4 and decorative panel.
Detailed Description
The present invention will be described in detail below with reference to examples to enable those skilled in the art to better understand the present invention, but the present invention is not limited to the following examples.
Example 1
A floor preparation process taking a composite material as a core plate comprises the following steps:
step one, preparing mixture particles. Feeding polylactic acid particles, waste paper pulp particles, wood fibers and an auxiliary agent into a crusher to be mixed according to the mass percentage range of 48 percent (40 percent) to 10 percent (2 percent). Decompose at 3000 rpm for 5 minutes. After fully mixing, putting the mixture into a co-rotating double-screw extruder to extrude the mixture, wherein the rotating speed of the double screws is 100r/min, and the extruding temperature of the double screws is 180 ℃.
Further optimizing the scheme, humidifying the waste paper pulp particles to ensure that the water content of the waste paper pulp particles is 20-23% by mass.
The scheme is further optimized, the wood fiber is screened through screening equipment with the mesh number of 18, the screened wood fiber is subjected to humidification treatment, and the water content of the wood fiber is controlled to be 20-23%.
And step two, assembling. A eucalyptus bottom plate 2 with the length and width of 950 multiplied by 190 multiplied by 1.6mm is arranged below a shaping mould with the inner diameter, the length, the width and the height of 1000 multiplied by 200 multiplied by 20mm, then the mixture is injected into the shaping mould, and a black walnut decoration panel 4 with the length, the width and the thickness of 950 multiplied by 190 multiplied by 1.5mm is arranged above the mixture. Cooling, forming plate blank to be shaped, and placing into a press.
And step three, hot-press forming, namely placing the plate blank into a hot press. The temperature of the upper plate and the lower plate of the hot press is set to be 200 ℃, the hot pressing time is set to be 220 seconds, and the gauge pressure is set to be 10 MPa.
Step four, cold pressing. Transferring the cold and post-pressed plate blank into a cold press, setting the pressure to be 2MPa, cooling the upper plate and the lower plate of the cold press through water cooling circulation, setting the plate blank cooling rate to be 20 ℃/min, and setting the time to be 180 seconds. And (5) cooling to room temperature and then moving out of the cold press.
And step five, stacking the cold-pressed plate blanks in sequence to form a stack. And (5) carrying out health preserving treatment on the uppermost layer of cover by using a heavy object for 3 days. And (3) sanding the two sides of the cured plate blank to eliminate unevenness of the plate surface, and processing a matched groove and a matched tenon according to the specification requirement of the product. The surface and the back of the floor are coated with transparent or semi-transparent coatings.
The composite wood floor manufactured according to the process is sequentially laminated with the decoration panel 4, the core plate 3 and the bottom plate 2 from top to bottom, the decoration panel 4 and the bottom plate 2 are coated with the transparent or semitransparent coating 1, the core plate 3 is made of a composite material with certain elasticity, the thickness of the plate is 8mm, and the decoration panel 4 is a wood veneer processed by natural wood black walnuts and is 1.5mm thick. The bottom plate 2 is a eucalyptus veneer with the thickness of 1.8mm, the decorative panel 4 is 100 mu m thick, and the bottom plate 2 is 30 mu m thick.
The core plate 3 is a composite material prepared according to the process, is prepared by mixing polylactic acid particles, waste paper pulp particles and wood fibers according to a certain proportion, feeding, pulping and extruding, is processed into particles and then is subjected to thermal forming, and the density of the core plate is 1.1g/cm3
The polylactic acid particles are polymers obtained by polymerizing lactic acid serving as a main raw material, and the adding mass percentage is 48%.
The waste paper pulp particles are prepared by taking waste paper as a raw material and mechanically stirring, and the adding mass percentage is 40%.
The wood fiber is subjected to hydrothermal treatment on the surface, and the addition mass percentage is 10%.
The length of the fiber is 0.4-0.6mm, the average diameter is 0.015-0.06mm,
further, in order to improve the crystallization effect of the polylactic acid, 2 mass percent of montmorillonite is added.
Example 2
A floor preparation process taking a composite material as a core plate comprises the following steps:
step one, preparing mixture particles. Feeding polylactic acid particles, waste paper pulp particles, wood fibers and an auxiliary agent into a crusher to be mixed according to the mass percentage ranges of (40%) (45%) (13.5%) (1.5%). Decompose at 3000 rpm for 5 minutes. After fully mixing, putting the mixture into a co-rotating double-screw extruder to extrude the mixture, wherein the rotating speed of the double screws is 100r/min, and the extruding temperature of the double screws is 170 ℃.
Further optimizing the scheme, humidifying the waste paper pulp particles to ensure that the water content of the waste paper pulp particles is 20-23% by mass.
The scheme is further optimized, the wood fiber is screened through screening equipment with the mesh number of 18, the screened wood fiber is subjected to humidification treatment, and the water content of the wood fiber is controlled to be 20-23%.
And step two, assembling. The eucalyptus bottom plate 2 with the length and width of 950 multiplied by 190 multiplied by 1.1mm is arranged below the inside diameter and length and width of 1000 multiplied by 200 multiplied by 22mm in the shaping mould, then the mixture is injected into the shaping mould, and the oak decorative panel 4 with the length and width of 950 multiplied by 190 multiplied by 1.0mm is arranged above the mixture. Cooling, forming plate blank to be shaped, and placing into a press.
And step three, hot-press forming, namely placing the plate blank into a hot press. The temperature of the upper plate and the lower plate of the hot press is set to 195 ℃, the hot pressing time is 210 seconds, and the gauge pressure is set to be 10 MPa.
Step four, cold pressing. Transferring the cold and post-pressed plate blank into a cold press, setting the pressure to be 3MPa, cooling the upper plate and the lower plate of the cold press through water cooling circulation, setting the plate blank cooling rate to be 15 ℃/min, and setting the time to be 200 seconds. And (5) cooling to room temperature and then moving out of the cold press.
And step five, stacking the cold-pressed plate blanks in sequence to form a stack. And (5) carrying out health preserving treatment on the uppermost layer of cover by using a heavy object for 3 days. And (3) sanding the two sides of the cured plate blank to eliminate unevenness of the plate surface, and processing a matched groove and a matched tenon according to the specification requirement of the product. And coating a transparent or semitransparent coating on the surface and the back of the floor.
The composite wood floor manufactured by the process is sequentially laminated with the decorative panel 4, the core plate 3 and the bottom plate 2 from top to bottom. The decorative panel 4 and the base plate 2 are painted with a transparent or translucent coating 1. The core plate 3 is made of a composite material with certain elasticity, the thickness of the plate is 13mm, and the decorative panel 4 is a wood veneer processed by natural wood oak and has the thickness of 1 mm. The bottom plate 2 is a eucalyptus veneer with the thickness of 1.1mm, the decorative panel 4 is 100 mu m thick, and the bottom plate 2 is 30 mu m thick.
The core plate 3 is prepared by mixing polylactic acid particles, waste paper pulp particles and wood fibers according to a certain proportion, feeding, pulping, extruding, processing into particles, and performing thermal forming to obtain the core plate with the density of 0.9g/cm3
The polylactic acid particles are polymers obtained by polymerizing lactic acid serving as a main raw material. The mass percentage of the additive is 40 percent.
The waste paper pulp particles are prepared by mechanically stirring the waste paper used as a raw material, and the adding mass percentage is 45%.
The wood fiber is wood fiber with the surface subjected to hydrothermal treatment and the like, and the added mass percentage is 13.5%.
The length of the fiber is 0.4-0.5mm, the average diameter is 0.015-0.04mm,
in order to improve the crystallization effect of polylactic acid, 1.5 percent of montmorillonite by mass is added.
The above description is only an embodiment of the present invention, and not intended to limit the scope of the present invention, and all modifications of equivalent structures and equivalent processes performed by the present invention or directly or indirectly applied to other related technical fields are included in the scope of the present invention.

Claims (10)

1. A floor preparation process taking a composite material as a core plate is characterized by comprising the following steps:
A. feeding polylactic acid particles, waste paper pulp particles, wood fibers and an auxiliary agent into a crusher according to a mass ratio of 30-50: 5-20: 0.5-8, and mixing at 2000-5000 r/min for 3-6 min;
B. after fully mixing, putting into a co-rotating double-screw extruder, and extruding the mixture, wherein the rotating speed of the double screws is 90-110 r/min, and the extrusion temperature is 170-190 ℃;
C. placing a bottom plate below the inside of the shaping mold, injecting the mixture into the shaping mold, arranging a decorative panel above the mixture, cooling to room temperature, and forming a plate blank to be shaped;
D. placing the plate blank into a hot press, wherein the temperature of an upper plate and a lower plate of the hot press is 190-220 ℃, the hot pressing time is 160-250 s, the surface pressure is 8-12 MPa, and cooling to room temperature after hot press forming;
E. transferring the plate blank into a cold press, cooling the upper plate and the lower plate of the cold press through water cooling circulation, setting the pressure to be 2-4 MPa, setting the plate blank cooling rate to be 10-20 ℃/min, setting the time to be 150-300 s, and moving the plate blank out of the cold press after the plate blank is cooled to the room temperature;
F. sequentially stacking cold-pressed plate blanks into a stack, covering a heavy object on the uppermost layer, curing for 1-5 d, sanding the two sides of the plate blanks after curing, and processing matched grooves and tenons to obtain the floor;
G. and coating a transparent or semitransparent coating on the surface and the back of the floor, and cooling to obtain the floor.
2. The process for preparing a floor with a composite material as a core plate according to claim 1, wherein the process comprises the following steps: and B, humidifying the waste paper pulp particles in the step A, wherein the water content is 15-25%.
3. The process for preparing a floor with a composite material as a core plate according to claim 1, wherein the process comprises the following steps: the wood fiber in the step A has the length of 0.1-10 mm and the average diameter of 0.01-0.4 mm, preferably the length of 0.3-4 mm and the average diameter of 0.01-0.06 mm.
4. The process for preparing a floor with a composite material as a core plate according to claim 1, wherein the process comprises the following steps: and B, screening the wood fibers in the step A by 16-18 meshes, and then humidifying the wood fibers to obtain the wood fibers with the water content of 15-25%.
5. The process for preparing a floor with a composite material as a core plate according to claim 1, wherein the process comprises the following steps: the auxiliary agent in the step A is calcium carbonate or montmorillonite.
6. The floor prepared by the process according to any one of the claims 1 to 5, which is provided with a decorative panel (4), a core plate (3) and a bottom plate (2) from top to bottom in sequence, and is characterized in that: the surfaces of the decorative panel (4) and the bottom plate (2) are coated with transparent or semitransparent coatings (1).
7. The floor of claim 6, wherein: the density of the core plate (3) is 0.5-1.3 g/cm3The thickness is 3 to 18mm, preferably 5 to 8 mm.
8. The floor of claim 6, wherein: the decoration panel (4) is a veneer or a jointed board or a recombined veneer which is processed by natural wood, and the thickness is 0.2-4 mm.
9. The floor of claim 6, wherein: the bottom plate (2) is a veneer or a jointed board or a recombined veneer processed by natural wood, and the thickness is 0.2-4 mm.
10. The floor of claim 6, wherein: the coating (1) is formed by naturally curing a cross-linked polymer of a mixture taking ultraviolet/electron beam cured acrylate functional resin as a main component or wood wax oil, and has the thickness of 30-400 mu m, preferably 50-100 mu m.
CN202110960412.XA 2021-08-20 2021-08-20 Floor board preparation process using composite material as core board and floor board Pending CN113696297A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101100830A (en) * 2007-06-26 2008-01-09 方隽云 Technique for producing sheet-type electronic component paper carrying base paper by using waste paper pulp
CN101428431A (en) * 2007-10-12 2009-05-13 中日精工株式会社 Method for producing xylon molded body and xylon molded body
CN101942118A (en) * 2010-10-25 2011-01-12 曾广胜 Plant fiber starch fully-biodegradable material and preparation method thereof
CN102877355A (en) * 2012-11-01 2013-01-16 红塔烟草(集团)有限责任公司 Polylactic acid forming paper and preparation method
CN102959058A (en) * 2010-07-12 2013-03-06 西门子Vai金属科技有限责任公司 Method for producing pressed articles containing coal particles
CN110205855A (en) * 2019-04-19 2019-09-06 东莞建晖纸业有限公司 A kind of coating coated duplex board with grey back center stock preparation process

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101100830A (en) * 2007-06-26 2008-01-09 方隽云 Technique for producing sheet-type electronic component paper carrying base paper by using waste paper pulp
CN101428431A (en) * 2007-10-12 2009-05-13 中日精工株式会社 Method for producing xylon molded body and xylon molded body
CN102959058A (en) * 2010-07-12 2013-03-06 西门子Vai金属科技有限责任公司 Method for producing pressed articles containing coal particles
CN101942118A (en) * 2010-10-25 2011-01-12 曾广胜 Plant fiber starch fully-biodegradable material and preparation method thereof
CN102877355A (en) * 2012-11-01 2013-01-16 红塔烟草(集团)有限责任公司 Polylactic acid forming paper and preparation method
CN110205855A (en) * 2019-04-19 2019-09-06 东莞建晖纸业有限公司 A kind of coating coated duplex board with grey back center stock preparation process

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