CN113634001A - Preparation process of ox gall powder - Google Patents

Preparation process of ox gall powder Download PDF

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Publication number
CN113634001A
CN113634001A CN202110814885.9A CN202110814885A CN113634001A CN 113634001 A CN113634001 A CN 113634001A CN 202110814885 A CN202110814885 A CN 202110814885A CN 113634001 A CN113634001 A CN 113634001A
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Prior art keywords
waste gas
casing
gall powder
gas adsorption
adsorption plate
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CN202110814885.9A
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Chinese (zh)
Inventor
黄春娇
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Zhejiang Shengbang Biopharmaceutical Co ltd
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Zhejiang Shengbang Biopharmaceutical Co ltd
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Priority to CN202110814885.9A priority Critical patent/CN113634001A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/14Evaporating with heated gases or vapours or liquids in contact with the liquid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D1/00Evaporating
    • B01D1/16Evaporating by spraying
    • B01D1/18Evaporating by spraying to obtain dry solids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/04Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with stationary adsorbents
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14Ultrafiltration; Microfiltration
    • B01D61/147Microfiltration
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D61/00Processes of separation using semi-permeable membranes, e.g. dialysis, osmosis or ultrafiltration; Apparatus, accessories or auxiliary operations specially adapted therefor
    • B01D61/14Ultrafiltration; Microfiltration
    • B01D61/16Feed pretreatment
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2253/00Adsorbents used in seperation treatment of gases and vapours
    • B01D2253/10Inorganic adsorbents
    • B01D2253/102Carbon

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Water Supply & Treatment (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Treating Waste Gases (AREA)

Abstract

The invention discloses a preparation process of ox gall powder, which comprises the following steps: heating and dissolving, filtering, spray drying, collecting materials, packaging finished products, inspecting the finished products and warehousing the finished products. The invention has the beneficial effects that: the method has the advantages of simplified process production flow, suitability for continuous control production, capability of realizing instantaneous drying, capability of drying feed liquid into powder at one time, high automation degree, time-saving and labor-saving operation, low labor cost, capability of orderly collecting and discharging waste gas, better environmental friendliness, capability of ensuring the quality of finished products of the ox gall powder and accordance with the requirements of mass production.

Description

Preparation process of ox gall powder
Technical Field
The invention relates to the technical field of biological pharmacy, in particular to a preparation process of cow gall powder.
Background
The ox gall powder is a dried product of animal ox gall, is green brown or tan block or powder, is in a semitransparent cutin shape, is slowly dissolved after being tasted, is slightly fishy in smell, is bitter in taste and is easy to absorb moisture. The ox gall powder is bitter in taste and cold in nature, has the functions of clearing liver and improving vision, benefiting gall and relaxing bowels, detoxifying and reducing swelling when being used in medicines, and can be used for treating wind-heat eye diseases, heat thirst of heart and abdomen, jaundice, cough and excessive phlegm, infantile convulsion, constipation, carbuncle swelling, hemorrhoids and the like.
At present, a boiling method is generally adopted in traditional ox gall powder preparation, the process flow sequentially comprises boiling, degreasing, filtering and drying, the process flow is complex, time and labor are wasted in operation, labor cost is high, waste gas is irregularly discharged in the ox gall powder preparation process, the environment is easily polluted, the environment is not environment-friendly enough, the product granularity is 80 meshes, and the finished product quality of the ox gall powder is affected due to the fact that the waste gas is easily damped.
Therefore, a new preparation process of the ox gall powder is needed to solve the above problems.
Disclosure of Invention
The invention aims to solve the problems, and provides a preparation process of the ox gall powder, which has the advantages of simple process flow, time-saving and labor-saving operation, low labor cost, capability of orderly collecting and discharging waste gas and capability of ensuring the quality of finished ox gall powder products.
The invention realizes the purpose through the following technical scheme, and the preparation process of the ox gall powder comprises the following steps:
1) heating for dissolving: heating and dissolving the raw material of the fel bovis seu Bubali ointment, and adding purified water to the original volume in the process to obtain a raw material mother liquor;
2) and (3) filtering treatment: putting the raw material mother liquor obtained in the step 1) into a microporous filtering membrane for filtering, wherein the aperture of the microporous filtering membrane is 1.2 mu m, and obtaining a supernatant after filtering;
3) spray drying: conveying the supernatant treated in the step 2) to a centrifugal atomizer at the top of a spray dryer through a feeding pump, spraying the supernatant into extremely small atomized liquid drops, simultaneously enabling outside air to sequentially pass through an air filter and a heater and then enter an air distributor at the top of the spray dryer, enabling the hot air to uniformly enter a drying tower in a spiral shape and to be in parallel flow contact with feed liquid, and further drying the hot air into ox gall powder at one time, wherein the waste gas is orderly collected and discharged through a waste gas collecting device;
4) receiving material treatment: opening a discharge valve at the bottom of the drying tower and the cyclone separator, and collecting the ox gall powder obtained by the treatment in the step 3);
5) packaging a finished product: sequentially carrying out inner packaging and outer packaging on the ox gall powder collected in the step 4), and obtaining a finished product after the packaging is finished;
6) and (4) inspecting a finished product: performing quality detection on the finished product obtained after the packaging in the step 5), distinguishing defective products from qualified products, and independently placing the qualified products in an empty box for storage;
7) finished products are put in storage: labeling the finished products which are qualified in the step 6), and then uniformly warehousing and storing.
Through adopting above-mentioned technical scheme, the production flow is simplified, suitable continuous control production, can realize instantaneous drying, make the feed liquid can once dry into powder, and degree of automation is high, can reduce and smash, the process of screening, the cost of labor is low, the product purity of finished product ox gall powder has effectively been improved, make the product have good dispersibility, mobility and solubility, and make ox gall powder be difficult for weing, the finished product quality of ox gall powder has effectively been guaranteed, accord with mass production's demand, and can carry out orderly collection and emission to waste gas in spray drying's process, thereby can avoid the polluted environment, the feature of environmental protection is better.
As a further arrangement of the invention, the waste gas collecting device in the step 3) comprises a casing, a plurality of waste gas adsorption plates are arranged in the casing, one end of the casing is connected with an air inlet pipe, the other end of the casing is connected with an exhaust pipe, and one end of the air inlet pipe, which is far away from the casing, is connected with a centrifugal fan.
Through adopting above-mentioned technical scheme, because waste gas collection device includes the casing, be provided with a plurality of waste gas adsorption plates in the casing inside, and casing one end has centrifugal fan through intake-tube connection, and the other end is connected with the blast pipe, then can adsorb the pollutant in the waste gas through waste gas adsorption plate to guarantee exhaust gas's purity, avoid the polluted environment.
As a further arrangement of the invention, the top wall of the shell is provided with a plurality of through grooves for the exhaust gas adsorption plates to penetrate out, slide rails are arranged at the positions inside the shell, which are positioned at the two sides of the through grooves, and the exhaust gas adsorption plates are connected between the slide rails in a sliding manner.
Through adopting above-mentioned technical scheme, owing to seted up a plurality of logical grooves on the casing roof, be located logical groove both sides position and be provided with the slide rail inside the casing, and waste gas adsorption plate sliding connection is between the slide rail, then when waste gas adsorption plate loses adsorption effect because of long-term the use, can pull out waste gas adsorption plate from leading to the inslot to the convenience carries out timely dismantlement to waste gas adsorption plate and changes, guarantees waste gas collection device's exhaust purification effect all the time.
According to the invention, as a further arrangement, a pushing and lifting plate for pushing the waste gas adsorption plate to penetrate out of the through groove is arranged on the inner bottom wall of the machine shell, a spring is connected between the pushing and lifting plate and the inner bottom wall of the machine shell, a locking piece is arranged at the top of the waste gas adsorption plate, and locking seats matched with the locking piece are arranged on the top wall of the machine shell at two sides of the through groove.
Through adopting above-mentioned technical scheme, owing to be provided with the promotion board on the diapire in the casing, and be connected with the spring between promotion board and the casing diapire, owing to be provided with the lock piece at waste gas adsorption plate top, and be provided with the locking seat that matches with the lock piece on the casing roof, then when needing to dismantle the change waste gas adsorption plate, only need relieve the locking of lock piece and locking seat, then the spring breaks away from the pressure constraint and can extend and resume original shape, thereby can wear out logical groove outside through promoting the waste gas adsorption plate through the promotion board, conveniently pull down the waste gas adsorption plate, thereby make the dismantlement of waste gas adsorption plate become more convenient simple.
According to the further arrangement of the exhaust gas adsorption device, the locking piece comprises a rotating seat which is rotatably connected to the top of the exhaust gas adsorption plate, limiting rods are connected to two sides of the rotating seat, the locking seat comprises an arc-shaped seat which is fixed on the top wall of the machine shell, and annular grooves for the limiting rods to be clamped in are formed in the opposite surfaces of the arc-shaped seat.
Through adopting above-mentioned technical scheme, because the lock piece is including rotating the seat and setting up the gag lever post that rotates the seat both sides, the locking seat includes the arc seat, and all seted up the ring channel in the one side that the arc seat is relative, then when the cooperation with lock piece and locking seat, rotatable rotation seat, make the gag lever post rotate thereupon and block inside the ring channel, it is spacing to the gag lever post through the ring channel, can realize the firm locking to waste gas adsorption plate, the operation is comparatively convenient simple, and when the cooperation of lock piece and locking seat is relieved to needs, rotatable rotation seat, make the gag lever post rotate thereupon and deviate from the ring channel is inside, can relieve the locking to waste gas adsorption plate, the operation is comparatively convenient simple.
As a further arrangement of the invention, the inner top walls of the annular grooves are provided with embedded grooves for embedding the limiting rods.
Through adopting above-mentioned technical scheme, owing to all seted up the caulking groove on the interior roof of ring channel, then go into the inside back of ring channel at the gag lever post card, can be with spacing embedding caulking groove inside, then spacing through the caulking groove to the gag lever post for the locking of gag lever post in the ring channel is more reliable and more stable, thereby makes the locking of waste gas adsorption plate in casing inside more reliable and more firm.
As a further arrangement of the invention, a lifting ring is arranged on the top of the rotating seat.
By adopting the technical scheme, the lifting ring is arranged at the top of the rotating seat, so that the rotating seat can be rotated by holding the lifting ring, the waste gas adsorption plate can be taken out of the shell by lifting the lifting ring, and the arrangement of the lifting ring can provide a force application point for the operation of rotating the rotating seat and taking the waste gas adsorption plate, so that the operation becomes easier and more labor-saving.
As a further arrangement of the invention, the waste gas adsorption plate comprises a frame and an activated carbon plate core arranged inside the frame, and the frame is made of stainless steel materials.
Through adopting above-mentioned technical scheme, because waste gas adsorption plate includes the frame and sets up at the inside active carbon plate core of frame, the active carbon plate core has fabulous adsorption effect to can carry out effective absorption to the pollutant that carries in the waste gas, and the frame adopts stainless steel material to make, intensity and hardness are higher, and is not fragile and difficult corrosion, and the durability is better.
In conclusion, the invention has the following beneficial effects:
1. the method has the advantages of simplified process production flow, suitability for continuous control production, capability of realizing instantaneous drying, capability of drying feed liquid into powder at one time, high automation degree, time-saving and labor-saving operation, low labor cost, capability of orderly collecting and discharging waste gas, better environmental friendliness, capability of ensuring the quality of finished products of the ox gall powder and accordance with the requirements of mass production;
2. the waste gas collecting device is arranged, pollutants carried in waste gas can be effectively adsorbed through the waste gas adsorption plate, and when the waste gas adsorption plate loses adsorption effect due to long-term use, the waste gas adsorption plate can be conveniently detached and replaced, and the using effect is good.
Drawings
FIG. 1 is a process flow diagram of the present invention;
FIG. 2 is a schematic view showing the construction of an exhaust gas collecting apparatus according to the present invention;
FIG. 3 is an enlarged schematic view of the structure at A in FIG. 2;
FIG. 4 is a half-sectional view of the exhaust gas collecting device of the present invention with the centrifugal fan removed;
FIG. 5 is a schematic structural view of the exhaust gas collecting device of the present invention after the centrifugal fan and the exhaust gas adsorption plate are removed;
fig. 6 is an enlarged schematic view of the structure at B in fig. 5.
Reference numerals: 1. a housing; 2. an exhaust gas adsorption plate; 21. a frame; 22. an activated carbon board core; 3. an air inlet pipe; 4. an exhaust pipe; 5. a centrifugal fan; 6. a through groove; 7. a slide rail; 8. a thrust plate; 9. a spring; 10. a rotating seat; 11. a limiting rod; 12. an arc-shaped seat; 13. an annular groove; 14. caulking grooves; 15. and (6) lifting the ring.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Referring to fig. 1, a preparation process of a fel bovis seu Bubali powder comprises the following steps:
1) heating for dissolving: heating and dissolving the raw material fel bovis Seu Bubali ointment for 1-2h, and adding purified water to the original volume to obtain raw material mother liquor;
2) and (3) filtering treatment: putting the raw material mother liquor obtained in the step 1) into a microporous filtering membrane for filtering, wherein the aperture of the microporous filtering membrane is 1.2 mu m, and obtaining a supernatant after filtering;
3) spray drying: conveying the supernatant treated in the step 2) to a centrifugal atomizer at the top of a spray dryer through a feeding pump, spraying the supernatant into extremely small atomized liquid drops, simultaneously enabling outside air to sequentially pass through an air filter and a heater and then enter an air distributor at the top of the spray dryer, enabling the hot air to uniformly enter a drying tower in a spiral shape and to be in parallel flow contact with feed liquid, and further drying the hot air into ox gall powder at one time, wherein the waste gas is orderly collected and discharged through a waste gas collecting device;
4) receiving material treatment: opening a discharge valve at the bottom of the drying tower and the cyclone separator, and collecting the ox gall powder obtained by the treatment in the step 3);
5) packaging a finished product: sequentially carrying out inner packaging and outer packaging on the ox gall powder collected in the step 4), and obtaining a finished product after the packaging is finished;
6) and (4) inspecting a finished product: performing quality detection on the finished product obtained after the packaging in the step 5), distinguishing defective products from qualified products, and independently placing the qualified products in an empty box for storage;
7) finished products are put in storage: labeling the finished products which are qualified in the step 6), and then uniformly warehousing and storing.
The invention adopts the preparation process flows of heating dissolution, filtration treatment, spray drying, material receiving treatment, finished product packaging, finished product inspection and finished product warehousing, the production flow is simplified, the invention is suitable for continuous control production, the spray drying is carried out by adopting a spray dryer, the drying speed is high, the surface area of the feed liquid after atomization is greatly increased, instantaneous drying can be realized, the feed liquid can be dried into powder at one time, the automation degree is high, the processes of crushing and screening can be reduced, the labor cost is low, the product purity of the finished product of the ox gall powder is effectively improved, the product has good dispersibility, fluidity and solubility, the product granularity can reach more than 200 meshes, the ox gall powder is not easy to be affected with damp, the finished product quality of the ox gall powder is effectively ensured, the requirements of mass production are met, and waste gas can be orderly collected and discharged by a waste gas collecting device in the spray drying process, thereby avoiding environmental pollution and having better environmental protection.
Referring to fig. 2 and 3, the waste gas collecting device in step 3) includes a housing 1, a plurality of waste gas adsorbing plates 2 are disposed inside the housing 1, each waste gas adsorbing plate 2 includes a frame 21 and an activated carbon plate core 22 disposed inside the frame 21, the frame 21 is made of stainless steel, an air inlet pipe 3 is connected to one end of the housing 1, an air outlet pipe 4 is connected to the other end of the housing, a centrifugal fan 5 is connected to one end of the air inlet pipe 3, which is far away from the housing 1, and an air inlet end of the centrifugal fan 5 is communicated with the spray dryer.
Referring to fig. 2-6, a plurality of through grooves 6 for the exhaust gas adsorption plate 2 to pass through are formed on the top wall of the housing 1, slide rails 7 are disposed at two sides of the through grooves 6 inside the housing 1, the exhaust gas adsorption plate 2 is slidably connected between the slide rails 7, a lifting plate 8 for pushing the exhaust gas adsorption plate 2 to pass through the through grooves 6 is disposed on the inner bottom wall of the housing 1, a spring 9 is connected between the lifting plate 8 and the inner bottom wall of the housing 1, a locking member is disposed at the top of the exhaust gas adsorption plate 2, locking seats matched with the locking member are disposed at two sides of the through grooves 6 on the top wall of the housing 1, the locking member includes a rotating seat 10 rotatably connected to the top of the exhaust gas adsorption plate 2, a lifting ring 15 is disposed at the top of the rotating seat 10, and limiting rods 11 are connected to two sides of the rotating seat 10, the locking seats include arc-shaped seats 12 fixed on the top wall of the housing 1, annular grooves 13 for the limiting rods 11 to be clamped in are formed on the opposite surfaces of the arc-shaped seats 12, and the inner top wall of the annular groove 13 is provided with an embedded groove 14 for embedding the limiting rod 11.
Because the waste gas collection device includes casing 1, be provided with a plurality of waste gas adsorption plates 2 in casing 1 inside, and 1 one end of casing is connected with centrifugal fan 5 through intake pipe 3, the other end is connected with blast pipe 4, then the waste gas that produces in the preparation process can be lasted the suction by centrifugal fan 5 and through intake pipe 3 input casing 1 inside, through blast pipe 4 discharge in order behind polylith waste gas adsorption plate 2, during can adsorb the pollutant in the waste gas through waste gas adsorption plate 2, thereby guarantee exhaust gas's purity, avoid the polluted environment.
Owing to seted up a plurality of logical grooves 6 on 1 roof of casing, it is provided with slide rail 7 to be located logical groove 6 both sides position in 1 inside of casing, and 2 sliding connection of waste gas adsorption plate are between slide rail 7, then when waste gas adsorption plate 2 loses adsorption effect because of long-term the use, pull waste gas adsorption plate 2 can make progress, make waste gas adsorption plate 2 follow 7 rectilinear direction of slide rail upwards slide until wearing out from leading to the inslot 6, thereby the convenience carries out timely dismantlement change to waste gas adsorption plate 2, guarantee waste gas collection device's exhaust purification effect all the time.
Because the bottom wall in the machine shell 1 is provided with the pushing and lifting plate 8, and the spring 9 is connected between the pushing and lifting plate 8 and the bottom wall in the machine shell 1, because the top of the waste gas adsorption plate 2 is provided with the locking piece, and the top wall of the machine shell 1 is provided with the locking seat matched with the locking piece, when the waste gas collecting device is used, the waste gas adsorption plate 2 is taken into the machine shell 1, the spring 9 can be extruded by the pushing and lifting plate 8, so that the spring 9 is compressed and deformed, and then the locking piece is matched with the locking seat, so that the waste gas adsorption plate 2 can be firmly locked, when the waste gas adsorption plate 2 needs to be disassembled and replaced, only the locking of the locking piece and the locking seat needs to be released, the spring 9 breaks away from the pressure constraint, can be expanded and restore to the original shape, thereby the waste gas adsorption plate 2 can be pushed by the pushing and lifting plate 8 to penetrate out of the through groove 6, the waste gas adsorption plate 2 is convenient to disassemble, so that the disassembly of the waste gas adsorption plate 2 becomes more convenient and simple, wherein, because the locking piece includes rotating seat 10 and the stop lever 11 that sets up in rotating seat 10 both sides, the locking seat includes arc seat 12, and all set up the ring channel 13 on the opposite side of arc seat 12, when locking piece and locking seat's cooperation, rotatable rotating seat 10, make stop lever 11 rotate along with it and block into the inside of ring channel 13, through the spacing of ring channel 13 to stop lever 11, can realize the firm locking to exhaust gas adsorption plate 2, the operation is comparatively convenient and simple, and when needing to remove locking piece and locking seat's cooperation, rotatable rotating seat 10, make stop lever 11 rotate along with it and deviate from the inside of ring channel 13, can remove the locking to exhaust gas adsorption plate 2, the operation is comparatively convenient and simple, and because all set up caulking groove 14 on the roof of ring channel 13, then after stop lever 11 blocks into the inside of ring channel 13, can continue to rotate rotating seat 10 and make stop lever 11 rotate along with it until imbedding inside caulking groove 14, then spacing through caulking groove 14 to gag lever post 11 for the locking of gag lever post 11 in ring channel 13 is more reliable and more stable, thereby make waste gas adsorption plate 2 more firm and reliable in the inside locking of casing 1, and owing to be provided with lifting ring 15 at rotation seat 10 top, then can rotate rotation seat 10 through gripping lifting ring 15, also can take out waste gas adsorption plate 2 from casing 1 through mentioning lifting ring 15, then lifting ring 15's setting can be for rotating rotation seat 10 and getting the operation of taking waste gas adsorption plate 2 and provide the point of application of force, thereby make the operation become more light laborsaving.
Because waste gas adsorption plate 2 includes frame 21 and sets up at the inside active carbon plate core 22 of frame 21, active carbon plate core 22 has fabulous adsorption effect to can carry out effective absorption to the pollutant that carries in the waste gas, and frame 21 adopts stainless steel material to make, intensity and hardness are higher, and is not fragile and difficult corrosion, and the durability is better.
The above description is only a preferred embodiment of the present invention, and the protection scope of the present invention is not limited to the above embodiments, and all technical solutions belonging to the idea of the present invention belong to the protection scope of the present invention. It should be noted that modifications and embellishments within the scope of the invention may occur to those skilled in the art without departing from the principle of the invention, and are considered to be within the scope of the invention.

Claims (8)

1. A preparation process of ox gall powder is characterized by comprising the following steps: the method comprises the following steps:
1) heating for dissolving: heating and dissolving the raw material of the fel bovis seu Bubali ointment, and adding purified water to the original volume in the process to obtain a raw material mother liquor;
2) and (3) filtering treatment: putting the raw material mother liquor obtained in the step 1) into a microporous filtering membrane for filtering, wherein the aperture of the microporous filtering membrane is 1.2 mu m, and obtaining a supernatant after filtering;
3) spray drying: conveying the supernatant treated in the step 2) to a centrifugal atomizer at the top of a spray dryer through a feeding pump, spraying the supernatant into extremely small atomized liquid drops, simultaneously enabling outside air to sequentially pass through an air filter and a heater and then enter an air distributor at the top of the spray dryer, enabling the hot air to uniformly enter a drying tower in a spiral shape and to be in parallel flow contact with feed liquid, and further drying the hot air into ox gall powder at one time, wherein the waste gas is orderly collected and discharged through a waste gas collecting device;
4) receiving material treatment: opening a discharge valve at the bottom of the drying tower and the cyclone separator, and collecting the ox gall powder obtained by the treatment in the step 3);
5) packaging a finished product: sequentially carrying out inner packaging and outer packaging on the ox gall powder collected in the step 4), and obtaining a finished product after the packaging is finished;
6) and (4) inspecting a finished product: performing quality detection on the finished product obtained after the packaging in the step 5), distinguishing defective products from qualified products, and independently placing the qualified products in an empty box for storage;
7) finished products are put in storage: labeling the finished products which are qualified in the step 6), and then uniformly warehousing and storing.
2. The process for preparing ox gall powder according to claim 1, wherein the process comprises the following steps: the waste gas collecting device in step 3) comprises a casing (1), a plurality of waste gas adsorption plates (2) are arranged inside the casing (1), one end of the casing (1) is connected with an air inlet pipe (3), the other end of the casing is connected with an exhaust pipe (4), and one end, away from the casing (1), of the air inlet pipe (3) is connected with a centrifugal fan (5).
3. The process for preparing ox gall powder according to claim 2, wherein: set up a plurality of logical grooves (6) that are used for waste gas adsorption plate (2) to wear out on casing (1) roof, casing (1) inside is located logical groove (6) both sides position and is provided with slide rail (7), waste gas adsorption plate (2) sliding connection is between slide rail (7).
4. The process for preparing ox gall powder according to claim 3, wherein the process comprises the following steps: be provided with on the diapire in casing (1) and be used for promoting waste gas adsorption plate (2) and wear out promotion board (8) that lead to groove (6), be connected with spring (9) between promotion board (8) and the bottom wall in casing (1), waste gas adsorption plate (2) top is provided with the locking piece, it is provided with the locking seat that matches with the locking piece to lie in logical groove (6) both sides position on casing (1) roof.
5. The process for preparing ox gall powder according to claim 4, wherein the process comprises the following steps: the locking piece is including rotating rotation seat (10) of connection at waste gas adsorption plate (2) top, rotation seat (10) both sides are connected with gag lever post (11), the locking seat is including fixing arc seat (12) on casing (1) roof, all offer ring channel (13) that are used for gag lever post (11) card to go into in the one side that arc seat (12) are relative.
6. The process for preparing ox gall powder according to claim 5, wherein the process comprises the following steps: and the inner top wall of the annular groove (13) is provided with an embedded groove (14) for embedding the limiting rod (11).
7. The process for preparing ox gall powder according to claim 5, wherein the process comprises the following steps: the top of the rotating seat (10) is provided with a lifting ring (15).
8. The process for preparing ox gall powder according to claim 2, wherein: the waste gas adsorption plate (2) comprises a frame (21) and an activated carbon plate core (22) arranged inside the frame (21), wherein the frame (21) is made of stainless steel materials.
CN202110814885.9A 2021-07-19 2021-07-19 Preparation process of ox gall powder Pending CN113634001A (en)

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Application publication date: 20211112