CN113583754A - Tobacco essence and preparation method and application thereof - Google Patents
Tobacco essence and preparation method and application thereof Download PDFInfo
- Publication number
- CN113583754A CN113583754A CN202110980451.6A CN202110980451A CN113583754A CN 113583754 A CN113583754 A CN 113583754A CN 202110980451 A CN202110980451 A CN 202110980451A CN 113583754 A CN113583754 A CN 113583754A
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- Prior art keywords
- banana peel
- extract
- essence
- tobacco
- chlorogenic acid
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- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 45
- 238000002360 preparation method Methods 0.000 title claims abstract description 14
- 244000061176 Nicotiana tabacum Species 0.000 title 1
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- 241000208125 Nicotiana Species 0.000 claims abstract description 44
- CWVRJTMFETXNAD-FWCWNIRPSA-N 3-O-Caffeoylquinic acid Natural products O[C@H]1[C@@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-FWCWNIRPSA-N 0.000 claims abstract description 31
- PZIRUHCJZBGLDY-UHFFFAOYSA-N Caffeoylquinic acid Natural products CC(CCC(=O)C(C)C1C(=O)CC2C3CC(O)C4CC(O)CCC4(C)C3CCC12C)C(=O)O PZIRUHCJZBGLDY-UHFFFAOYSA-N 0.000 claims abstract description 31
- CWVRJTMFETXNAD-KLZCAUPSSA-N Neochlorogenin-saeure Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O CWVRJTMFETXNAD-KLZCAUPSSA-N 0.000 claims abstract description 31
- 235000001368 chlorogenic acid Nutrition 0.000 claims abstract description 31
- CWVRJTMFETXNAD-JUHZACGLSA-N chlorogenic acid Chemical compound O[C@@H]1[C@H](O)C[C@@](O)(C(O)=O)C[C@H]1OC(=O)\C=C\C1=CC=C(O)C(O)=C1 CWVRJTMFETXNAD-JUHZACGLSA-N 0.000 claims abstract description 31
- 229940074393 chlorogenic acid Drugs 0.000 claims abstract description 31
- FFQSDFBBSXGVKF-KHSQJDLVSA-N chlorogenic acid Natural products O[C@@H]1C[C@](O)(C[C@@H](CC(=O)C=Cc2ccc(O)c(O)c2)[C@@H]1O)C(=O)O FFQSDFBBSXGVKF-KHSQJDLVSA-N 0.000 claims abstract description 31
- BMRSEYFENKXDIS-KLZCAUPSSA-N cis-3-O-p-coumaroylquinic acid Natural products O[C@H]1C[C@@](O)(C[C@@H](OC(=O)C=Cc2ccc(O)cc2)[C@@H]1O)C(=O)O BMRSEYFENKXDIS-KLZCAUPSSA-N 0.000 claims abstract description 31
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 claims abstract description 26
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 claims abstract description 26
- 229940041616 menthol Drugs 0.000 claims abstract description 26
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 22
- 238000002156 mixing Methods 0.000 claims abstract description 14
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- 239000002994 raw material Substances 0.000 claims abstract description 10
- 238000000034 method Methods 0.000 claims abstract description 6
- 241000234295 Musa Species 0.000 claims abstract 16
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical group CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 39
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 20
- 239000000796 flavoring agent Substances 0.000 claims description 11
- 235000019634 flavors Nutrition 0.000 claims description 11
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 10
- AUNGANRZJHBGPY-SCRDCRAPSA-N Riboflavin Chemical compound OC[C@@H](O)[C@@H](O)[C@@H](O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-SCRDCRAPSA-N 0.000 claims description 10
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 10
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 10
- 108090000790 Enzymes Proteins 0.000 claims description 9
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- 238000001914 filtration Methods 0.000 claims description 7
- 108010059892 Cellulase Proteins 0.000 claims description 5
- AUNGANRZJHBGPY-UHFFFAOYSA-N D-Lyxoflavin Natural products OCC(O)C(O)C(O)CN1C=2C=C(C)C(C)=CC=2N=C2C1=NC(=O)NC2=O AUNGANRZJHBGPY-UHFFFAOYSA-N 0.000 claims description 5
- 108010059820 Polygalacturonase Proteins 0.000 claims description 5
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 claims description 5
- 239000000654 additive Substances 0.000 claims description 5
- 235000011037 adipic acid Nutrition 0.000 claims description 5
- 239000001361 adipic acid Substances 0.000 claims description 5
- 229940106157 cellulase Drugs 0.000 claims description 5
- 108010093305 exopolygalacturonase Proteins 0.000 claims description 5
- 239000002151 riboflavin Substances 0.000 claims description 5
- 229960002477 riboflavin Drugs 0.000 claims description 5
- 235000019192 riboflavin Nutrition 0.000 claims description 5
- 239000002893 slag Substances 0.000 claims description 5
- WXMKPNITSTVMEF-UHFFFAOYSA-M sodium benzoate Chemical compound [Na+].[O-]C(=O)C1=CC=CC=C1 WXMKPNITSTVMEF-UHFFFAOYSA-M 0.000 claims description 5
- 235000010234 sodium benzoate Nutrition 0.000 claims description 5
- 239000004299 sodium benzoate Substances 0.000 claims description 5
- 229910052938 sodium sulfate Inorganic materials 0.000 claims description 5
- 235000011152 sodium sulphate Nutrition 0.000 claims description 5
- 239000004408 titanium dioxide Substances 0.000 claims description 5
- 239000003571 electronic cigarette Substances 0.000 claims description 2
- 235000010215 titanium dioxide Nutrition 0.000 claims description 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 235000013305 food Nutrition 0.000 claims 1
- 230000000694 effects Effects 0.000 abstract description 9
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- 230000008569 process Effects 0.000 abstract description 2
- 230000001590 oxidative effect Effects 0.000 abstract 1
- 239000000686 essence Substances 0.000 description 41
- 240000008790 Musa x paradisiaca Species 0.000 description 39
- 239000000203 mixture Substances 0.000 description 15
- 230000000052 comparative effect Effects 0.000 description 13
- 239000000047 product Substances 0.000 description 12
- 230000003078 antioxidant effect Effects 0.000 description 9
- 230000003647 oxidation Effects 0.000 description 6
- 238000007254 oxidation reaction Methods 0.000 description 6
- 230000000391 smoking effect Effects 0.000 description 6
- 239000003963 antioxidant agent Substances 0.000 description 5
- 238000002835 absorbance Methods 0.000 description 3
- HHEAADYXPMHMCT-UHFFFAOYSA-N dpph Chemical compound [O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1[N]N(C=1C=CC=CC=1)C1=CC=CC=C1 HHEAADYXPMHMCT-UHFFFAOYSA-N 0.000 description 3
- 239000000779 smoke Substances 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- 244000246386 Mentha pulegium Species 0.000 description 2
- 235000016257 Mentha pulegium Nutrition 0.000 description 2
- 235000004357 Mentha x piperita Nutrition 0.000 description 2
- JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 2
- KAESVJOAVNADME-UHFFFAOYSA-N Pyrrole Chemical compound C=1C=CNC=1 KAESVJOAVNADME-UHFFFAOYSA-N 0.000 description 2
- 230000009286 beneficial effect Effects 0.000 description 2
- 239000008280 blood Substances 0.000 description 2
- 210000004369 blood Anatomy 0.000 description 2
- 235000001050 hortel pimenta Nutrition 0.000 description 2
- 150000002632 lipids Chemical class 0.000 description 2
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- 230000009044 synergistic interaction Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- QAIPRVGONGVQAS-DUXPYHPUSA-N trans-caffeic acid Chemical compound OC(=O)\C=C\C1=CC=C(O)C(O)=C1 QAIPRVGONGVQAS-DUXPYHPUSA-N 0.000 description 2
- AAWZDTNXLSGCEK-LNVDRNJUSA-N (3r,5r)-1,3,4,5-tetrahydroxycyclohexane-1-carboxylic acid Chemical compound O[C@@H]1CC(O)(C(O)=O)C[C@@H](O)C1O AAWZDTNXLSGCEK-LNVDRNJUSA-N 0.000 description 1
- ACEAELOMUCBPJP-UHFFFAOYSA-N (E)-3,4,5-trihydroxycinnamic acid Natural products OC(=O)C=CC1=CC(O)=C(O)C(O)=C1 ACEAELOMUCBPJP-UHFFFAOYSA-N 0.000 description 1
- OCZVHBZNPVABKX-UHFFFAOYSA-N 1,1-diphenyl-2-(2,4,6-trinitrophenyl)hydrazine;ethanol Chemical compound CCO.[O-][N+](=O)C1=CC([N+](=O)[O-])=CC([N+]([O-])=O)=C1NN(C=1C=CC=CC=1)C1=CC=CC=C1 OCZVHBZNPVABKX-UHFFFAOYSA-N 0.000 description 1
- 241000205585 Aquilegia canadensis Species 0.000 description 1
- 241000894006 Bacteria Species 0.000 description 1
- 102000030523 Catechol oxidase Human genes 0.000 description 1
- 108010031396 Catechol oxidase Proteins 0.000 description 1
- AAWZDTNXLSGCEK-UHFFFAOYSA-N Cordycepinsaeure Natural products OC1CC(O)(C(O)=O)CC(O)C1O AAWZDTNXLSGCEK-UHFFFAOYSA-N 0.000 description 1
- 241000208688 Eucommia Species 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- QIVBCDIJIAJPQS-VIFPVBQESA-N L-tryptophane Chemical compound C1=CC=C2C(C[C@H](N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-VIFPVBQESA-N 0.000 description 1
- 240000007707 Mentha arvensis Species 0.000 description 1
- 235000018978 Mentha arvensis Nutrition 0.000 description 1
- 235000016278 Mentha canadensis Nutrition 0.000 description 1
- 239000005925 Pymetrozine Substances 0.000 description 1
- AAWZDTNXLSGCEK-ZHQZDSKASA-N Quinic acid Natural products O[C@H]1CC(O)(C(O)=O)C[C@H](O)C1O AAWZDTNXLSGCEK-ZHQZDSKASA-N 0.000 description 1
- 102000007562 Serum Albumin Human genes 0.000 description 1
- 108010071390 Serum Albumin Proteins 0.000 description 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 1
- QIVBCDIJIAJPQS-UHFFFAOYSA-N Tryptophan Natural products C1=CC=C2C(CC(N)C(O)=O)=CNC2=C1 QIVBCDIJIAJPQS-UHFFFAOYSA-N 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 150000001299 aldehydes Chemical class 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- 239000010692 aromatic oil Substances 0.000 description 1
- 235000004883 caffeic acid Nutrition 0.000 description 1
- 229940074360 caffeic acid Drugs 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- QAIPRVGONGVQAS-UHFFFAOYSA-N cis-caffeic acid Natural products OC(=O)C=CC1=CC=C(O)C(O)=C1 QAIPRVGONGVQAS-UHFFFAOYSA-N 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 150000005690 diesters Chemical class 0.000 description 1
- 230000003467 diminishing effect Effects 0.000 description 1
- 230000008451 emotion Effects 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 150000002215 flavonoids Chemical class 0.000 description 1
- 235000003599 food sweetener Nutrition 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 150000002241 furanones Chemical class 0.000 description 1
- 210000000232 gallbladder Anatomy 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 210000004185 liver Anatomy 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 210000004877 mucosa Anatomy 0.000 description 1
- 230000000704 physical effect Effects 0.000 description 1
- 239000011148 porous material Substances 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- QHMTXANCGGJZRX-WUXMJOGZSA-N pymetrozine Chemical compound C1C(C)=NNC(=O)N1\N=C\C1=CC=CN=C1 QHMTXANCGGJZRX-WUXMJOGZSA-N 0.000 description 1
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 230000002000 scavenging effect Effects 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 239000003765 sweetening agent Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 235000018553 tannin Nutrition 0.000 description 1
- 239000001648 tannin Substances 0.000 description 1
- 229920001864 tannin Polymers 0.000 description 1
- 150000003573 thiols Chemical class 0.000 description 1
- 235000019505 tobacco product Nutrition 0.000 description 1
- 239000011726 vitamin B6 Substances 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention belongs to the technical field of essence, and particularly relates to essence for cigarettes as well as a preparation method and application thereof. The essence for the cigarettes comprises the following raw material components: chlorogenic acid, banana peel extract, menthol extract and solvent. The preparation method of the tobacco essence comprises the following steps: preparing a banana peel extract by taking banana peel as a raw material; mixing chlorogenic acid, banana peel extract, menthol extract and solvent to obtain the tobacco essence. The tobacco essence provided by the invention has the advantages of obvious effect of preventing and controlling oxidative deterioration, no negative influence on sensory evaluation, cooling and moistening throat, simple process, easy realization and the like.
Description
Technical Field
The invention belongs to the technical field of essence, and particularly relates to essence for cigarettes as well as a preparation method and application thereof.
Background
In the production of cigarettes, the flavor substances and the sweetener in the product are enriched by adding flavor and material so as to improve the flavor of smoke and improve the physical properties and the smoking taste of tobacco shreds, thereby ensuring that the smoking quality of cigarette products is more perfect and perfect. However, the essence and flavor are inevitably contacted with air in the production and processing processes, and some of the aroma components of the essence and flavor contain chemical bonds which are easy to oxidize and can be deteriorated due to oxidation. Such as: esters, aldehydes, thiols, furanones, aromatic oils with high amounts of unsaturated double bonds are very susceptible to deterioration during storage. Therefore, the existing tobacco essence generally has the defect of weak oxidation resistance.
Disclosure of Invention
The present invention is directed to solving at least one of the problems of the prior art described above. Therefore, the invention provides the tobacco essence and the preparation method and the application thereof, and aims to solve the problem that the existing tobacco essence is weak in oxidation resistance.
The invention provides a tobacco essence which comprises the following raw material components: chlorogenic acid, banana peel extract, menthol extract and solvent.
According to some embodiments of the invention, the essence for tobacco comprises the following raw material components in parts by weight: 20-40 parts of chlorogenic acid, 20-40 parts of banana peel extract, 1-5 parts of menthol extract and 10-40 parts of solvent.
Chlorogenic acid, also known as coffee tannin, is a diester of caffeic acid and quinic acid, has weak faint scent, can form polyquinone under the action of polyphenol oxidase, and can perform non-enzymatic browning reaction with amino acid to generate substances such as pymetrozine, pyridine, pyrrole and the like. The flavonoids can endow smoke with sweet and roasted fragrance. Chlorogenic acid is a main effective component of a plurality of Chinese herbal medicines such as honeysuckle, eucommia bark and the like, and researches show that the chlorogenic acid has multiple effects of resisting oxidation, resisting bacteria, diminishing inflammation, resisting viruses, reducing blood sugar, reducing blood fat, protecting liver and benefiting gallbladder and the like.
The menthol extract is a white crystal extracted from the leaf and stem of Mentha arvensis, and has a molecular formula of C10H200Essential components of peppermint and peppermint essential oils; can be used for cooling skin or mucosa to relieve discomfort and pain.
The banana peel is rich in tryptophan and vitamin B6The serum albumin is rich, comfortable, satisfied and optimistic emotion can be generated, and the antioxidant effect is certain.
Although chlorogenic acid and banana peel in the raw materials may have certain antioxidant performance, the antioxidant performance of the chlorogenic acid and banana peel is limited, and the antioxidant requirement of the tobacco essence cannot be met. The invention creatively discovers that the reasonable compounding of the chlorogenic acid, the banana peel extract and the menthol extract can generate a synergistic interaction effect and can achieve better expected oxidation resistance.
According to some embodiments of the invention, the solvent is selected from propylene glycol and water.
According to some embodiments of the invention, the solvent is propylene glycol and water, and the mass ratio of propylene glycol to water is 1: 1.
According to some embodiments of the invention, the chlorogenic acid and the menthol extract are both food-grade additives.
The second aspect of the invention provides a preparation method of the tobacco essence, which comprises the following steps:
(1) preparing a banana peel extract by taking banana peel as a raw material;
(2) mixing chlorogenic acid, menthol extract, solvent and banana peel extract to obtain the tobacco essence.
According to some embodiments of the invention, the banana peel extract is prepared by the steps of:
(1-1) crushing the banana peel into slag to obtain crushed banana peel;
(1-2) mixing and heating the complex enzyme, water and the crushed banana peel to obtain a heated product;
(1-3) adding sodium benzoate, titanium dioxide, riboflavin, adipic acid, sodium sulfate and n-butanol into the heated product, heating, and filtering to obtain the banana peel extract.
According to some embodiments of the invention, the complex enzyme comprises pectinase and cellulase.
According to some embodiments of the invention, the step (1-2) comprises: mixing the complex enzyme, water and the crushed banana peel, adjusting the pH value of the mixture to 5.0-5.3, adjusting the temperature of the mixture to 40-50 ℃, and keeping the temperature for 40-60 min so as to fully mix the complex enzyme and the banana peel for enzymolysis; and then adjusting the temperature of the mixture to 100 ℃, and keeping the temperature for 10min to ensure that the complex enzyme loses activity, thereby obtaining a heated product.
According to some embodiments of the present invention, the heating temperature in step (1-3) is 100 ℃, the heating time is 90min, the filtration step further comprises a concentration step, and the filtrate obtained by filtration is concentrated.
The third aspect of the invention provides an application of the tobacco essence in preparing an electronic cigarette.
The fourth aspect of the invention provides an application of the tobacco essence in preparing cigarettes.
According to some embodiments of the invention, the tobacco essence is added into tobacco leaves according to the proportion of 0.1-0.15% of the mass of the tobacco leaves, and the tobacco is prepared into cigarettes.
Compared with the prior art, the invention has the following beneficial effects:
(1) the chlorogenic acid, the banana peel extract and the menthol extract are compatible together to generate a synergistic effect, and the prepared tobacco essence has the advantages of obvious oxidation deterioration prevention and control effect and no negative influence on sensory evaluation;
(2) the menthol extract contained in the essence for cigarettes has certain cooling and throat moistening effects, and is beneficial to reducing the irritation of smoke generated by burning cigarettes to the throat and improving the smoking taste of the cigarettes;
(3) the preparation process of the tobacco essence is simple, and industrial production can be realized.
Detailed Description
In order to make the technical solutions of the present invention more apparent to those skilled in the art, the following examples are given for illustration. It should be noted that the following examples are not intended to limit the scope of the claimed invention.
The starting materials, reagents or apparatuses used in the following examples are conventionally commercially available or can be obtained by conventionally known methods, unless otherwise specified.
Example 1
An essence for cigarette comprises 20g of chlorogenic acid, 15g of banana peel extract, 5g of menthol extract, 20g of propylene glycol and 20g of water, wherein the chlorogenic acid and the menthol extract are purchased food-grade additives.
The preparation method of the tobacco essence comprises the following steps:
(1) crushing banana peel into slag to obtain crushed banana peel;
(2) mixing the pulverized banana peel, pectinase, cellulase and water, adjusting the pH value of the mixture to 5.0-5.3, adjusting the temperature of the mixture to 40-50 ℃, and keeping the temperature for 40-60 min;
(3) adjusting the temperature of the mixture to 100 ℃ and keeping the temperature for 10 min; obtaining a heated product;
(4) adding 1.1g of sodium benzoate, 0.7g of titanium dioxide, 8.2g of riboflavin, 4g of adipic acid, 13g of sodium sulfate and 15ml of n-butanol into the heated product, heating at 100 ℃ for 90min, filtering, and concentrating to obtain a banana peel extract;
(5) mixing chlorogenic acid, menthol extract, propylene glycol, water and banana peel extract to obtain the tobacco essence.
Example 2
An essence for cigarette comprises chlorogenic acid 15g, banana peel extract 20g, menthol extract 5g, propylene glycol 20g and water 20g, wherein the chlorogenic acid and the menthol extract are edible additives purchased from outsourcing.
The preparation method of the tobacco essence comprises the following steps:
(1) crushing banana peel into slag to obtain crushed banana peel;
(2) mixing the pulverized banana peel, pectinase, cellulase and water, adjusting the pH value of the mixture to 5.0-5.3, adjusting the temperature of the mixture to 40-50 ℃, and keeping the temperature for 40-60 min;
(3) adjusting the temperature of the mixture to 100 ℃ and keeping the temperature for 10 min; obtaining a heated product;
(4) adding 0.55g of sodium benzoate, 0.35g of titanium dioxide, 4.1g of riboflavin, 2g of adipic acid, 6.5g of sodium sulfate and 7.5ml of n-butanol into the heated product, heating at 100 ℃ for 90min, filtering, and concentrating to obtain a banana peel extract;
(5) mixing chlorogenic acid, menthol extract, propylene glycol, water and banana peel extract to obtain the tobacco essence.
Example 3
An essence for cigarette comprises chlorogenic acid 10g, banana peel extract 25g, menthol extract 5g, propylene glycol 20g and water 20g, wherein the chlorogenic acid and the menthol extract are edible additives purchased from outsourcing.
The preparation method of the tobacco essence comprises the following steps:
(1) crushing banana peel into slag to obtain crushed banana peel;
(2) mixing the pulverized banana peel, pectinase, cellulase and water, adjusting the pH value of the mixture to 5.0-5.3, adjusting the temperature of the mixture to 40-50 ℃, and keeping the temperature for 40-60 min;
(3) adjusting the temperature of the mixture to 100 ℃ and keeping the temperature for 10 min; obtaining a heated product;
(4) adding 0.55g of sodium benzoate, 0.35g of titanium dioxide, 4.1g of riboflavin, 2g of adipic acid, 6.5g of sodium sulfate and 7.5ml of n-butanol into the heated product, heating at 100 ℃ for 90min, filtering, and concentrating to obtain a banana peel extract;
(5) mixing chlorogenic acid, menthol extract, propylene glycol, water and banana peel extract to obtain the tobacco essence.
Comparative example 1
This comparative example provides an essence for cigarette, compares with example 1, and its difference lies in: the tobacco essence comprises 40g of chlorogenic acid, 20g of propylene glycol and 20g of water.
Comparative example 2
This comparative example provides an essence for cigarette, compares with example 1, and its difference lies in: the tobacco essence comprises 20g of chlorogenic acid, 20g of banana peel extract, 20g of propylene glycol and 20g of water.
Comparative example 3
This comparative example provides an essence for cigarette, compares with example 1, and its difference lies in: the tobacco essence comprises 10g of chlorogenic acid, 20g of banana peel extract, 10g of menthol extract, 20g of propylene glycol and 20g of water.
Product effectiveness testing
(1) The antioxidant activity of the tobacco flavor prepared in examples 1 to 3 and comparative examples 1 to 3 was measured
The tobacco essences prepared in examples 1 to 3 and comparative examples 1 to 3 were tested for their activity of scavenging lipid free radical DPPH (1, 1-diphenyl-2-trinitrophenylhydrazine) at a concentration of 50. mu.g/mL as a primary sieve.
Taking a costar96 pore plate, adding the mixture into the prepared mixture with the molar concentration of 6.5 multiplied by 105Adding 190 mu L/hole of a DPPH ethanol solution of mol/L, adding 10 mu L/hole of a sample to be tested (the essence for cigarettes prepared in examples 1-3 and comparative examples 1-3), adding 10 mu L of normal saline into blank holes, fully mixing, sealing the blank holes with a sealing plate film, standing in a dark place for 30 minutes at room temperature, and measuring the absorbance value of each hole on a UV2401 spectrophotometer determinator, wherein the measurement wavelength is 517 nm; according to the formula: DPPH clearance (%) - (a)Blank space-ASample (I))/ABlank spaceX 100%, calculating the DPPH clearance rate of each sample to the lipid free radicals; wherein A isBlank spaceThe absorbance value of the blank control group is obtained; a. theSample (I)Calculating the half clearance concentration IC of the sample for the absorbance value of the sample-added group50And (6) measuring results.
The test results are: IC of tobacco flavor prepared in examples 1 to 3 and comparative examples 1 to 350The antioxidant activity of the tobacco essence prepared in the embodiments 1-3 is better than that of the tobacco essence prepared in the comparative examples 1-3, as shown by 3.87 mug/L, 3.88 mug/L, 3.85 mug/L, 4.52 mug/L, 4.92 mug/L and 4.86 mug/L respectively. The results show that the reasonable compatibility of the chlorogenic acid, the banana peel extract and the menthol extract can generate a synergistic interaction effect, so that the antioxidant effect which is obviously superior to that of a single raw material component is generated, the antioxidant performance of the chlorogenic acid, the banana peel extract and the menthol extract is more outstanding, and the requirement of a tobacco product on the antioxidant performance of the essence can be met.
(2) The tobacco essence prepared in the examples 1-3 and the comparative examples 1-3 is added into cigarettes for sensory evaluation.
The smoking result shows that the tobacco essence prepared in the examples 1-3 and the comparative example 3 has no obvious negative effect on the sensory smoking result of the cigarette; and the coolness and softness of cigarette smoking are slightly improved.
The above embodiments are preferred embodiments of the present invention, but the embodiments of the present invention are not limited to the above embodiments, and any other changes, modifications, substitutions, combinations, and simplifications which do not depart from the spirit and principle of the present invention should be construed as equivalents thereof, and all such changes, modifications, substitutions, combinations, and simplifications are intended to be included in the scope of the present invention.
Claims (10)
1. The essence for the cigarettes is characterized by comprising the following raw material components: chlorogenic acid, banana peel extract, menthol extract and solvent.
2. The tobacco essence according to claim 1, which comprises the following raw material components in parts by weight: 20-40 parts of chlorogenic acid, 10-40 parts of banana peel extract, 1-5 parts of menthol extract and 10-60 parts of solvent.
3. The tobacco flavor according to claim 1, wherein the solvent is selected from propylene glycol and water.
4. The tobacco flavor according to claim 1, wherein the chlorogenic acid and the menthol extract are food grade additives.
5. A preparation method of the tobacco essence as claimed in any one of claims 1 to 4, which is characterized by comprising the following steps:
preparing a banana peel extract by taking banana peel as a raw material;
mixing chlorogenic acid, a menthol extract, a solvent and a banana peel extract to obtain the tobacco essence.
6. The method for preparing the banana peel extract according to claim 5, wherein the banana peel extract is prepared by the steps of:
(1) crushing the banana peel into slag to obtain crushed banana peel;
(2) mixing and heating the complex enzyme, water and the crushed banana peel to obtain a heated product;
adding sodium benzoate, titanium dioxide, riboflavin, adipic acid, sodium sulfate and n-butanol into the heated product, heating, and filtering to obtain banana peel extract.
7. The method for preparing the compound enzyme of claim 6, wherein the compound enzyme comprises pectinase and cellulase.
8. The method according to claim 6, wherein the step (2) is a step of: mixing the complex enzyme, water and the crushed banana peel, standing, and heating to 100 ℃ to obtain a heated product.
9. Use of the tobacco flavor according to any one of claims 1 to 4 in the preparation of an electronic cigarette.
10. Use of the tobacco flavor according to any one of claims 1 to 4 in the preparation of cigarettes.
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| CN108283329A (en) * | 2018-01-25 | 2018-07-17 | 云南中烟工业有限责任公司 | A kind of methods and applications extracting polyphenol compound from tobacco waste |
| CN112641027A (en) * | 2019-10-10 | 2021-04-13 | 湖北文理学院 | Banana peel antioxidant additive and preparation method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN108283329A (en) * | 2018-01-25 | 2018-07-17 | 云南中烟工业有限责任公司 | A kind of methods and applications extracting polyphenol compound from tobacco waste |
| CN112641027A (en) * | 2019-10-10 | 2021-04-13 | 湖北文理学院 | Banana peel antioxidant additive and preparation method thereof |
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