CN113399234A - Epoxy spraying insulation treatment method for superconducting undulator framework - Google Patents

Epoxy spraying insulation treatment method for superconducting undulator framework Download PDF

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Publication number
CN113399234A
CN113399234A CN202110570664.1A CN202110570664A CN113399234A CN 113399234 A CN113399234 A CN 113399234A CN 202110570664 A CN202110570664 A CN 202110570664A CN 113399234 A CN113399234 A CN 113399234A
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CN
China
Prior art keywords
superconducting undulator
framework
skeleton
superconducting
undulator
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Pending
Application number
CN202110570664.1A
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Chinese (zh)
Inventor
杨向臣
张亮
戴旭文
李煜辉
陆辉华
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Institute of High Energy Physics of CAS
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Institute of High Energy Physics of CAS
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Priority to CN202110570664.1A priority Critical patent/CN113399234A/en
Publication of CN113399234A publication Critical patent/CN113399234A/en
Pending legal-status Critical Current

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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D7/00Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials
    • B05D7/14Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials to metal, e.g. car bodies
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D1/00Processes for applying liquids or other fluent materials
    • B05D1/02Processes for applying liquids or other fluent materials performed by spraying
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D1/00Processes for applying liquids or other fluent materials
    • B05D1/18Processes for applying liquids or other fluent materials performed by dipping
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D1/00Processes for applying liquids or other fluent materials
    • B05D1/32Processes for applying liquids or other fluent materials using means for protecting parts of a surface not to be coated, e.g. using stencils, resists
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D7/00Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials
    • B05D7/24Processes, other than flocking, specially adapted for applying liquids or other fluent materials to particular surfaces or for applying particular liquids or other fluent materials for applying particular liquids or other fluent materials
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F41/00Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
    • H01F41/02Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets
    • H01F41/04Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets for manufacturing coils
    • H01F41/12Insulating of windings
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01FMAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
    • H01F41/00Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties
    • H01F41/02Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets
    • H01F41/04Apparatus or processes specially adapted for manufacturing or assembling magnets, inductances or transformers; Apparatus or processes specially adapted for manufacturing materials characterised by their magnetic properties for manufacturing cores, coils, or magnets for manufacturing coils
    • H01F41/12Insulating of windings
    • H01F41/127Encapsulating or impregnating
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D2202/00Metallic substrate
    • B05D2202/10Metallic substrate based on Fe
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05DPROCESSES FOR APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05D2504/00Epoxy polymers

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  • Engineering & Computer Science (AREA)
  • Power Engineering (AREA)
  • Manufacturing & Machinery (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Superconductors And Manufacturing Methods Therefor (AREA)

Abstract

The invention discloses an epoxy spraying insulation treatment method for a superconducting undulator framework, which comprises the following steps: 1) integrally processing and preparing an iron core framework and a magnetic pole of the superconducting undulator framework to obtain the superconducting undulator framework; wherein, the thickness L1 of the epoxy coating is reserved on the prepared superconducting undulator skeleton; 2) spraying an epoxy coating with the thickness of L2 on the superconducting undulator skeleton prepared in the step 1); wherein L2 is greater than L1; 3) curing the sprayed epoxy coating of step 2); 4) and (4) performing finish machining on the superconducting undulator skeleton of the cured epoxy coating, and removing redundant spraying to obtain the superconducting undulator skeleton after insulation treatment. The invention mainly adopts low-temperature epoxy as an insulating coating, solves the problem of insulating the superconducting undulator framework to the ground, and can ensure the bonding strength between the superconducting undulator framework and the coil and between the superconducting undulator framework and the impregnating epoxy.

Description

Epoxy spraying insulation treatment method for superconducting undulator framework
Technical Field
The invention relates to an epoxy spraying insulation treatment method for a superconducting undulator framework, and belongs to the technical field of low-temperature superconduction of accelerators.
Background
The superconducting undulator magnetic pole mainly comprises a superconducting coil and an iron core framework, a plurality of wire grooves are processed on the framework, the coil is wound on the iron core framework, the process needs to ensure the insulation between the coil and the framework, and the general insulation treatment process comprises the following steps:
1. insulating materials (such as insulating tapes or insulating plates) are pasted inside the wire grooves, but the geometric dimension of the wire grooves is very limited for the short-period superconducting undulator, and the insulating treatment process cannot be applied.
2. The framework is processed in a split way and is divided into an upper side plate, a magnetic pole and an iron core framework. The upper side plate is processed into G10 insulating material, and the magnetic poles are subjected to independent insulation treatment and then all the parts are integrally assembled.
If the superconducting undulator does not perform insulation treatment on the iron core framework, the superconducting undulator only depends on the self insulating layer of the superconducting wire to realize ground insulation, and the voltage-resistant effect is poor. Especially for magnets with high stored energy, the high voltage generated by quench can damage the magnet coils. Meanwhile, the superconducting undulator has high requirements on the phase error of a magnetic field, and the size precision of a magnetic pole and an iron core framework is greatly influenced by the subjectivity of an operator and has poor repeatability by the process of manually bonding an insulating material; the split machining and the integral assembling of the iron core framework can introduce larger assembling errors, which can all have fatal influence on the precision of the magnetic field.
After the winding of the superconducting undulator coil is finished, vacuum epoxy impregnation is needed, the coil, the framework and the impregnating epoxy need to have enough bonding strength, and the bonding force of the common insulating material with the metal framework and the impregnating epoxy is very limited. Especially, after the coil is cooled, the skeleton is often stripped from the impregnated epoxy, which affects the overall performance of the magnet.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to disclose an epoxy spraying insulation treatment method for a framework of a superconducting undulator and a preparation method for a magnetic pole of the superconducting undulator. The invention mainly adopts low-temperature epoxy as an insulating coating, solves the problem of insulating the superconducting undulator framework to the ground, and can ensure the bonding strength between the superconducting undulator framework and the coil and between the superconducting undulator framework and the impregnating epoxy.
Because the superconducting undulator has very high requirements on the phase error of the magnetic field, the invention adopts an integrated processing mode for the magnetic pole and the iron core framework; and (4) cleaning the surface of the superconducting undulator skeleton obtained after the processing is finished, and then subsequently finishing spraying insulation after the cleaning is finished.
And (3) performing epoxy spraying after the low-temperature epoxy adhesive required by spraying reaches the spraying viscosity, and placing the sprayed superconducting undulator skeleton into an oven for curing. And after the solidification is finished, performing finish machining on the superconducting undulator skeleton by using a numerical control machine tool, removing redundant spraying thickness, and performing a subsequent coil winding process after the required precision is achieved.
The spraying material of the superconducting undulator framework selects low-temperature epoxy resin, so that the bonding strength with the coil, the framework and the impregnated epoxy glue is ensured.
The technical scheme of the invention is as follows:
an epoxy spraying insulation treatment method for a superconducting undulator framework comprises the following steps:
1) integrally processing and preparing an iron core framework and a magnetic pole of the superconducting undulator framework to obtain the superconducting undulator framework; wherein, the thickness L1 of the epoxy coating is reserved on the prepared superconducting undulator skeleton;
2) spraying an epoxy coating with the thickness of L2 on the superconducting undulator skeleton prepared in the step 1); wherein L2 is greater than L1;
3) curing the sprayed epoxy coating of step 2);
4) and (4) performing finish machining on the superconducting undulator skeleton of the cured epoxy coating, and removing redundant spraying to obtain the superconducting undulator skeleton after insulation treatment.
Further, in the step 2), the low-temperature epoxy adhesive is diluted by a diluent and then atomized and sprayed, and high-pressure gas used for spraying is high-purity nitrogen.
Further, in the step 2), the part which does not need to be adhered by the epoxy coating is protected before spraying.
Further, the sprayed epoxy coating in the step 2) is cured according to a set epoxy glue temperature curing curve.
Further, the superconducting undulator framework sprayed with the epoxy coating in the step 2) is placed in an oven for curing.
Further, the thickness L1 of the epoxy coating is 0.1 mm; the spraying thickness L2 is 0.15-0.2 mm.
A preparation method of a superconducting undulator magnetic pole comprises the following steps:
1) integrally processing and preparing an iron core framework and a magnetic pole of the superconducting undulator framework to obtain the superconducting undulator framework; wherein, the thickness L1 of the epoxy coating is reserved on the prepared superconducting undulator skeleton;
2) spraying an epoxy coating with the thickness of L2 on the superconducting undulator skeleton prepared in the step 1); wherein L2 is greater than L1;
3) curing the sprayed epoxy coating of step 2);
4) performing finish machining on the superconducting undulator skeleton of the cured epoxy coating, and removing redundant spraying to obtain the superconducting undulator skeleton after insulation treatment;
5) and preparing a superconducting undulator coil skeleton based on the superconducting undulator skeleton after insulation treatment, and then carrying out coil winding and vacuum epoxy impregnation on the superconducting undulator coil skeleton to obtain the superconducting undulator magnetic pole.
Compared with the prior art, the invention has the following advantages:
1. the superconducting undulator framework is integrally processed, so that the quality of a magnetic field can be ensured, and the phase error of the magnetic field can be ensured.
2. The winding groove of the superconducting undulator adopts epoxy spraying, so that the insulation quality can be ensured, and the bonding strength of an insulation layer, a framework and impregnated low-temperature glue can also be ensured.
Drawings
FIG. 1 is a process flow diagram of the present invention.
Detailed Description
To facilitate an understanding of the key technology of the present invention, the following description is given by way of a specific example:
the iron core framework and the magnetic pole pieces are integrally processed to obtain the superconducting undulator framework, and the main purpose is to ensure the position precision of each magnetic pole piece generating a magnetic field and ensure the quality of the magnetic field. The low-temperature epoxy is adopted as the insulating coating, and the insulating layer has good low-temperature performance and adhesive force. The processing size of the superconducting undulator framework needs to reserve the size allowance (designed to be 0.1mm) of the thickness of the epoxy coating.
The surface of the superconducting undulator skeleton is firstly cleaned by gasoline to remove oil stains, impurities and the like on the surface, after the surface is sufficiently cleaned, the superconducting undulator skeleton is placed in acetone again to finish further cleaning, and the epoxy coating sprayed subsequently can be bonded with the superconducting undulator skeleton and fall off due to insufficient cleaning. And after the superconducting undulator framework is cleaned, drying the superconducting undulator framework to wait for the subsequent epoxy spraying operation. The insulating coating is made of low-temperature epoxy glue with good toughness, atomization spraying can be carried out only when the viscosity reaches an ideal condition after the epoxy glue is diluted by a diluent, and high-pressure gas used for spraying is high-purity nitrogen. The part which does not need to be adhered with the epoxy coating is protected before spraying, and the unilateral thickness of the insulating coating is larger than the designed size allowance. The thickness of a single side of a common insulating coating is designed to be 0.15-0.2 mm. And after the spraying is finished, placing the framework in an oven, and curing according to a set epoxy glue temperature curing curve. And after the curing is finished, performing finish machining on the superconducting undulator framework by using a numerical control milling machine, cutting for multiple times in the machining process, avoiding the cutting force of the machine tool from damaging the surface of the coating, and finally ensuring that the thickness of the epoxy insulation layer is 0.1mm without using cutting fluid in the whole process. After the machining is finished, alcohol cleaning needs to be carried out on the superconducting undulator framework, and subsequent winding work is prepared.
The above description is only a preferred embodiment of the present invention, and is not intended to limit the technical scope of the present invention, and those skilled in the art may make modifications and variations within the spirit of the present invention, and all modifications, equivalents and modifications of the above embodiments according to the technical spirit of the present invention are within the scope of the present invention.

Claims (9)

1. An epoxy spraying insulation treatment method for a superconducting undulator framework comprises the following steps:
1) integrally processing and preparing an iron core framework and a magnetic pole of the superconducting undulator framework to obtain the superconducting undulator framework; wherein, the thickness L1 of the epoxy coating is reserved on the prepared superconducting undulator skeleton;
2) spraying an epoxy coating with the thickness of L2 on the superconducting undulator skeleton prepared in the step 1); wherein L2 is greater than L1;
3) curing the sprayed epoxy coating of step 2);
4) and (4) performing finish machining on the superconducting undulator skeleton of the cured epoxy coating, and removing redundant spraying to obtain the superconducting undulator skeleton after insulation treatment.
2. The method as claimed in claim 1, wherein in the step 2), the low-temperature epoxy glue is diluted by a diluent and then atomized and sprayed, and the high-pressure gas used for spraying is high-purity nitrogen.
3. A method according to claim 1 or 2, characterised in that in step 2) the areas which do not require the epoxy coating to adhere are protected before spraying.
4. The method of claim 3, wherein the sprayed epoxy coating of step 2) is cured according to a set epoxy glue temperature cure profile.
5. The method of claim 1 or 2, wherein the superconducting undulator skeleton after the epoxy coating of step 2) is placed in an oven for curing.
6. The method of claim 1, wherein the epoxy coating thickness L1 is 0.1 mm; the spraying thickness L2 is 0.15-0.2 mm.
7. A preparation method of a superconducting undulator magnetic pole comprises the following steps:
1) integrally processing and preparing an iron core framework and a magnetic pole of the superconducting undulator framework to obtain the superconducting undulator framework; wherein, the thickness L1 of the epoxy coating is reserved on the prepared superconducting undulator skeleton;
2) spraying an epoxy coating with the thickness of L2 on the superconducting undulator skeleton prepared in the step 1); wherein L2 is greater than L1;
3) curing the sprayed epoxy coating of step 2);
4) performing finish machining on the superconducting undulator skeleton of the cured epoxy coating, and removing redundant spraying to obtain the superconducting undulator skeleton after insulation treatment;
5) and preparing a superconducting undulator coil skeleton based on the superconducting undulator skeleton after insulation treatment, and then carrying out coil winding and vacuum epoxy impregnation on the superconducting undulator coil skeleton to obtain the superconducting undulator magnetic pole.
8. The method as claimed in claim 7, wherein in the step 2), the low-temperature epoxy glue is diluted by a diluent and then atomized and sprayed, and the high-pressure gas used for spraying is high-purity nitrogen.
9. The method of claim 7, wherein the epoxy coating thickness L1 is 0.1 mm; the spraying thickness L2 is 0.15-0.2 mm.
CN202110570664.1A 2021-05-25 2021-05-25 Epoxy spraying insulation treatment method for superconducting undulator framework Pending CN113399234A (en)

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Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6344287B1 (en) * 1997-04-14 2002-02-05 Florida State University High temperature compatible insulation for superconductors and method of applying insulation to superconductors
CN102755955A (en) * 2012-07-31 2012-10-31 东莞市晶磁科技有限公司 Amorphous magnetic core surface coating process
CN102945722A (en) * 2012-11-27 2013-02-27 中国科学院上海应用物理研究所 Magnesium diboride superconductive undulator
CN102956279A (en) * 2012-10-25 2013-03-06 中国科学院上海应用物理研究所 Undulator and manufacture method thereof
CN103128039A (en) * 2011-12-01 2013-06-05 上海电气集团股份有限公司 Coating method of winding amorphous iron core insulating coating
CN103440953A (en) * 2013-09-17 2013-12-11 中国科学院上海应用物理研究所 Superconducting undulator magnet

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6344287B1 (en) * 1997-04-14 2002-02-05 Florida State University High temperature compatible insulation for superconductors and method of applying insulation to superconductors
CN103128039A (en) * 2011-12-01 2013-06-05 上海电气集团股份有限公司 Coating method of winding amorphous iron core insulating coating
CN102755955A (en) * 2012-07-31 2012-10-31 东莞市晶磁科技有限公司 Amorphous magnetic core surface coating process
CN102956279A (en) * 2012-10-25 2013-03-06 中国科学院上海应用物理研究所 Undulator and manufacture method thereof
CN102945722A (en) * 2012-11-27 2013-02-27 中国科学院上海应用物理研究所 Magnesium diboride superconductive undulator
CN103440953A (en) * 2013-09-17 2013-12-11 中国科学院上海应用物理研究所 Superconducting undulator magnet

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