CN113351952B - Butt brazing method for valvable alloy and copper - Google Patents
Butt brazing method for valvable alloy and copper Download PDFInfo
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- CN113351952B CN113351952B CN202110706854.1A CN202110706854A CN113351952B CN 113351952 B CN113351952 B CN 113351952B CN 202110706854 A CN202110706854 A CN 202110706854A CN 113351952 B CN113351952 B CN 113351952B
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K1/00—Soldering, e.g. brazing, or unsoldering
- B23K1/0008—Soldering, e.g. brazing, or unsoldering specially adapted for particular articles or work
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K1/00—Soldering, e.g. brazing, or unsoldering
- B23K1/002—Soldering by means of induction heating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K1/00—Soldering, e.g. brazing, or unsoldering
- B23K1/20—Preliminary treatment of work or areas to be soldered, e.g. in respect of a galvanic coating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K1/00—Soldering, e.g. brazing, or unsoldering
- B23K1/20—Preliminary treatment of work or areas to be soldered, e.g. in respect of a galvanic coating
- B23K1/206—Cleaning
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K13/00—Welding by high-frequency current heating
- B23K13/01—Welding by high-frequency current heating by induction heating
- B23K13/02—Seam welding
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K3/00—Tools, devices, or special appurtenances for soldering, e.g. brazing, or unsoldering, not specially adapted for particular methods
- B23K3/04—Heating appliances
- B23K3/047—Heating appliances electric
- B23K3/0475—Heating appliances electric using induction effects, e.g. Kelvin or skin effects
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
- B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
- B23K3/00—Tools, devices, or special appurtenances for soldering, e.g. brazing, or unsoldering, not specially adapted for particular methods
- B23K3/08—Auxiliary devices therefor
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/25—Process efficiency
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- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Health & Medical Sciences (AREA)
- Dermatology (AREA)
- General Health & Medical Sciences (AREA)
- General Induction Heating (AREA)
Abstract
The invention provides a butt brazing method of a valvable alloy and copper, which comprises the following steps: firstly, butting a workpiece A made of a valve alloy and a workpiece B made of copper, placing a proper amount of brazing filler metal and soldering flux at the joint, and placing a heating rod of high-frequency induction heating equipment around the joint; heating the brazing filler metal and the brazing flux to a preheating temperature and keeping the preheating temperature for a proper time; heating to a melting temperature to melt the brazing filler metal, the brazing flux and part of the material of the workpiece to form a welding seam; naturally standing the welding line for a proper time, heating the welding line to a melting temperature, keeping the welding line for a proper time, and naturally cooling the welding line to the normal temperature. By adopting the technical scheme of the invention, the heating rod is set to be in a closed annular shape, the periphery of the joint of the workpiece is uniformly heated, and the step-by-step procedures of preheating, reheating and strengthening are adopted in the welding process, so that the brazing filler metal is uniformly fused with the workpiece material and penetrates into the workpiece material through the capillary effect, and the welding seam strength and the welding quality are improved.
Description
Technical Field
The invention belongs to the technical field of brazing processes, and particularly relates to a butt brazing method of a valvable alloy and copper.
Background
In the welding process, the welding between dissimilar metal materials is always difficult, the brazing process technology is a welding technology which leads brazing filler metal to be filled in gaps between the joints of workpieces under the action of capillary and gravity by heating the brazing filler metal in a liquid state, the brazing process technology has the advantages of short welding time, high efficiency, high precision and the like, and is particularly suitable for welding and connecting workpieces with complex shapes, the existing brazing process technology mainly comprises two processes of high-frequency heating brazing and flame heating brazing, however, the research on the brazing process technology of two dissimilar metal materials of valvable alloy and copper is not reported at present, in the brazing process of the valvable alloy and the thin-wall copper pipe, because the wall of the copper pipe is thick and thin, the valvable alloy and the thin-wall copper pipe are connected through a thread pair, the thread pair has small tooth profile, and the heating temperature of the brazing filler metal is difficult to control through high-frequency induction heating equipment, if the temperature is too high, the temperature is easy to exceed the melting point of the copper pipe, the copper pipe is melted, and parts are scrapped; if the heating temperature is too low, the melting point of the silver solder cannot be reached, the solder is difficult to permeate into the threads through the capillary action and the gravity action, secondary heating is needed, in addition, the capillary action is very weak during brazing heating, if a corner interrupting the capillary action of the solder is formed, the fluidity of the solder is poor, meanwhile, the solder accumulation is easy to occur at the root of the threads, the control of uneven brazing gaps is difficult, and the requirement on the thread machining precision is high; the clearance is too small, and the threads are difficult to screw; too large gaps cause insufficient brazing filler metal amount and low brazing filler metal penetration rate; when the amount of the brazing filler metal is insufficient, the external brazing filler metal is difficult to supplement, and the strength of a welding seam is influenced.
Disclosure of Invention
In order to solve the technical problem, the invention provides a butt brazing method of a valvable alloy and copper.
The invention is realized by the following technical scheme.
The invention provides a butt brazing method of a valvable alloy and copper, which comprises the following steps:
step one; a preparation stage: providing high-frequency induction heating equipment, wherein the high-frequency induction heating equipment comprises a heating rod, the heating rod is of a closed annular structure, a workpiece A made of a valvable alloy is butted with a workpiece B made of copper, then a proper amount of brazing filler metal is placed at the butted position of the workpiece A and the workpiece B, then a proper amount of soldering flux is coated at the butted position of the workpiece A and the workpiece B, and then the heating rod is placed around the butted position of the workpiece A and the workpiece B;
step two: a preheating stage: heating the brazing filler metal and the brazing flux to a preheating temperature by high-frequency induction heating equipment, and keeping the preheating temperature for a proper time, and then carrying out the next step;
step three: and (3) brazing: heating the brazing filler metal and the brazing flux to a melting temperature by high-frequency induction heating equipment, keeping the melting temperature for a proper time, melting the brazing filler metal and the brazing flux with part of materials of the workpiece A or the workpiece B to form a welding seam, and then carrying out the next step;
step four: and (3) strengthening stage: naturally standing the welding line in the third step for a proper time, heating the welding line to a melting temperature through high-frequency induction heating equipment, keeping the temperature for a proper time, naturally cooling the welding line to normal temperature, and finishing.
In the first step, the workpiece A and the workpiece B are butted together through a thread pair.
The butt brazing method of the valvable alloy and the copper further comprises the following steps: before the first step, cleaning the workpiece A and the workpiece B by using an ultrasonic cleaning machine, wherein a cleaning solvent is a mixed solvent of acetone and alcohol, the cleaning duration is 25-35 min, and the workpiece A or the workpiece B is vibrated at the frequency of 30-50 Hz in the cleaning process.
The butt brazing method of the valvable alloy and the copper further comprises the following steps: after the workpiece A and the workpiece B are cleaned by using an ultrasonic cleaning machine, the workpiece A and the workpiece B are placed in an oven for drying, a fan is installed in the oven, and the temperature in the oven is controlled to be 70 ℃ and is maintained for 40-60 min.
In the second step, the preheating temperature is 400-450 ℃, and the preheating temperature holding time is 5-8 s.
And in the third step, in the process of heating the brazing filler metal and the brazing flux to the melting temperature, the heating speed of the brazing filler metal and the brazing flux is controlled not to exceed 150 ℃/s.
The melting temperature in the third step is 730-780 ℃, and the holding time of the melting temperature is 5-8 s.
In the fourth step, the standing time of the welding line is 1s, the melting temperature is 730-780 ℃, and the holding time of the melting temperature is 2-3 s.
The butt brazing method of the valvable alloy and the copper further comprises the following steps: before the second step, starting high-frequency induction heating equipment to preheat the heating rod for 10-20 min, and then carrying out the next step.
And in the process of performing the second step, the third step or the fourth step, argon is blown aiming at the brazing filler metal and the brazing flux, the purity of the argon is not less than 99.99 percent, the pressure of the argon is not less than 1.5MPa, and the flow of the argon is 10L/min-14L/min.
The invention has the beneficial effects that: by adopting the technical scheme of the invention, the heating rod on the high-frequency induction heating equipment is set into a closed circular ring shape, so that the periphery of the joint of the workpieces is uniformly heated, the welding quality is improved, the heating and temperature rising are quicker by adopting the high-frequency induction heating equipment, the energy transferred by induction heating per square millimeter is more and more uniform, compared with other brazing processes, more workpieces can be welded in unit time by high-frequency induction heating, and the welding efficiency is improved; the ultrasonic cleaning equipment is used for cleaning the workpiece in the early stage of brazing, oil stains attached to the surface of the workpiece are removed, the capillary effect in the brazing process is enhanced, inclusions in a welding seam are prevented, moisture remained on the surface of the workpiece is dried, the pore defect in the welding seam is avoided, the welding quality is improved, the brazing flux is coated, on one hand, the brazing flux has a protection effect on the surface of the workpiece, the surface of the workpiece is prevented from being oxidized, on the other hand, the fluidity of the brazing filler metal in the heating process is improved, the capillary effect at the welding seam is more sufficient and prominent, in addition, in the welding process, the step-by-step procedures of preheating, reheating and then strengthening are adopted, the thermal impact on the workpiece material caused by too fast temperature rise in the heating process can be avoided, the material at the joint of the workpiece is uniformly melted, the brazing filler metal and the workpiece material can be better combined and can penetrate into the workpiece material through the capillary effect, the welding seam has good strength, and the welding quality is improved.
Drawings
FIG. 1 is a process flow diagram of the present invention;
fig. 2 is a schematic view of the structure of the brazing process of the present invention.
In the figure: 1-high-frequency induction heating equipment, 2-heating rods, 3-workpiece A, 4-workpiece B, 5-welding seams, 6-infrared thermometers and 7-argon pipes.
Detailed Description
The technical solution of the present invention is further described below, but the scope of the claimed invention is not limited to the described.
As shown in fig. 1, the present invention provides a method for butt brazing a valve alloy and copper, comprising the steps of:
step one; a preparation stage: providing high-frequency induction heating equipment 1, wherein the high-frequency induction heating equipment 1 comprises a heating rod 2, the heating rod 2 is of a closed annular structure, a workpiece A3 made of a valve-adjustable alloy is butted with a workpiece B4 made of copper, then a proper amount of brazing filler metal is placed at the butt joint of the workpiece A3 and the workpiece B4, then a proper amount of soldering flux is coated at the butt joint of the workpiece A3 and the workpiece B4, and then the heating rod 2 is placed around the butt joint of the workpiece A3 and the workpiece B4; in step one, workpiece A3 and workpiece B4 are butted together through a thread pair. In the first step, workpiece a3 is a valve-able alloy seat with M4 × 10 internal screw holes, and workpiece B4 is a steel plate with specification and size: the outer diameter x the inner diameter x the length is phi 4mm x phi 2.6mm x 1400 mm. In the first step, the brazing filler metal is a brazing filler metal ring which surrounds a brazing filler metal with the outer diameter of phi 2mm at the periphery of the joint of the workpiece A3 and the workpiece B4, and the outer diameter of the brazing filler metal ring is phi 6 mm. The model number of the high-frequency induction heating equipment 1 in the first step is TS-50.
Step two: a preheating stage: heating the brazing filler metal and the brazing flux to a preheating temperature by using high-frequency induction heating equipment 1, and keeping the preheating temperature for a proper time, and then carrying out the next step; further, the preheating temperature in the second step is 400-450 ℃, and the preheating temperature holding time is 5-8 s.
Step three: and (3) brazing: heating the brazing filler metal and the brazing flux to a melting temperature by using the high-frequency induction heating equipment 1, keeping the temperature for a proper time, melting the brazing filler metal and the brazing flux with part of materials of the workpiece A3 or the workpiece B4 to form a welding seam 5, and then carrying out the next step; further, in the third step, in the process of heating the brazing filler metal and the brazing flux to the melting temperature, the heating speed of the brazing filler metal and the brazing flux is controlled not to exceed 150 ℃/s. The melting temperature in the third step is 730-780 ℃, and the melting temperature holding time is 5-8 s.
Step four: and (3) strengthening stage: naturally standing the welding seam 5 in the third step for a proper time, heating the welding seam 5 to a melting temperature through the high-frequency induction heating equipment 1, keeping the temperature for a proper time, and naturally cooling the welding seam 5 to a normal temperature. Furthermore, in the fourth step, the standing time of the welding line 5 is 1s, the melting temperature is 730 ℃ to 780 ℃, and the holding time of the melting temperature is 2s to 3 s.
In addition, the butt brazing method of the valve alloy and the copper further comprises the following steps: before the first step, cleaning the workpiece A3 and the workpiece B4 by using an ultrasonic cleaning machine, wherein the cleaning solvent is a mixed solvent of acetone and alcohol, the cleaning duration is 25min to 35min, and the workpiece A3 or the workpiece B4 is vibrated at the frequency of 30Hz to 50Hz in the cleaning process.
In addition, the butt brazing method of the valve alloy and the copper further comprises the following steps: after the workpiece A3 and the workpiece B4 are cleaned by an ultrasonic cleaning machine, the workpiece A3 and the workpiece B4 are placed in an oven to be dried, a fan is arranged in the oven, and the temperature in the oven is controlled to be 70 ℃ and is maintained for 40-60 min.
In addition, the butt brazing method of the valve alloy and the copper further comprises the following steps: before the second step, the high-frequency induction heating equipment 1 is started, the heating rod 2 is enabled to be preheated for 10min to 20min, and then the next step is carried out. And in the process of the second step, the third step or the fourth step, argon is blown by aiming at the brazing filler metal and the brazing flux, the purity of the argon is not less than 99.99 percent, the pressure of the argon is not less than 1.5MPa, and the flow of the argon is 10L/min-14L/min. According to the technical scheme, in the brazing process, argon is used as protective gas and is used for preventing the brazing filler metal, the brazing flux and workpiece materials in a high-temperature state from being oxidized by air in the environment, blackening of formed welding seams is avoided, meanwhile, the flow and the pressure of the argon are proper, and the argon cannot play a role of protection when the flow is too small, so that more welding slag remains on the surfaces of the welding seams, the cleaning is difficult, the brazing filler metal can splash when the flow of the argon is too large, the filling amount of the welding seams is insufficient, pores and other defects occur, and parts are scrapped. And in the process of the second step, the third step or the fourth step, an infrared thermometer 6 is adopted to measure the temperature of the brazing filler metal or the brazing flux.
By adopting the technical scheme of the invention, the heating rod on the high-frequency induction heating equipment is set into a closed circular ring shape, so that the periphery of the joint of the workpieces is uniformly heated, the welding quality is improved, the heating and temperature rising are quicker by adopting the high-frequency induction heating equipment, the energy transferred by induction heating per square millimeter is more and more uniform, compared with other brazing processes, more workpieces can be welded in unit time by high-frequency induction heating, and the welding efficiency is improved; the ultrasonic cleaning equipment is used for cleaning the workpiece in the early stage of brazing to remove oil stains attached to the surface of the workpiece, so that the capillary effect in the brazing process is enhanced, impurities are prevented from being generated in a welding seam, moisture remained on the surface of the workpiece is dried, the defect of air holes in the welding seam is avoided, the welding quality is improved, the brazing flux is coated, on one hand, the brazing flux has a protection effect on the surface of the workpiece, the surface of the workpiece is prevented from being oxidized, on the other hand, the fluidity of the brazing filler metal in the heating process is increased, so that the capillary effect at the welding seam is more sufficient and prominent, in addition, in the welding process, the substep procedures of preheating, reheating and then strengthening are adopted, the thermal impact on the workpiece material caused by too fast temperature rise in the heating process can be avoided, the material at the joint of the workpiece is uniformly melted, the brazing filler metal and the workpiece material can be better combined, and can penetrate into the workpiece material through the capillary effect, the welding seam has good strength, and the welding quality is improved.
Claims (5)
1. A butt brazing method of a valvable alloy and copper is characterized by comprising the following steps: the method comprises the following steps:
step one; a preparation stage: providing high-frequency induction heating equipment (1), wherein the high-frequency induction heating equipment (1) comprises a heating rod (2), the heating rod (2) is of a closed annular structure, butt-jointing a workpiece A (3) made of valve alloy and a workpiece B (4) made of copper, placing a proper amount of brazing filler metal at the butt-joint position of the workpiece A (3) and the workpiece B (4), then coating a proper amount of brazing flux at the butt-joint position of the workpiece A (3) and the workpiece B (4), and then placing the heating rod (2) around the butt-joint position of the workpiece A (3) and the workpiece B (4); in the first step, the workpiece A (3) and the workpiece B (4) are butted together through a thread pair;
step two: a preheating stage: heating the brazing filler metal and the brazing flux to a preheating temperature by high-frequency induction heating equipment (1) and keeping the preheating temperature for a proper time, and then carrying out the next step; in the second step, the preheating temperature is 400-450 ℃, and the preheating temperature holding time is 5-8 s;
step three: and (3) brazing: heating the brazing filler metal and the brazing flux to a melting temperature by high-frequency induction heating equipment (1) and keeping the melting temperature for a proper time, melting the brazing filler metal and the brazing flux with partial materials of the workpiece A (3) or the workpiece B (4) to form a welding seam (5), and then carrying out the next step; in the third step, in the process of heating the brazing filler metal and the brazing flux to the melting temperature, the heating speed of the brazing filler metal and the brazing flux is controlled not to exceed 150 ℃/s; in the third step, the melting temperature is 730-780 ℃, and the holding time of the melting temperature is 5-8 s;
step four: and (3) strengthening stage: naturally standing the welding seam (5) in the third step for a proper time, heating the welding seam (5) to a melting temperature through high-frequency induction heating equipment (1), keeping the temperature for a proper time, and naturally cooling the welding seam (5) to a normal temperature; in the fourth step, the standing time of the welding line (5) is 1s, the melting temperature is 730 ℃ to 780 ℃, and the holding time of the melting temperature is 2s to 3 s.
2. The method of butt brazing a valvable alloy to copper as claimed in claim 1, wherein: the butt brazing method of the valvable alloy and the copper further comprises the following steps: before the first step, cleaning the workpiece A (3) and the workpiece B (4) by using an ultrasonic cleaning machine, wherein a cleaning solvent is a mixed solvent of acetone and alcohol, the cleaning duration is 25min to 35min, and the workpiece A (3) or the workpiece B (4) is vibrated at the frequency of 30Hz to 50Hz in the cleaning process.
3. The method of butt brazing a valvable alloy to copper as claimed in claim 2, wherein: the butt brazing method of the valvable alloy and the copper further comprises the following steps: after the workpiece A (3) and the workpiece B (4) are cleaned by using an ultrasonic cleaning machine, the workpiece A (3) and the workpiece B (4) are placed in an oven to be dried, a fan is installed in the oven, and the temperature in the oven is controlled to be 70 ℃ and is maintained for 40-60 min.
4. The method of butt brazing a valvable alloy to copper as claimed in claim 1, wherein: the butt brazing method of the valvable alloy and the copper further comprises the following steps: before the second step, the high-frequency induction heating equipment (1) is started, the heating rod (2) is preheated for 10min to 20min, and then the next step is carried out.
5. The method of butt brazing a valvable alloy to copper as claimed in claim 1, wherein: and in the process of the second step, the third step or the fourth step, argon is blown aiming at the brazing filler metal and the brazing flux, the purity of the argon is not less than 99.99%, the pressure of the argon is not less than 1.5MPa, and the flow of the argon is 10-14L/min.
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CN114043029A (en) * | 2021-11-05 | 2022-02-15 | 天津航空机电有限公司 | Brazing method for welding molybdenum alloy and kovar alloy by using copper-platinum solder |
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CN103273212B (en) * | 2013-03-19 | 2015-10-07 | 上海大学 | High temperature resistant Ag-Cu-Mn metal sealing material, preparation method and its usage |
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CN103269821A (en) * | 2010-12-28 | 2013-08-28 | 大金工业株式会社 | Joint structure for metallic pipes |
CN102211235A (en) * | 2011-04-18 | 2011-10-12 | 哈尔滨工业大学 | Soldering method and device of heterogeneous stainless steel oil injection nozzle nut of engine |
CN106735664A (en) * | 2015-11-19 | 2017-05-31 | 松下知识产权经营株式会社 | Method for welding |
WO2019216497A1 (en) * | 2018-05-08 | 2019-11-14 | 두성산업 (주) | Method for manufacturing distributor for air conditioner |
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CN112025018A (en) * | 2020-08-28 | 2020-12-04 | 郑州郑飞机电技术有限责任公司 | Capillary tube joint brazing method |
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