CN113349407A - Tobacco stem pulp sheet, preparation method and application - Google Patents
Tobacco stem pulp sheet, preparation method and application Download PDFInfo
- Publication number
- CN113349407A CN113349407A CN202110756201.4A CN202110756201A CN113349407A CN 113349407 A CN113349407 A CN 113349407A CN 202110756201 A CN202110756201 A CN 202110756201A CN 113349407 A CN113349407 A CN 113349407A
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- pulp
- tobacco
- tobacco stem
- pulping
- preparation
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B5/00—Stripping tobacco; Treatment of stems or ribs
- A24B5/16—Other treatment of stems or ribs, e.g. bending, chopping, incising
Abstract
The invention discloses a method for preparing tobacco stem pulp sheets, and belongs to the field of processing and recycling of cigarette byproducts. The preparation method comprises the following steps: (1) extracting; (2) solid-phase filter pressing; (3) high-concentration pulping; (4) preparing slurry; (5) screening the pulp; (6) molding on the net; (7) and (5) drying. The invention also discloses the tobacco stem pulp sheet obtained by the preparation method and application thereof. The tobacco stem pulp sheet belongs to mechanical pulp, and compared with chemical pulp of tobacco stems, the chemical pulp sheet does not need to be used in the production process, is green and environment-friendly in production, high in pulping yield and convenient to store and transport. The tobacco stem pulp can be added and used on the surface layer or the core layer or the bottom layer of the coated ivory board on line.
Description
Technical Field
The invention belongs to the technical field of tobacco, and particularly relates to a tobacco stem pulp sheet, a preparation method and application thereof.
Background
The tobacco stems are important byproducts in the tobacco processing process, have similar components with tobacco leaves, have the functions of improving the cigarette structure, reducing the cost and reducing the tar, and are always important components of cigarette raw materials, and the tobacco stems used by cigarette industry enterprises at present mainly adopt cut stems and reconstituted tobacco leaves. With continuous innovation of the processing technology of the reconstituted tobacco and the cut stems, the quality of the reconstituted tobacco and the cut stems of the tobacco is improved to a great extent, and the application range and the application proportion of the reconstituted tobacco and the cut stems of the tobacco in cigarette products are increased day by day. Nevertheless, each cigarette industry enterprise still has a large amount of tobacco stalk raw materials to be scrapped and burned without effective utilization, which not only pollutes the environment, but also causes waste of tobacco resources. Resource development and application of tobacco stems become one of the key research directions of tobacco science and technology workers.
At present, the resource development application of the tobacco stems in the coated white cardboard is relatively reported, for example, patent CN102127878A discloses a cigarette packet cardboard, which comprises a core layer, a surface layer and a back layer, wherein the surface layer and the back layer of the cardboard are mixed fiber pulp paper containing tobacco fibers and bast fibers, and the mixed fiber pulp comprises 6-30% by weight of tobacco fiber pulp, 5-25% by weight of bast fiber pulp, 0-25% by weight of bleached needle pulp and 40-70% by weight of bleached broad leaf pulp. Patent CN110916238A provides a tobacco stem pretreatment method for a high-speed paper machine and a white cardboard for the tobacco, the method comprises the steps of filter pressing treatment, after three times of plate frame filter pressing, organic matters in the tobacco stems are removed, the tobacco stems can be put into the high-speed paper machine, and the organic matters in the tobacco stems are more thoroughly removed by crushing the tobacco stems into powder and then carrying out a plurality of times of plate frame filter pretreatment. Patent CN106283929A discloses a coated white cardboard containing tobacco stems and/or tobacco leaves, which comprises a raw paper layer, wherein the raw paper layer comprises a surface paper layer, a core paper layer and a bottom paper layer which are sequentially stacked from top to bottom, and an optional liner paper layer located between the surface paper layer and the core paper layer, and at least one of the surface paper layer, the core paper layer, the bottom paper layer and the liner paper layer contains tobacco stems and/or tobacco leaves. Patent CN109082928B discloses a tobacco stem coated white cardboard and a preparation method and application thereof, and the preparation steps are as follows: taking tobacco stem powder with the particle size of 1-120 mu m, adding water to prepare suspension, leaching and/or filter pressing the suspension, coating cationic starch, mixing with paper pulp, and then preparing the tobacco stem coated ivory board after pulp distribution, water filtration, squeezing dehydration, drying and coating.
In the above many published reports, the application form of the tobacco stems in the coated white cardboard can be divided into tobacco stem pulp and tobacco stem powder, wherein the tobacco stem powder is directly added into the production process of the coated white cardboard, so that a large amount of tobacco waste water is caused, the pretreatment process of the tobacco stem powder is complicated, the treatment efficiency is low, and the cost is high; the tobacco stem pulp can be continuously added on line in the production process of the coated ivory board, but the publicly reported tobacco stem chemical pulp needs a large amount of cooking chemicals in the preparation process, and the yield of the tobacco stem pulp is low.
The present invention has been made to solve the above problems.
Disclosure of Invention
The invention provides a tobacco stem pulp sheet, a preparation method thereof and application of the obtained tobacco stem pulp sheet in a cigarette coated white cardboard surface layer, a core layer or a bottom layer.
The tobacco stem pulp sheet is prepared by extracting tobacco stem raw materials, carrying out solid-phase filter pressing, pulping at high concentration, preparing pulp, screening pulp, forming on a net and drying, the preparation process is green and environment-friendly, the pulping yield is high, the storage and the transportation are convenient, the tobacco stem pulp sheet can be added and used in a surface layer or a core layer or a bottom layer of coated white cardboard, and the quality index of the coated white cardboard is equivalent to that of the normally produced coated white cardboard.
The technical scheme of the invention is as follows:
the invention discloses a preparation method of tobacco stem pulp sheets in a first aspect, which comprises the following steps:
(1) carrying out hot reflux extraction on the tobacco stem raw material by using water under certain conditions;
(2) performing solid-liquid separation on the material extracted in the step (1), and performing filter pressing treatment on a solid phase part to ensure that the water content of a solid matter is less than or equal to 75 wt%;
(3) performing three-stage high-concentration pulping on the solid matters in the step (2), wherein the freeness of the tobacco stalk pulp after pulping is 300-500ml, and the water content of the tobacco stalk pulp is less than or equal to 85 wt%;
(4) adding water into the tobacco stalk high-consistency pulp obtained in the step (3) to prepare tobacco stalk low-consistency pulp, and then adding additional fiber pulp to form mixed pulp;
(5) sieving the mixed pulp obtained in the step (4) to remove impurities;
(6) screening the mixed slurry with impurities removed in the step (5), and papermaking to obtain wet tobacco stem pulp sheets;
(7) and (4) drying the wet tobacco stem pulp sheet obtained in the step (6) to enable the water content to be less than or equal to 15 wt%, and obtaining the tobacco stem pulp sheet.
Preferably, the length dimension of the tobacco stems in the step (1) is 5-20 mm; the solid-liquid ratio is 1: (4-7), the extraction temperature is 60-90 ℃, and the extraction time is 30-60 min.
Preferably, in the step (3), the gap between the first-level pulping disc mill for the three-level high-concentration pulping is 0.5-1mm, the gap between the second-level pulping disc mill is 0.3-0.5mm, and the gap between the third-level pulping disc mill is 0.1-0.3 mm.
Preferably, the concentration of the tobacco stalk low-concentration pulp in the step (4) is 4-8 wt%.
Preferably, the fiber pulp added in the step (4) is one or more of wood pulp, bamboo pulp, mulberry bark pulp and hemp pulp; the concentration of the added fiber pulp is 4-10 wt%, and the freeness is 300-500 ml.
Preferably, the dry weight of the stem pulp in the mixing paddle in step (4) is 90-95 wt%.
Preferably, the sieve used for screening the pulp in step (5) has a mesh size of 0.3-0.6 mm.
Preferably, the concentration of the mixed slurry on the net in the step (6) is 1-5 wt%, and the quantitative amount of the tobacco stalk slurry sheet is 70-100g/m2。
The second aspect of the invention discloses a tobacco stem pulp sheet prepared by the preparation method.
The third aspect of the invention discloses the application of the tobacco stem pulp sheet in coating the surface layer, the core layer or the bottom layer of the ivory board.
The invention has the beneficial effects that:
1. the tobacco stem pulp sheet is sheet-shaped and contains more than 90 wt% of tobacco stem fibers. The sheet tobacco stalk pulp sheet is convenient for the storage and transportation of the tobacco stalk pulp sheet.
2. The tobacco stem pulp sheet is firstly used in the online adding application of the surface layer or the core layer or the bottom layer of the coated white cardboard, and the quality index of the obtained coated white cardboard is the same as or close to that of the normally produced coated white cardboard.
3. The tobacco stem pulp sheet belongs to mechanical pulp, and compared with chemical pulp of tobacco stems, the chemical pulp sheet does not need to be used in the production process, the production is green and environment-friendly, and the pulping yield is higher.
Detailed Description
The present invention will be described in detail and fully with reference to the accompanying drawings, in which some, but not all embodiments of the invention are shown. All other embodiments obtained by a person skilled in the art without inventive step are within the scope of protection of the present invention.
Example 1
The preparation method of the tobacco stem pulp sheet is prepared by the following steps:
step (1): carrying out hot reflux extraction on a tobacco stem raw material with the length of 5mm by using water, wherein the solid-to-liquid ratio of the extraction is 1: 4, the extraction temperature is 90 ℃, and the extraction time is 60 min;
step (2): performing solid-liquid separation on the material obtained in the step (1), performing filter pressing treatment on a solid phase part, wherein the water content of a solid matter obtained after filter pressing is 75 wt%;
and (3): performing three-stage high-concentration pulping on the solid matter subjected to filter pressing in the step (2), wherein the disc grinding clearance of the first-stage pulping is 1mm, the disc grinding clearance of the second-stage pulping is 0.5mm, the disc grinding clearance of the third-stage pulping is 0.3mm, the freeness of the high-concentration tobacco stalk pulp after pulping is 500ml, and the water content of the high-concentration tobacco stalk pulp is 85 wt%;
and (4): preparing the tobacco stalk high-consistency slurry in the step (3) into 4 wt% low-consistency slurry, and then mixing the low-consistency slurry with wood pulp and hemp pulp to form mixed pulp; wherein the pulping concentration of the wood pulp is 4 wt%, the freeness of the wood pulp is 500ml, the pulping concentration of the hemp pulp is 4 wt%, and the freeness of the hemp pulp is 300 ml; the mass ratio of the wood pulp to the hemp pulp is 7: 3; the dry weight content of the tobacco stalk pulp in the mixing paddle is 90 wt%, the dry weight content of the wood pulp is 7 wt%, and the dry weight content of the hemp pulp is 3 wt%;
and (5): sieving the tobacco stem mixed pulp prepared in the step (4) to remove impurities; the mesh of the used sieve is 0.6 mm;
and (6): carrying out net surfing and papermaking molding on the mixed slurry obtained in the step (5) to obtain wet tobacco stem slurry sheets; the concentration of the upper wire is 1 wt%, and the quantitative is 100g/m2;
And (7): and (4) drying the wet tobacco stem pulp sheet prepared in the step (6) to obtain the tobacco stem pulp sheet, wherein the dryness is 85 wt%, namely the water content in the tobacco stem pulp sheet is 15 wt%.
And adding the obtained tobacco stem pulp sheet into the surface layer of the coated ivory board on line according to the mass ratio of 4 wt% to prepare the coated ivory board containing the stem fibers.
Example 2
The preparation method of the tobacco stem pulp sheet is prepared by the following steps:
step (1) extraction: carrying out hot reflux extraction on a tobacco stem raw material with the length of 10mm by using water, wherein the extraction solid-liquid ratio is 1: 7, the extraction temperature is 60 ℃, and the extraction time is 30 min;
step (2) solid-phase filter pressing: performing solid-liquid separation on the material extracted in the step (1), and performing filter pressing treatment on a solid phase part, wherein the water content of a solid substance after filter pressing is 70 wt%;
step (3), high-consistency pulping: performing three-stage high-concentration pulping on the solid matter subjected to filter pressing in the step (2), wherein the disc grinding clearance of the first-stage pulping is 0.5mm, the disc grinding clearance of the second-stage pulping is 0.3mm, the disc grinding clearance of the third-stage pulping is 0.1mm, the freeness of the tobacco stem high-concentration pulp after pulping is 300ml, and the water content of the tobacco stem high-concentration pulp is 80 wt%;
step (4), slurry preparation: preparing the tobacco stalk high-consistency slurry in the step (3) into 8 wt% low-consistency slurry, and then mixing the low-consistency slurry with hemp pulp to form mixed pulp; wherein the pulping concentration of the hemp pulp is 8 wt%, and the freeness of the hemp pulp is 450 ml; the dry weight content of the tobacco stalk pulp in the mixing paddle is 95 wt%, and the dry weight content of the hemp pulp is 5 wt%;
screening pulp in step (5): sieving the tobacco stem mixed pulp prepared in the step (4) to remove impurities; the mesh of the used sieve is 0.3 mm;
step (6), forming the net: carrying out net surfing and papermaking molding on the mixed slurry obtained in the step (5) to obtain wet tobacco stem slurry sheets; the concentration of the upper wire is 1 wt%, and the quantitative rate is 70g/m2;
And (7) drying: and (4) drying the wet tobacco stem pulp sheet prepared in the step (6) to obtain the tobacco stem pulp sheet, wherein the dryness is 87 wt%, namely the water content in the tobacco stem pulp sheet is 13 wt%.
Adding the obtained tobacco stem pulp sheet into the bottom layer of the coated ivory board according to the mass ratio of 7 wt% on line to prepare the coated ivory board containing stem fibers.
Example 3
The preparation method of the tobacco stem pulp sheet is prepared by the following steps:
step (1) extraction: carrying out hot reflux extraction on the tobacco stem raw material with the length of 20mm by using water, wherein the extraction solid-liquid ratio is 1: 6, the extraction temperature is 85 ℃, and the extraction time is 40 min;
step (2) solid-phase filter pressing: performing solid-liquid separation on the material extracted in the step (1), performing filter pressing treatment on a solid phase part, wherein the water content of a solid matter after filter pressing is 72 wt%;
step (3), high-consistency pulping: performing three-stage high-concentration pulping on the solid matter subjected to filter pressing in the step (2), wherein the disc grinding clearance of the first-stage pulping is 0.6mm, the disc grinding clearance of the second-stage pulping is 0.4mm, the disc grinding clearance of the third-stage pulping is 0.2mm, the freeness of the tobacco stem high-concentration pulp after pulping is 400ml, and the water content of the tobacco stem high-concentration pulp is 80 wt%;
step (4), slurry preparation: preparing the tobacco stalk high-consistency pulp obtained in the step (3) into 5 wt% low-consistency pulp, and then mixing the low-consistency pulp with wood pulp to form mixed pulp; wherein the pulping concentration of the wood pulp is 5 wt%, and the freeness of the wood pulp is 400 ml; the dry weight content of the tobacco stalk pulp in the mixing paddle is 93 wt%, and the dry weight content of the hemp pulp is 7 wt%;
screening pulp in step (5): sieving the tobacco stem mixed pulp prepared in the step (4) to remove impurities; the mesh of the used sieve is 0.4 mm;
step (6), forming the net: carrying out net surfing and papermaking molding on the mixed slurry obtained in the step (5) to obtain wet tobacco stem slurry sheets; the concentration of the upper wire is 1 wt%, and the quantitative rate is 80g/m2;
And (7) drying: and (4) drying the wet tobacco stem pulp sheet prepared in the step (6) to obtain the tobacco stem pulp sheet, wherein the dryness is 88 wt%, namely the water content in the tobacco stem pulp sheet is 12 wt%.
And adding the obtained tobacco stem pulp sheet into a core layer of the coated ivory board on line according to the mass ratio of 10 wt% to prepare the coated ivory board containing the stem fibers.
The quality indexes of the coated white cardboard containing the tobacco stem pulp sheets prepared in examples 1 to 3 were measured, and the results of comparative analysis of the quality indexes are shown in table 1, with the coated white cardboard produced normally as a control:
TABLE 1 quality index test results of coated white cardboard samples
From the test comparison results in table 1, it can be seen that, compared with the control sample, when the tobacco stalk pulp sheet prepared by the present invention is added to the coated white cardboard, the quality index of the coated white cardboard is equivalent to the quality index of the normally produced coated white cardboard, and both meet the technical standard requirements.
The above description is only for the purpose of illustrating the preferred embodiments of the present invention and is not to be construed as limiting the invention, and any modifications, equivalents, improvements and the like that fall within the spirit and principle of the present invention are intended to be included therein.
Claims (10)
1. The preparation method of the tobacco stem pulp sheet is characterized by comprising the following steps:
(1) carrying out hot reflux extraction on the tobacco stem raw material by using water under certain conditions;
(2) performing solid-liquid separation on the material extracted in the step (1), and performing filter pressing treatment on a solid phase part to ensure that the water content of a solid matter is less than or equal to 75 wt%;
(3) performing three-stage high-concentration pulping on the solid matters in the step (2), wherein the freeness of the tobacco stalk pulp after pulping is 300-500ml, and the water content of the tobacco stalk pulp is less than or equal to 85 wt%;
(4) adding water into the tobacco stalk pulp obtained in the step (3) to prepare tobacco stalk low-consistency pulp, and then adding additional fiber pulp to form mixed pulp;
(5) sieving the mixed pulp obtained in the step (4) to remove impurities;
(6) screening the mixed slurry with impurities removed in the step (5), and papermaking to obtain wet tobacco stem pulp sheets;
(7) and (4) drying the wet tobacco stem pulp sheet obtained in the step (6) to enable the water content to be less than or equal to 15 wt%, and obtaining the tobacco stem pulp sheet.
2. The method for preparing the tobacco stalk as claimed in claim 1, wherein the length dimension of the tobacco stalk in the step (1) is 5-20 mm; the solid-liquid ratio is 1: (4-7), the extraction temperature is 60-90 ℃, and the extraction time is 30-60 min.
3. The preparation method according to claim 1, wherein the gap between the first-stage pulping disc mill of the three-stage high-consistency pulping in the step (3) is 0.5-1mm, the gap between the second-stage pulping disc mill is 0.3-0.5mm, and the gap between the third-stage pulping disc mill is 0.1-0.3 mm.
4. The preparation method according to claim 1, wherein the concentration of the tobacco stem low-consistency stock in the step (4) is 5-10 wt%.
5. The preparation method according to claim 1, wherein the additional fiber pulp in the step (4) is one or more of wood pulp, bamboo pulp, mulberry bark pulp and hemp pulp; the concentration of the added fiber pulp is 5-10 wt%, and the freeness is 300-500 ml.
6. The method of claim 1, wherein the mixing paddle in step (4) comprises 90-95 wt% of tobacco stem.
7. The method according to claim 1, wherein the screen used for screening the slurry in the step (5) has a mesh size of 0.3 to 0.6 mm.
8. The preparation method according to claim 1, wherein the mixed slurry in the step (6) is fed to a screen with a concentration of 1-5 wt% and the quantitative amount of the tobacco stem pulp sheet is 70-100g/m2。
9. A tobacco stem pulp sheet produced by the method according to any one of claims 1 to 8.
10. Use of the stem pulp sheet according to claim 9 for coating the top, core or bottom layer of ivory board.
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Cited By (1)
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