CN113337331A - 一种环保型水基线切割工作液及其制备方法 - Google Patents

一种环保型水基线切割工作液及其制备方法 Download PDF

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CN113337331A
CN113337331A CN202110600952.7A CN202110600952A CN113337331A CN 113337331 A CN113337331 A CN 113337331A CN 202110600952 A CN202110600952 A CN 202110600952A CN 113337331 A CN113337331 A CN 113337331A
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刘茂林
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Abstract

本发明公开了一种环保型水基线切割工作液及其制备方法，配方是由以下质量百分含量的原料制备而成的：防锈剂2‑4％，清洗剂3‑5％，电解质0.2‑0.5‰，润滑剂5‑8％，PH值调节剂8‑12％，杀菌剂0.5‑2％，消泡剂1‑3‰，降凝剂0‑5％，渗透剂2‑4％，余量为去离子水。本发明制备的水基线切割工作液不添加基础油，减少环境污染；不添加亚硝酸钠、苯胺等对人体有害的物质，对人体无害；生产工艺简单合理；成本较低性价比高；防锈、润滑、清洗、提高切割效率、降低切面粗糙度等性能优良。

Description

一种环保型水基线切割工作液及其制备方法
技术领域
本发明涉及线切割工作液技术领域，具体为一种环保型水基线切割工作液及其制备方法。
背景技术
线切割工作液是电火花线切割机床专用的金属加工液，作为电火花线切割加工过程中的放电介质，起到冷却、绝缘、润滑、清洗、防锈等方面作用。线切割工作液对于电火花线切割加工的效率、加工精度、表面粗糙度、钼丝损耗等因素起着至关重要的作用。目前线切割工作液存在性能参差不齐、成本较高性价偏低、环境污染严重、对操作人员身体健康有害等缺点。本发明旨在研制一种各方面性能优异，减轻环境污染，对人体无毒害作用且经济实惠的线切割工作液。
发明内容
针对上述存在的技术不足，本发明的目的是提供一种环保型水基线切割工作液及其制备方法，以解决背景技术中提出的问题。
为解决上述技术问题，本发明采用如下技术方案：
本发明提供一种环保型水基线切割工作液，是由以下质量百分含量的原料制备而成的：
防锈剂2-4％，清洗剂3-5％，电解质0.2-0.5‰，润滑剂5-8％，PH值调节剂8-12％，杀菌剂0.5-2％，消泡剂1-3‰，降凝剂0-5％，渗透剂2-4％，余量为去离子水。
一种环保型水基线切割工作液，是由以下质量百分含量的原料制备而成的：
防锈剂2％，清洗剂3％，电解质0.2‰，润滑剂5％，PH值调节剂8％，杀菌剂0.5％，消泡剂1‰，降凝剂0.5％，渗透剂2％，余量为去离子水。
一种环保型水基线切割工作液，是由以下质量百分含量的原料制备而成的：
防锈剂4％，清洗剂5％，电解质0.5‰，润滑剂8％，PH值调节剂12％，杀菌剂2％，消泡剂3‰，降凝剂5％，渗透剂4％，余量为去离子水。
一种环保型水基线切割工作液，是由以下质量百分含量的原料制备而成的：
防锈剂3％，清洗剂4％，电解质0.3‰，润滑剂6.5％，PH值调节剂10％，杀菌剂1.5％，消泡剂2‰，降凝剂2.5％，渗透剂3％，余量为去离子水。
优选地，所述防锈剂为三乙醇胺硼酸酯、癸二酸、十二碳二元酸的一种或几种。
优选地，所述清洗剂为壬基酚聚氧乙烯醚、脂肪酸甲酯乙氧基化物、椰子油脂肪酸二乙醇酰胺的一种或几种。
优选地，所述电解质选用聚乙烯酸钠；所述润滑剂选用四聚蓖麻油酸酯。
优选地，所述PH值调节剂选用三乙醇胺；所述杀菌剂选用MBM杀菌剂。
优选地，所述消泡剂选用有机硅消泡剂；所述降凝剂选用乙二醇。
优选地，所述渗透剂选用脂肪醇聚氧乙烯醚。
一种环保型水基线切割工作液上午制备方法，包括如下步骤：
(1)将PH值调节剂通过抽料泵抽入电加热不锈钢反应釜内，从反应釜人孔加入防锈剂，开启电加热升温至100-110℃，保温反应2h。
(2)开启冷却水降温至60℃，依次加入清洗剂、润滑剂、渗透剂，搅拌30-40min。
(3)加入去离子水，自然降温至30-40℃，依次加入电解质、杀菌剂、降凝剂、消泡剂，搅拌2h；
(4)成品经20微米过滤器过滤，灌装。
本发明的有益效果在于：
1、本发明制备的水基线切割工作液不添加基础油，减少环境污染；不添加亚硝酸钠、苯胺等对人体有害的物质，对人体无害；生产工艺简单合理；成本较低性价比高；防锈、润滑、清洗、提高切割效率、降低切面粗糙度等性能优良。
2、本发明的产品环保安全性能好，避免了使用油类物质产生的油污、油烟问题，提高了工件的表面质量，同时也改善了工作环境，降低了工业废水的排放和污染，节约了成本，本发明的产品经实验证明对人体无毒，没有致癌性，保障了工作人员的安全；
3、本发明的产品使用后工艺效果好，提高了加工速度，加工后的工件表面光洁度高，不存在线痕、水纹问题；
4、本发明的产品颜色透明淡黄色，避免了油性线切割工作液的分层问题，化学性能稳定，保质期较长。
具体实施方式
实施例1
一种环保型水基线切割工作液，是由以下质量百分含量的原料制备而成的：
防锈剂2％，清洗剂3％，电解质0.2‰，润滑剂5％，PH值调节剂8％，杀菌剂0.5％，消泡剂1‰，降凝剂0.5％，渗透剂2％，余量为去离子水。
所述防锈剂为三乙醇胺硼酸酯、癸二酸、十二碳二元酸的一种或几种。
所述清洗剂为壬基酚聚氧乙烯醚、脂肪酸甲酯乙氧基化物、椰子油脂肪酸二乙醇酰胺的一种或几种。
所述电解质选用聚乙烯酸钠；所述润滑剂选用四聚蓖麻油酸酯。
所述PH值调节剂选用三乙醇胺；所述杀菌剂选用MBM杀菌剂。
所述消泡剂选用有机硅消泡剂；所述降凝剂选用乙二醇。
所述渗透剂选用脂肪醇聚氧乙烯醚。
一种环保型水基线切割工作液上午制备方法，包括如下步骤：
(1)将PH值调节剂通过抽料泵抽入电加热不锈钢反应釜内，从反应釜人孔加入防锈剂，开启电加热升温至100-110℃，保温反应2h。
(2)开启冷却水降温至60℃，依次加入清洗剂、润滑剂、渗透剂，搅拌30min。
(3)加入去离子水，自然降温至30-40℃，依次加入电解质、杀菌剂、降凝剂、消泡剂，搅拌2小时；
(4)成品经20微米过滤器过滤，灌装。
实施例2
一种环保型水基线切割工作液，是由以下质量百分含量的原料制备而成的：
防锈剂4％，清洗剂5％，电解质0.5‰，润滑剂8％，PH值调节剂12％，杀菌剂2％，消泡剂3‰，降凝剂5％，渗透剂4％，余量为去离子水。
所述防锈剂为三乙醇胺硼酸酯、癸二酸、十二碳二元酸的一种或几种。
所述清洗剂为壬基酚聚氧乙烯醚、脂肪酸甲酯乙氧基化物、椰子油脂肪酸二乙醇酰胺的一种或几种。
所述电解质选用聚乙烯酸钠；所述润滑剂选用四聚蓖麻油酸酯。
所述PH值调节剂选用三乙醇胺；所述杀菌剂选用MBM杀菌剂。
所述消泡剂选用有机硅消泡剂；所述降凝剂选用乙二醇。
所述渗透剂选用脂肪醇聚氧乙烯醚。
一种环保型水基线切割工作液上午制备方法，包括如下步骤：
(1)将PH值调节剂通过抽料泵抽入电加热不锈钢反应釜内，从反应釜人孔加入防锈剂，开启电加热升温至100-110℃，保温反应2h。
(2)开启冷却水降温至60℃，依次加入清洗剂、润滑剂、渗透剂，搅拌0.5小时。
(3)加入去离子水，自然降温至30-40℃，依次加入电解质、杀菌剂、降凝剂、消泡剂，搅拌2小时；
(4)成品经20微米过滤器过滤，灌装。
实施例3
一种环保型水基线切割工作液，是由以下质量百分含量的原料制备而成的：
防锈剂3％，清洗剂4％，电解质0.3‰，润滑剂6.5％，PH值调节剂10％，杀菌剂1.5％，消泡剂2‰，降凝剂2.5％，渗透剂3％，余量为去离子水。
所述防锈剂为三乙醇胺硼酸酯、癸二酸、十二碳二元酸的一种或几种。
所述清洗剂为壬基酚聚氧乙烯醚、脂肪酸甲酯乙氧基化物、椰子油脂肪酸二乙醇酰胺的一种或几种。
所述电解质选用聚乙烯酸钠；所述润滑剂选用四聚蓖麻油酸酯。
所述PH值调节剂选用三乙醇胺；所述杀菌剂选用MBM杀菌剂。
所述消泡剂选用有机硅消泡剂；所述降凝剂选用乙二醇。
所述渗透剂选用脂肪醇聚氧乙烯醚。
一种环保型水基线切割工作液上午制备方法，包括如下步骤：
(1)将PH值调节剂通过抽料泵抽入电加热不锈钢反应釜内，从反应釜人孔加入防锈剂，开启电加热升温至100-110℃，保温反应2h。
(2)开启冷却水降温至60℃，依次加入清洗剂、润滑剂、渗透剂，搅拌0.5小时。
(3)加入去离子水，自然降温至30-40℃，依次加入电解质、杀菌剂、降凝剂、消泡剂，搅拌2小时；
(4)成品经20微米过滤器过滤，灌装。
实验检测
一、实施例3所得的线切割工作液经泰州国创环保科技有限公司进行检测，结果如表1所示：
表1实施例3所得的线切割工作液的产品质量检验报告
产品质量检验报告
Figure BDA0003092902000000071
二、稳定性、反应性、毒性测试
实施例3所得的线切割工作液经检测稳定性、反应性、毒性测试，检测单位：上海化工院检测有限公司(NO.2019114391)，检测结果如表2和表3所示：
表2实施例3所得的线切割工作液的稳定性和反应性
Figure BDA0003092902000000072
Figure BDA0003092902000000081
表3实施例3所得的线切割工作液的毒理学信息
Figure BDA0003092902000000082
三、切割试验
实施例3所得的线切割工作液切割试验，结果如表4所示：
表4实施例3所得的线切割工作液切割试验结果线切割工作液切割试验
Figure BDA0003092902000000083
Figure BDA0003092902000000091
显然，本领域的技术人员可以对本发明进行各种改动和变型而不脱离本发明的精神和范围。这样，倘若本发明的这些修改和变型属于本发明权利要求及其等同技术的范围之内，则本发明也意图包含这些改动和变型在内。

Claims (10)

1.一种环保型水基线切割工作液，其特征在于，是由以下质量百分含量的原料制备而成的：
防锈剂2-4％，清洗剂3-5％，电解质0.2-0.5‰，润滑剂5-8％，PH值调节剂8-12％，杀菌剂0.5-2％，消泡剂1-3‰，降凝剂0-5％，渗透剂2-4％，余量为去离子水。
2.如权利要求1所述的一种环保型水基线切割工作液，其特征在于，是由以下质量百分含量的原料制备而成的：
防锈剂2％，清洗剂3％，电解质0.2‰，润滑剂5％，PH值调节剂8％，杀菌剂0.5％，消泡剂1‰，降凝剂0.5％，渗透剂2％，余量为去离子水。
3.如权利要求1所述的一种环保型水基线切割工作液，其特征在于，是由以下质量百分含量的原料制备而成的：
防锈剂4％，清洗剂5％，电解质0.5‰，润滑剂8％，PH值调节剂12％，杀菌剂2％，消泡剂3‰，降凝剂5％，渗透剂4％，余量为去离子水。
4.如权利要求1所述的一种环保型水基线切割工作液，其特征在于，是由以下质量百分含量的原料制备而成的：
防锈剂3％，清洗剂4％，电解质0.3‰，润滑剂6.5％，PH值调节剂10％，杀菌剂1.5％，消泡剂2‰，降凝剂2.5％，渗透剂3％，余量为去离子水。
5.如权利要求1-4所述的一种环保型水基线切割工作液，其特征在于，所述防锈剂为三乙醇胺硼酸酯、癸二酸、十二碳二元酸的一种或几种。
6.如权利要求1-4所述的一种环保型水基线切割工作液，其特征在于，所述清洗剂为壬基酚聚氧乙烯醚、脂肪酸甲酯乙氧基化物、椰子油脂肪酸二乙醇酰胺的一种或几种。
7.如权利要求1-4所述的一种环保型水基线切割工作液，其特征在于，所述电解质选用聚乙烯酸钠；所述润滑剂选用四聚蓖麻油酸酯。
8.如权利要求1-4所述的一种环保型水基线切割工作液，其特征在于，所述PH值调节剂选用三乙醇胺；所述杀菌剂选用MBM杀菌剂。
9.如权利要求1-4所述的一种环保型水基线切割工作液，其特征在于，所述消泡剂选用有机硅消泡剂；所述降凝剂选用乙二醇；所述渗透剂选用脂肪醇聚氧乙烯醚。
10.一种环保型水基线切割工作液及其制备方法，其特征在于，包括如下步骤：
(1)将PH值调节剂通过抽料泵抽入电加热不锈钢反应釜内，从反应釜人孔加入防锈剂，边搅拌边开启电加热升温至100-110℃，保温反应2h；
(2)开启冷却水降温至60℃，依次加入清洗剂、润滑剂、渗透剂，搅拌30-40min；
(3)加入去离子水，自然降温至30-40℃，依次加入电解质、杀菌剂、降凝剂、消泡剂，搅拌2h；
(4)成品经20微米过滤器过滤，灌装。
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