CN113295327A - Zero-stress sample for ultrasonic stress measurement method and preparation method thereof - Google Patents

Zero-stress sample for ultrasonic stress measurement method and preparation method thereof Download PDF

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CN113295327A
CN113295327A CN202010108643.3A CN202010108643A CN113295327A CN 113295327 A CN113295327 A CN 113295327A CN 202010108643 A CN202010108643 A CN 202010108643A CN 113295327 A CN113295327 A CN 113295327A
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stress
sample
zero
rolling direction
cutting
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CN113295327B (en
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李丽锋
罗金恒
武刚
王珂
朱丽霞
吴锦强
邹斌
徐春燕
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China National Petroleum Corp
Pipeline Research Institute of CNPC
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China National Petroleum Corp
Pipeline Research Institute of CNPC
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01LMEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
    • G01L25/00Testing or calibrating of apparatus for measuring force, torque, work, mechanical power, or mechanical efficiency
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/286Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q involving mechanical work, e.g. chopping, disintegrating, compacting, homogenising
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N29/00Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
    • G01N29/22Details, e.g. general constructional or apparatus details
    • G01N29/30Arrangements for calibrating or comparing, e.g. with standard objects
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/286Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q involving mechanical work, e.g. chopping, disintegrating, compacting, homogenising
    • G01N2001/2873Cutting or cleaving
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N2001/2893Preparing calibration standards
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00Indexing codes associated with group G01N29/00
    • G01N2291/02Indexing codes associated with the analysed material
    • G01N2291/028Material parameters
    • G01N2291/02827Elastic parameters, strength or force

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  • General Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
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  • Pathology (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

The invention discloses a zero-stress sample for an ultrasonic stress measurement method and a preparation method thereof, and the method mainly comprises the following steps: (1) selecting and preparing the supplied materials for zero-stress sample calibration; (2) preparing a sample and marking; (3) detecting zero stress for the first time; (4) determining a stress relief annealing process of a zero-stress sample; (5) stress relief annealing treatment of the sample; (6) detecting zero stress for the second time; (7) the wire cutting further releases the stress; (8) detecting zero stress for the third time; (9) and (6) carrying out cross sample sealing and storing. The invention provides a new technical means for the preparation and calibration of the zero stress sample, can solve the problem that the high-accuracy zero stress sample is difficult to process and evaluate in the ultrasonic method stress measurement caused by the uneven residual stress level of the in-service steel pipe and the plate, can provide the zero stress sample represented in a higher precision and a wider range for the ultrasonic method stress measurement of the high-steel-grade pipeline steel, and has important significance for standardizing the preparation of the ultrasonic zero stress sample and improving the residual stress test precision of the pipeline steel.

Description

Zero-stress sample for ultrasonic stress measurement method and preparation method thereof
Technical Field
The invention relates to the technical field of residual stress measurement, in particular to a zero-stress sample for an ultrasonic stress measurement method and a preparation method thereof.
Background
The residual stress is one of the main factors for controlling the quality of the pipe, is one of the factors causing the defect expansion failure of the in-service pipeline, is one of the important parameters for evaluating the defect applicability, and has important significance for nondestructively measuring the residual stress in the structure of the in-service pipeline and the plate. The methods for measuring the residual stress are many, but the methods applied at present have great limitations, such as the pinhole method is accurate but causes damage to the workpiece, and the X-ray diffraction method has too low measurement depth. The traditional residual stress measuring method is difficult to meet the stress measurement of pipelines and plates in service, while the ultrasonic method based on the acoustic elasticity principle can nondestructively detect the stress in the pipelines, and the nondestructive property and the portability determine that the method is one of the most promising technologies for measuring the residual stress and the working stress of the pipelines in service.
Before each measurement of the ultrasonic method, an absolute zero stress sample must be calibrated, and the proximity of the zero stress sample and the absolute zero is one of main factors influencing the stress precision of the ultrasonic method. The existing ultrasonic method stress measurement zero stress sample usually only adopts an annealing process, however, for pipeline steel with relatively large wall thickness (for example, the wall thickness is more than 10mm) or a plate with thicker thickness (for example, the thickness is more than 10mm), even if a strict annealing process is adopted, the temperature field difference caused by uneven heat dissipation of the thickness cannot be avoided in the cooling stage, so that new residual stress is brought, and the absolute zero of the zero stress is difficult to achieve; the existing zero-stress sample processing and manufacturing has no strict process flow, random sampling is carried out on an original base material, non-batch sampling processing is carried out, and the representativeness to different manufacturers, thicknesses and regions is poor; the stress release degree of the existing annealing zero-stress sample is not enough. Therefore, the development of the novel zero-stress test sample has important significance for the integrity management of the in-service pipeline and the plate by measuring and calibrating the stress by the ultrasonic method.
Disclosure of Invention
In order to solve the problems in the prior art, the invention aims to provide a zero-stress sample for an ultrasonic stress measurement method and a preparation method thereof, aims to solve the problem that the high-accuracy zero-stress sample for ultrasonic stress measurement is difficult to process and evaluate due to uneven residual stress level of a steel pipe, provides a zero-stress sample with higher precision and wider representation range for ultrasonic stress measurement, and has important significance for standardizing preparation of the ultrasonic zero-stress sample and improving the residual stress test precision.
In order to realize the purpose of the invention, the following technical scheme is adopted:
a method for preparing a zero-stress sample for an ultrasonic stress measurement method comprises the following steps:
step 1, selecting incoming materials of a zero-stress sample;
step 2, cutting the material into a plurality of samples in a linear mode, during linear cutting, performing linear cutting on the incoming material along a direction parallel to the material rolling direction and a direction perpendicular to the material rolling direction, and performing linear cutting to obtain a rectangular sample;
step 3, selecting a plurality of samples obtained in the step 2 to perform zero stress detection, detecting the stress on the samples in the direction parallel to the rolling direction of the material and in the direction vertical to the rolling direction of the material when the samples are subjected to the zero stress detection, and if the absolute value of the stress measured value of the detected samples is not greater than a first preset value, taking the samples obtained in the step 2 as zero stress samples; if the absolute value of the stress measured value of the tested sample is greater than the first preset value, performing step 4, and invalidating the sample subjected to zero-stress detection;
step 4, performing stress relief annealing on the residual sample obtained in the step 2;
step 5, carrying out zero stress detection on the sample obtained in the step 4, and if the absolute value of the stress measurement value of the sample to be detected is not greater than a first preset value, taking the sample obtained in the step 4 as a zero stress sample; if the absolute value of the stress measured value of the tested sample is larger than the first preset value and is not larger than the second preset value, the sample after zero stress detection is discarded, and then the step 4 is carried out; if the absolute value of the stress measured value of the tested sample is greater than the second preset value, the sample after zero stress detection is discarded, and then the step 6 is carried out;
step 6, performing linear cutting on the sample obtained in the step 4, releasing stress, and performing linear cutting on the incoming material along the parallel material rolling direction and the vertical material rolling direction during the linear cutting, wherein the length ratio of the cut sample in the parallel material rolling direction to the vertical material rolling direction is (1:1) - (1:3), or the length ratio of the cut sample in the vertical material rolling direction to the parallel material rolling direction is (1:1) - (1: 3); 1/6, the length of the sample in the direction parallel to the material rolling direction and the length of the sample in the direction vertical to the material rolling direction are not more than the height of the sample;
and 7, taking the sample subjected to the stress release in the step 6 by wire cutting as a zero-stress sample.
In the step 1, when the incoming material of the zero-stress sample is selected, the material which has the same processing process with the material used for the residual stress and the stress test object is selected.
And cutting the selected material by adopting linear cutting, flame or plasma cutting, and cutting off the heat affected zone of the material by adopting linear cutting after the cutting is finished when the flame or plasma cutting is adopted.
And 3, when the sample is subjected to zero stress detection, stress measurement is carried out by adopting a small hole method, a plurality of detection points are measured, and the average value of the stress of each detection point is taken as a stress measurement value.
And 5, when the sample is subjected to zero stress detection, stress measurement is carried out by adopting a small hole method, a plurality of detection points are measured, and the average value of the stress of each detection point is taken as a stress measurement value.
The first preset value is 12Mpa, and the second preset value is 30 Mpa.
A zero-stress sample is prepared by the preparation method.
The zero-stress sample is cuboid in shape.
When the zero-stress sample is in a cuboid shape, the length direction of the sample is parallel to the material rolling direction, the width direction of the sample is perpendicular to the material rolling direction, and the height direction of the sample is the thickness direction of the material.
The invention has the following beneficial effects:
the zero stress sample preparation method for the ultrasonic stress measurement method provides a new technical means for the preparation of the zero stress sample, the stress sample closer to zero can be obtained by comprehensively eliminating stress annealing, releasing stress by linear cutting and calibrating during zero stress detection, and the stress value of the sample can be quantified by calibrating during the zero stress detection, so that the precision of ultrasonic stress detection is improved, the applicability of the ultrasonic stress detection is improved, technical support is provided for the in-service pipeline stress detection, and the method has important significance for standardizing the preparation of the ultrasonic zero stress sample and improving the residual stress testing precision of in-service pipeline steel and plates. In the invention, when the stress relief is carried out by linear cutting, the incoming material is subjected to linear cutting along the parallel material rolling direction and the vertical material rolling direction, a rectangular sample is cut by linear cutting, the length ratio of the cut sample in the parallel material rolling direction and the vertical material rolling direction is (1:1) - (1:3), or the length ratio of the cut sample in the vertical material rolling direction and the parallel material rolling direction is (1:1) - (1: 3); 1/6, the length of the sample in the direction parallel to the material rolling direction and the length of the sample in the direction vertical to the material rolling direction are not more than the height of the sample; according to the cutting direction and the cutting of the cuboid sample, the stress of the sample in each direction can be effectively released, the shrinkage stress caused by nonuniform heat distribution caused by the anisotropy of the material can be eliminated, and meanwhile, the stress of the sample is released thoroughly, so that the sample is stable in performance and can be stored for a long time, and the measurement is facilitated. In conclusion, the zero-stress sample preparation method can obtain the zero-stress sample with lower residual stress, and is beneficial to the ultrasonic stress measurement method to measure more accurate results.
The zero-stress sample disclosed by the invention is low in residual stress, and the stress testing precision of an ultrasonic method can be improved by taking the sample as a standard sample.
Drawings
FIG. 1 is a process diagram of the zero stress specimen processing of the present invention;
FIG. 2(a) is a left side view of a structure after cutting a raw material into a plurality of samples according to an embodiment of the present invention;
FIG. 2(b) is a front view of a starting material cut into a plurality of test pieces in an embodiment of the present invention;
FIG. 2(c) is a top view of a sample after being cut into a plurality of samples;
FIG. 2(d) is a left side view of an embodiment of the present invention after cutting a raw material into a plurality of samples;
fig. 2(e) is a plan view of a sample obtained by cutting a raw material into a plurality of samples in an embodiment of the present invention.
Detailed Description
The present invention is described in further detail below with reference to specific embodiments, which are given for the purpose of illustration only and are not intended to limit the scope of the invention. The invention is described in detail below with reference to the attached drawing figures:
the invention is mainly applied to zero stress calibration before stress measurement by an ultrasonic method, and performs calibration work before stress measurement aiming at different structures and different materials so as to conveniently and accurately measure the stress.
As shown in fig. 1, the method for preparing a zero-stress sample for an ultrasonic stress measurement method according to the present invention obtains the zero-stress sample by a process method of comprehensive annealing, linear cutting and multiple small-hole detection and calibration, and provides a guarantee for engineering measurement accuracy of residual stress in an ultrasonic method, and specifically includes the following steps:
step 1: selection and preparation of supplied materials for zero-stress sample calibration
Specifically, when selecting the supplied material calibrated by the zero-stress test sample, selecting a material having the same processing technological process as the material used for the residual stress and stress test object; when cutting, cutting from a rolled plate and a parent metal by adopting a linear cutting process, if a processing mode which brings heat influence such as flame cutting and plasma cutting is adopted, carrying out 2 times of linear cutting on a sample which is cut by heat, and removing a heat affected zone;
step 2: sample preparation and marking
As shown in fig. 2(a) to 2(e), in particular, sampling and cutting of the sample requires that no additional heat input can be brought, so that batch sampling is performed from the incoming materials on the rolled plate and the base metal by adopting a linear cutting process, and during sampling, rectangular parallelepiped samples are cut by performing linear cutting along a direction perpendicular to the material rolling direction and a direction parallel to the material rolling direction, wherein the length direction of the sample is parallel to the material rolling direction, the width direction of the sample is perpendicular to the material rolling direction, and the height direction of the sample is the thickness direction of the material;
and step 3: first time zero stress detection
Two samples in the samples obtained in the step 2 are extracted, wherein one sample is used for measuring the stress in the length direction, the other sample is used for measuring the stress in the width direction, the stress measurement is carried out by adopting a small hole method during measurement, each sample is used for measuring three points, the average value is obtained, and the stress measurement value is marked as sigma1The sample after punching measurement is discarded; the calibrated stress absolute value is detected according to a pinhole method, and whether the stress absolute value can be used as a zero-stress sample is determined according to a zero judgment condition, if sigma is1If not more than 12Mpa, taking the sample obtained in the step (2) as a zero-stress sample, otherwise, performing the step (4);
and 4, step 4: stress relief annealing process for determining zero-stress sample
Determining the annealing temperature, heating rate, heating speed, heat preservation time and cooling speed of each steel material according to the heat treatment temperature of different materials and considering a phase change curve; the heat treatment furnace is required to ensure uniform furnace temperature and can also carry out annealing under the vacuum condition;
and 5: stress relief annealing of test specimens
Stress relief annealing treatment is carried out on the samples in the same batch according to the annealing process in the step 4;
step 6: second zero stress test
Extracting two samples in the samples obtained in the step 5, wherein one sample is used for measuring the stress in the length direction, the other sample is used for measuring the stress in the width direction, the stress detection is carried out by adopting a small hole method during measurement, three points are measured, the average value is taken, and the marked stress measurement value is sigma2E.g. σ2If the absolute value of (a) is not more than 12MPa, the sample obtained in step (5) is taken as a zero-stress sample, and the process proceeds to step (9), if sigma is2Is greater than 30MPa, is returned to and is subjected to stress relief annealing again according to step 5, e.g. sigma2When the absolute value of the pressure difference is not more than 30MPa and more than 12MPa, entering a step 7, and abandoning the sample after punching measurement;
and 7: wire cutting further releases stress
The extra heat input cannot be brought in during cutting, so that the stress is further released by adopting linear cutting on the rest samples, and the samples are cut into cuboids by performing linear cutting along the direction vertical to the material rolling direction and the direction parallel to the material rolling direction during the linear cutting; generally, the length of the specimen is greater than the width, the width is greater than the thickness, the thickness is minimal, the ratio of the width to the length is (1:1) to (1:3), and a minimum cut size (i.e., width) of 4mm is generally recommended;
and 8: third time zero stress test
Two samples are extracted from the samples subjected to stress release in the step 7 of wire-electrode cutting, wherein one sample is used for measuring the stress in the length direction, the other sample is used for measuring the stress in the width direction, the stress detection is carried out by adopting a small hole method during measurement, three points are measured, the average value is taken, and the marked stress measurement value is sigma3The sample after punching measurement is discarded;
and step 9: and (3) the rest samples are subjected to sample handing and sealing to serve as zero-stress samples, the number of the zero-stress samples is not less than 2, 1 is used for field measurement, and 1 is used for retention.
Examples
The preparation method of the zero-stress sample for the ultrasonic stress measurement method comprises the following steps:
step 1: selection and preparation of supplied materials for zero-stress sample calibration
According to the residual stress measurement requirement of an X80 high-steel pipeline structure (the wall thickness is 21.5mm) at a certain site of a long-distance oil and gas pipeline of a certain oil company, original record information of purchasing, production and the like is consulted, and an X80 high-steel grade pipeline material which is the same as a material supplying manufacturer and a same pipe manufacturing processing technology of a tested object is selected as a zero-stress sample processing sampling material.
The raw material for preparing the sample is obtained by cutting the X80 parent metal by adopting a linear cutting process, and the processing and sampling mode which brings thermal influence by flame, plasma cutting and the like is avoided as much as possible.
If a processing mode which brings heat influence by flame, plasma cutting and the like is adopted for sampling from the X80 parent metal, the heat affected area of four sides of a heat cut sample needs to be removed by adopting a linear cutting process again, and the distance between the cutting position of each single side of the four sides and the edge of a material needs to be more than 100mm by adopting the linear cutting process, so that the heat cutting influence of flame and the like is eliminated.
Step 2: sample preparation and marking
The method comprises the following steps of 1, preparing a sample on a raw material obtained by linear cutting in step 1 by adopting a linear cutting process, carrying out linear cutting along the direction vertical to the rolling direction and the direction parallel to the rolling direction during sample preparation, and cutting out a cuboid sample, wherein the length direction of the sample is parallel to the material rolling direction, the width direction is vertical to the material rolling direction, the height direction is the thickness direction of the material, one batch of samples are generally not less than 8, 4 of the samples are used for measuring the residual stress parallel to the rolling direction, and 4 of the samples are used for measuring the residual stress vertical to the rolling direction.
And step 3: first time zero stress detection
Two samples in the samples obtained in the step 2 are extracted, wherein one sample is used for measuring the stress in the length direction, the other sample is used for measuring the stress in the width direction, the stress measurement is carried out by adopting a small hole method during measurement, each sample is used for measuring three points, the average value is obtained, and the stress measurement value is marked as sigma1. The sample after the measurement of the punched hole is discarded.
E.g. sigma1When the absolute value of the pressure difference is less than 12MPa, the pressure difference can be regarded as a zero-stress sample, and the subsequent process is avoidedAnd (5) carrying out the following steps.
And 4, step 4: stress relief annealing process for determining zero-stress sample
According to the heat treatment temperature of the material, the phase change curve is considered, and the annealing temperature, the heating rate, the heating speed, the heat preservation time and the cooling speed are determined.
In the embodiment, the annealing temperature of the sample is 480 ℃, the heat preservation time is not less than 2 hours, and the sample is taken after being cooled to the room temperature along with the furnace.
The heat treatment furnace requires uniform furnace temperature, and the furnace temperature maintaining precision is not lower than plus or minus 10 ℃; the annealing may be performed under vacuum if necessary.
And 5: stress relief annealing of test specimens
And 4, annealing the other samples in a heat treatment furnace according to the annealing process in the step 4.
Step 6: second zero stress test
Extracting two samples in the samples obtained in the step 5, wherein one sample is used for measuring the stress in the length direction, the other sample is used for measuring the stress in the width direction, the stress detection is carried out by adopting a small hole method during measurement, three points are measured, the average value is taken, and the marked stress measurement value is sigma2E.g. σ2Until the absolute value of (a) is not more than 12MPa, the sample obtained in step (5) is taken as a zero-stress sample, and the process proceeds to step (9), where σ is2Is greater than 30MPa, and returns to step 5 to carry out annealing again, such as sigma2When the absolute value of the pressure difference is not more than 30MPa and more than 12MPa, the step 7 is carried out, and the sample after punching measurement is discarded.
And 7: wire cutting further releases stress
And (4) further releasing the stress of the residual test sample after the detection by adopting linear cutting. Wherein, the minimum block size of the wire cutting is 2mm for the pipeline structure material with the wall thickness of 20mm, and the reserved size of the sample in the thickness direction is not less than 3 mm.
And 8: third time zero stress test
Two samples after the stress release of the wire-electrode cutting in the step 7 are extracted, wherein one sample is used for measuring the stress in the length direction, and the other sample is used for measuring the stress in the width directionThe stress is detected by a small hole method during measurement, three points are measured, the average value is taken, and the stress measurement value is marked as sigma3And the sample after punching measurement is discarded. Sigma3Is less than 12 MPa.
And step 9: hand-over sample sealing
The residual zero-stress sample is not less than 2, 1 is used for field measurement, and 1 is used for retention.
Numbering zero samples at the same time, recording the processing process including raw material furnace batch number information, processing, sampling and cutting method, and sigma1、σ2、σ3And calibrating the type, parameters and the like of the strain gauge by a small hole method, and checking after preparation.

Claims (9)

1. A method for preparing a zero-stress sample for an ultrasonic stress measurement method is characterized by comprising the following steps of:
step 1, selecting incoming materials of a zero-stress sample;
step 2, cutting the material into a plurality of samples in a linear mode, during linear cutting, performing linear cutting on the incoming material along a direction parallel to the material rolling direction and a direction perpendicular to the material rolling direction, and performing linear cutting to obtain a rectangular sample;
step 3, selecting a plurality of samples obtained in the step 2 to perform zero stress detection, detecting the stress on the samples in the direction parallel to the rolling direction of the material and in the direction vertical to the rolling direction of the material when the samples are subjected to the zero stress detection, and if the absolute value of the stress measured value of the detected samples is not greater than a first preset value, taking the samples obtained in the step 2 as zero stress samples; if the absolute value of the stress measured value of the tested sample is greater than the first preset value, performing step 4, and invalidating the sample subjected to zero-stress detection;
step 4, performing stress relief annealing on the residual sample obtained in the step 2;
step 5, carrying out zero stress detection on the sample obtained in the step 4, and if the absolute value of the stress measurement value of the sample to be detected is not greater than a first preset value, taking the sample obtained in the step 4 as a zero stress sample; if the absolute value of the stress measured value of the tested sample is larger than the first preset value and is not larger than the second preset value, the sample after zero stress detection is discarded, and then the step 4 is carried out; if the absolute value of the stress measured value of the tested sample is greater than the second preset value, the sample after zero stress detection is discarded, and then the step 6 is carried out;
step 6, performing linear cutting on the sample obtained in the step 4, releasing stress, and performing linear cutting on the incoming material along the parallel material rolling direction and the vertical material rolling direction during the linear cutting, wherein the length ratio of the cut sample in the parallel material rolling direction to the vertical material rolling direction is (1:1) - (1:3), or the length ratio of the cut sample in the vertical material rolling direction to the parallel material rolling direction is (1:1) - (1: 3); 1/6, the length of the sample in the direction parallel to the material rolling direction and the length of the sample in the direction vertical to the material rolling direction are not more than the height of the sample;
and 7, taking the sample subjected to the stress release in the step 6 by wire cutting as a zero-stress sample.
2. The method for preparing the zero-stress sample for the ultrasonic stress measurement method according to claim 1, wherein in the step 1, when the material of the zero-stress sample is selected, a material having the same processing technology as that of the material of the residual stress and stress test object is selected.
3. The method for preparing a zero-stress sample for an ultrasonic stress measurement method according to claim 2, wherein the selected material is cut by wire cutting, flame cutting or plasma cutting, and when the flame cutting or plasma cutting is adopted, the heat affected zone of the material is cut off by wire cutting after the cutting is finished.
4. The method for preparing the zero-stress sample for the ultrasonic stress measurement method according to claim 1, wherein in the step 3, when the sample is subjected to zero-stress detection, stress measurement is performed by using a pinhole method, a plurality of detection points are measured, and an average value of the stress of each detection point is taken as a stress measurement value.
5. The method for preparing the zero-stress sample for the ultrasonic stress measurement method according to claim 1, wherein in the step 5, when the sample is subjected to zero-stress detection, stress measurement is performed by using a pinhole method, a plurality of detection points are measured, and an average value of the stress of each detection point is taken as a stress measurement value.
6. The method of any one of claims 1-5, wherein the first predetermined value is 12MPa and the second predetermined value is 30 MPa.
7. A zero-stress test specimen obtained by the production method according to any one of claims 1 to 6.
8. The zero stress specimen according to claim 7, wherein the zero stress specimen is in the shape of a rectangular parallelepiped.
9. The zero stress specimen according to claim 8, wherein the zero stress specimen has a length direction parallel to the material rolling direction, a width direction perpendicular to the material rolling direction, and a height direction in the thickness direction of the material.
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